================================================================================ Quantitative Microprobe Analysis Thu Mar 23 12:13:05 2006 ================================================================================ point n : 1 x= 14491.0 y= -3405.0 z= -250. carb3 trav 3 bkg pt Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 12.4 6.4 4.5 2.71 0.0099 6.4 0.0309 Mg 104.0 2.2 3.8 27.43 0.0551 2.2 0.0126 Sr 24.9 3.2 14.5 1.72 0.0015 3.2 0.0390 P 42.0 3.4 2.0 21.52 0.0505 3.5 0.0358 K 12.1 6.4 7.1 1.70 0.0045 6.4 0.0207 Cl 30.2 3.3 2.3 13.34 0.0061 3.3 0.0222 Ca 3666.0 0.4 18.0 203.66 0.7938 0.5 0.0328 Ba 11.7 4.6 11.2 1.04 0.0003 4.6 0.0744 Fe 4.2 7.8 3.5 1.18 0.0003 7.8 0.0559 Mn 3.5 11.9 3.3 1.05 0.0002 12.0 0.0660 Elt. k-ratio Correc. Na 0.0005 2.3340 Mg 0.0040 1.6982 Sr 0.0009 1.3753 P 0.0079 1.1949 K 0.0004 1.0206 Cl 0.0034 1.1147 Ca 0.2881 1.0924 Ba 0.0001 1.5397 Fe 0.0002 1.2537 Mn 0.0001 1.2767 iteration : 3 Analysis no. 1 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1150 0.013557 0.1150 0.0945 Mg 0.6777 0.015838 0.6777 0.5266 Sr 0.1249 0.011866 0.1249 0.0269 P 0.9458 0.035318 0.9458 0.5767 K 0.0410 0.008027 0.0410 0.0198 Cl 0.3756 0.013995 0.3756 0.2001 Ca 31.4717 0.143788 31.4717 14.8298 Ba 0.0116 0.019446 0.0116 0.0016 Fe 0.0205 0.014396 0.0205 0.0069 Mn 0.0065 0.020861 0.0065 0.0022 C 14.1867 14.1867 22.3073 O 52.0231 52.0231 61.4076 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 2 x= 14424.0 y= -3369.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 34.6 3.8 4.5 7.60 0.0380 3.8 0.0308 Mg 128.9 2.0 3.8 34.01 0.0688 2.0 0.0127 Sr 38.9 2.5 14.5 2.68 0.0034 2.6 0.0390 P 13.4 6.1 2.0 6.87 0.0144 6.1 0.0357 K 11.4 6.6 7.1 1.60 0.0038 6.6 0.0203 Cl 30.9 3.3 2.3 13.64 0.0062 3.3 0.0219 Ca 4195.9 0.3 18.0 233.09 0.9091 0.4 0.0325 Ba 13.0 4.4 11.2 1.16 0.0010 4.4 0.0744 Fe 4.6 7.4 3.5 1.29 0.0006 7.4 0.0556 Mn 5.0 10.0 3.3 1.49 0.0016 10.1 0.0658 Elt. k-ratio Correc. Na 0.0019 2.3300 Mg 0.0050 1.7011 Sr 0.0021 1.3739 P 0.0023 1.1930 K 0.0003 1.0027 Cl 0.0034 1.1036 Ca 0.3299 1.0852 Ba 0.0003 1.5409 Fe 0.0003 1.2479 Mn 0.0005 1.2720 iteration : 3 Analysis no. 2 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4415 0.020648 0.4415 0.3766 Mg 0.8476 0.017644 0.8476 0.6840 Sr 0.2910 0.013806 0.2910 0.0652 P 0.2703 0.020719 0.2703 0.1712 K 0.0342 0.007731 0.0342 0.0172 Cl 0.3807 0.013997 0.3807 0.2106 Ca 35.8027 0.156485 35.8027 17.5212 Ba 0.0450 0.020006 0.0450 0.0064 Fe 0.0335 0.014698 0.0335 0.0118 Mn 0.0580 0.022888 0.0580 0.0207 C 12.6729 12.6729 20.6954 O 49.1225 49.1225 60.2197 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 3 x= 14428.0 y= -3369.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 51.8 3.1 4.5 11.39 0.0598 3.1 0.0306 Mg 246.6 1.4 3.8 65.05 0.1336 1.5 0.0126 Sr 46.9 2.3 14.5 3.24 0.0046 2.3 0.0390 P 22.0 4.8 2.0 11.28 0.0253 4.8 0.0358 K 10.9 6.8 7.1 1.54 0.0034 6.8 0.0202 Cl 14.2 4.8 2.3 6.28 0.0026 4.8 0.0219 Ca 4507.5 0.3 18.0 250.41 0.9769 0.4 0.0324 Ba 12.7 4.4 11.2 1.13 0.0009 4.4 0.0745 Fe 4.0 7.9 3.5 1.12 0.0002 8.0 0.0554 Mn 5.3 9.7 3.3 1.60 0.0019 9.7 0.0656 Elt. k-ratio Correc. Na 0.0030 2.3130 Mg 0.0097 1.6958 Sr 0.0028 1.3760 P 0.0040 1.1942 K 0.0003 0.9957 Cl 0.0014 1.1016 Ca 0.3545 1.0812 Ba 0.0002 1.5412 Fe 0.0001 1.2436 Mn 0.0006 1.2684 iteration : 3 Analysis no. 3 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6903 0.024673 0.6903 0.6069 Mg 1.6396 0.024423 1.6396 1.3635 Sr 0.3878 0.014846 0.3878 0.0895 P 0.4738 0.025955 0.4738 0.3092 K 0.0304 0.007582 0.0304 0.0157 Cl 0.1588 0.009846 0.1588 0.0905 Ca 38.3323 0.163796 38.3323 19.3311 Ba 0.0379 0.019895 0.0379 0.0056 Fe 0.0139 0.014092 0.0139 0.0050 Mn 0.0703 0.023301 0.0703 0.0259 C 11.1514 11.1514 18.7659 O 47.0135 47.0135 59.3913 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 4 x= 14432.0 y= -3370.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 44.8 3.3 4.5 9.84 0.0509 3.4 0.0306 Mg 244.3 1.4 3.8 64.44 0.1323 1.5 0.0126 Sr 48.5 2.3 14.5 3.35 0.0048 2.3 0.0389 P 30.7 4.0 2.0 15.74 0.0363 4.0 0.0356 K 10.0 7.1 7.1 1.40 0.0026 7.1 0.0200 Cl 16.4 4.5 2.3 7.25 0.0031 4.5 0.0218 Ca 4839.3 0.3 18.0 268.84 1.0491 0.4 0.0323 Ba 13.3 4.3 11.2 1.18 0.0012 4.3 0.0745 Fe 4.6 7.4 3.5 1.30 0.0006 7.4 0.0553 Mn 4.4 10.7 3.3 1.31 0.0010 10.7 0.0655 Elt. k-ratio Correc. Na 0.0025 2.3113 Mg 0.0096 1.6920 Sr 0.0030 1.3713 P 0.0057 1.1900 K 0.0002 0.9875 Cl 0.0017 1.0968 Ca 0.3807 1.0774 Ba 0.0003 1.5424 Fe 0.0003 1.2402 Mn 0.0003 1.2656 iteration : 3 Analysis no. 4 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5868 0.023036 0.5868 0.5298 Mg 1.6204 0.024250 1.6204 1.3838 Sr 0.4055 0.014990 0.4055 0.0961 P 0.6770 0.030255 0.6770 0.4536 K 0.0226 0.007318 0.0226 0.0120 Cl 0.1872 0.010437 0.1872 0.1096 Ca 41.0201 0.171505 41.0201 21.2431 Ba 0.0521 0.020139 0.0521 0.0079 Fe 0.0341 0.014629 0.0341 0.0127 Mn 0.0365 0.021931 0.0365 0.0138 C 10.0361 10.0361 17.3434 O 45.3215 45.3215 58.7943 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 5 x= 14437.0 y= -3370.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 35.4 3.8 4.5 7.77 0.0390 3.8 0.0306 Mg 232.0 1.5 3.8 61.19 0.1255 1.5 0.0126 Sr 44.5 2.4 14.5 3.07 0.0042 2.4 0.0389 P 49.0 3.2 2.0 25.11 0.0593 3.2 0.0356 K 10.9 6.8 7.1 1.53 0.0034 6.8 0.0202 Cl 20.1 4.1 2.3 8.88 0.0039 4.1 0.0219 Ca 4590.6 0.3 18.0 255.02 0.9949 0.4 0.0324 Ba 13.7 4.3 11.2 1.22 0.0015 4.3 0.0745 Fe 4.4 7.5 3.5 1.25 0.0005 7.5 0.0554 Mn 4.6 10.4 3.3 1.39 0.0012 10.4 0.0655 Elt. k-ratio Correc. Na 0.0019 2.3116 Mg 0.0091 1.6901 Sr 0.0026 1.3714 P 0.0093 1.1907 K 0.0003 0.9962 Cl 0.0022 1.1023 Ca 0.3611 1.0805 Ba 0.0004 1.5413 Fe 0.0002 1.2422 Mn 0.0004 1.2672 iteration : 3 Analysis no. 5 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4497 0.020696 0.4497 0.3995 Mg 1.5356 0.023587 1.5356 1.2904 Sr 0.3573 0.014495 0.3573 0.0833 P 1.1074 0.037952 1.1074 0.7302 K 0.0300 0.007575 0.0300 0.0157 Cl 0.2372 0.011482 0.2372 0.1367 Ca 39.0157 0.165775 39.0157 19.8809 Ba 0.0624 0.020288 0.0624 0.0093 Fe 0.0285 0.014494 0.0285 0.0104 Mn 0.0454 0.022313 0.0454 0.0169 C 10.6194 10.6194 18.0570 O 46.5114 46.5114 59.3699 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 6 x= 14441.0 y= -3370.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 39.9 3.5 4.5 8.76 0.0447 3.6 0.0305 Mg 234.4 1.5 3.8 61.82 0.1268 1.5 0.0126 Sr 47.8 2.3 14.5 3.30 0.0047 2.3 0.0389 P 57.1 3.0 2.0 29.26 0.0696 3.0 0.0357 K 14.9 5.8 7.1 2.09 0.0070 5.8 0.0204 Cl 35.0 3.1 2.3 15.46 0.0071 3.1 0.0220 Ca 4324.1 0.3 18.0 240.21 0.9371 0.4 0.0325 Ba 12.9 4.4 11.2 1.15 0.0010 4.4 0.0744 Fe 3.9 8.0 3.5 1.11 0.0002 8.0 0.0555 Mn 5.1 9.9 3.3 1.52 0.0017 10.0 0.0656 Elt. k-ratio Correc. Na 0.0022 2.3068 Mg 0.0092 1.6891 Sr 0.0029 1.3728 P 0.0109 1.1930 K 0.0006 1.0063 Cl 0.0039 1.1077 Ca 0.3401 1.0839 Ba 0.0003 1.5398 Fe 0.0001 1.2439 Mn 0.0005 1.2684 iteration : 3 Analysis no. 6 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5144 0.021805 0.5144 0.4498 Mg 1.5511 0.023702 1.5511 1.2832 Sr 0.3974 0.014920 0.3974 0.0912 P 1.3010 0.041019 1.3010 0.8445 K 0.0626 0.008464 0.0626 0.0322 Cl 0.4373 0.014904 0.4373 0.2480 Ca 36.8599 0.159570 36.8599 18.4910 Ba 0.0437 0.019973 0.0437 0.0064 Fe 0.0122 0.014050 0.0122 0.0044 Mn 0.0614 0.022965 0.0614 0.0225 C 11.2306 11.2306 18.7999 O 47.5284 47.5284 59.7268 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 7 x= 14445.0 y= -3371.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 54.3 3.0 4.5 11.93 0.0629 3.1 0.0305 Mg 230.3 1.5 3.8 60.74 0.1246 1.5 0.0126 Sr 49.3 2.2 14.5 3.41 0.0049 2.3 0.0390 P 47.6 3.2 2.0 24.39 0.0576 3.3 0.0358 K 15.4 5.7 7.1 2.16 0.0075 5.7 0.0204 Cl 37.9 3.0 2.3 16.74 0.0077 3.0 0.0221 Ca 4230.0 0.3 18.0 234.99 0.9169 0.4 0.0325 Ba 12.7 4.4 11.2 1.13 0.0009 4.4 0.0744 Fe 4.3 7.7 3.5 1.21 0.0004 7.7 0.0555 Mn 3.9 11.3 3.3 1.18 0.0006 11.3 0.0657 Elt. k-ratio Correc. Na 0.0031 2.3053 Mg 0.0090 1.6926 Sr 0.0030 1.3748 P 0.0090 1.1949 K 0.0007 1.0085 Cl 0.0043 1.1086 Ca 0.3327 1.0849 Ba 0.0002 1.5395 Fe 0.0002 1.2449 Mn 0.0002 1.2692 iteration : 3 Analysis no. 7 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7240 0.025140 0.7240 0.6283 Mg 1.5270 0.023542 1.5270 1.2536 Sr 0.4163 0.015131 0.4163 0.0948 P 1.0786 0.037561 1.0786 0.6948 K 0.0668 0.008582 0.0668 0.0341 Cl 0.4766 0.015493 0.4766 0.2682 Ca 36.1001 0.157377 36.1001 17.9712 Ba 0.0379 0.019881 0.0379 0.0055 Fe 0.0237 0.014393 0.0237 0.0085 Mn 0.0206 0.021347 0.0206 0.0075 C 11.5899 11.5899 19.2528 O 47.9385 47.9385 59.7807 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 8 x= 14449.0 y= -3371.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 46.0 3.3 4.5 10.11 0.0525 3.3 0.0306 Mg 216.2 1.5 3.8 57.04 0.1170 1.6 0.0126 Sr 47.0 2.3 14.5 3.25 0.0046 2.3 0.0390 P 48.5 3.2 2.0 24.85 0.0587 3.2 0.0358 K 17.9 5.3 7.1 2.52 0.0098 5.3 0.0205 Cl 44.5 2.7 2.3 19.65 0.0092 2.7 0.0221 Ca 4102.5 0.3 18.0 227.90 0.8895 0.4 0.0326 Ba 12.0 4.6 11.2 1.07 0.0004 4.6 0.0745 Fe 4.0 7.9 3.5 1.14 0.0003 7.9 0.0556 Mn 4.7 10.3 3.3 1.42 0.0013 10.3 0.0658 Elt. k-ratio Correc. Na 0.0026 2.3082 Mg 0.0085 1.6921 Sr 0.0028 1.3748 P 0.0092 1.1951 K 0.0009 1.0124 Cl 0.0051 1.1103 Ca 0.3228 1.0866 Ba 0.0001 1.5392 Fe 0.0001 1.2463 Mn 0.0004 1.2703 iteration : 3 Analysis no. 8 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6048 0.023320 0.6048 0.5198 Mg 1.4327 0.022801 1.4327 1.1648 Sr 0.3890 0.014859 0.3890 0.0877 P 1.1006 0.037932 1.1006 0.7021 K 0.0878 0.009097 0.0878 0.0444 Cl 0.5660 0.016756 0.5660 0.3154 Ca 35.0782 0.154432 35.0782 17.2939 Ba 0.0193 0.019583 0.0193 0.0028 Fe 0.0163 0.014205 0.0163 0.0058 Mn 0.0491 0.022529 0.0491 0.0177 C 12.0341 12.0341 19.7978 O 48.6220 48.6220 60.0478 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 9 x= 14453.0 y= -3371.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 19.2 5.1 4.5 4.22 0.0186 5.1 0.0309 Mg 129.4 2.0 3.8 34.14 0.0692 2.0 0.0126 Sr 35.2 2.7 14.5 2.43 0.0029 2.7 0.0390 P 44.8 3.3 2.0 22.98 0.0542 3.4 0.0358 K 17.0 5.4 7.1 2.39 0.0090 5.4 0.0206 Cl 37.9 3.0 2.3 16.71 0.0077 3.0 0.0222 Ca 3903.6 0.4 18.0 216.86 0.8468 0.4 0.0327 Ba 10.3 4.9 11.2 0.91 0.0000 4.9 0.0000 Fe 4.4 7.5 3.5 1.26 0.0005 7.5 0.0559 Mn 3.7 11.6 3.3 1.11 0.0004 11.6 0.0660 Elt. k-ratio Correc. Na 0.0009 2.3262 Mg 0.0050 1.6950 Sr 0.0018 1.3730 P 0.0085 1.1935 K 0.0008 1.0151 Cl 0.0043 1.1114 Ca 0.3073 1.0894 Ba 0.0000 NaN Fe 0.0002 1.2502 Mn 0.0001 1.2737 iteration : 3 Analysis no. 9 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2156 0.016055 0.2156 0.1810 Mg 0.8493 0.017642 0.8493 0.6746 Sr 0.2474 0.013329 0.2474 0.0545 P 1.0135 0.036479 1.0135 0.6317 K 0.0808 0.008961 0.0808 0.0399 Cl 0.4774 0.015536 0.4774 0.2600 Ca 33.4788 0.149795 33.4788 16.1259 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0295 0.014633 0.0295 0.0102 Mn 0.0136 0.021148 0.0136 0.0048 C 13.1870 13.1870 21.1959 O 50.4071 50.4072 60.8215 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 10 x= 14457.0 y= -3372.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 13.4 6.1 4.5 2.93 0.0112 6.1 0.0309 Mg 133.3 1.9 3.8 35.17 0.0714 2.0 0.0126 Sr 44.8 2.4 14.5 3.09 0.0043 2.4 0.0390 P 48.8 3.2 2.0 25.03 0.0592 3.2 0.0358 K 18.4 5.2 7.1 2.58 0.0102 5.2 0.0205 Cl 34.4 3.1 2.3 15.18 0.0070 3.1 0.0221 Ca 4079.9 0.3 18.0 226.65 0.8856 0.4 0.0327 Ba 12.1 4.5 11.2 1.08 0.0005 4.5 0.0746 Fe 3.7 8.2 3.5 1.04 0.0001 8.3 0.0558 Mn 4.0 11.2 3.3 1.21 0.0007 11.2 0.0660 Elt. k-ratio Correc. Na 0.0006 2.3243 Mg 0.0052 1.6919 Sr 0.0026 1.3703 P 0.0093 1.1921 K 0.0009 1.0104 Cl 0.0039 1.1091 Ca 0.3214 1.0871 Ba 0.0002 1.5403 Fe 0.0000 1.2479 Mn 0.0002 1.2719 iteration : 3 Analysis no. 10 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1294 0.013922 0.1294 0.1103 Mg 0.8744 0.017880 0.8744 0.7047 Sr 0.3613 0.014549 0.3613 0.0808 P 1.1073 0.038013 1.1073 0.7003 K 0.0914 0.009170 0.0914 0.0458 Cl 0.4302 0.014822 0.4302 0.2377 Ca 34.9380 0.154089 34.9380 17.0755 Ba 0.0232 0.019681 0.0232 0.0033 Fe 0.0049 0.013905 0.0049 0.0017 Mn 0.0243 0.021572 0.0243 0.0087 C 12.5590 12.5590 20.4822 O 49.4565 49.4565 60.5490 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 11 x= 14462.0 y= -3372.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 12.2 6.4 4.5 2.68 0.0097 6.4 0.0310 Mg 120.4 2.0 3.8 31.75 0.0643 2.1 0.0127 Sr 24.4 3.2 14.5 1.68 0.0014 3.2 0.0392 P 54.0 3.0 2.0 27.70 0.0659 3.1 0.0360 K 12.4 6.3 7.1 1.75 0.0048 6.4 0.0210 Cl 33.6 3.1 2.3 14.83 0.0068 3.2 0.0224 Ca 3301.7 0.4 18.0 183.42 0.7162 0.5 0.0330 Ba 9.8 5.1 11.2 0.87 0.0000 5.1 0.0000 Fe 3.8 8.1 3.5 1.07 0.0001 8.1 0.0562 Mn 3.3 12.3 3.3 0.99 0.0000 12.3 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3300 Mg 0.0047 1.6967 Sr 0.0009 1.3784 P 0.0103 1.1986 K 0.0004 1.0338 Cl 0.0038 1.1227 Ca 0.2599 1.0970 Ba 0.0000 NaN Fe 0.0001 1.2568 Mn 0.0000 NaN iteration : 2 Analysis no. 11 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1128 0.013505 0.1128 0.0907 Mg 0.7895 0.017050 0.7895 0.6001 Sr 0.1189 0.011837 0.1189 0.0251 P 1.2375 0.040196 1.2375 0.7380 K 0.0441 0.008215 0.0441 0.0208 Cl 0.4248 0.014846 0.4248 0.2214 Ca 28.5155 0.135038 28.5155 13.1428 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0083 0.014108 0.0083 0.0027 Mn 0.0000 0.000000 0.0000 0.0000 C 15.0840 15.0840 23.1992 O 53.6646 53.6646 61.9592 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 12 x= 14466.0 y= -3372.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 15.0 5.8 4.5 3.30 0.0133 5.8 0.0309 Mg 145.4 1.9 3.8 38.35 0.0781 1.9 0.0127 Sr 34.6 2.7 14.5 2.39 0.0028 2.7 0.0392 P 66.8 2.7 2.0 34.24 0.0820 2.8 0.0360 K 13.1 6.2 7.1 1.84 0.0054 6.2 0.0209 Cl 34.9 3.1 2.3 15.40 0.0071 3.1 0.0224 Ca 3599.4 0.4 18.0 199.96 0.7816 0.5 0.0329 Ba 9.3 5.2 11.2 0.83 0.0000 5.2 0.0000 Fe 3.6 8.4 3.5 1.01 0.0000 8.4 0.0561 Mn 4.6 10.5 3.3 1.37 0.0012 10.5 0.0663 Elt. k-ratio Correc. Na 0.0007 2.3220 Mg 0.0057 1.6922 Sr 0.0017 1.3749 P 0.0129 1.1961 K 0.0005 1.0265 Cl 0.0039 1.1192 Ca 0.2837 1.0931 Ba 0.0000 NaN Fe 0.0000 1.2525 Mn 0.0003 1.2754 iteration : 3 Analysis no. 12 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1537 0.014553 0.1537 0.1268 Mg 0.9570 0.018693 0.9570 0.7470 Sr 0.2406 0.013281 0.2406 0.0521 P 1.5384 0.044600 1.5384 0.9423 K 0.0492 0.008296 0.0492 0.0239 Cl 0.4413 0.015075 0.4413 0.2362 Ca 31.0068 0.142543 31.0068 14.6769 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0008 0.013849 0.0008 0.0003 Mn 0.0441 0.022454 0.0441 0.0152 C 13.7963 13.7963 21.7917 O 51.7719 51.7719 61.3877 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 13 x= 14470.0 y= -3373.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 21.0 4.9 4.5 4.62 0.0209 4.9 0.0308 Mg 148.0 1.8 3.8 39.04 0.0796 1.9 0.0126 Sr 35.4 2.7 14.5 2.45 0.0030 2.7 0.0391 P 66.7 2.7 2.0 34.19 0.0819 2.8 0.0359 K 17.4 5.4 7.1 2.45 0.0093 5.4 0.0207 Cl 39.4 2.9 2.3 17.39 0.0081 2.9 0.0223 Ca 3907.3 0.4 18.0 217.06 0.8488 0.4 0.0328 Ba 10.9 4.8 11.2 0.97 0.0000 4.8 0.0000 Fe 3.5 8.4 3.5 0.99 0.0000 8.5 0.0000 Mn 4.1 11.0 3.3 1.24 0.0008 11.0 0.0662 Elt. k-ratio Correc. Na 0.0010 2.3186 Mg 0.0058 1.6911 Sr 0.0018 1.3718 P 0.0128 1.1928 K 0.0008 1.0175 Cl 0.0045 1.1136 Ca 0.3080 1.0894 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2728 iteration : 3 Analysis no. 13 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2416 0.016626 0.2416 0.2041 Mg 0.9740 0.018848 0.9740 0.7783 Sr 0.2502 0.013367 0.2502 0.0555 P 1.5317 0.044443 1.5317 0.9605 K 0.0844 0.009070 0.0844 0.0419 Cl 0.4997 0.015887 0.4997 0.2738 Ca 33.5593 0.150109 33.5593 16.2620 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0279 0.021758 0.0279 0.0099 C 12.7647 12.7647 20.6404 O 50.0664 50.0664 60.7737 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 14 x= 14474.0 y= -3373.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 8.5 7.7 4.5 1.87 0.0050 7.7 0.0309 Mg 128.8 2.0 3.8 33.97 0.0690 2.0 0.0127 Sr 27.5 3.0 14.5 1.90 0.0018 3.0 0.0391 P 68.5 2.7 2.0 35.14 0.0843 2.7 0.0359 K 16.4 5.5 7.1 2.31 0.0084 5.5 0.0208 Cl 41.0 2.8 2.3 18.08 0.0084 2.9 0.0223 Ca 3665.9 0.4 18.0 203.65 0.7964 0.5 0.0329 Ba 8.7 5.3 11.2 0.78 0.0000 5.4 0.0000 Fe 4.1 7.8 3.5 1.17 0.0003 7.8 0.0561 Mn 3.3 12.4 3.3 0.98 0.0000 12.4 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3245 Mg 0.0050 1.6915 Sr 0.0011 1.3730 P 0.0132 1.1938 K 0.0007 1.0244 Cl 0.0047 1.1173 Ca 0.2890 1.0926 Ba 0.0000 NaN Fe 0.0002 1.2522 Mn 0.0000 NaN iteration : 2 Analysis no. 14 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0582 0.011898 0.0582 0.0482 Mg 0.8446 0.017592 0.8446 0.6618 Sr 0.1562 0.012273 0.1562 0.0340 P 1.5773 0.045108 1.5773 0.9698 K 0.0767 0.008945 0.0767 0.0374 Cl 0.5227 0.016243 0.5227 0.2808 Ca 31.5783 0.144277 31.5783 15.0040 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0198 0.014402 0.0198 0.0067 Mn 0.0000 0.000000 0.0000 0.0000 C 13.6495 13.6495 21.6414 O 51.5166 51.5166 61.3160 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 15 x= 14478.0 y= -3373.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 15.7 5.6 4.5 3.44 0.0141 5.7 0.0309 Mg 132.8 1.9 3.8 35.04 0.0712 2.0 0.0127 Sr 34.2 2.7 14.5 2.36 0.0028 2.7 0.0391 P 69.3 2.7 2.0 35.55 0.0853 2.7 0.0360 K 15.3 5.7 7.1 2.15 0.0074 5.7 0.0208 Cl 38.7 2.9 2.3 17.09 0.0079 2.9 0.0223 Ca 3706.6 0.4 18.0 205.91 0.8053 0.5 0.0329 Ba 11.0 4.8 11.2 0.98 0.0000 4.8 0.0000 Fe 3.9 8.1 3.5 1.09 0.0002 8.1 0.0561 Mn 3.7 11.6 3.3 1.11 0.0004 11.6 0.0663 Elt. k-ratio Correc. Na 0.0007 2.3215 Mg 0.0052 1.6917 Sr 0.0017 1.3729 P 0.0134 1.1943 K 0.0007 1.0235 Cl 0.0044 1.1172 Ca 0.2922 1.0919 Ba 0.0000 NaN Fe 0.0001 1.2514 Mn 0.0001 1.2746 iteration : 3 Analysis no. 15 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1633 0.014796 0.1633 0.1358 Mg 0.8721 0.017869 0.8721 0.6863 Sr 0.2364 0.013222 0.2364 0.0516 P 1.5970 0.045391 1.5970 0.9862 K 0.0676 0.008725 0.0676 0.0331 Cl 0.4925 0.015814 0.4925 0.2657 Ca 31.9109 0.145256 31.9109 15.2285 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0107 0.014131 0.0107 0.0037 Mn 0.0136 0.021199 0.0136 0.0047 C 13.4410 13.4410 21.4042 O 51.1949 51.1949 61.2002 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 16 x= 14482.0 y= -3374.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 13.0 6.2 4.5 2.85 0.0107 6.2 0.0309 Mg 114.6 2.1 3.8 30.23 0.0612 2.1 0.0127 Sr 32.6 2.8 14.5 2.25 0.0026 2.8 0.0391 P 82.7 2.5 2.0 42.39 0.1022 2.5 0.0360 K 15.3 5.7 7.1 2.15 0.0074 5.7 0.0210 Cl 44.0 2.7 2.3 19.43 0.0091 2.8 0.0224 Ca 3476.6 0.4 18.0 193.14 0.7551 0.5 0.0330 Ba 11.3 4.7 11.2 1.00 0.0000 4.7 0.0747 Fe 3.4 8.6 3.5 0.96 0.0000 8.6 0.0000 Mn 3.2 12.6 3.3 0.95 0.0000 12.6 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3206 Mg 0.0044 1.6909 Sr 0.0016 1.3730 P 0.0160 1.1952 K 0.0007 1.0321 Cl 0.0050 1.1223 Ca 0.2740 1.0950 Ba 0.0000 1.5379 Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 16 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1235 0.013762 0.1235 0.1013 Mg 0.7486 0.016599 0.7486 0.5806 Sr 0.2164 0.012992 0.2164 0.0466 P 1.9152 0.049647 1.9152 1.1654 K 0.0682 0.008799 0.0682 0.0329 Cl 0.5667 0.016887 0.5667 0.3013 Ca 30.0048 0.139578 30.0048 14.1103 Ba 0.0006 0.019305 0.0006 0.0001 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 14.0394 14.0394 22.0314 O 52.3166 52.3166 61.6303 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 17 x= 14487.0 y= -3374.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 11.0 6.8 4.5 2.41 0.0081 6.8 0.0309 Mg 102.7 2.2 3.8 27.09 0.0546 2.2 0.0127 Sr 30.9 2.8 14.5 2.13 0.0023 2.9 0.0392 P 75.4 2.6 2.0 38.65 0.0929 2.6 0.0360 K 13.1 6.2 7.1 1.84 0.0054 6.2 0.0211 Cl 41.6 2.8 2.3 18.34 0.0085 2.8 0.0225 Ca 3325.3 0.4 18.0 184.73 0.7219 0.5 0.0330 Ba 9.4 5.2 11.2 0.84 0.0000 5.2 0.0000 Fe 3.4 8.6 3.5 0.95 0.0000 8.6 0.0000 Mn 3.5 11.9 3.3 1.05 0.0002 12.0 0.0664 Elt. k-ratio Correc. Na 0.0004 2.3249 Mg 0.0040 1.6932 Sr 0.0014 1.3748 P 0.0146 1.1969 K 0.0005 1.0358 Cl 0.0048 1.1242 Ca 0.2620 1.0968 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2778 iteration : 2 Analysis no. 17 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0943 0.012971 0.0943 0.0763 Mg 0.6690 0.015743 0.6690 0.5119 Sr 0.1969 0.012775 0.1969 0.0418 P 1.7441 0.047440 1.7441 1.0472 K 0.0496 0.008373 0.0496 0.0236 Cl 0.5340 0.016455 0.5340 0.2802 Ca 28.7362 0.135746 28.7362 13.3347 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0065 0.020945 0.0065 0.0022 C 14.6948 14.6948 22.7545 O 53.2746 53.2746 61.9276 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 18 x= 14491.0 y= -3374.0 z= -250. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 19.2 5.1 4.5 4.21 0.0185 5.1 0.0307 Mg 185.5 1.6 3.8 48.93 0.1003 1.7 0.0126 Sr 45.0 2.4 14.5 3.11 0.0043 2.4 0.0391 P 100.1 2.2 2.0 51.35 0.1243 2.3 0.0359 K 18.1 5.3 7.1 2.54 0.0099 5.3 0.0208 Cl 43.2 2.8 2.3 19.08 0.0089 2.8 0.0224 Ca 3842.4 0.4 18.0 213.45 0.8350 0.4 0.0329 Ba 13.0 4.4 11.2 1.15 0.0010 4.4 0.0747 Fe 3.8 8.2 3.5 1.06 0.0001 8.2 0.0559 Mn 4.1 11.1 3.3 1.22 0.0007 11.1 0.0661 Elt. k-ratio Correc. Na 0.0009 2.3064 Mg 0.0073 1.6839 Sr 0.0027 1.3705 P 0.0195 1.1935 K 0.0009 1.0240 Cl 0.0050 1.1189 Ca 0.3030 1.0901 Ba 0.0003 1.5378 Fe 0.0001 1.2477 Mn 0.0002 1.2713 iteration : 3 Analysis no. 18 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2134 0.015932 0.2134 0.1813 Mg 1.2226 0.021041 1.2226 0.9826 Sr 0.3652 0.014608 0.3652 0.0814 P 2.3263 0.054663 2.3263 1.4671 K 0.0903 0.009253 0.0903 0.0451 Cl 0.5542 0.016692 0.5542 0.3053 Ca 33.0345 0.148580 33.0345 16.0995 Ba 0.0444 0.020024 0.0444 0.0063 Fe 0.0074 0.013996 0.0074 0.0026 Mn 0.0261 0.021669 0.0261 0.0093 C 12.3000 12.3000 20.0032 O 49.8156 49.8156 60.8163 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 19 x= 14495.0 y= -3374.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 15.3 5.7 4.5 3.35 0.0136 5.7 0.0308 Mg 181.2 1.7 3.8 47.79 0.0979 1.7 0.0126 Sr 34.0 2.7 14.5 2.35 0.0028 2.7 0.0392 P 98.1 2.3 2.0 50.30 0.1217 2.3 0.0360 K 16.9 5.4 7.1 2.37 0.0089 5.5 0.0211 Cl 46.4 2.7 2.3 20.45 0.0096 2.7 0.0225 Ca 3456.3 0.4 18.0 192.01 0.7508 0.5 0.0330 Ba 9.3 5.2 11.2 0.83 0.0000 5.2 0.0000 Fe 3.9 8.0 3.5 1.11 0.0002 8.0 0.0561 Mn 3.6 11.8 3.3 1.08 0.0003 11.8 0.0663 Elt. k-ratio Correc. Na 0.0007 2.3102 Mg 0.0071 1.6859 Sr 0.0017 1.3746 P 0.0191 1.1966 K 0.0008 1.0353 Cl 0.0053 1.1251 Ca 0.2725 1.0952 Ba 0.0000 NaN Fe 0.0001 1.2524 Mn 0.0001 1.2751 iteration : 2 Analysis no. 19 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1567 0.014581 0.1567 0.1291 Mg 1.1952 0.020819 1.1952 0.9316 Sr 0.2338 0.013208 0.2338 0.0506 P 2.2839 0.054235 2.2839 1.3970 K 0.0813 0.009130 0.0813 0.0394 Cl 0.5995 0.017351 0.5995 0.3204 Ca 29.8435 0.139106 29.8435 14.1067 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0124 0.014194 0.0124 0.0042 Mn 0.0101 0.021063 0.0101 0.0035 C 13.6315 13.6315 21.5015 O 51.9522 51.9522 61.5161 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 20 x= 14499.0 y= -3375.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 19.0 5.1 4.5 4.18 0.0183 5.1 0.0308 Mg 174.2 1.7 3.8 45.96 0.0941 1.7 0.0126 Sr 34.1 2.7 14.5 2.36 0.0028 2.7 0.0392 P 98.6 2.2 2.0 50.58 0.1224 2.3 0.0361 K 14.8 5.8 7.1 2.08 0.0069 5.8 0.0211 Cl 42.8 2.8 2.3 18.90 0.0088 2.8 0.0225 Ca 3373.9 0.4 18.0 187.43 0.7329 0.5 0.0330 Ba 9.2 5.2 11.2 0.82 0.0000 5.2 0.0000 Fe 4.0 7.9 3.5 1.12 0.0002 8.0 0.0562 Mn 3.7 11.6 3.3 1.11 0.0004 11.6 0.0664 Elt. k-ratio Correc. Na 0.0009 2.3107 Mg 0.0068 1.6874 Sr 0.0017 1.3755 P 0.0192 1.1976 K 0.0006 1.0377 Cl 0.0049 1.1267 Ca 0.2660 1.0961 Ba 0.0000 NaN Fe 0.0001 1.2532 Mn 0.0001 1.2758 iteration : 2 Analysis no. 20 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2116 0.015914 0.2116 0.1733 Mg 1.1494 0.020430 1.1494 0.8904 Sr 0.2355 0.013235 0.2355 0.0506 P 2.2991 0.054441 2.2991 1.3976 K 0.0640 0.008739 0.0640 0.0308 Cl 0.5527 0.016737 0.5527 0.2935 Ca 29.1549 0.137033 29.1549 13.6961 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0140 0.014253 0.0140 0.0047 Mn 0.0136 0.021227 0.0136 0.0047 C 13.8987 13.8987 21.7875 O 52.4065 52.4065 61.6708 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 21 x= 14503.0 y= -3375.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 18.8 5.2 4.5 4.13 0.0181 5.2 0.0307 Mg 169.8 1.7 3.8 44.78 0.0916 1.7 0.0126 Sr 37.8 2.6 14.5 2.61 0.0033 2.6 0.0392 P 95.4 2.3 2.0 48.94 0.1184 2.3 0.0360 K 13.2 6.1 7.1 1.86 0.0055 6.2 0.0210 Cl 47.1 2.7 2.3 20.79 0.0097 2.7 0.0225 Ca 3512.6 0.4 18.0 195.13 0.7629 0.5 0.0330 Ba 10.5 4.9 11.2 0.94 0.0000 4.9 0.0000 Fe 3.5 8.4 3.5 1.00 0.0000 8.4 NaN Mn 3.5 11.9 3.3 1.05 0.0002 12.0 0.0663 Elt. k-ratio Correc. Na 0.0009 2.3101 Mg 0.0066 1.6866 Sr 0.0020 1.3738 P 0.0186 1.1962 K 0.0005 1.0334 Cl 0.0054 1.1239 Ca 0.2769 1.0944 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2747 iteration : 2 Analysis no. 21 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2086 0.015836 0.2086 0.1725 Mg 1.1185 0.020149 1.1185 0.8748 Sr 0.2794 0.013712 0.2794 0.0606 P 2.2197 0.053450 2.2197 1.3623 K 0.0508 0.008386 0.0508 0.0247 Cl 0.6092 0.017466 0.6092 0.3266 Ca 30.3023 0.140466 30.3023 14.3725 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0065 0.020897 0.0065 0.0022 C 13.5110 13.5110 21.3842 O 51.6941 51.6941 61.4196 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 22 x= 14507.0 y= -3375.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 21.4 4.8 4.5 4.69 0.0213 4.9 0.0307 Mg 159.6 1.8 3.8 42.10 0.0860 1.8 0.0126 Sr 41.9 2.4 14.5 2.89 0.0039 2.5 0.0391 P 94.5 2.3 2.0 48.47 0.1172 2.3 0.0359 K 16.4 5.5 7.1 2.31 0.0084 5.5 0.0209 Cl 47.7 2.6 2.3 21.05 0.0099 2.6 0.0224 Ca 3690.0 0.4 18.0 204.99 0.8014 0.5 0.0329 Ba 11.6 4.6 11.2 1.03 0.0002 4.7 0.0746 Fe 3.7 8.2 3.5 1.05 0.0001 8.2 0.0560 Mn 2.6 13.9 3.3 0.78 0.0000 13.9 0.0000 Elt. k-ratio Correc. Na 0.0011 2.3096 Mg 0.0062 1.6865 Sr 0.0024 1.3715 P 0.0184 1.1944 K 0.0007 1.0281 Cl 0.0055 1.1207 Ca 0.2909 1.0922 Ba 0.0001 1.5377 Fe 0.0000 1.2498 Mn 0.0000 NaN iteration : 3 Analysis no. 22 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2458 0.016676 0.2458 0.2060 Mg 1.0496 0.019525 1.0496 0.8319 Sr 0.3276 0.014215 0.3276 0.0720 P 2.1943 0.053096 2.1943 1.3647 K 0.0770 0.008975 0.0770 0.0379 Cl 0.6154 0.017517 0.6154 0.3344 Ca 31.7669 0.144819 31.7669 15.2676 Ba 0.0090 0.019437 0.0090 0.0013 Fe 0.0058 0.013966 0.0058 0.0020 Mn 0.0000 0.000000 0.0000 0.0000 C 12.9571 12.9571 20.7803 O 50.7515 50.7515 61.1019 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Mn ( 0.00) point n : 23 x= 14512.0 y= -3376.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 23.2 4.6 4.5 5.10 0.0237 4.7 0.0307 Mg 165.7 1.7 3.8 43.70 0.0893 1.8 0.0126 Sr 38.9 2.5 14.5 2.69 0.0034 2.5 0.0391 P 96.8 2.3 2.0 49.63 0.1201 2.3 0.0360 K 17.0 5.4 7.1 2.39 0.0090 5.4 0.0210 Cl 53.0 2.5 2.3 23.39 0.0110 2.5 0.0224 Ca 3582.3 0.4 18.0 199.01 0.7781 0.5 0.0329 Ba 10.2 5.0 11.2 0.90 0.0000 5.0 0.0000 Fe 2.9 9.3 3.5 0.82 0.0000 9.3 0.0000 Mn 4.1 11.1 3.3 1.22 0.0007 11.1 0.0662 Elt. k-ratio Correc. Na 0.0012 2.3083 Mg 0.0065 1.6866 Sr 0.0021 1.3727 P 0.0188 1.1952 K 0.0008 1.0319 Cl 0.0061 1.1227 Ca 0.2824 1.0936 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2738 iteration : 3 Analysis no. 23 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2728 0.017260 0.2728 0.2270 Mg 1.0907 0.019900 1.0907 0.8587 Sr 0.2923 0.013845 0.2923 0.0638 P 2.2497 0.053787 2.2497 1.3899 K 0.0823 0.009125 0.0823 0.0403 Cl 0.6886 0.018465 0.6886 0.3717 Ca 30.8809 0.142193 30.8809 14.7441 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0261 0.021707 0.0261 0.0091 C 13.2220 13.2220 21.0656 O 51.1946 51.1946 61.2297 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 24 x= 14516.0 y= -3376.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 18.1 5.3 4.5 3.98 0.0172 5.3 0.0307 Mg 135.6 1.9 3.8 35.76 0.0727 1.9 0.0126 Sr 42.7 2.4 14.5 2.95 0.0040 2.4 0.0390 P 98.3 2.3 2.0 50.40 0.1219 2.3 0.0359 K 17.7 5.3 7.1 2.49 0.0096 5.3 0.0210 Cl 57.0 2.4 2.3 25.14 0.0119 2.4 0.0224 Ca 3632.4 0.4 18.0 201.79 0.7889 0.5 0.0329 Ba 12.2 4.5 11.2 1.08 0.0006 4.5 0.0746 Fe 4.1 7.8 3.5 1.16 0.0003 7.8 0.0560 Mn 3.3 12.4 3.3 0.98 0.0000 12.4 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3107 Mg 0.0053 1.6864 Sr 0.0025 1.3702 P 0.0191 1.1938 K 0.0008 1.0306 Cl 0.0066 1.1215 Ca 0.2863 1.0929 Ba 0.0002 1.5373 Fe 0.0002 1.2501 Mn 0.0000 NaN iteration : 3 Analysis no. 24 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1984 0.015597 0.1984 0.1657 Mg 0.8877 0.017992 0.8877 0.7013 Sr 0.3366 0.014301 0.3366 0.0738 P 2.2823 0.054139 2.2823 1.4148 K 0.0875 0.009234 0.0875 0.0430 Cl 0.7416 0.019099 0.7416 0.4016 Ca 31.2914 0.143409 31.2914 14.9912 Ba 0.0245 0.019688 0.0245 0.0034 Fe 0.0189 0.014352 0.0189 0.0065 Mn 0.0000 0.000000 0.0000 0.0000 C 13.1321 13.1321 20.9939 O 50.9992 50.9992 61.2047 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Mn ( 0.00) point n : 25 x= 14520.0 y= -3376.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 22.7 4.7 4.5 4.99 0.0230 4.7 0.0308 Mg 149.1 1.8 3.8 39.34 0.0802 1.9 0.0126 Sr 43.7 2.4 14.5 3.02 0.0041 2.4 0.0391 P 90.7 2.3 2.0 46.53 0.1124 2.4 0.0360 K 16.3 5.5 7.1 2.29 0.0083 5.6 0.0210 Cl 48.2 2.6 2.3 21.24 0.0100 2.6 0.0224 Ca 3585.8 0.4 18.0 199.20 0.7788 0.5 0.0329 Ba 11.1 4.7 11.2 0.99 0.0000 4.7 0.0000 Fe 3.6 8.4 3.5 1.01 0.0000 8.4 0.0561 Mn 4.1 11.1 3.3 1.22 0.0007 11.1 0.0662 Elt. k-ratio Correc. Na 0.0012 2.3112 Mg 0.0058 1.6880 Sr 0.0025 1.3724 P 0.0176 1.1956 K 0.0007 1.0309 Cl 0.0055 1.1221 Ca 0.2827 1.0934 Ba 0.0000 NaN Fe 0.0000 1.2509 Mn 0.0002 1.2740 iteration : 3 Analysis no. 25 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2658 0.017124 0.2658 0.2209 Mg 0.9802 0.018892 0.9802 0.7706 Sr 0.3494 0.014456 0.3494 0.0762 P 2.1068 0.052060 2.1068 1.2996 K 0.0760 0.008973 0.0760 0.0371 Cl 0.6222 0.017620 0.6222 0.3353 Ca 30.9052 0.142259 30.9052 14.7327 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0008 0.013835 0.0008 0.0003 Mn 0.0261 0.021710 0.0261 0.0091 C 13.3521 13.3521 21.2397 O 51.3154 51.3154 61.2785 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 26 x= 14524.0 y= -3377.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 16.5 5.5 4.5 3.63 0.0152 5.5 0.0309 Mg 75.6 2.6 3.8 19.93 0.0396 2.6 0.0127 Sr 27.1 3.0 14.5 1.87 0.0018 3.1 0.0392 P 80.8 2.5 2.0 41.42 0.0998 2.5 0.0361 K 14.7 5.8 7.1 2.07 0.0069 5.8 0.0213 Cl 49.9 2.6 2.3 22.01 0.0103 2.6 0.0226 Ca 3043.9 0.4 18.0 169.10 0.6606 0.5 0.0332 Ba 8.9 5.3 11.2 0.79 0.0000 5.3 0.0000 Fe 3.5 8.4 3.5 1.00 0.0000 8.4 NaN Mn 4.1 11.1 3.3 1.22 0.0007 11.1 0.0666 Elt. k-ratio Correc. Na 0.0008 2.3254 Mg 0.0029 1.6957 Sr 0.0011 1.3763 P 0.0156 1.1986 K 0.0006 1.0458 Cl 0.0058 1.1294 Ca 0.2398 1.1004 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2799 iteration : 2 Analysis no. 26 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1761 0.015132 0.1761 0.1398 Mg 0.4863 0.013580 0.4863 0.3653 Sr 0.1509 0.012233 0.1509 0.0314 P 1.8754 0.049207 1.8754 1.1053 K 0.0640 0.008795 0.0640 0.0299 Cl 0.6500 0.018040 0.6500 0.3347 Ca 26.3829 0.128582 26.3829 12.0163 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0263 0.021813 0.0263 0.0087 C 15.5425 15.5425 23.6220 O 54.6456 54.6456 62.3465 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 27 x= 14528.0 y= -3377.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 23.9 4.6 4.5 5.24 0.0245 4.6 0.0308 Mg 91.9 2.3 3.8 24.25 0.0486 2.4 0.0127 Sr 34.8 2.7 14.5 2.40 0.0029 2.7 0.0391 P 86.1 2.4 2.0 44.16 0.1066 2.4 0.0360 K 16.7 5.5 7.1 2.35 0.0087 5.5 0.0211 Cl 54.4 2.5 2.3 24.00 0.0113 2.5 0.0225 Ca 3375.2 0.4 18.0 187.50 0.7328 0.5 0.0330 Ba 11.7 4.6 11.2 1.04 0.0003 4.6 0.0746 Fe 4.3 7.6 3.5 1.23 0.0004 7.6 0.0562 Mn 3.9 11.4 3.3 1.16 0.0005 11.4 0.0664 Elt. k-ratio Correc. Na 0.0012 2.3188 Mg 0.0035 1.6931 Sr 0.0018 1.3729 P 0.0167 1.1958 K 0.0008 1.0364 Cl 0.0063 1.1243 Ca 0.2660 1.0961 Ba 0.0001 1.5369 Fe 0.0002 1.2537 Mn 0.0001 1.2763 iteration : 3 Analysis no. 27 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2835 0.017541 0.2835 0.2314 Mg 0.5962 0.014912 0.5962 0.4602 Sr 0.2433 0.013299 0.2433 0.0521 P 1.9977 0.050703 1.9977 1.2099 K 0.0801 0.009107 0.0801 0.0384 Cl 0.7081 0.018718 0.7081 0.3747 Ca 29.1508 0.136995 29.1508 13.6441 Ba 0.0122 0.019482 0.0122 0.0017 Fe 0.0264 0.014605 0.0264 0.0089 Mn 0.0190 0.021450 0.0190 0.0065 C 14.2621 14.2621 22.2755 O 52.6207 52.6207 61.6967 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 28 x= 14532.0 y= -3377.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 24.5 4.5 4.5 5.38 0.0253 4.5 0.0307 Mg 165.3 1.7 3.8 43.59 0.0891 1.8 0.0126 Sr 39.4 2.5 14.5 2.72 0.0035 2.5 0.0392 P 86.2 2.4 2.0 44.22 0.1067 2.4 0.0361 K 18.4 5.2 7.1 2.58 0.0102 5.2 0.0212 Cl 66.0 2.2 2.3 29.12 0.0138 2.2 0.0225 Ca 3286.6 0.4 18.0 182.58 0.7135 0.5 0.0331 Ba 11.2 4.7 11.2 1.00 0.0000 4.7 0.0000 Fe 3.4 8.5 3.5 0.97 0.0000 8.6 0.0000 Mn 3.4 12.1 3.3 1.02 0.0001 12.1 0.0664 Elt. k-ratio Correc. Na 0.0013 2.3088 Mg 0.0065 1.6881 Sr 0.0022 1.3759 P 0.0167 1.1986 K 0.0009 1.0413 Cl 0.0077 1.1269 Ca 0.2590 1.0974 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2762 iteration : 2 Analysis no. 28 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2911 0.017652 0.2911 0.2371 Mg 1.0890 0.019893 1.0890 0.8388 Sr 0.2993 0.013947 0.2993 0.0640 P 2.0049 0.050855 2.0049 1.2118 K 0.0943 0.009463 0.0943 0.0452 Cl 0.8679 0.020611 0.8679 0.4583 Ca 28.4163 0.134785 28.4163 13.2739 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0029 0.020767 0.0029 0.0010 C 14.2744 14.2744 22.2503 O 52.6599 52.6599 61.6197 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 29 x= 14537.0 y= -3378.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 14.6 5.9 4.5 3.20 0.0127 5.9 0.0308 Mg 118.2 2.1 3.8 31.18 0.0631 2.1 0.0126 Sr 37.0 2.6 14.5 2.56 0.0032 2.6 0.0391 P 81.0 2.5 2.0 41.52 0.1000 2.5 0.0360 K 17.5 5.3 7.1 2.46 0.0094 5.4 0.0210 Cl 59.1 2.4 2.3 26.06 0.0123 2.4 0.0224 Ca 3517.0 0.4 18.0 195.38 0.7639 0.5 0.0330 Ba 10.4 4.9 11.2 0.92 0.0000 4.9 0.0000 Fe 3.2 8.8 3.5 0.91 0.0000 8.8 0.0000 Mn 3.2 12.5 3.3 0.96 0.0000 12.5 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3174 Mg 0.0046 1.6894 Sr 0.0020 1.3720 P 0.0157 1.1947 K 0.0008 1.0322 Cl 0.0069 1.1214 Ca 0.2772 1.0945 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 29 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1468 0.014360 0.1468 0.1210 Mg 0.7723 0.016840 0.7723 0.6019 Sr 0.2698 0.013591 0.2698 0.0583 P 1.8740 0.049106 1.8740 1.1461 K 0.0860 0.009213 0.0860 0.0417 Cl 0.7697 0.019433 0.7697 0.4113 Ca 30.3427 0.140593 30.3427 14.3411 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 13.8510 13.8510 21.8454 O 51.8877 51.8877 61.4332 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 30 x= 14541.0 y= -3378.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 17.7 5.3 4.5 3.88 0.0166 5.3 0.0310 Mg 88.8 2.4 3.8 23.43 0.0469 2.4 0.0127 Sr 22.8 3.3 14.5 1.57 0.0012 3.3 0.0394 P 65.1 2.8 2.0 33.39 0.0800 2.8 0.0363 K 13.8 6.0 7.1 1.94 0.0061 6.0 0.0216 Cl 53.4 2.5 2.3 23.54 0.0111 2.5 0.0227 Ca 2630.6 0.4 18.0 146.14 0.5705 0.5 0.0333 Ba 7.9 5.6 11.2 0.70 0.0000 5.6 0.0000 Fe 3.1 9.0 3.5 0.87 0.0000 9.1 0.0000 Mn 3.8 11.5 3.3 1.13 0.0004 11.6 0.0668 Elt. k-ratio Correc. Na 0.0008 2.3284 Mg 0.0034 1.6990 Sr 0.0007 1.3826 P 0.0125 1.2040 K 0.0005 1.0588 Cl 0.0062 1.1359 Ca 0.2070 1.1057 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2838 iteration : 2 Analysis no. 30 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1933 0.015563 0.1933 0.1488 Mg 0.5773 0.014718 0.5773 0.4203 Sr 0.1001 0.011637 0.1001 0.0202 P 1.5098 0.044358 1.5098 0.8626 K 0.0571 0.008719 0.0571 0.0259 Cl 0.7014 0.018743 0.7014 0.3501 Ca 22.8904 0.117688 22.8904 10.1061 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0155 0.021432 0.0155 0.0050 C 17.0688 17.0688 25.1469 O 56.8862 56.8862 62.9142 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 31 x= 14545.0 y= -3378.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 13.5 6.1 4.5 2.97 0.0114 6.1 0.0310 Mg 112.4 2.1 3.8 29.64 0.0599 2.1 0.0127 Sr 29.2 2.9 14.5 2.02 0.0021 2.9 0.0394 P 57.1 3.0 2.0 29.26 0.0698 3.0 0.0362 K 14.2 5.9 7.1 2.00 0.0064 5.9 0.0214 Cl 52.2 2.5 2.3 23.04 0.0108 2.5 0.0227 Ca 2790.0 0.4 18.0 154.99 0.6053 0.5 0.0333 Ba 9.1 5.2 11.2 0.81 0.0000 5.2 0.0000 Fe 3.2 8.9 3.5 0.90 0.0000 8.9 0.0000 Mn 2.8 13.5 3.3 0.83 0.0000 13.5 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3273 Mg 0.0043 1.6969 Sr 0.0013 1.3820 P 0.0109 1.2036 K 0.0006 1.0530 Cl 0.0060 1.1326 Ca 0.2197 1.1035 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 31 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1320 0.014022 0.1320 0.1027 Mg 0.7362 0.016499 0.7362 0.5417 Sr 0.1775 0.012602 0.1775 0.0362 P 1.3171 0.041528 1.3171 0.7605 K 0.0602 0.008755 0.0602 0.0275 Cl 0.6839 0.018498 0.6839 0.3450 Ca 24.2432 0.121952 24.2432 10.8175 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.6066 16.6066 24.7266 O 56.0433 56.0433 62.6423 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 32 x= 14549.0 y= -3379.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 22.1 4.8 4.5 4.85 0.0222 4.8 0.0308 Mg 161.5 1.8 3.8 42.60 0.0871 1.8 0.0127 Sr 38.9 2.5 14.5 2.68 0.0034 2.6 0.0393 P 72.7 2.6 2.0 37.29 0.0896 2.6 0.0361 K 18.0 5.3 7.1 2.53 0.0099 5.3 0.0212 Cl 67.2 2.2 2.3 29.65 0.0141 2.2 0.0225 Ca 3293.8 0.4 18.0 182.98 0.7154 0.5 0.0331 Ba 11.9 4.6 11.2 1.06 0.0004 4.6 0.0747 Fe 3.6 8.4 3.5 1.01 0.0000 8.4 0.0562 Mn 3.8 11.5 3.3 1.13 0.0004 11.6 0.0664 Elt. k-ratio Correc. Na 0.0011 2.3128 Mg 0.0063 1.6898 Sr 0.0021 1.3767 P 0.0141 1.1989 K 0.0009 1.0398 Cl 0.0079 1.1254 Ca 0.2596 1.0971 Ba 0.0001 1.5363 Fe 0.0000 1.2542 Mn 0.0001 1.2766 iteration : 3 Analysis no. 32 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2566 0.016937 0.2566 0.2085 Mg 1.0652 0.019693 1.0652 0.8189 Sr 0.2927 0.013886 0.2927 0.0624 P 1.6848 0.046695 1.6848 1.0164 K 0.0909 0.009379 0.0909 0.0434 Cl 0.8835 0.020773 0.8835 0.4656 Ca 28.4862 0.135012 28.4862 13.2804 Ba 0.0161 0.019550 0.0161 0.0022 Fe 0.0016 0.013902 0.0016 0.0006 Mn 0.0154 0.021317 0.0154 0.0053 C 14.4614 14.4614 22.4975 O 52.7456 52.7456 61.5988 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 33 x= 14553.0 y= -3379.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 29.6 4.1 4.5 6.50 0.0317 4.1 0.0308 Mg 145.5 1.9 3.8 38.38 0.0782 1.9 0.0127 Sr 37.6 2.6 14.5 2.60 0.0033 2.6 0.0393 P 69.1 2.7 2.0 35.42 0.0850 2.7 0.0361 K 18.0 5.3 7.1 2.53 0.0099 5.3 0.0212 Cl 65.7 2.3 2.3 28.99 0.0138 2.3 0.0225 Ca 3286.2 0.4 18.0 182.56 0.7138 0.5 0.0331 Ba 10.6 4.9 11.2 0.94 0.0000 4.9 0.0000 Fe 3.3 8.7 3.5 0.93 0.0000 8.7 0.0000 Mn 3.2 12.5 3.3 0.96 0.0000 12.5 0.0000 Elt. k-ratio Correc. Na 0.0016 2.3136 Mg 0.0057 1.6923 Sr 0.0020 1.3769 P 0.0133 1.1989 K 0.0009 1.0395 Cl 0.0077 1.1250 Ca 0.2590 1.0973 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 3 Analysis no. 33 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3667 0.019205 0.3667 0.2974 Mg 0.9585 0.018715 0.9585 0.7354 Sr 0.2778 0.013723 0.2778 0.0591 P 1.5979 0.045503 1.5979 0.9621 K 0.0909 0.009376 0.0909 0.0433 Cl 0.8628 0.020540 0.8628 0.4538 Ca 28.4236 0.134825 28.4236 13.2253 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 14.5675 14.5675 22.6184 O 52.8545 52.8545 61.6052 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 34 x= 14557.0 y= -3379.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 21.1 4.9 4.5 4.63 0.0210 4.9 0.0310 Mg 99.5 2.2 3.8 26.26 0.0529 2.3 0.0127 Sr 30.0 2.9 14.5 2.07 0.0022 2.9 0.0393 P 63.9 2.8 2.0 32.75 0.0785 2.8 0.0362 K 19.7 5.0 7.1 2.77 0.0114 5.0 0.0213 Cl 57.8 2.4 2.3 25.48 0.0121 2.4 0.0226 Ca 3085.9 0.4 18.0 171.43 0.6704 0.5 0.0332 Ba 10.4 4.9 11.2 0.92 0.0000 4.9 0.0000 Fe 3.7 8.3 3.5 1.04 0.0001 8.3 0.0564 Mn 3.1 12.7 3.3 0.93 0.0000 12.7 0.0000 Elt. k-ratio Correc. Na 0.0010 2.3237 Mg 0.0038 1.6961 Sr 0.0014 1.3778 P 0.0123 1.1996 K 0.0010 1.0439 Cl 0.0067 1.1273 Ca 0.2433 1.0998 Ba 0.0000 NaN Fe 0.0000 1.2577 Mn 0.0000 NaN iteration : 2 Analysis no. 34 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2432 0.016700 0.2432 0.1936 Mg 0.6494 0.015546 0.6494 0.4890 Sr 0.1861 0.012680 0.1861 0.0389 P 1.4755 0.043799 1.4755 0.8718 K 0.1060 0.009745 0.1060 0.0496 Cl 0.7566 0.019342 0.7566 0.3905 Ca 26.7574 0.129771 26.7574 12.2168 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0041 0.014021 0.0041 0.0014 Mn 0.0000 0.000000 0.0000 0.0000 C 15.5112 15.5112 23.6323 O 54.3104 54.3104 62.1163 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 35 x= 14562.0 y= -3380.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 16.3 5.5 4.5 3.58 0.0149 5.5 0.0311 Mg 95.2 2.3 3.8 25.11 0.0505 2.3 0.0127 Sr 24.1 3.2 14.5 1.67 0.0014 3.2 0.0395 P 49.4 3.2 2.0 25.31 0.0601 3.2 0.0364 K 16.1 5.6 7.1 2.26 0.0081 5.6 0.0217 Cl 53.7 2.5 2.3 23.67 0.0112 2.5 0.0228 Ca 2479.9 0.4 18.0 137.77 0.5379 0.5 0.0334 Ba 8.4 5.5 11.2 0.74 0.0000 5.5 0.0000 Fe 3.3 8.7 3.5 0.94 0.0000 8.7 0.0000 Mn 2.8 13.5 3.3 0.83 0.0000 13.5 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3313 Mg 0.0037 1.7008 Sr 0.0008 1.3856 P 0.0094 1.2067 K 0.0007 1.0630 Cl 0.0062 1.1374 Ca 0.1952 1.1076 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 35 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1737 0.015110 0.1737 0.1320 Mg 0.6216 0.015251 0.6216 0.4469 Sr 0.1167 0.011881 0.1167 0.0233 P 1.1366 0.038780 1.1366 0.6412 K 0.0767 0.009221 0.0767 0.0343 Cl 0.7070 0.018834 0.7070 0.3485 Ca 21.6230 0.113678 21.6230 9.4270 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.7658 17.7658 25.8459 O 57.7788 57.7788 63.1009 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 36 x= 14566.0 y= -3380.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 24.2 4.5 4.5 5.32 0.0250 4.6 0.0311 Mg 89.3 2.4 3.8 23.55 0.0472 2.4 0.0128 Sr 25.4 3.1 14.5 1.75 0.0015 3.2 0.0395 P 42.2 3.4 2.0 21.62 0.0510 3.5 0.0363 K 18.5 5.2 7.1 2.61 0.0104 5.2 0.0215 Cl 56.6 2.4 2.3 24.98 0.0118 2.4 0.0226 Ca 2757.6 0.4 18.0 153.19 0.5987 0.5 0.0333 Ba 8.8 5.3 11.2 0.78 0.0000 5.3 0.0000 Fe 3.8 8.2 3.5 1.06 0.0001 8.2 0.0566 Mn 3.1 12.8 3.3 0.92 0.0000 12.8 0.0000 Elt. k-ratio Correc. Na 0.0012 2.3306 Mg 0.0034 1.7019 Sr 0.0009 1.3832 P 0.0080 1.2039 K 0.0009 1.0527 Cl 0.0066 1.1312 Ca 0.2173 1.1039 Ba 0.0000 NaN Fe 0.0001 1.2621 Mn 0.0000 NaN iteration : 2 Analysis no. 36 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2905 0.017759 0.2905 0.2249 Mg 0.5819 0.014792 0.5819 0.4262 Sr 0.1313 0.012049 0.1313 0.0267 P 0.9618 0.035817 0.9618 0.5527 K 0.0967 0.009605 0.0967 0.0440 Cl 0.7438 0.019226 0.7438 0.3735 Ca 23.9839 0.121169 23.9839 10.6522 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0075 0.014169 0.0075 0.0024 Mn 0.0000 0.000000 0.0000 0.0000 C 16.9270 16.9270 25.0868 O 56.2757 56.2757 62.6106 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 37 x= 14570.0 y= -3380.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 23.6 4.6 4.5 5.18 0.0241 4.6 0.0310 Mg 102.6 2.2 3.8 27.06 0.0546 2.2 0.0127 Sr 27.2 3.0 14.5 1.88 0.0018 3.0 0.0395 P 43.4 3.4 2.0 22.23 0.0525 3.4 0.0363 K 19.4 5.1 7.1 2.73 0.0111 5.1 0.0214 Cl 62.7 2.3 2.3 27.68 0.0131 2.3 0.0226 Ca 2898.6 0.4 18.0 161.02 0.6296 0.5 0.0333 Ba 9.7 5.1 11.2 0.86 0.0000 5.1 0.0000 Fe 3.4 8.5 3.5 0.97 0.0000 8.6 0.0000 Mn 3.3 12.3 3.3 0.99 0.0000 12.3 0.0000 Elt. k-ratio Correc. Na 0.0012 2.3276 Mg 0.0040 1.6996 Sr 0.0011 1.3817 P 0.0082 1.2024 K 0.0010 1.0486 Cl 0.0073 1.1287 Ca 0.2285 1.1022 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 37 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2806 0.017537 0.2806 0.2197 Mg 0.6718 0.015817 0.6718 0.4975 Sr 0.1529 0.012310 0.1529 0.0314 P 0.9895 0.036276 0.9895 0.5751 K 0.1036 0.009728 0.1036 0.0477 Cl 0.8258 0.020165 0.8258 0.4193 Ca 25.1854 0.124933 25.1854 11.3120 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.3899 16.3899 24.5649 O 55.4007 55.4007 62.3324 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 38 x= 14574.0 y= -3381.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 27.2 4.3 4.5 5.98 0.0288 4.3 0.0309 Mg 136.5 1.9 3.8 36.00 0.0733 1.9 0.0127 Sr 34.8 2.7 14.5 2.40 0.0029 2.7 0.0393 P 42.0 3.4 2.0 21.52 0.0507 3.5 0.0361 K 19.5 5.1 7.1 2.74 0.0112 5.1 0.0210 Cl 70.1 2.2 2.3 30.93 0.0147 2.2 0.0224 Ca 3502.9 0.4 18.0 194.59 0.7618 0.5 0.0330 Ba 11.1 4.7 11.2 0.99 0.0000 4.8 0.0000 Fe 3.8 8.1 3.5 1.07 0.0001 8.1 0.0563 Mn 4.1 11.0 3.3 1.24 0.0008 11.0 0.0665 Elt. k-ratio Correc. Na 0.0014 2.3208 Mg 0.0053 1.6952 Sr 0.0018 1.3764 P 0.0080 1.1970 K 0.0010 1.0299 Cl 0.0082 1.1179 Ca 0.2765 1.0944 Ba 0.0000 NaN Fe 0.0001 1.2533 Mn 0.0002 1.2761 iteration : 3 Analysis no. 38 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3335 0.018598 0.3335 0.2734 Mg 0.8998 0.018173 0.8998 0.6976 Sr 0.2440 0.013348 0.2440 0.0525 P 0.9518 0.035542 0.9518 0.5790 K 0.1026 0.009573 0.1026 0.0494 Cl 0.9177 0.021085 0.9177 0.4877 Ca 30.2561 0.140385 30.2561 14.2246 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0083 0.014100 0.0083 0.0028 Mn 0.0280 0.021849 0.0280 0.0096 C 14.2932 14.2932 22.4237 O 51.9651 51.9651 61.1996 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 39 x= 14578.0 y= -3381.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 29.7 4.1 4.5 6.53 0.0320 4.1 0.0310 Mg 128.7 2.0 3.8 33.95 0.0691 2.0 0.0127 Sr 33.8 2.7 14.5 2.34 0.0027 2.7 0.0394 P 42.2 3.4 2.0 21.64 0.0510 3.5 0.0362 K 22.1 4.8 7.1 3.11 0.0136 4.8 0.0211 Cl 63.9 2.3 2.3 28.19 0.0134 2.3 0.0225 Ca 3360.6 0.4 18.0 186.69 0.7309 0.5 0.0331 Ba 11.9 4.6 11.2 1.06 0.0004 4.6 0.0748 Fe 3.6 8.3 3.5 1.03 0.0001 8.3 0.0564 Mn 2.9 13.2 3.3 0.86 0.0000 13.2 0.0000 Elt. k-ratio Correc. Na 0.0016 2.3217 Mg 0.0050 1.6969 Sr 0.0017 1.3780 P 0.0080 1.1986 K 0.0012 1.0339 Cl 0.0075 1.1205 Ca 0.2653 1.0962 Ba 0.0001 1.5375 Fe 0.0000 1.2549 Mn 0.0000 NaN iteration : 3 Analysis no. 39 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3706 0.019337 0.3706 0.3005 Mg 0.8483 0.017673 0.8483 0.6506 Sr 0.2326 0.013233 0.2326 0.0495 P 0.9593 0.035702 0.9593 0.5773 K 0.1247 0.010075 0.1247 0.0594 Cl 0.8359 0.020206 0.8359 0.4395 Ca 29.0755 0.136846 29.0755 13.5231 Ba 0.0168 0.019598 0.0168 0.0023 Fe 0.0033 0.013976 0.0033 0.0011 Mn 0.0000 0.000000 0.0000 0.0000 C 14.7692 14.7692 22.9222 O 52.7639 52.7639 61.4745 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Mn ( 0.00) point n : 40 x= 14583.0 y= -3381.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 23.2 4.6 4.5 5.09 0.0236 4.7 0.0311 Mg 133.5 1.9 3.8 35.22 0.0717 2.0 0.0128 Sr 30.0 2.9 14.5 2.07 0.0022 2.9 0.0395 P 27.7 4.2 2.0 14.21 0.0327 4.3 0.0363 K 16.9 5.4 7.1 2.37 0.0089 5.5 0.0212 Cl 52.9 2.5 2.3 23.35 0.0110 2.5 0.0225 Ca 3169.6 0.4 18.0 176.08 0.6893 0.5 0.0332 Ba 10.0 5.0 11.2 0.89 0.0000 5.0 0.0000 Fe 3.5 8.4 3.5 1.00 0.0000 8.4 NaN Mn 4.3 10.8 3.3 1.28 0.0009 10.8 0.0667 Elt. k-ratio Correc. Na 0.0012 2.3290 Mg 0.0052 1.6997 Sr 0.0014 1.3818 P 0.0051 1.2016 K 0.0008 1.0376 Cl 0.0061 1.1227 Ca 0.2501 1.0984 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2799 iteration : 3 Analysis no. 40 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2750 0.017431 0.2750 0.2189 Mg 0.8826 0.018033 0.8826 0.6647 Sr 0.1871 0.012732 0.1871 0.0391 P 0.6153 0.029242 0.6153 0.3636 K 0.0816 0.009163 0.0816 0.0382 Cl 0.6885 0.018482 0.6885 0.3555 Ca 27.4754 0.131993 27.4754 12.5478 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0335 0.022145 0.0335 0.0112 C 15.6694 15.6694 23.8795 O 54.0916 54.0916 61.8816 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 41 x= 14587.0 y= -3382.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 26.5 4.3 4.5 5.83 0.0279 4.4 0.0311 Mg 118.8 2.0 3.8 31.34 0.0636 2.1 0.0128 Sr 30.5 2.9 14.5 2.11 0.0023 2.9 0.0394 P 29.4 4.1 2.0 15.08 0.0348 4.1 0.0362 K 19.4 5.1 7.1 2.73 0.0111 5.1 0.0210 Cl 64.1 2.3 2.3 28.28 0.0135 2.3 0.0224 Ca 3495.4 0.4 18.0 194.18 0.7608 0.5 0.0331 Ba 11.4 4.7 11.2 1.02 0.0001 4.7 0.0750 Fe 3.9 8.1 3.5 1.09 0.0002 8.1 0.0564 Mn 3.3 12.4 3.3 0.98 0.0000 12.4 0.0000 Elt. k-ratio Correc. Na 0.0014 2.3266 Mg 0.0046 1.6984 Sr 0.0014 1.3772 P 0.0055 1.1971 K 0.0010 1.0278 Cl 0.0075 1.1164 Ca 0.2761 1.0945 Ba 0.0000 1.5386 Fe 0.0001 1.2543 Mn 0.0000 NaN iteration : 3 Analysis no. 41 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3243 0.018453 0.3243 0.2645 Mg 0.7822 0.017009 0.7822 0.6035 Sr 0.1926 0.012767 0.1926 0.0412 P 0.6538 0.029979 0.6538 0.3958 K 0.1016 0.009544 0.1016 0.0487 Cl 0.8360 0.020175 0.8360 0.4422 Ca 30.2198 0.140318 30.2198 14.1395 Ba 0.0052 0.019432 0.0052 0.0007 Fe 0.0107 0.014196 0.0107 0.0036 Mn 0.0000 0.000000 0.0000 0.0000 C 14.5917 14.5917 22.7822 O 52.2822 52.2822 61.2780 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Mn ( 0.00) point n : 42 x= 14591.0 y= -3382.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 19.8 5.0 4.5 4.35 0.0194 5.0 0.0311 Mg 130.6 2.0 3.8 34.46 0.0702 2.0 0.0127 Sr 37.8 2.6 14.5 2.61 0.0033 2.6 0.0393 P 31.4 4.0 2.0 16.10 0.0374 4.0 0.0361 K 20.6 4.9 7.1 2.89 0.0122 4.9 0.0208 Cl 64.6 2.3 2.3 28.48 0.0136 2.3 0.0223 Ca 3786.8 0.4 18.0 210.37 0.8248 0.5 0.0330 Ba 11.6 4.6 11.2 1.04 0.0002 4.6 0.0750 Fe 4.1 7.8 3.5 1.15 0.0003 7.9 0.0563 Mn 3.9 11.4 3.3 1.16 0.0005 11.4 0.0665 Elt. k-ratio Correc. Na 0.0010 2.3248 Mg 0.0051 1.6947 Sr 0.0020 1.3738 P 0.0059 1.1944 K 0.0011 1.0193 Cl 0.0075 1.1116 Ca 0.2993 1.0907 Ba 0.0001 1.5394 Fe 0.0001 1.2509 Mn 0.0001 1.2742 iteration : 3 Analysis no. 42 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2252 0.016317 0.2252 0.1879 Mg 0.8609 0.017796 0.8609 0.6794 Sr 0.2795 0.013739 0.2795 0.0612 P 0.7000 0.030872 0.7000 0.4335 K 0.1107 0.009681 0.1107 0.0543 Cl 0.8390 0.020165 0.8390 0.4539 Ca 32.6498 0.147561 32.6498 15.6265 Ba 0.0103 0.019533 0.0103 0.0014 Fe 0.0173 0.014352 0.0173 0.0059 Mn 0.0190 0.021472 0.0190 0.0066 C 13.5934 13.5934 21.7100 O 50.6948 50.6948 60.7791 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 43 x= 14595.0 y= -3382.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 19.9 5.0 4.5 4.36 0.0195 5.0 0.0310 Mg 154.3 1.8 3.8 40.71 0.0833 1.8 0.0127 Sr 39.1 2.5 14.5 2.70 0.0035 2.5 0.0393 P 32.2 3.9 2.0 16.49 0.0383 4.0 0.0361 K 22.4 4.7 7.1 3.16 0.0139 4.7 0.0207 Cl 63.9 2.3 2.3 28.21 0.0134 2.3 0.0222 Ca 3984.1 0.4 18.0 221.33 0.8680 0.4 0.0329 Ba 12.7 4.4 11.2 1.13 0.0009 4.4 0.0751 Fe 3.8 8.1 3.5 1.08 0.0002 8.1 0.0562 Mn 4.7 10.4 3.3 1.40 0.0013 10.4 0.0664 Elt. k-ratio Correc. Na 0.0010 2.3219 Mg 0.0060 1.6928 Sr 0.0021 1.3727 P 0.0060 1.1929 K 0.0012 1.0137 Cl 0.0075 1.1085 Ca 0.3150 1.0882 Ba 0.0003 1.5398 Fe 0.0001 1.2485 Mn 0.0004 1.2723 iteration : 3 Analysis no. 43 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2257 0.016314 0.2257 0.1914 Mg 1.0207 0.019323 1.0207 0.8187 Sr 0.2949 0.013900 0.2949 0.0656 P 0.7170 0.031185 0.7170 0.4513 K 0.1252 0.009946 0.1252 0.0624 Cl 0.8281 0.020012 0.8281 0.4554 Ca 34.2776 0.152348 34.2776 16.6730 Ba 0.0388 0.020003 0.0388 0.0055 Fe 0.0091 0.014086 0.0091 0.0032 Mn 0.0477 0.022604 0.0477 0.0169 C 12.8654 12.8654 20.8821 O 49.5499 49.5499 60.3746 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 44 x= 14599.0 y= -3383.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 25.1 4.5 4.5 5.52 0.0261 4.5 0.0310 Mg 152.2 1.8 3.8 40.15 0.0821 1.8 0.0127 Sr 36.5 2.6 14.5 2.52 0.0031 2.6 0.0393 P 32.4 3.9 2.0 16.59 0.0386 3.9 0.0361 K 24.8 4.5 7.1 3.49 0.0161 4.5 0.0207 Cl 66.4 2.2 2.3 29.31 0.0140 2.2 0.0223 Ca 3951.9 0.4 18.0 219.54 0.8610 0.4 0.0329 Ba 11.4 4.7 11.2 1.02 0.0001 4.7 0.0751 Fe 3.8 8.1 3.5 1.07 0.0001 8.1 0.0562 Mn 4.7 10.4 3.3 1.40 0.0013 10.4 0.0664 Elt. k-ratio Correc. Na 0.0013 2.3210 Mg 0.0059 1.6936 Sr 0.0019 1.3731 P 0.0061 1.1930 K 0.0014 1.0148 Cl 0.0078 1.1089 Ca 0.3125 1.0887 Ba 0.0000 1.5399 Fe 0.0001 1.2489 Mn 0.0004 1.2727 iteration : 3 Analysis no. 44 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3030 0.017991 0.3030 0.2564 Mg 1.0067 0.019198 1.0067 0.8057 Sr 0.2644 0.013566 0.2644 0.0587 P 0.7218 0.031282 0.7218 0.4533 K 0.1446 0.010348 0.1446 0.0719 Cl 0.8621 0.020399 0.8621 0.4730 Ca 34.0196 0.151603 34.0196 16.5100 Ba 0.0045 0.019444 0.0045 0.0006 Fe 0.0082 0.014067 0.0082 0.0029 Mn 0.0477 0.022612 0.0477 0.0169 C 12.9458 12.9458 20.9650 O 49.6715 49.6715 60.3857 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 45 x= 14603.0 y= -3383.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 18.6 5.2 4.5 4.08 0.0178 5.2 0.0313 Mg 78.3 2.5 3.8 20.66 0.0413 2.5 0.0128 Sr 18.6 3.7 14.5 1.29 0.0006 3.7 0.0396 P 25.3 4.4 2.0 12.95 0.0296 4.5 0.0364 K 20.1 5.0 7.1 2.83 0.0118 5.0 0.0215 Cl 56.6 2.4 2.3 24.97 0.0118 2.4 0.0227 Ca 2695.1 0.4 18.0 149.72 0.5861 0.5 0.0334 Ba 8.2 5.5 11.2 0.73 0.0000 5.5 0.0000 Fe 3.5 8.5 3.5 0.99 0.0000 8.5 0.0000 Mn 3.3 12.3 3.3 0.99 0.0000 12.3 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3378 Mg 0.0030 1.7046 Sr 0.0004 1.3848 P 0.0046 1.2043 K 0.0010 1.0527 Cl 0.0066 1.1301 Ca 0.2127 1.1047 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 45 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2080 0.015985 0.2080 0.1597 Mg 0.5091 0.013928 0.5091 0.3697 Sr 0.0503 0.011015 0.0503 0.0101 P 0.5587 0.028087 0.5587 0.3183 K 0.1105 0.009920 0.1105 0.0499 Cl 0.7441 0.019238 0.7441 0.3704 Ca 23.4991 0.119732 23.4991 10.3478 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.4517 17.4517 25.6437 O 56.8687 56.8687 62.7304 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 46 x= 14608.0 y= -3383.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 24.0 4.6 4.5 5.27 0.0247 4.6 0.0312 Mg 67.6 2.7 3.8 17.82 0.0353 2.7 0.0128 Sr 34.4 2.7 14.5 2.37 0.0028 2.7 0.0394 P 28.0 4.2 2.0 14.33 0.0330 4.2 0.0362 K 20.0 5.0 7.1 2.82 0.0117 5.0 0.0211 Cl 57.7 2.4 2.3 25.44 0.0121 2.4 0.0225 Ca 3309.1 0.4 18.0 183.83 0.7207 0.5 0.0332 Ba 8.7 5.4 11.2 0.78 0.0000 5.4 0.0000 Fe 3.3 8.7 3.5 0.94 0.0000 8.7 0.0000 Mn 3.3 12.3 3.3 0.99 0.0000 12.3 0.0000 Elt. k-ratio Correc. Na 0.0012 2.3328 Mg 0.0026 1.7015 Sr 0.0017 1.3770 P 0.0052 1.1983 K 0.0010 1.0326 Cl 0.0067 1.1192 Ca 0.2615 1.0967 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 3 Analysis no. 46 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2876 0.017734 0.2876 0.2310 Mg 0.4349 0.012949 0.4349 0.3303 Sr 0.2394 0.013319 0.2394 0.0504 P 0.6204 0.029321 0.6204 0.3698 K 0.1076 0.009715 0.1076 0.0508 Cl 0.7515 0.019228 0.7515 0.3913 Ca 28.6830 0.135726 28.6830 13.2119 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 15.3762 15.3762 23.6341 O 53.4995 53.4995 61.7304 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 47 x= 14612.0 y= -3384.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.7 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.7 15.0 Na 30.3 4.1 4.5 6.66 0.0328 4.1 0.0310 Mg 125.4 2.0 3.8 33.08 0.0673 2.0 0.0127 Sr 42.9 2.4 14.5 2.97 0.0040 2.4 0.0393 P 31.2 4.0 2.0 16.00 0.0372 4.0 0.0361 K 26.2 4.4 7.1 3.69 0.0174 4.4 0.0208 Cl 71.4 2.2 2.3 31.49 0.0151 2.2 0.0223 Ca 3848.2 0.4 18.0 213.78 0.8388 0.4 0.0330 Ba 11.6 4.6 11.2 1.03 0.0002 4.7 0.0751 Fe 3.4 8.6 3.5 0.96 0.0000 8.6 0.0000 Mn 4.4 10.6 3.3 1.33 0.0011 10.7 0.0665 Elt. k-ratio Correc. Na 0.0016 2.3209 Mg 0.0049 1.6952 Sr 0.0025 1.3728 P 0.0058 1.1939 K 0.0015 1.0183 Cl 0.0084 1.1106 Ca 0.3044 1.0899 Ba 0.0001 1.5393 Fe 0.0000 NaN Mn 0.0003 1.2732 iteration : 3 Analysis no. 47 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3799 0.019531 0.3799 0.3192 Mg 0.8263 0.017456 0.8263 0.6567 Sr 0.3416 0.014411 0.3416 0.0753 P 0.6955 0.030788 0.6955 0.4337 K 0.1571 0.010626 0.1571 0.0776 Cl 0.9304 0.021170 0.9304 0.5069 Ca 33.1789 0.149156 33.1789 15.9906 Ba 0.0091 0.019523 0.0091 0.0013 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0388 0.022277 0.0388 0.0136 C 13.2978 13.2978 21.3861 O 50.1445 50.1445 60.5389 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 48 x= 14616.0 y= -3384.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 25.6 4.4 4.5 5.63 0.0268 4.4 0.0311 Mg 133.0 1.9 3.8 35.08 0.0715 2.0 0.0128 Sr 33.3 2.7 14.5 2.30 0.0027 2.8 0.0394 P 25.9 4.4 2.0 13.26 0.0304 4.4 0.0362 K 19.8 5.0 7.1 2.78 0.0115 5.0 0.0209 Cl 70.2 2.2 2.3 30.96 0.0148 2.2 0.0224 Ca 3639.2 0.4 18.0 202.17 0.7931 0.5 0.0331 Ba 11.9 4.6 11.2 1.06 0.0004 4.6 0.0751 Fe 4.0 7.9 3.5 1.14 0.0003 7.9 0.0564 Mn 3.6 11.8 3.3 1.08 0.0003 11.8 0.0667 Elt. k-ratio Correc. Na 0.0013 2.3248 Mg 0.0052 1.6968 Sr 0.0016 1.3761 P 0.0048 1.1960 K 0.0010 1.0236 Cl 0.0082 1.1135 Ca 0.2878 1.0926 Ba 0.0001 1.5390 Fe 0.0001 1.2525 Mn 0.0001 1.2756 iteration : 3 Analysis no. 48 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3111 0.018185 0.3111 0.2567 Mg 0.8786 0.017990 0.8786 0.6858 Sr 0.2263 0.013164 0.2263 0.0490 P 0.5693 0.028211 0.5693 0.3487 K 0.1046 0.009587 0.1046 0.0508 Cl 0.9167 0.021052 0.9167 0.4906 Ca 31.4466 0.144029 31.4466 14.8850 Ba 0.0162 0.019638 0.0162 0.0022 Fe 0.0165 0.014357 0.0165 0.0056 Mn 0.0101 0.021132 0.0101 0.0035 C 14.0994 14.0994 22.2703 O 51.4046 51.4046 60.9519 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 49 x= 14620.0 y= -3384.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 33.0 3.9 4.5 7.25 0.0362 3.9 0.0311 Mg 128.9 2.0 3.8 33.99 0.0692 2.0 0.0128 Sr 31.1 2.8 14.5 2.15 0.0024 2.8 0.0396 P 24.6 4.5 2.0 12.59 0.0287 4.5 0.0364 K 21.1 4.9 7.1 2.97 0.0128 4.9 0.0213 Cl 67.0 2.2 2.3 29.54 0.0141 2.2 0.0226 Ca 3154.8 0.4 18.0 175.26 0.6870 0.5 0.0333 Ba 10.8 4.8 11.2 0.96 0.0000 4.8 0.0000 Fe 3.4 8.6 3.5 0.96 0.0000 8.6 0.0000 Mn 3.6 11.8 3.3 1.08 0.0003 11.8 0.0669 Elt. k-ratio Correc. Na 0.0018 2.3254 Mg 0.0050 1.7006 Sr 0.0015 1.3817 P 0.0045 1.2015 K 0.0011 1.0389 Cl 0.0078 1.1224 Ca 0.2493 1.0987 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2796 iteration : 3 Analysis no. 49 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4206 0.020322 0.4206 0.3351 Mg 0.8525 0.017751 0.8525 0.6426 Sr 0.2006 0.012907 0.2006 0.0419 P 0.5408 0.027664 0.5408 0.3199 K 0.1175 0.009973 0.1175 0.0551 Cl 0.8805 0.020743 0.8805 0.4550 Ca 27.3919 0.131810 27.3919 12.5200 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0101 0.021199 0.0101 0.0034 C 15.6595 15.6595 23.8840 O 53.9260 53.9260 61.7431 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 50 x= 14624.0 y= -3385.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 25.9 4.4 4.5 5.69 0.0272 4.4 0.0312 Mg 86.5 2.4 3.8 22.81 0.0458 2.4 0.0128 Sr 24.5 3.2 14.5 1.69 0.0014 3.2 0.0397 P 22.9 4.7 2.0 11.72 0.0265 4.7 0.0365 K 17.9 5.3 7.1 2.52 0.0098 5.3 0.0216 Cl 62.6 2.3 2.3 27.63 0.0131 2.3 0.0227 Ca 2678.8 0.4 18.0 148.81 0.5827 0.5 0.0335 Ba 9.0 5.3 11.2 0.80 0.0000 5.3 0.0000 Fe 3.2 8.8 3.5 0.91 0.0000 8.8 0.0000 Mn 3.6 11.9 3.3 1.07 0.0002 11.9 0.0671 Elt. k-ratio Correc. Na 0.0014 2.3342 Mg 0.0033 1.7048 Sr 0.0009 1.3853 P 0.0042 1.2054 K 0.0009 1.0539 Cl 0.0073 1.1306 Ca 0.2115 1.1048 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2844 iteration : 2 Analysis no. 50 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3168 0.018351 0.3168 0.2433 Mg 0.5650 0.014621 0.5650 0.4105 Sr 0.1209 0.011957 0.1209 0.0244 P 0.5017 0.026837 0.5017 0.2860 K 0.0920 0.009523 0.0920 0.0415 Cl 0.8274 0.020224 0.8274 0.4121 Ca 23.3649 0.119318 23.3649 10.2941 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0084 0.021200 0.0084 0.0027 C 17.4359 17.4359 25.6341 O 56.7670 56.7670 62.6513 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 51 x= 14628.0 y= -3385.0 z= -249. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 27.9 4.2 4.5 6.13 0.0297 4.2 0.0312 Mg 99.5 2.2 3.8 26.26 0.0530 2.3 0.0128 Sr 26.2 3.1 14.5 1.81 0.0017 3.1 0.0397 P 25.3 4.4 2.0 12.95 0.0296 4.5 0.0365 K 18.4 5.2 7.1 2.59 0.0103 5.2 0.0216 Cl 80.7 2.0 2.3 35.58 0.0171 2.0 0.0227 Ca 2631.3 0.4 18.0 146.17 0.5724 0.5 0.0335 Ba 10.4 4.9 11.2 0.93 0.0000 4.9 0.0000 Fe 2.8 9.4 3.5 0.80 0.0000 9.4 0.0000 Mn 3.2 12.5 3.3 0.96 0.0000 12.5 0.0000 Elt. k-ratio Correc. Na 0.0015 2.3292 Mg 0.0038 1.7026 Sr 0.0010 1.3853 P 0.0046 1.2056 K 0.0009 1.0574 Cl 0.0095 1.1318 Ca 0.2077 1.1056 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 51 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3458 0.018910 0.3458 0.2655 Mg 0.6535 0.015643 0.6535 0.4746 Sr 0.1418 0.012221 0.1418 0.0286 P 0.5595 0.028128 0.5595 0.3189 K 0.0965 0.009651 0.0965 0.0436 Cl 1.0756 0.022908 1.0756 0.5356 Ca 22.9652 0.118063 22.9652 10.1151 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.4440 17.4440 25.6386 O 56.7182 56.7182 62.5795 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 52 x= 14633.0 y= -3385.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 26.1 4.4 4.5 5.73 0.0274 4.4 0.0311 Mg 111.6 2.1 3.8 29.45 0.0597 2.1 0.0128 Sr 31.5 2.8 14.5 2.17 0.0024 2.8 0.0396 P 21.8 4.8 2.0 11.18 0.0252 4.8 0.0364 K 21.4 4.8 7.1 3.01 0.0130 4.8 0.0214 Cl 83.3 2.0 2.3 36.74 0.0176 2.0 0.0226 Ca 2934.4 0.4 18.0 163.01 0.6388 0.5 0.0334 Ba 10.7 4.8 11.2 0.95 0.0000 4.8 0.0000 Fe 3.5 8.4 3.5 0.99 0.0000 8.5 0.0000 Mn 3.4 12.2 3.3 1.01 0.0000 12.2 0.0670 Elt. k-ratio Correc. Na 0.0014 2.3272 Mg 0.0043 1.7001 Sr 0.0015 1.3823 P 0.0040 1.2028 K 0.0012 1.0471 Cl 0.0098 1.1258 Ca 0.2318 1.1016 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2814 iteration : 2 Analysis no. 52 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3181 0.018342 0.3181 0.2496 Mg 0.7351 0.016529 0.7351 0.5456 Sr 0.2056 0.012970 0.2056 0.0423 P 0.4755 0.026202 0.4755 0.2769 K 0.1206 0.010097 0.1206 0.0556 Cl 1.1059 0.023150 1.1059 0.5627 Ca 25.5383 0.126121 25.5383 11.4942 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0011 0.020843 0.0011 0.0004 C 16.4519 16.4519 24.7088 O 55.0479 55.0479 62.0638 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 53 x= 14637.0 y= -3385.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 40.8 3.5 4.5 8.97 0.0462 3.5 0.0311 Mg 115.5 2.1 3.8 30.45 0.0618 2.1 0.0128 Sr 32.1 2.8 14.5 2.21 0.0025 2.8 0.0396 P 22.6 4.7 2.0 11.56 0.0262 4.7 0.0364 K 30.7 4.0 7.1 4.32 0.0215 4.0 0.0215 Cl 78.6 2.1 2.3 34.68 0.0166 2.1 0.0227 Ca 2870.3 0.4 18.0 159.45 0.6247 0.5 0.0334 Ba 9.9 5.0 11.2 0.88 0.0000 5.0 0.0000 Fe 3.7 8.2 3.5 1.05 0.0001 8.2 0.0568 Mn 3.1 12.7 3.3 0.93 0.0000 12.7 0.0000 Elt. k-ratio Correc. Na 0.0023 2.3238 Mg 0.0045 1.7027 Sr 0.0015 1.3839 P 0.0041 1.2042 K 0.0019 1.0494 Cl 0.0093 1.1273 Ca 0.2267 1.1024 Ba 0.0000 NaN Fe 0.0000 1.2602 Mn 0.0000 NaN iteration : 2 Analysis no. 53 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5356 0.022346 0.5356 0.4190 Mg 0.7621 0.016830 0.7621 0.5641 Sr 0.2128 0.013068 0.2128 0.0437 P 0.4941 0.026649 0.4941 0.2869 K 0.1997 0.011665 0.1997 0.0919 Cl 1.0435 0.022533 1.0435 0.5295 Ca 24.9942 0.124429 24.9943 11.2178 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0058 0.014132 0.0058 0.0019 Mn 0.0000 0.000000 0.0000 0.0000 C 16.5390 16.5390 24.7699 O 55.2132 55.2132 62.0753 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 54 x= 14641.0 y= -3386.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 28.9 4.2 4.5 6.34 0.0309 4.2 0.0311 Mg 116.0 2.1 3.8 30.59 0.0621 2.1 0.0128 Sr 36.9 2.6 14.5 2.55 0.0032 2.6 0.0396 P 25.8 4.4 2.0 13.21 0.0302 4.4 0.0364 K 20.0 5.0 7.1 2.81 0.0117 5.0 0.0214 Cl 76.7 2.1 2.3 33.83 0.0162 2.1 0.0226 Ca 3031.4 0.4 18.0 168.40 0.6600 0.5 0.0333 Ba 10.5 4.9 11.2 0.94 0.0000 4.9 0.0000 Fe 3.2 8.9 3.5 0.90 0.0000 8.9 0.0000 Mn 3.6 11.9 3.3 1.07 0.0002 11.9 0.0669 Elt. k-ratio Correc. Na 0.0015 2.3253 Mg 0.0045 1.6995 Sr 0.0020 1.3813 P 0.0047 1.2025 K 0.0010 1.0440 Cl 0.0090 1.1248 Ca 0.2395 1.1002 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2803 iteration : 3 Analysis no. 54 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3592 0.019155 0.3592 0.2841 Mg 0.7641 0.016835 0.7641 0.5716 Sr 0.2710 0.013712 0.2710 0.0562 P 0.5700 0.028314 0.5700 0.3346 K 0.1084 0.009815 0.1084 0.0504 Cl 1.0148 0.022210 1.0148 0.5204 Ca 26.3538 0.128631 26.3538 11.9545 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0083 0.021135 0.0083 0.0028 C 16.0527 16.0527 24.2989 O 54.4976 54.4976 61.9265 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 55 x= 14645.0 y= -3386.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 26.6 4.3 4.5 5.85 0.0281 4.3 0.0311 Mg 99.2 2.2 3.8 26.18 0.0529 2.3 0.0128 Sr 28.4 3.0 14.5 1.96 0.0020 3.0 0.0396 P 28.8 4.2 2.0 14.74 0.0340 4.2 0.0364 K 20.9 4.9 7.1 2.94 0.0126 4.9 0.0214 Cl 87.9 1.9 2.3 38.79 0.0187 1.9 0.0226 Ca 2914.2 0.4 18.0 161.89 0.6344 0.5 0.0334 Ba 10.5 4.9 11.2 0.93 0.0000 4.9 0.0000 Fe 3.1 8.9 3.5 0.89 0.0000 9.0 0.0000 Mn 3.6 11.8 3.3 1.08 0.0003 11.8 0.0670 Elt. k-ratio Correc. Na 0.0014 2.3268 Mg 0.0038 1.7000 Sr 0.0012 1.3814 P 0.0053 1.2019 K 0.0011 1.0485 Cl 0.0104 1.1265 Ca 0.2302 1.1020 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2814 iteration : 2 Analysis no. 55 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3262 0.018506 0.3262 0.2559 Mg 0.6505 0.015598 0.6505 0.4826 Sr 0.1686 0.012522 0.1686 0.0347 P 0.6416 0.029817 0.6416 0.3735 K 0.1169 0.010030 0.1169 0.0539 Cl 1.1700 0.023791 1.1700 0.5951 Ca 25.3711 0.125609 25.3711 11.4145 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0101 0.021232 0.0101 0.0033 C 16.4436 16.4436 24.6867 O 55.1013 55.1013 62.0997 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 56 x= 14649.0 y= -3386.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 32.7 3.9 4.5 7.19 0.0358 3.9 0.0311 Mg 116.3 2.1 3.8 30.67 0.0623 2.1 0.0128 Sr 28.7 2.9 14.5 1.98 0.0020 3.0 0.0396 P 25.2 4.5 2.0 12.90 0.0295 4.5 0.0364 K 21.1 4.9 7.1 2.97 0.0128 4.9 0.0215 Cl 78.2 2.1 2.3 34.52 0.0166 2.1 0.0227 Ca 2831.1 0.4 18.0 157.28 0.6162 0.5 0.0334 Ba 9.8 5.0 11.2 0.87 0.0000 5.1 0.0000 Fe 3.6 8.3 3.5 1.02 0.0000 8.3 0.0568 Mn 3.1 12.7 3.3 0.93 0.0000 12.7 0.0000 Elt. k-ratio Correc. Na 0.0018 2.3259 Mg 0.0045 1.7017 Sr 0.0012 1.3841 P 0.0046 1.2042 K 0.0011 1.0506 Cl 0.0092 1.1283 Ca 0.2236 1.1029 Ba 0.0000 NaN Fe 0.0000 1.2609 Mn 0.0000 NaN iteration : 2 Analysis no. 56 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4163 0.020248 0.4163 0.3245 Mg 0.7672 0.016879 0.7672 0.5656 Sr 0.1720 0.012583 0.1720 0.0352 P 0.5565 0.028044 0.5565 0.3219 K 0.1188 0.010086 0.1188 0.0545 Cl 1.0394 0.022501 1.0394 0.5254 Ca 24.6644 0.123405 24.6644 11.0270 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0025 0.014043 0.0025 0.0008 Mn 0.0000 0.000000 0.0000 0.0000 C 16.7093 16.7093 24.9284 O 55.5536 55.5536 62.2169 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 57 x= 14653.0 y= -3387.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 24.6 4.5 4.5 5.41 0.0255 4.5 0.0311 Mg 116.5 2.1 3.8 30.73 0.0624 2.1 0.0128 Sr 30.7 2.8 14.5 2.12 0.0023 2.9 0.0395 P 26.3 4.4 2.0 13.46 0.0309 4.4 0.0363 K 26.6 4.3 7.1 3.75 0.0178 4.3 0.0213 Cl 84.8 2.0 2.3 37.42 0.0180 2.0 0.0226 Ca 3095.9 0.4 18.0 171.99 0.6742 0.5 0.0333 Ba 11.4 4.7 11.2 1.01 0.0001 4.7 0.0750 Fe 4.2 7.8 3.5 1.18 0.0004 7.8 0.0567 Mn 4.7 10.3 3.3 1.42 0.0014 10.3 0.0669 Elt. k-ratio Correc. Na 0.0013 2.3265 Mg 0.0045 1.6988 Sr 0.0014 1.3803 P 0.0048 1.2006 K 0.0016 1.0422 Cl 0.0100 1.1230 Ca 0.2447 1.0995 Ba 0.0000 1.5366 Fe 0.0002 1.2578 Mn 0.0004 1.2796 iteration : 2 Analysis no. 57 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2966 0.017894 0.2966 0.2358 Mg 0.7676 0.016869 0.7676 0.5773 Sr 0.1962 0.012846 0.1962 0.0409 P 0.5811 0.028531 0.5811 0.3430 K 0.1642 0.010942 0.1642 0.0768 Cl 1.1241 0.023301 1.1241 0.5796 Ca 26.9023 0.130323 26.9023 12.2695 Ba 0.0032 0.019396 0.0032 0.0004 Fe 0.0207 0.014538 0.0207 0.0068 Mn 0.0498 0.022826 0.0498 0.0166 C 15.8176 15.8176 24.0727 O 54.0765 54.0765 61.7807 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 58 x= 14658.0 y= -3387.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 29.6 4.1 4.5 6.51 0.0319 4.1 0.0311 Mg 143.1 1.9 3.8 37.74 0.0771 1.9 0.0128 Sr 30.8 2.8 14.5 2.13 0.0023 2.9 0.0395 P 24.2 4.5 2.0 12.39 0.0282 4.6 0.0363 K 23.7 4.6 7.1 3.33 0.0151 4.6 0.0212 Cl 67.0 2.2 2.3 29.56 0.0141 2.2 0.0225 Ca 3308.5 0.4 18.0 183.79 0.7207 0.5 0.0332 Ba 10.6 4.8 11.2 0.95 0.0000 4.9 0.0000 Fe 4.1 7.8 3.5 1.15 0.0003 7.9 0.0566 Mn 4.1 11.0 3.3 1.24 0.0008 11.0 0.0668 Elt. k-ratio Correc. Na 0.0016 2.3250 Mg 0.0056 1.6990 Sr 0.0014 1.3805 P 0.0044 1.2000 K 0.0013 1.0339 Cl 0.0078 1.1196 Ca 0.2616 1.0967 Ba 0.0000 NaN Fe 0.0001 1.2559 Mn 0.0002 1.2783 iteration : 3 Analysis no. 58 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3703 0.019369 0.3703 0.2985 Mg 0.9486 0.018686 0.9486 0.7233 Sr 0.1969 0.012854 0.1969 0.0416 P 0.5306 0.027419 0.5306 0.3175 K 0.1383 0.010367 0.1383 0.0655 Cl 0.8787 0.020696 0.8787 0.4593 Ca 28.6843 0.135741 28.6843 13.2623 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0174 0.014421 0.0174 0.0058 Mn 0.0281 0.021930 0.0281 0.0095 C 15.1297 15.1297 23.3428 O 53.0772 53.0772 61.4740 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 59 x= 14662.0 y= -3387.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 28.1 4.2 4.5 6.17 0.0299 4.2 0.0312 Mg 88.6 2.4 3.8 23.38 0.0470 2.4 0.0128 Sr 25.4 3.1 14.5 1.75 0.0015 3.2 0.0396 P 25.1 4.5 2.0 12.87 0.0294 4.5 0.0364 K 21.3 4.8 7.1 3.00 0.0129 4.9 0.0215 Cl 73.7 2.1 2.3 32.53 0.0156 2.1 0.0227 Ca 2807.7 0.4 18.0 155.98 0.6111 0.5 0.0334 Ba 10.7 4.8 11.2 0.96 0.0000 4.8 0.0000 Fe 3.1 9.0 3.5 0.87 0.0000 9.0 0.0000 Mn 3.3 12.4 3.3 0.98 0.0000 12.4 0.0000 Elt. k-ratio Correc. Na 0.0015 2.3309 Mg 0.0034 1.7031 Sr 0.0010 1.3833 P 0.0046 1.2034 K 0.0011 1.0505 Cl 0.0087 1.1282 Ca 0.2218 1.1033 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 59 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3483 0.018969 0.3483 0.2704 Mg 0.5792 0.014785 0.5792 0.4254 Sr 0.1316 0.012079 0.1316 0.0268 P 0.5549 0.028001 0.5549 0.3198 K 0.1205 0.010121 0.1205 0.0550 Cl 0.9777 0.021856 0.9777 0.4923 Ca 24.4668 0.122791 24.4668 10.8968 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.9222 16.9222 25.1494 O 55.8987 55.8987 62.3640 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 60 x= 14666.0 y= -3388.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 32.3 3.9 4.5 7.10 0.0353 3.9 0.0311 Mg 112.5 2.1 3.8 29.68 0.0602 2.1 0.0128 Sr 27.9 3.0 14.5 1.93 0.0019 3.0 0.0396 P 26.1 4.4 2.0 13.36 0.0306 4.4 0.0364 K 25.4 4.4 7.1 3.57 0.0166 4.5 0.0214 Cl 73.7 2.1 2.3 32.50 0.0156 2.1 0.0226 Ca 2943.2 0.4 18.0 163.50 0.6408 0.5 0.0334 Ba 11.1 4.8 11.2 0.98 0.0000 4.8 0.0000 Fe 3.3 8.7 3.5 0.93 0.0000 8.7 0.0000 Mn 3.6 11.9 3.3 1.07 0.0002 11.9 0.0670 Elt. k-ratio Correc. Na 0.0018 2.3266 Mg 0.0044 1.7016 Sr 0.0012 1.3828 P 0.0048 1.2028 K 0.0015 1.0464 Cl 0.0087 1.1261 Ca 0.2326 1.1015 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2814 iteration : 2 Analysis no. 60 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4105 0.020145 0.4105 0.3224 Mg 0.7416 0.016608 0.7416 0.5509 Sr 0.1627 0.012462 0.1627 0.0335 P 0.5774 0.028481 0.5774 0.3366 K 0.1543 0.010781 0.1543 0.0713 Cl 0.9751 0.021807 0.9751 0.4966 Ca 25.6156 0.126365 25.6156 11.5392 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0083 0.021155 0.0083 0.0027 C 16.3495 16.3495 24.5768 O 55.0049 55.0049 62.0700 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 61 x= 14670.0 y= -3388.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 37.1 3.7 4.5 8.16 0.0415 3.7 0.0311 Mg 112.9 2.1 3.8 29.77 0.0604 2.1 0.0128 Sr 31.2 2.8 14.5 2.15 0.0024 2.8 0.0395 P 25.8 4.4 2.0 13.21 0.0302 4.4 0.0363 K 24.3 4.5 7.1 3.42 0.0156 4.6 0.0212 Cl 86.0 2.0 2.3 37.95 0.0182 2.0 0.0225 Ca 3264.8 0.4 18.0 181.37 0.7113 0.5 0.0332 Ba 10.1 5.0 11.2 0.90 0.0000 5.0 0.0000 Fe 3.7 8.2 3.5 1.04 0.0001 8.3 0.0566 Mn 3.6 11.9 3.3 1.07 0.0002 11.9 0.0668 Elt. k-ratio Correc. Na 0.0021 2.3229 Mg 0.0044 1.6999 Sr 0.0015 1.3790 P 0.0047 1.1991 K 0.0014 1.0367 Cl 0.0102 1.1200 Ca 0.2581 1.0974 Ba 0.0000 NaN Fe 0.0000 1.2561 Mn 0.0001 1.2783 iteration : 3 Analysis no. 61 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4808 0.021399 0.4808 0.3869 Mg 0.7433 0.016618 0.7433 0.5658 Sr 0.2015 0.012900 0.2015 0.0425 P 0.5685 0.028241 0.5685 0.3396 K 0.1437 0.010498 0.1437 0.0680 Cl 1.1376 0.023403 1.1376 0.5936 Ca 28.3284 0.134682 28.3284 13.0758 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0050 0.014064 0.0050 0.0016 Mn 0.0083 0.021106 0.0083 0.0028 C 15.2475 15.2475 23.4851 O 53.1354 53.1354 61.4383 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 62 x= 14674.0 y= -3388.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 22.3 4.7 4.5 4.90 0.0226 4.7 0.0311 Mg 109.3 2.1 3.8 28.83 0.0584 2.2 0.0128 Sr 32.3 2.8 14.5 2.23 0.0025 2.8 0.0396 P 23.1 4.7 2.0 11.82 0.0268 4.7 0.0364 K 25.5 4.4 7.1 3.58 0.0167 4.4 0.0214 Cl 87.3 2.0 2.3 38.50 0.0185 2.0 0.0226 Ca 3048.5 0.4 18.0 169.35 0.6639 0.5 0.0333 Ba 10.5 4.9 11.2 0.93 0.0000 4.9 0.0000 Fe 3.4 8.6 3.5 0.96 0.0000 8.6 0.0000 Mn 3.2 12.6 3.3 0.95 0.0000 12.6 0.0000 Elt. k-ratio Correc. Na 0.0011 2.3270 Mg 0.0042 1.6985 Sr 0.0016 1.3804 P 0.0042 1.2011 K 0.0015 1.0436 Cl 0.0103 1.1236 Ca 0.2410 1.1003 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 62 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2627 0.017175 0.2627 0.2079 Mg 0.7185 0.016346 0.7185 0.5379 Sr 0.2153 0.013073 0.2153 0.0447 P 0.5049 0.026859 0.5049 0.2966 K 0.1548 0.010770 0.1548 0.0720 Cl 1.1581 0.023645 1.1581 0.5944 Ca 26.5118 0.129142 26.5118 12.0357 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.0646 16.0646 24.3361 O 54.4093 54.4093 61.8747 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 63 x= 14678.0 y= -3389.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 20.5 4.9 4.5 4.50 0.0203 5.0 0.0312 Mg 89.8 2.4 3.8 23.70 0.0476 2.4 0.0128 Sr 28.9 2.9 14.5 1.99 0.0020 3.0 0.0395 P 23.6 4.6 2.0 12.10 0.0275 4.6 0.0363 K 21.6 4.8 7.1 3.04 0.0132 4.8 0.0213 Cl 75.4 2.1 2.3 33.27 0.0159 2.1 0.0226 Ca 3056.5 0.4 18.0 169.79 0.6656 0.5 0.0333 Ba 10.3 4.9 11.2 0.92 0.0000 4.9 0.0000 Fe 3.0 9.2 3.5 0.84 0.0000 9.2 0.0000 Mn 3.7 11.7 3.3 1.10 0.0003 11.7 0.0670 Elt. k-ratio Correc. Na 0.0010 2.3316 Mg 0.0034 1.7006 Sr 0.0013 1.3802 P 0.0043 1.2006 K 0.0012 1.0420 Cl 0.0089 1.1232 Ca 0.2416 1.1001 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2808 iteration : 2 Analysis no. 63 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2357 0.016600 0.2357 0.1862 Mg 0.5866 0.014862 0.5866 0.4383 Sr 0.1736 0.012575 0.1736 0.0360 P 0.5178 0.027144 0.5178 0.3036 K 0.1221 0.010094 0.1221 0.0567 Cl 0.9963 0.022002 0.9963 0.5103 Ca 26.5750 0.129328 26.5750 12.0407 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0119 0.021301 0.0119 0.0039 C 16.1562 16.1562 24.4267 O 54.6246 54.6246 61.9976 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 64 x= 14683.0 y= -3389.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 17.4 5.4 4.5 3.83 0.0164 5.4 0.0312 Mg 86.1 2.4 3.8 22.71 0.0456 2.4 0.0128 Sr 25.5 3.1 14.5 1.76 0.0016 3.1 0.0396 P 23.3 4.6 2.0 11.95 0.0271 4.6 0.0364 K 17.3 5.4 7.1 2.44 0.0093 5.4 0.0215 Cl 79.2 2.0 2.3 34.95 0.0168 2.1 0.0227 Ca 2857.4 0.4 18.0 158.74 0.6221 0.5 0.0334 Ba 10.0 5.0 11.2 0.89 0.0000 5.0 0.0000 Fe 3.6 8.3 3.5 1.03 0.0001 8.3 0.0568 Mn 3.7 11.7 3.3 1.10 0.0003 11.7 0.0671 Elt. k-ratio Correc. Na 0.0008 2.3334 Mg 0.0033 1.7012 Sr 0.0010 1.3820 P 0.0043 1.2024 K 0.0008 1.0488 Cl 0.0093 1.1268 Ca 0.2258 1.1027 Ba 0.0000 NaN Fe 0.0000 1.2613 Mn 0.0001 1.2826 iteration : 2 Analysis no. 64 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1907 0.015561 0.1907 0.1484 Mg 0.5613 0.014563 0.5613 0.4134 Sr 0.1336 0.012097 0.1336 0.0273 P 0.5114 0.027024 0.5114 0.2955 K 0.0865 0.009365 0.0865 0.0396 Cl 1.0516 0.022613 1.0516 0.5309 Ca 24.8936 0.124132 24.8936 11.1168 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0033 0.014075 0.0033 0.0011 Mn 0.0120 0.021333 0.0120 0.0039 C 16.8421 16.8421 25.0978 O 55.7140 55.7140 62.3254 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 65 x= 14687.0 y= -3389.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 33.8 3.8 4.5 7.43 0.0373 3.9 0.0311 Mg 118.8 2.0 3.8 31.33 0.0637 2.1 0.0128 Sr 31.4 2.8 14.5 2.17 0.0024 2.8 0.0395 P 23.3 4.6 2.0 11.95 0.0271 4.6 0.0363 K 30.4 4.1 7.1 4.27 0.0212 4.1 0.0212 Cl 76.7 2.1 2.3 33.84 0.0162 2.1 0.0225 Ca 3337.8 0.4 18.0 185.43 0.7273 0.5 0.0332 Ba 10.3 4.9 11.2 0.91 0.0000 4.9 0.0000 Fe 3.7 8.2 3.5 1.05 0.0001 8.2 0.0566 Mn 3.5 11.9 3.3 1.05 0.0002 12.0 0.0668 Elt. k-ratio Correc. Na 0.0019 2.3244 Mg 0.0046 1.6996 Sr 0.0015 1.3789 P 0.0043 1.1987 K 0.0019 1.0335 Cl 0.0090 1.1184 Ca 0.2640 1.0965 Ba 0.0000 NaN Fe 0.0000 1.2555 Mn 0.0001 1.2779 iteration : 3 Analysis no. 65 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4324 0.020539 0.4324 0.3494 Mg 0.7835 0.017041 0.7835 0.5989 Sr 0.2045 0.012935 0.2045 0.0434 P 0.5099 0.026942 0.5099 0.3058 K 0.1942 0.011445 0.1942 0.0923 Cl 1.0098 0.022094 1.0098 0.5292 Ca 28.9437 0.136548 28.9437 13.4163 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0058 0.014083 0.0058 0.0019 Mn 0.0065 0.021025 0.0065 0.0022 C 15.0586 15.0586 23.2924 O 52.8512 52.8512 61.3683 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 66 x= 14691.0 y= -3390.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 29.3 4.1 4.5 6.43 0.0315 4.1 0.0311 Mg 121.8 2.0 3.8 32.12 0.0653 2.1 0.0128 Sr 37.5 2.6 14.5 2.59 0.0033 2.6 0.0395 P 27.8 4.2 2.0 14.23 0.0328 4.3 0.0363 K 32.3 3.9 7.1 4.54 0.0229 3.9 0.0211 Cl 84.8 2.0 2.3 37.39 0.0180 2.0 0.0225 Ca 3421.8 0.4 18.0 190.09 0.7457 0.5 0.0332 Ba 12.2 4.5 11.2 1.08 0.0006 4.5 0.0751 Fe 3.8 8.1 3.5 1.07 0.0001 8.1 0.0565 Mn 3.3 12.3 3.3 0.99 0.0000 12.3 0.0000 Elt. k-ratio Correc. Na 0.0016 2.3218 Mg 0.0047 1.6967 Sr 0.0020 1.3768 P 0.0051 1.1977 K 0.0020 1.0322 Cl 0.0100 1.1174 Ca 0.2706 1.0954 Ba 0.0002 1.5378 Fe 0.0001 1.2540 Mn 0.0000 NaN iteration : 3 Analysis no. 66 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3647 0.019247 0.3647 0.2972 Mg 0.8025 0.017224 0.8025 0.6187 Sr 0.2771 0.013748 0.2771 0.0593 P 0.6156 0.029222 0.6156 0.3724 K 0.2098 0.011718 0.2098 0.1005 Cl 1.1179 0.023182 1.1179 0.5908 Ca 29.6465 0.138666 29.6465 13.8596 Ba 0.0239 0.019756 0.0239 0.0033 Fe 0.0083 0.014139 0.0083 0.0028 Mn 0.0000 0.000000 0.0000 0.0000 C 14.6831 14.6831 22.9058 O 52.2505 52.2505 61.1896 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Mn ( 0.00) point n : 67 x= 14695.0 y= -3390.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 33.6 3.9 4.5 7.38 0.0369 3.9 0.0311 Mg 133.3 1.9 3.8 35.15 0.0717 2.0 0.0128 Sr 39.2 2.5 14.5 2.71 0.0035 2.5 0.0395 P 26.0 4.4 2.0 13.31 0.0305 4.4 0.0364 K 31.0 4.0 7.1 4.36 0.0217 4.0 0.0213 Cl 81.9 2.0 2.3 36.11 0.0173 2.0 0.0226 Ca 3195.3 0.4 18.0 177.51 0.6961 0.5 0.0333 Ba 11.6 4.6 11.2 1.03 0.0002 4.7 0.0750 Fe 3.3 8.7 3.5 0.94 0.0000 8.7 0.0000 Mn 4.2 10.9 3.3 1.27 0.0009 10.9 0.0669 Elt. k-ratio Correc. Na 0.0018 2.3210 Mg 0.0052 1.6981 Sr 0.0022 1.3801 P 0.0048 1.2010 K 0.0019 1.0394 Cl 0.0097 1.1219 Ca 0.2526 1.0981 Ba 0.0001 1.5366 Fe 0.0000 NaN Mn 0.0002 1.2783 iteration : 3 Analysis no. 67 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4280 0.020441 0.4280 0.3434 Mg 0.8816 0.018030 0.8816 0.6690 Sr 0.2983 0.014006 0.2983 0.0628 P 0.5743 0.028391 0.5743 0.3420 K 0.2004 0.011603 0.2004 0.0945 Cl 1.0828 0.022878 1.0828 0.5633 Ca 27.7422 0.132895 27.7422 12.7672 Ba 0.0090 0.019497 0.0090 0.0012 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0317 0.022085 0.0317 0.0107 C 15.3770 15.3770 23.6143 O 53.3747 53.3747 61.5316 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 68 x= 14699.0 y= -3390.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 34.3 3.8 4.5 7.53 0.0378 3.8 0.0311 Mg 100.3 2.2 3.8 26.47 0.0535 2.3 0.0128 Sr 31.4 2.8 14.5 2.17 0.0024 2.8 0.0396 P 23.8 4.6 2.0 12.18 0.0277 4.6 0.0364 K 22.4 4.7 7.1 3.16 0.0139 4.7 0.0213 Cl 79.8 2.0 2.3 35.21 0.0169 2.0 0.0226 Ca 3082.7 0.4 18.0 171.25 0.6716 0.5 0.0333 Ba 9.5 5.1 11.2 0.84 0.0000 5.1 0.0000 Fe 3.7 8.2 3.5 1.06 0.0001 8.2 0.0567 Mn 3.8 11.5 3.3 1.13 0.0004 11.6 0.0670 Elt. k-ratio Correc. Na 0.0019 2.3265 Mg 0.0039 1.7016 Sr 0.0015 1.3808 P 0.0043 1.2011 K 0.0012 1.0419 Cl 0.0094 1.1231 Ca 0.2437 1.0996 Ba 0.0000 NaN Fe 0.0001 1.2582 Mn 0.0001 1.2801 iteration : 3 Analysis no. 68 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4395 0.020683 0.4395 0.3486 Mg 0.6589 0.015704 0.6589 0.4943 Sr 0.2042 0.012948 0.2042 0.0425 P 0.5218 0.027244 0.5218 0.3072 K 0.1289 0.010236 0.1289 0.0601 Cl 1.0565 0.022627 1.0565 0.5434 Ca 26.8006 0.130029 26.8006 12.1938 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0066 0.014141 0.0066 0.0022 Mn 0.0155 0.021446 0.0155 0.0052 C 15.9315 15.9315 24.1880 O 54.2360 54.2360 61.8147 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 69 x= 14704.0 y= -3391.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 28.4 4.2 4.5 6.24 0.0304 4.2 0.0312 Mg 104.8 2.2 3.8 27.66 0.0560 2.2 0.0128 Sr 27.4 3.0 14.5 1.89 0.0018 3.0 0.0396 P 27.4 4.3 2.0 14.05 0.0323 4.3 0.0364 K 25.2 4.5 7.1 3.54 0.0164 4.5 0.0214 Cl 73.9 2.1 2.3 32.59 0.0156 2.1 0.0226 Ca 2965.2 0.4 18.0 164.72 0.6459 0.5 0.0334 Ba 10.6 4.9 11.2 0.94 0.0000 4.9 0.0000 Fe 3.2 8.9 3.5 0.89 0.0000 8.9 0.0000 Mn 3.3 12.4 3.3 0.98 0.0000 12.4 0.0000 Elt. k-ratio Correc. Na 0.0015 2.3279 Mg 0.0041 1.7011 Sr 0.0011 1.3819 P 0.0051 1.2021 K 0.0015 1.0456 Cl 0.0087 1.1256 Ca 0.2344 1.1013 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 69 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3532 0.019056 0.3532 0.2777 Mg 0.6894 0.016042 0.6894 0.5127 Sr 0.1560 0.012378 0.1560 0.0322 P 0.6096 0.029162 0.6096 0.3558 K 0.1526 0.010744 0.1526 0.0705 Cl 0.9778 0.021835 0.9778 0.4985 Ca 25.8134 0.126998 25.8134 11.6419 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.3037 16.3037 24.5365 O 54.9443 54.9443 62.0741 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 70 x= 14708.0 y= -3391.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 32.9 3.9 4.5 7.22 0.0361 3.9 0.0312 Mg 97.4 2.3 3.8 25.70 0.0519 2.3 0.0128 Sr 30.3 2.9 14.5 2.09 0.0022 2.9 0.0396 P 26.6 4.3 2.0 13.62 0.0313 4.3 0.0364 K 26.9 4.3 7.1 3.78 0.0180 4.3 0.0214 Cl 69.4 2.2 2.3 30.63 0.0146 2.2 0.0226 Ca 2936.0 0.4 18.0 163.10 0.6394 0.5 0.0334 Ba 8.6 5.4 11.2 0.76 0.0000 5.4 0.0000 Fe 4.0 7.9 3.5 1.13 0.0003 7.9 0.0568 Mn 3.2 12.6 3.3 0.95 0.0000 12.6 0.0000 Elt. k-ratio Correc. Na 0.0018 2.3281 Mg 0.0038 1.7026 Sr 0.0014 1.3823 P 0.0049 1.2028 K 0.0016 1.0463 Cl 0.0081 1.1262 Ca 0.2320 1.1015 Ba 0.0000 NaN Fe 0.0001 1.2599 Mn 0.0000 NaN iteration : 2 Analysis no. 70 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4190 0.020315 0.4190 0.3288 Mg 0.6394 0.015486 0.6394 0.4746 Sr 0.1915 0.012808 0.1915 0.0394 P 0.5896 0.028745 0.5896 0.3434 K 0.1670 0.011031 0.1670 0.0771 Cl 0.9176 0.021193 0.9176 0.4669 Ca 25.5601 0.126203 25.5601 11.5048 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0158 0.014425 0.0158 0.0051 Mn 0.0000 0.000000 0.0000 0.0000 C 16.4024 16.4024 24.6360 O 55.0977 55.0977 62.1239 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 71 x= 14712.0 y= -3391.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 32.6 3.9 4.5 7.17 0.0357 3.9 0.0311 Mg 115.1 2.1 3.8 30.35 0.0616 2.1 0.0128 Sr 35.9 2.6 14.5 2.48 0.0030 2.7 0.0396 P 28.3 4.2 2.0 14.49 0.0334 4.2 0.0364 K 33.1 3.9 7.1 4.66 0.0236 3.9 0.0214 Cl 88.7 1.9 2.3 39.13 0.0188 1.9 0.0226 Ca 3061.5 0.4 18.0 170.07 0.6669 0.5 0.0333 Ba 11.1 4.7 11.2 0.99 0.0000 4.8 0.0000 Fe 3.3 8.8 3.5 0.92 0.0000 8.8 0.0000 Mn 3.0 13.0 3.3 0.89 0.0000 13.0 0.0000 Elt. k-ratio Correc. Na 0.0018 2.3218 Mg 0.0045 1.6985 Sr 0.0019 1.3802 P 0.0052 1.2013 K 0.0021 1.0443 Cl 0.0105 1.1241 Ca 0.2420 1.1001 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 71 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4142 0.020191 0.4142 0.3291 Mg 0.7578 0.016768 0.7578 0.5696 Sr 0.2582 0.013564 0.2582 0.0538 P 0.6295 0.029564 0.6295 0.3713 K 0.2190 0.011978 0.2190 0.1023 Cl 1.1784 0.023850 1.1784 0.6072 Ca 26.6249 0.129495 26.6249 12.1352 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 15.8307 15.8307 24.0775 O 54.0872 54.0872 61.7539 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 72 x= 14716.0 y= -3392.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 34.5 3.8 4.5 7.57 0.0381 3.8 0.0311 Mg 105.8 2.2 3.8 27.91 0.0565 2.2 0.0128 Sr 30.5 2.9 14.5 2.11 0.0023 2.9 0.0395 P 28.0 4.2 2.0 14.36 0.0331 4.2 0.0363 K 29.9 4.1 7.1 4.20 0.0207 4.1 0.0213 Cl 86.6 2.0 2.3 38.20 0.0184 2.0 0.0226 Ca 3093.4 0.4 18.0 171.85 0.6738 0.5 0.0333 Ba 9.3 5.2 11.2 0.83 0.0000 5.2 0.0000 Fe 4.0 7.9 3.5 1.13 0.0003 7.9 0.0567 Mn 2.9 13.1 3.3 0.87 0.0000 13.1 0.0000 Elt. k-ratio Correc. Na 0.0019 2.3239 Mg 0.0041 1.7001 Sr 0.0014 1.3801 P 0.0052 1.2005 K 0.0018 1.0426 Cl 0.0102 1.1231 Ca 0.2445 1.0997 Ba 0.0000 NaN Fe 0.0001 1.2577 Mn 0.0000 NaN iteration : 2 Analysis no. 72 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4419 0.020709 0.4419 0.3514 Mg 0.6953 0.016100 0.6953 0.5231 Sr 0.1932 0.012811 0.1932 0.0403 P 0.6230 0.029416 0.6230 0.3678 K 0.1917 0.011468 0.1917 0.0897 Cl 1.1486 0.023547 1.1486 0.5924 Ca 26.8903 0.130303 26.8903 12.2680 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0149 0.014374 0.0149 0.0049 Mn 0.0000 0.000000 0.0000 0.0000 C 15.7826 15.7826 24.0273 O 54.0184 54.0184 61.7349 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 73 x= 14720.0 y= -3392.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 38.0 3.6 4.5 8.35 0.0426 3.6 0.0311 Mg 112.3 2.1 3.8 29.62 0.0601 2.1 0.0128 Sr 36.8 2.6 14.5 2.54 0.0032 2.6 0.0395 P 28.9 4.2 2.0 14.80 0.0342 4.2 0.0363 K 32.3 3.9 7.1 4.54 0.0229 3.9 0.0213 Cl 78.9 2.1 2.3 34.83 0.0167 2.1 0.0226 Ca 3191.8 0.4 18.0 177.31 0.6953 0.5 0.0333 Ba 11.6 4.6 11.2 1.03 0.0002 4.7 0.0750 Fe 4.1 7.8 3.5 1.15 0.0003 7.9 0.0566 Mn 3.6 11.8 3.3 1.08 0.0003 11.8 0.0669 Elt. k-ratio Correc. Na 0.0021 2.3221 Mg 0.0044 1.6999 Sr 0.0020 1.3795 P 0.0054 1.2004 K 0.0020 1.0393 Cl 0.0093 1.1219 Ca 0.2523 1.0982 Ba 0.0001 1.5367 Fe 0.0001 1.2564 Mn 0.0001 1.2785 iteration : 3 Analysis no. 73 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4939 0.021625 0.4939 0.3960 Mg 0.7396 0.016578 0.7396 0.5608 Sr 0.2692 0.013680 0.2692 0.0566 P 0.6433 0.029833 0.6433 0.3828 K 0.2112 0.011799 0.2112 0.0996 Cl 1.0433 0.022476 1.0433 0.5424 Ca 27.7121 0.132802 27.7121 12.7440 Ba 0.0090 0.019497 0.0090 0.0012 Fe 0.0174 0.014429 0.0174 0.0057 Mn 0.0101 0.021186 0.0101 0.0034 C 15.4011 15.4011 23.6340 O 53.4498 53.4498 61.5734 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 74 x= 14724.0 y= -3392.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 41.1 3.5 4.5 9.04 0.0466 3.5 0.0311 Mg 121.2 2.0 3.8 31.97 0.0650 2.1 0.0128 Sr 31.1 2.8 14.5 2.15 0.0024 2.8 0.0396 P 26.5 4.3 2.0 13.57 0.0311 4.4 0.0364 K 30.6 4.0 7.1 4.30 0.0214 4.1 0.0215 Cl 81.5 2.0 2.3 35.96 0.0173 2.0 0.0227 Ca 2894.0 0.4 18.0 160.77 0.6301 0.5 0.0334 Ba 10.7 4.8 11.2 0.95 0.0000 4.8 0.0000 Fe 3.5 8.4 3.5 0.99 0.0000 8.5 0.0000 Mn 3.0 12.9 3.3 0.90 0.0000 12.9 0.0000 Elt. k-ratio Correc. Na 0.0023 2.3219 Mg 0.0047 1.7016 Sr 0.0015 1.3835 P 0.0049 1.2037 K 0.0019 1.0492 Cl 0.0096 1.1272 Ca 0.2287 1.1022 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 74 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5397 0.022408 0.5397 0.4234 Mg 0.8011 0.017234 0.8011 0.5945 Sr 0.2010 0.012927 0.2010 0.0414 P 0.5875 0.028710 0.5875 0.3421 K 0.1988 0.011649 0.1988 0.0917 Cl 1.0834 0.022940 1.0834 0.5512 Ca 25.2016 0.125086 25.2016 11.3421 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.3800 16.3800 24.5994 O 55.0070 55.0070 62.0141 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 75 x= 14729.0 y= -3393.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 32.0 4.0 4.5 7.02 0.0349 4.0 0.0311 Mg 111.5 2.1 3.8 29.41 0.0596 2.1 0.0128 Sr 36.9 2.6 14.5 2.55 0.0032 2.6 0.0395 P 28.2 4.2 2.0 14.46 0.0334 4.2 0.0363 K 31.1 4.0 7.1 4.38 0.0219 4.0 0.0211 Cl 74.7 2.1 2.3 32.96 0.0158 2.1 0.0225 Ca 3380.6 0.4 18.0 187.80 0.7367 0.5 0.0332 Ba 11.6 4.6 11.2 1.03 0.0002 4.7 0.0751 Fe 3.5 8.4 3.5 1.00 0.0000 8.4 NaN Mn 3.7 11.6 3.3 1.11 0.0004 11.6 0.0668 Elt. k-ratio Correc. Na 0.0017 2.3237 Mg 0.0043 1.6985 Sr 0.0020 1.3774 P 0.0052 1.1983 K 0.0019 1.0326 Cl 0.0088 1.1183 Ca 0.2673 1.0959 Ba 0.0001 1.5377 Fe 0.0000 NaN Mn 0.0001 1.2773 iteration : 3 Analysis no. 75 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4049 0.020024 0.4049 0.3285 Mg 0.7335 0.016506 0.7335 0.5630 Sr 0.2697 0.013669 0.2697 0.0574 P 0.6266 0.029459 0.6266 0.3774 K 0.2003 0.011549 0.2003 0.0956 Cl 0.9824 0.021806 0.9824 0.5170 Ca 29.2978 0.137610 29.2978 13.6373 Ba 0.0084 0.019499 0.0084 0.0011 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0137 0.021318 0.0137 0.0047 C 14.8628 14.8628 23.0858 O 52.5999 52.5999 61.3322 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 76 x= 14733.0 y= -3393.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 23.7 4.6 4.5 5.20 0.0243 4.6 0.0311 Mg 98.2 2.3 3.8 25.90 0.0523 2.3 0.0128 Sr 38.3 2.6 14.5 2.65 0.0034 2.6 0.0395 P 30.1 4.1 2.0 15.44 0.0358 4.1 0.0364 K 30.1 4.1 7.1 4.23 0.0209 4.1 0.0214 Cl 84.2 2.0 2.3 37.16 0.0179 2.0 0.0226 Ca 3030.3 0.4 18.0 168.34 0.6599 0.5 0.0333 Ba 11.2 4.7 11.2 1.00 0.0000 4.7 0.0000 Fe 2.9 9.2 3.5 0.83 0.0000 9.3 0.0000 Mn 4.1 11.1 3.3 1.22 0.0007 11.1 0.0669 Elt. k-ratio Correc. Na 0.0012 2.3258 Mg 0.0038 1.6982 Sr 0.0021 1.3793 P 0.0056 1.2012 K 0.0019 1.0449 Cl 0.0099 1.1247 Ca 0.2395 1.1004 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2799 iteration : 2 Analysis no. 76 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2824 0.017593 0.2824 0.2237 Mg 0.6427 0.015500 0.6427 0.4815 Sr 0.2875 0.013881 0.2875 0.0598 P 0.6736 0.030458 0.6736 0.3960 K 0.1938 0.011523 0.1938 0.0902 Cl 1.1177 0.023257 1.1177 0.5740 Ca 26.3522 0.128639 26.3522 11.9717 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0264 0.021888 0.0264 0.0087 C 16.0103 16.0103 24.2710 O 54.4135 54.4135 61.9234 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 77 x= 14737.0 y= -3393.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 31.1 4.0 4.5 6.83 0.0338 4.0 0.0311 Mg 89.5 2.4 3.8 23.62 0.0475 2.4 0.0128 Sr 29.7 2.9 14.5 2.05 0.0022 2.9 0.0395 P 29.8 4.1 2.0 15.26 0.0353 4.1 0.0363 K 28.6 4.2 7.1 4.03 0.0196 4.2 0.0214 Cl 87.4 2.0 2.3 38.54 0.0185 2.0 0.0226 Ca 3025.7 0.4 18.0 168.08 0.6589 0.5 0.0333 Ba 9.6 5.1 11.2 0.85 0.0000 5.1 0.0000 Fe 3.0 9.1 3.5 0.86 0.0000 9.1 0.0000 Mn 3.0 12.9 3.3 0.90 0.0000 12.9 0.0000 Elt. k-ratio Correc. Na 0.0017 2.3258 Mg 0.0034 1.7003 Sr 0.0013 1.3798 P 0.0055 1.2005 K 0.0017 1.0448 Cl 0.0103 1.1243 Ca 0.2391 1.1006 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 77 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3919 0.019789 0.3919 0.3100 Mg 0.5845 0.014835 0.5845 0.4373 Sr 0.1841 0.012698 0.1841 0.0382 P 0.6648 0.030271 0.6648 0.3903 K 0.1815 0.011293 0.1815 0.0844 Cl 1.1601 0.023671 1.1601 0.5951 Ca 26.3170 0.128538 26.3170 11.9403 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.0530 16.0530 24.3044 O 54.4631 54.4631 61.9000 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 78 x= 14741.0 y= -3394.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 29.8 4.1 4.5 6.55 0.0322 4.1 0.0311 Mg 97.8 2.3 3.8 25.81 0.0521 2.3 0.0128 Sr 33.6 2.7 14.5 2.32 0.0027 2.7 0.0395 P 31.7 4.0 2.0 16.26 0.0378 4.0 0.0363 K 28.5 4.2 7.1 4.01 0.0195 4.2 0.0213 Cl 81.6 2.0 2.3 36.01 0.0173 2.0 0.0225 Ca 3200.6 0.4 18.0 177.80 0.6972 0.5 0.0333 Ba 11.2 4.7 11.2 0.99 0.0000 4.7 0.0000 Fe 3.4 8.6 3.5 0.96 0.0000 8.6 0.0000 Mn 3.7 11.7 3.3 1.10 0.0003 11.7 0.0669 Elt. k-ratio Correc. Na 0.0016 2.3248 Mg 0.0038 1.6989 Sr 0.0017 1.3782 P 0.0059 1.1992 K 0.0017 1.0390 Cl 0.0096 1.1216 Ca 0.2530 1.0983 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2788 iteration : 3 Analysis no. 78 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3733 0.019428 0.3733 0.2991 Mg 0.6406 0.015481 0.6406 0.4855 Sr 0.2300 0.013226 0.2300 0.0484 P 0.7107 0.031170 0.7107 0.4227 K 0.1793 0.011207 0.1793 0.0845 Cl 1.0793 0.022839 1.0793 0.5607 Ca 27.7903 0.133048 27.7903 12.7720 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0119 0.021267 0.0119 0.0040 C 15.4420 15.4420 23.6818 O 53.5426 53.5426 61.6414 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 79 x= 14745.0 y= -3394.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 20.3 5.0 4.5 4.46 0.0201 5.0 0.0312 Mg 81.5 2.5 3.8 21.51 0.0430 2.5 0.0128 Sr 25.4 3.1 14.5 1.75 0.0015 3.2 0.0396 P 29.6 4.1 2.0 15.16 0.0351 4.1 0.0364 K 23.0 4.7 7.1 3.24 0.0145 4.7 0.0216 Cl 72.0 2.1 2.3 31.75 0.0152 2.2 0.0227 Ca 2692.5 0.4 18.0 149.57 0.5858 0.5 0.0335 Ba 8.5 5.4 11.2 0.76 0.0000 5.4 0.0000 Fe 3.7 8.2 3.5 1.05 0.0001 8.2 0.0569 Mn 3.6 11.9 3.3 1.07 0.0002 11.9 0.0671 Elt. k-ratio Correc. Na 0.0010 2.3329 Mg 0.0031 1.7022 Sr 0.0010 1.3835 P 0.0055 1.2041 K 0.0013 1.0547 Cl 0.0085 1.1307 Ca 0.2126 1.1048 Ba 0.0000 NaN Fe 0.0000 1.2629 Mn 0.0001 1.2839 iteration : 2 Analysis no. 79 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2336 0.016557 0.2336 0.1800 Mg 0.5305 0.014189 0.5305 0.3866 Sr 0.1316 0.012081 0.1316 0.0266 P 0.6620 0.030264 0.6620 0.3785 K 0.1355 0.010463 0.1355 0.0614 Cl 0.9556 0.021645 0.9556 0.4774 Ca 23.4886 0.119721 23.4886 10.3798 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0058 0.014163 0.0058 0.0018 Mn 0.0083 0.021195 0.0083 0.0027 C 17.2878 17.2878 25.4931 O 56.5606 56.5606 62.6120 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 80 x= 14749.0 y= -3394.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 25.9 4.4 4.5 5.69 0.0272 4.4 0.0311 Mg 93.6 2.3 3.8 24.69 0.0497 2.3 0.0128 Sr 32.0 2.8 14.5 2.21 0.0025 2.8 0.0394 P 32.7 3.9 2.0 16.77 0.0391 3.9 0.0363 K 35.0 3.8 7.1 4.93 0.0254 3.8 0.0213 Cl 95.5 1.9 2.3 42.13 0.0203 1.9 0.0225 Ca 3223.6 0.4 18.0 179.08 0.7022 0.5 0.0333 Ba 10.5 4.9 11.2 0.94 0.0000 4.9 0.0000 Fe 3.6 8.3 3.5 1.03 0.0001 8.3 0.0566 Mn 3.6 11.8 3.3 1.08 0.0003 11.8 0.0668 Elt. k-ratio Correc. Na 0.0014 2.3240 Mg 0.0036 1.6972 Sr 0.0015 1.3768 P 0.0061 1.1978 K 0.0023 1.0393 Cl 0.0113 1.1207 Ca 0.2548 1.0982 Ba 0.0000 NaN Fe 0.0000 1.2561 Mn 0.0001 1.2784 iteration : 2 Analysis no. 80 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3155 0.018272 0.3155 0.2535 Mg 0.6109 0.015131 0.6109 0.4644 Sr 0.2111 0.012994 0.2111 0.0445 P 0.7337 0.031596 0.7337 0.4376 K 0.2343 0.012205 0.2343 0.1107 Cl 1.2670 0.024653 1.2670 0.6602 Ca 27.9862 0.133649 27.9862 12.9002 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0033 0.014014 0.0033 0.0011 Mn 0.0101 0.021181 0.0101 0.0034 C 15.3353 15.3353 23.5882 O 53.2926 53.2926 61.5361 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 81 x= 14754.0 y= -3395.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 28.0 4.2 4.5 6.16 0.0299 4.2 0.0311 Mg 110.0 2.1 3.8 29.02 0.0588 2.2 0.0128 Sr 37.5 2.6 14.5 2.59 0.0033 2.6 0.0395 P 32.7 3.9 2.0 16.75 0.0390 3.9 0.0363 K 32.5 3.9 7.1 4.58 0.0231 3.9 0.0213 Cl 96.3 1.9 2.3 42.49 0.0205 1.9 0.0226 Ca 3169.9 0.4 18.0 176.09 0.6904 0.5 0.0333 Ba 11.6 4.6 11.2 1.03 0.0002 4.7 0.0750 Fe 3.9 8.0 3.5 1.10 0.0002 8.0 0.0566 Mn 3.3 12.4 3.3 0.98 0.0000 12.4 0.0000 Elt. k-ratio Correc. Na 0.0015 2.3211 Mg 0.0043 1.6964 Sr 0.0020 1.3778 P 0.0061 1.1994 K 0.0021 1.0416 Cl 0.0114 1.1223 Ca 0.2506 1.0988 Ba 0.0001 1.5366 Fe 0.0001 1.2563 Mn 0.0000 NaN iteration : 2 Analysis no. 81 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3461 0.018876 0.3461 0.2775 Mg 0.7223 0.016375 0.7223 0.5478 Sr 0.2779 0.013763 0.2779 0.0585 P 0.7335 0.031617 0.7335 0.4365 K 0.2138 0.011861 0.2138 0.1008 Cl 1.2797 0.024791 1.2797 0.6654 Ca 27.5322 0.132262 27.5322 12.6617 Ba 0.0090 0.019495 0.0090 0.0012 Fe 0.0116 0.014259 0.0116 0.0038 Mn 0.0000 0.000000 0.0000 0.0000 C 15.4275 15.4275 23.6754 O 53.4463 53.4463 61.5715 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Mn ( 0.00) point n : 82 x= 14758.0 y= -3395.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 24.5 4.5 4.5 5.39 0.0254 4.5 0.0311 Mg 93.6 2.3 3.8 24.69 0.0497 2.3 0.0128 Sr 32.4 2.8 14.5 2.24 0.0025 2.8 0.0395 P 36.1 3.7 2.0 18.51 0.0434 3.7 0.0364 K 31.4 4.0 7.1 4.42 0.0221 4.0 0.0214 Cl 75.2 2.1 2.3 33.18 0.0159 2.1 0.0227 Ca 2920.0 0.4 18.0 162.21 0.6357 0.5 0.0334 Ba 10.9 4.8 11.2 0.97 0.0000 4.8 0.0000 Fe 3.6 8.4 3.5 1.01 0.0000 8.4 0.0567 Mn 3.7 11.7 3.3 1.10 0.0003 11.7 0.0670 Elt. k-ratio Correc. Na 0.0013 2.3269 Mg 0.0036 1.6994 Sr 0.0016 1.3806 P 0.0068 1.2020 K 0.0020 1.0483 Cl 0.0088 1.1272 Ca 0.2307 1.1019 Ba 0.0000 NaN Fe 0.0000 1.2596 Mn 0.0001 1.2811 iteration : 2 Analysis no. 82 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2951 0.017866 0.2951 0.2318 Mg 0.6117 0.015150 0.6117 0.4545 Sr 0.2162 0.013082 0.2162 0.0446 P 0.8176 0.033250 0.8176 0.4767 K 0.2054 0.011761 0.2054 0.0949 Cl 0.9970 0.022049 0.9970 0.5078 Ca 25.4196 0.125759 25.4196 11.4526 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.014003 0.0017 0.0005 Mn 0.0119 0.021303 0.0119 0.0039 C 16.3349 16.3349 24.5585 O 55.0889 55.0889 62.1742 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 83 x= 14762.0 y= -3395.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 24.4 4.5 4.5 5.36 0.0253 4.5 0.0311 Mg 88.7 2.4 3.8 23.39 0.0470 2.4 0.0128 Sr 28.4 3.0 14.5 1.96 0.0020 3.0 0.0395 P 38.5 3.6 2.0 19.75 0.0464 3.6 0.0364 K 31.8 4.0 7.1 4.47 0.0225 4.0 0.0215 Cl 77.1 2.1 2.3 34.01 0.0163 2.1 0.0227 Ca 2915.6 0.4 18.0 161.97 0.6347 0.5 0.0334 Ba 9.1 5.2 11.2 0.81 0.0000 5.2 0.0000 Fe 3.6 8.4 3.5 1.01 0.0000 8.4 0.0568 Mn 3.3 12.3 3.3 0.99 0.0000 12.3 0.0000 Elt. k-ratio Correc. Na 0.0013 2.3271 Mg 0.0034 1.6995 Sr 0.0012 1.3803 P 0.0073 1.2013 K 0.0020 1.0485 Cl 0.0091 1.1272 Ca 0.2303 1.1021 Ba 0.0000 NaN Fe 0.0000 1.2598 Mn 0.0000 NaN iteration : 2 Analysis no. 83 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2937 0.017837 0.2937 0.2306 Mg 0.5783 0.014758 0.5783 0.4295 Sr 0.1679 0.012505 0.1679 0.0346 P 0.8746 0.034283 0.8746 0.5097 K 0.2089 0.011825 0.2089 0.0964 Cl 1.0225 0.022316 1.0225 0.5206 Ca 25.3860 0.125661 25.3860 11.4325 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0008 0.013981 0.0008 0.0003 Mn 0.0000 0.000000 0.0000 0.0000 C 16.3412 16.3412 24.5572 O 55.1260 55.1260 62.1887 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 84 x= 14766.0 y= -3396.0 z= -248. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 46.9 3.3 4.5 10.31 0.0539 3.3 0.0309 Mg 135.7 1.9 3.8 35.80 0.0731 1.9 0.0128 Sr 41.1 2.5 14.5 2.84 0.0038 2.5 0.0395 P 43.7 3.4 2.0 22.39 0.0530 3.4 0.0364 K 34.8 3.8 7.1 4.89 0.0252 3.8 0.0214 Cl 90.5 1.9 2.3 39.93 0.0192 1.9 0.0226 Ca 3070.6 0.4 18.0 170.58 0.6687 0.5 0.0333 Ba 12.1 4.5 11.2 1.08 0.0005 4.6 0.0749 Fe 3.8 8.1 3.5 1.08 0.0002 8.1 0.0566 Mn 3.2 12.6 3.3 0.95 0.0000 12.6 0.0000 Elt. k-ratio Correc. Na 0.0027 2.3123 Mg 0.0053 1.6972 Sr 0.0023 1.3802 P 0.0083 1.2019 K 0.0022 1.0462 Cl 0.0107 1.1261 Ca 0.2427 1.0998 Ba 0.0001 1.5354 Fe 0.0001 1.2563 Mn 0.0000 NaN iteration : 3 Analysis no. 84 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6226 0.023708 0.6226 0.4980 Mg 0.8976 0.018182 0.8976 0.6791 Sr 0.3218 0.014260 0.3218 0.0675 P 0.9983 0.036458 0.9983 0.5927 K 0.2338 0.012249 0.2338 0.1099 Cl 1.2047 0.024122 1.2047 0.6248 Ca 26.6889 0.129668 26.6889 12.2447 Ba 0.0226 0.019701 0.0226 0.0030 Fe 0.0091 0.014186 0.0091 0.0030 Mn 0.0000 0.000000 0.0000 0.0000 C 15.3947 15.3947 23.5688 O 53.6058 53.6058 61.6083 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Mn ( 0.00) point n : 85 x= 14770.0 y= -3396.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 24.7 4.5 4.5 5.43 0.0257 4.5 0.0313 Mg 26.1 4.4 3.8 6.87 0.0123 4.4 0.0129 Sr 22.0 3.4 14.5 1.52 0.0011 3.4 0.0397 P 27.2 4.3 2.0 13.92 0.0320 4.3 0.0365 K 31.2 4.0 7.1 4.39 0.0219 4.0 0.0218 Cl 56.0 2.4 2.3 24.69 0.0117 2.4 0.0228 Ca 2376.6 0.5 18.0 132.03 0.5166 0.5 0.0336 Ba 9.1 5.3 11.2 0.81 0.0000 5.3 0.0000 Fe 3.0 9.2 3.5 0.84 0.0000 9.2 0.0000 Mn 2.7 13.6 3.3 0.81 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0013 2.3409 Mg 0.0009 1.7088 Sr 0.0007 1.3858 P 0.0050 1.2069 K 0.0019 1.0641 Cl 0.0065 1.1360 Ca 0.1875 1.1089 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 85 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2999 0.018036 0.2999 0.2253 Mg 0.1525 0.008381 0.1525 0.1084 Sr 0.0909 0.011574 0.0909 0.0179 P 0.6058 0.029138 0.6058 0.3378 K 0.2068 0.011908 0.2068 0.0914 Cl 0.7396 0.019243 0.7396 0.3603 Ca 20.7918 0.111105 20.7918 8.9607 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 18.5397 18.5397 26.6628 O 58.5730 58.5730 63.2353 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 86 x= 14774.0 y= -3396.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 46.2 3.3 4.5 10.15 0.0530 3.3 0.0309 Mg 147.8 1.8 3.8 39.00 0.0798 1.9 0.0128 Sr 39.7 2.5 14.5 2.74 0.0036 2.5 0.0396 P 58.4 2.9 2.0 29.95 0.0717 2.9 0.0365 K 34.0 3.8 7.1 4.79 0.0245 3.8 0.0216 Cl 80.7 2.0 2.3 35.61 0.0171 2.0 0.0228 Ca 2788.6 0.4 18.0 154.91 0.6069 0.5 0.0334 Ba 11.0 4.8 11.2 0.98 0.0000 4.8 0.0000 Fe 3.5 8.4 3.5 0.99 0.0000 8.5 0.0000 Mn 2.8 13.3 3.3 0.84 0.0000 13.4 0.0000 Elt. k-ratio Correc. Na 0.0026 2.3098 Mg 0.0058 1.6964 Sr 0.0022 1.3828 P 0.0112 1.2049 K 0.0022 1.0564 Cl 0.0095 1.1331 Ca 0.2202 1.1035 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 86 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6110 0.023507 0.6110 0.4800 Mg 0.9796 0.018966 0.9796 0.7279 Sr 0.3055 0.014104 0.3055 0.0630 P 1.3549 0.042187 1.3549 0.7901 K 0.2296 0.012256 0.2296 0.1061 Cl 1.0779 0.022946 1.0779 0.5491 Ca 24.3049 0.122285 24.3049 10.9522 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.0928 16.0928 24.1984 O 55.0439 55.0439 62.1334 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 87 x= 14779.0 y= -3396.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 12.5 6.3 4.5 2.75 0.0101 6.3 0.0314 Mg 30.4 4.1 3.8 8.02 0.0147 4.1 0.0129 Sr 12.7 4.4 14.5 0.88 0.0000 4.4 0.0000 P 8.0 7.9 2.0 4.08 0.0076 7.9 0.0373 K 7.7 8.1 7.1 1.08 0.0005 8.1 0.0237 Cl 126.2 1.6 2.3 55.66 0.0270 1.6 0.0238 Ca 198.1 1.6 18.0 11.00 0.0394 1.6 0.0345 Ba 6.1 6.4 11.2 0.54 0.0000 6.4 0.0000 Fe 2.0 11.2 3.5 0.56 0.0000 11.3 0.0000 Mn 1.3 20.0 3.3 0.38 0.0000 20.0 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3469 Mg 0.0011 1.7150 Sr 0.0000 NaN P 0.0012 1.2319 K 0.0000 1.1603 Cl 0.0150 1.1820 Ca 0.0143 1.1395 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 87 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1186 0.013783 0.1186 0.0775 Mg 0.1830 0.009007 0.1830 0.1131 Sr 0.0000 0.000000 0.0000 0.0000 P 0.1472 0.017277 0.1472 0.0714 K 0.0056 0.008065 0.0056 0.0022 Cl 1.7756 0.029851 1.7756 0.7522 Ca 1.6312 0.030087 1.6312 0.6112 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.0725 26.0725 32.6020 O 70.0663 70.0663 65.7705 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 88 x= 14783.0 y= -3397.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 8.8 7.5 4.5 1.93 0.0054 7.5 0.0315 Mg 8.6 7.6 3.8 2.26 0.0026 7.7 0.0129 Sr 11.5 4.7 14.5 0.80 0.0000 4.7 0.0000 P 1.5 18.2 2.0 0.77 0.0000 18.3 0.0000 K 5.3 9.7 7.1 0.75 0.0000 9.7 0.0000 Cl 93.6 1.9 2.3 41.28 0.0199 1.9 0.0238 Ca 26.4 4.3 18.0 1.47 0.0018 4.4 0.0346 Ba 6.7 6.1 11.2 0.59 0.0000 6.1 0.0000 Fe 2.0 11.1 3.5 0.57 0.0000 11.1 0.0000 Mn 1.5 18.6 3.3 0.44 0.0000 18.6 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3577 Mg 0.0002 1.7205 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0111 1.1866 Ca 0.0007 1.1418 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 88 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0637 0.012247 0.0637 0.0410 Mg 0.0328 0.005419 0.0328 0.0200 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.3136 0.025840 1.3136 0.5481 Ca 0.0763 0.013526 0.0763 0.0281 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9460 26.9460 33.1894 O 71.5676 71.5676 66.1733 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 89 x= 14787.0 y= -3397.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 6.8 8.6 4.5 1.48 0.0028 8.6 0.0315 Mg 7.9 7.9 3.8 2.08 0.0023 8.0 0.0129 Sr 9.9 5.0 14.5 0.68 0.0000 5.0 0.0000 P 1.2 20.8 2.0 0.59 0.0000 20.9 0.0000 K 5.3 9.7 7.1 0.74 0.0000 9.8 0.0000 Cl 103.5 1.8 2.3 45.65 0.0220 1.8 0.0238 Ca 25.4 4.4 18.0 1.41 0.0016 4.4 0.0346 Ba 6.5 6.2 11.2 0.58 0.0000 6.2 0.0000 Fe 1.8 11.7 3.5 0.52 0.0000 11.7 0.0000 Mn 1.6 17.7 3.3 0.48 0.0000 17.7 0.0000 Elt. k-ratio Correc. Na 0.0001 2.3568 Mg 0.0002 1.7193 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0123 1.1863 Ca 0.0006 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 89 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0330 0.011262 0.0330 0.0212 Mg 0.0283 0.005270 0.0283 0.0172 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.4559 0.027152 1.4559 0.6079 Ca 0.0667 0.013366 0.0667 0.0246 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9329 26.9329 33.1935 O 71.4832 71.4832 66.1355 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 90 x= 14791.0 y= -3397.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 9.8 7.1 4.5 2.15 0.0067 7.2 0.0315 Mg 15.8 5.6 3.8 4.17 0.0067 5.6 0.0129 Sr 11.2 4.7 14.5 0.77 0.0000 4.7 0.0000 P 1.6 17.7 2.0 0.82 0.0000 17.7 0.0000 K 7.1 8.4 7.1 1.00 0.0000 8.4 NaN Cl 96.1 1.9 2.3 42.38 0.0204 1.9 0.0238 Ca 27.7 4.2 18.0 1.54 0.0021 4.3 0.0346 Ba 6.6 6.2 11.2 0.58 0.0000 6.2 0.0000 Fe 1.8 11.8 3.5 0.51 0.0000 11.8 0.0000 Mn 1.3 19.6 3.3 0.39 0.0000 19.6 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3563 Mg 0.0005 1.7201 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0114 1.1866 Ca 0.0008 1.1418 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 90 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0787 0.012691 0.0787 0.0506 Mg 0.0828 0.006829 0.0828 0.0504 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.3496 0.026179 1.3496 0.5635 Ca 0.0876 0.013715 0.0876 0.0324 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9059 26.9059 33.1589 O 71.4954 71.4954 66.1442 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 91 x= 14795.0 y= -3398.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 6.3 8.9 4.5 1.37 0.0022 9.0 0.0315 Mg 8.8 7.6 3.8 2.31 0.0027 7.6 0.0129 Sr 9.5 5.1 14.5 0.66 0.0000 5.1 0.0000 P 1.4 19.2 2.0 0.69 0.0000 19.2 0.0000 K 4.9 10.1 7.1 0.68 0.0000 10.2 0.0000 Cl 97.1 1.9 2.3 42.84 0.0207 1.9 0.0238 Ca 22.5 4.7 18.0 1.25 0.0010 4.7 0.0346 Ba 7.0 6.0 11.2 0.63 0.0000 6.0 0.0000 Fe 2.3 10.5 3.5 0.64 0.0000 10.5 0.0000 Mn 1.4 18.9 3.3 0.42 0.0000 18.9 0.0000 Elt. k-ratio Correc. Na 0.0001 2.3578 Mg 0.0002 1.7198 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0115 1.1866 Ca 0.0004 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 91 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0255 0.011014 0.0255 0.0164 Mg 0.0342 0.005460 0.0342 0.0208 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.3645 0.026317 1.3645 0.5693 Ca 0.0404 0.012910 0.0404 0.0149 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9623 26.9623 33.2064 O 71.5731 71.5731 66.1721 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 92 x= 14799.0 y= -3398.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 8.4 7.7 4.5 1.84 0.0048 7.7 0.0315 Mg 12.9 6.2 3.8 3.40 0.0050 6.2 0.0129 Sr 11.1 4.8 14.5 0.76 0.0000 4.8 0.0000 P 1.3 19.6 2.0 0.67 0.0000 19.6 0.0000 K 5.0 10.0 7.1 0.70 0.0000 10.1 0.0000 Cl 124.6 1.6 2.3 54.97 0.0266 1.6 0.0238 Ca 23.7 4.6 18.0 1.31 0.0012 4.6 0.0346 Ba 6.8 6.1 11.2 0.60 0.0000 6.1 0.0000 Fe 1.6 12.6 3.5 0.45 0.0000 12.6 0.0000 Mn 2.5 14.1 3.3 0.75 0.0000 14.1 0.0000 Elt. k-ratio Correc. Na 0.0002 2.3526 Mg 0.0004 1.7174 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0148 1.1858 Ca 0.0004 1.1421 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 92 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0568 0.012012 0.0568 0.0367 Mg 0.0627 0.006292 0.0627 0.0383 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.7587 0.029760 1.7587 0.7357 Ca 0.0513 0.013103 0.0513 0.0190 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8504 26.8504 33.1542 O 71.2200 71.2200 66.0162 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 93 x= 14804.0 y= -3398.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 6.5 8.8 4.5 1.43 0.0025 8.8 0.0316 Mg 10.7 6.8 3.8 2.81 0.0038 6.9 0.0130 Sr 9.4 5.1 14.5 0.65 0.0000 5.2 0.0000 P 1.3 20.0 2.0 0.64 0.0000 20.0 0.0000 K 4.4 10.6 7.1 0.62 0.0000 10.7 0.0000 Cl 74.8 2.1 2.3 32.99 0.0158 2.1 0.0239 Ca 19.0 5.1 18.0 1.05 0.0002 5.1 0.0346 Ba 6.6 6.2 11.2 0.58 0.0000 6.2 0.0000 Fe 2.3 10.5 3.5 0.64 0.0000 10.5 0.0000 Mn 1.8 16.9 3.3 0.53 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0001 2.3611 Mg 0.0003 1.7218 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0088 1.1873 Ca 0.0001 1.1417 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 93 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0293 0.011158 0.0293 0.0188 Mg 0.0474 0.005868 0.0474 0.0288 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.0440 0.023162 1.0440 0.4348 Ca 0.0086 0.012339 0.0086 0.0032 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0348 27.0348 33.2302 O 71.8359 71.8358 66.2843 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 94 x= 14808.0 y= -3399.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 6.6 8.7 4.5 1.44 0.0025 8.7 0.0315 Mg 12.0 6.5 3.8 3.15 0.0045 6.5 0.0129 Sr 8.4 5.5 14.5 0.58 0.0000 5.5 0.0000 P 1.7 17.4 2.0 0.85 0.0000 17.4 0.0000 K 6.4 8.9 7.1 0.89 0.0000 8.9 0.0000 Cl 122.0 1.7 2.3 53.82 0.0261 1.7 0.0238 Ca 22.9 4.7 18.0 1.27 0.0011 4.7 0.0346 Ba 7.0 6.0 11.2 0.62 0.0000 6.0 0.0000 Fe 2.1 10.9 3.5 0.60 0.0000 10.9 0.0000 Mn 1.8 16.6 3.3 0.54 0.0000 16.7 0.0000 Elt. k-ratio Correc. Na 0.0001 2.3535 Mg 0.0003 1.7174 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0145 1.1858 Ca 0.0004 1.1421 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 94 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0299 0.011147 0.0299 0.0193 Mg 0.0562 0.006111 0.0562 0.0343 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.7216 0.029455 1.7216 0.7199 Ca 0.0440 0.012978 0.0440 0.0163 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8739 26.8739 33.1700 O 71.2743 71.2743 66.0402 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 95 x= 14812.0 y= -3399.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 9.6 7.2 4.5 2.10 0.0064 7.2 0.0315 Mg 14.0 6.0 3.8 3.69 0.0057 6.0 0.0129 Sr 9.5 5.1 14.5 0.65 0.0000 5.2 0.0000 P 1.7 17.4 2.0 0.85 0.0000 17.4 0.0000 K 7.2 8.4 7.1 1.01 0.0000 8.4 0.0239 Cl 87.5 1.9 2.3 38.61 0.0186 2.0 0.0239 Ca 20.8 4.9 18.0 1.16 0.0006 4.9 0.0346 Ba 6.6 6.1 11.2 0.59 0.0000 6.1 0.0000 Fe 2.3 10.4 3.5 0.65 0.0000 10.4 0.0000 Mn 1.5 18.2 3.3 0.45 0.0000 18.3 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3580 Mg 0.0004 1.7209 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1683 Cl 0.0103 1.1870 Ca 0.0002 1.1418 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 95 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0750 0.012590 0.0750 0.0482 Mg 0.0704 0.006511 0.0704 0.0428 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0005 0.007968 0.0005 0.0002 Cl 1.2272 0.025014 1.2272 0.5118 Ca 0.0254 0.012644 0.0254 0.0094 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9623 26.9623 33.1890 O 71.6392 71.6392 66.1986 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 96 x= 14816.0 y= -3399.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 6.6 8.7 4.5 1.44 0.0025 8.7 0.0316 Mg 8.7 7.6 3.8 2.28 0.0027 7.6 0.0129 Sr 9.3 5.2 14.5 0.64 0.0000 5.2 0.0000 P 1.6 17.7 2.0 0.82 0.0000 17.7 0.0000 K 5.9 9.2 7.1 0.83 0.0000 9.2 0.0000 Cl 86.2 2.0 2.3 38.04 0.0183 2.0 0.0239 Ca 21.4 4.8 18.0 1.19 0.0007 4.8 0.0346 Ba 6.6 6.2 11.2 0.59 0.0000 6.2 0.0000 Fe 1.7 12.1 3.5 0.48 0.0000 12.1 0.0000 Mn 1.4 18.9 3.3 0.42 0.0000 18.9 0.0000 Elt. k-ratio Correc. Na 0.0001 2.3595 Mg 0.0002 1.7208 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0102 1.1869 Ca 0.0003 1.1418 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 96 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0300 0.011177 0.0300 0.0193 Mg 0.0335 0.005443 0.0335 0.0204 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.2086 0.024834 1.2086 0.5038 Ca 0.0309 0.012744 0.0309 0.0114 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9976 26.9976 33.2185 O 71.6994 71.6994 66.2266 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 97 x= 14820.0 y= -3400.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 9.1 7.4 4.5 1.99 0.0057 7.4 0.0316 Mg 10.0 7.1 3.8 2.64 0.0034 7.1 0.0130 Sr 8.8 5.3 14.5 0.61 0.0000 5.3 0.0000 P 1.3 20.0 2.0 0.64 0.0000 20.0 0.0000 K 5.4 9.7 7.1 0.75 0.0000 9.7 0.0000 Cl 78.6 2.1 2.3 34.67 0.0166 2.1 0.0239 Ca 17.9 5.3 18.0 0.99 0.0000 5.3 0.0000 Ba 6.7 6.1 11.2 0.60 0.0000 6.1 0.0000 Fe 2.2 10.8 3.5 0.61 0.0000 10.8 0.0000 Mn 1.6 17.9 3.3 0.47 0.0000 18.0 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3599 Mg 0.0002 1.7219 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0093 1.1873 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 97 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0676 0.012378 0.0676 0.0434 Mg 0.0429 0.005736 0.0429 0.0261 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.0991 0.023737 1.0991 0.4579 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0145 27.0145 33.2180 O 71.7760 71.7760 66.2547 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 98 x= 14824.0 y= -3400.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 7.7 8.1 4.5 1.69 0.0040 8.1 0.0316 Mg 8.9 7.5 3.8 2.35 0.0028 7.5 0.0130 Sr 10.7 4.8 14.5 0.74 0.0000 4.8 0.0000 P 1.8 16.9 2.0 0.90 0.0000 16.9 0.0000 K 5.6 9.4 7.1 0.79 0.0000 9.5 0.0000 Cl 72.5 2.1 2.3 31.99 0.0153 2.1 0.0239 Ca 16.3 5.5 18.0 0.91 0.0000 5.5 0.0000 Ba 6.4 6.2 11.2 0.57 0.0000 6.3 0.0000 Fe 1.6 12.4 3.5 0.46 0.0000 12.4 0.0000 Mn 1.9 16.2 3.3 0.57 0.0000 16.2 0.0000 Elt. k-ratio Correc. Na 0.0002 2.3613 Mg 0.0002 1.7223 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0085 1.1874 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 98 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0473 0.011754 0.0473 0.0304 Mg 0.0353 0.005503 0.0353 0.0214 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.0117 0.022824 1.0117 0.4212 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0438 27.0438 33.2337 O 71.8619 71.8619 66.2933 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 99 x= 14829.0 y= -3400.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 8.1 7.9 4.5 1.77 0.0045 7.9 0.0315 Mg 11.0 6.7 3.8 2.90 0.0040 6.7 0.0129 Sr 10.9 4.8 14.5 0.75 0.0000 4.8 0.0000 P 1.6 17.9 2.0 0.79 0.0000 18.0 0.0000 K 5.2 9.8 7.1 0.73 0.0000 9.8 0.0000 Cl 122.8 1.6 2.3 54.17 0.0263 1.6 0.0239 Ca 14.6 5.9 18.0 0.81 0.0000 5.9 0.0000 Ba 6.1 6.4 11.2 0.54 0.0000 6.4 0.0000 Fe 1.9 11.4 3.5 0.55 0.0000 11.4 0.0000 Mn 2.0 16.0 3.3 0.59 0.0000 16.0 0.0000 Elt. k-ratio Correc. Na 0.0002 2.3531 Mg 0.0003 1.7176 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0146 1.1859 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 99 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0524 0.011884 0.0524 0.0338 Mg 0.0497 0.005928 0.0497 0.0303 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.7345 0.029573 1.7345 0.7252 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8827 26.8827 33.1754 O 71.2808 71.2808 66.0354 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 100 x= 14833.0 y= -3401.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 12.2 6.4 4.5 2.67 0.0097 6.4 0.0316 Mg 9.7 7.2 3.8 2.56 0.0033 7.2 0.0130 Sr 10.5 4.9 14.5 0.72 0.0000 4.9 0.0000 P 2.2 15.2 2.0 1.10 0.0003 15.3 0.0375 K 5.6 9.5 7.1 0.78 0.0000 9.5 0.0000 Cl 67.2 2.2 2.3 29.66 0.0142 2.2 0.0239 Ca 16.8 5.4 18.0 0.93 0.0000 5.5 0.0000 Ba 6.8 6.1 11.2 0.61 0.0000 6.1 0.0000 Fe 1.9 11.4 3.5 0.55 0.0000 11.4 0.0000 Mn 1.0 22.3 3.3 0.30 0.0000 22.4 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3609 Mg 0.0002 1.7235 Sr 0.0000 NaN P 0.0000 1.2371 K 0.0000 NaN Cl 0.0079 1.1876 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 100 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1141 0.013729 0.1141 0.0733 Mg 0.0409 0.005679 0.0409 0.0248 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0049 0.011162 0.0049 0.0023 K 0.0000 0.000000 0.0000 0.0000 Cl 0.9361 0.022005 0.9361 0.3897 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0296 27.0296 33.2125 O 71.8744 71.8744 66.2974 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 101 x= 14837.0 y= -3401.0 z= -247. carb3 2 vertical samp trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 9.8 7.2 4.5 2.14 0.0066 7.2 0.0316 Mg 7.8 8.0 3.8 2.06 0.0022 8.0 0.0130 Sr 11.7 4.6 14.5 0.80 0.0000 4.6 0.0000 P 3.9 11.3 2.0 2.00 0.0025 11.3 0.0374 K 5.5 9.6 7.1 0.77 0.0000 9.6 0.0000 Cl 99.6 1.8 2.3 43.95 0.0212 1.8 0.0239 Ca 13.7 6.0 18.0 0.76 0.0000 6.0 0.0000 Ba 6.9 6.0 11.2 0.61 0.0000 6.0 0.0000 Fe 2.0 11.3 3.5 0.55 0.0000 11.3 0.0000 Mn 1.5 18.2 3.3 0.45 0.0000 18.3 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3562 Mg 0.0002 1.7199 Sr 0.0000 NaN P 0.0004 1.2353 K 0.0000 NaN Cl 0.0118 1.1868 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 101 within carb3 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0780 0.012678 0.0780 0.0502 Mg 0.0277 0.005254 0.0277 0.0168 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0480 0.013318 0.0480 0.0229 K 0.0000 0.000000 0.0000 0.0000 Cl 1.4018 0.026675 1.4018 0.5852 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9235 26.9235 33.1727 O 71.5210 71.5210 66.1522 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) Analyze complete at Thu Mar 23 16:17:35 2006 Note: IEEE floating-point exception flags raised: Inexact; Invalid Operation; See the Numerical Computation Guide, ieee_flags(3M) quanta : complete ================================================================================ Quantitative Microprobe Analysis Thu Mar 23 16:17:42 2006 ================================================================================ point n : 1 x= -12939.0 y= 2626.0 z= -278. carb2 trav 1 bkg Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 13.2 6.2 3.6 3.63 0.0121 6.2 0.0285 Mg 68.3 2.7 2.5 27.13 0.0365 2.7 0.0109 Sr 29.9 2.9 14.3 2.09 0.0022 2.9 0.0391 P 70.4 2.7 2.4 29.96 0.0865 2.7 0.0388 K 11.0 6.8 5.1 2.15 0.0053 6.8 0.0183 Cl 25.5 3.6 2.2 11.59 0.0051 3.6 0.0222 Ca 3544.0 0.4 17.7 200.78 0.7732 0.5 0.0329 Ba 10.9 4.8 10.8 1.02 0.0001 4.8 0.0737 Fe 4.0 7.9 3.3 1.20 0.0004 8.0 0.0549 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0618 Elt. k-ratio Correc. Na 0.0006 2.3305 Mg 0.0026 1.6966 Sr 0.0014 1.3725 P 0.0136 1.1943 K 0.0005 1.0261 Cl 0.0028 1.1191 Ca 0.2806 1.0937 Ba 0.0000 1.5387 Fe 0.0002 1.2537 Mn 0.0000 1.2765 iteration : 3 Analysis no. 1 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1412 0.013593 0.1412 0.1158 Mg 0.4480 0.012886 0.4480 0.3473 Sr 0.1878 0.012639 0.1878 0.0404 P 1.6206 0.046067 1.6206 0.9860 K 0.0485 0.007435 0.0485 0.0234 Cl 0.3165 0.013067 0.3165 0.1682 Ca 30.6874 0.141806 30.6874 14.4280 Ba 0.0045 0.019051 0.0045 0.0006 Fe 0.0215 0.014098 0.0215 0.0073 Mn 0.0015 0.018804 0.0015 0.0005 C 14.1518 14.1518 22.2027 O 52.3706 52.3706 61.6799 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 2 x= -12967.0 y= 2555.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 2.5 14.1 3.6 0.69 0.0000 14.1 0.0000 Mg 4.0 11.2 2.5 1.59 0.0008 11.2 0.0110 Sr 9.7 5.1 14.3 0.68 0.0000 5.1 0.0000 P 1.0 22.9 2.4 0.40 0.0000 22.9 0.0000 K 2.8 13.3 5.1 0.55 0.0000 13.4 0.0000 Cl 97.8 1.8 2.2 44.44 0.0208 1.8 0.0236 Ca 11.3 6.6 17.7 0.64 0.0000 6.7 0.0000 Ba 6.3 6.3 10.8 0.58 0.0000 6.3 0.0000 Fe 1.9 11.5 3.3 0.58 0.0000 11.5 0.0000 Mn 1.8 16.6 2.7 0.66 0.0000 16.7 0.0000 Elt. k-ratio Correc. Na 0.0000 NaN Mg 0.0001 1.7196 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0116 1.1866 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 2 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0000 0.000000 0.0000 0.0000 Mg 0.0102 0.003940 0.0102 0.0062 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.3768 0.026431 1.3768 0.5742 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9954 26.9954 33.2335 O 71.6176 71.6176 66.1861 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Na ( 0.00) be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 3 x= -12966.0 y= 2559.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 4.4 10.6 3.6 1.21 0.0010 10.7 0.0289 Mg 5.5 9.5 2.5 2.18 0.0017 9.5 0.0111 Sr 11.8 4.6 14.3 0.83 0.0000 4.6 0.0000 P 1.0 22.9 2.4 0.40 0.0000 22.9 0.0000 K 3.3 12.3 5.1 0.65 0.0000 12.3 0.0000 Cl 53.2 2.5 2.2 24.19 0.0111 2.5 0.0236 Ca 22.5 4.7 17.7 1.27 0.0011 4.7 0.0343 Ba 6.9 6.0 10.8 0.64 0.0000 6.0 0.0000 Fe 2.0 11.2 3.3 0.61 0.0000 11.2 0.0000 Mn 1.3 19.6 2.7 0.48 0.0000 19.6 0.0000 Elt. k-ratio Correc. Na 0.0000 2.3651 Mg 0.0001 1.7237 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0062 1.1878 Ca 0.0004 1.1415 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 3 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0116 0.009536 0.0116 0.0075 Mg 0.0206 0.004381 0.0206 0.0125 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.7357 0.019650 0.7357 0.3058 Ca 0.0436 0.012865 0.0436 0.0160 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.1052 27.1052 33.2596 O 72.0832 72.0832 66.3986 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 4 x= -12965.0 y= 2563.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 19.5 5.1 3.6 5.36 0.0202 5.1 0.0288 Mg 19.6 5.0 2.5 7.78 0.0095 5.1 0.0111 Sr 15.7 4.0 14.3 1.10 0.0002 4.0 0.0403 P 4.3 10.8 2.4 1.81 0.0024 10.9 0.0401 K 9.0 7.4 5.1 1.76 0.0036 7.5 0.0207 Cl 74.3 2.1 2.2 33.78 0.0157 2.1 0.0235 Ca 162.5 1.8 17.7 9.21 0.0318 1.8 0.0343 Ba 7.1 5.9 10.8 0.66 0.0000 5.9 0.0000 Fe 5.9 6.5 3.3 1.78 0.0014 6.5 0.0566 Mn 1.4 18.9 2.7 0.52 0.0000 18.9 0.0000 Elt. k-ratio Correc. Na 0.0010 2.3563 Mg 0.0007 1.7230 Sr 0.0001 1.4134 P 0.0004 1.2353 K 0.0003 1.1603 Cl 0.0088 1.1838 Ca 0.0115 1.1392 Ba 0.0000 NaN Fe 0.0007 1.2929 Mn 0.0000 NaN iteration : 2 Analysis no. 4 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2373 0.016134 0.2373 0.1541 Mg 0.1181 0.007280 0.1181 0.0726 Sr 0.0179 0.010719 0.0179 0.0031 P 0.0468 0.014150 0.0468 0.0226 K 0.0366 0.007880 0.0366 0.0140 Cl 1.0361 0.023034 1.0361 0.4364 Ca 1.3129 0.027428 1.3129 0.4891 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0879 0.016359 0.0879 0.0235 Mn 0.0000 0.000000 0.0000 0.0000 C 26.3520 26.3520 32.7581 O 70.7543 70.7543 66.0267 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 5 x= -12964.0 y= 2568.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 34.0 3.8 3.6 9.36 0.0387 3.9 0.0285 Mg 136.2 1.9 2.5 54.08 0.0741 1.9 0.0109 Sr 42.9 2.4 14.3 3.01 0.0041 2.4 0.0391 P 11.3 6.6 2.4 4.81 0.0114 6.7 0.0386 K 7.7 8.1 5.1 1.50 0.0023 8.1 0.0176 Cl 10.2 5.7 2.2 4.62 0.0017 5.7 0.0218 Ca 4634.2 0.3 17.7 262.55 1.0125 0.4 0.0325 Ba 12.2 4.5 10.8 1.13 0.0008 4.5 0.0739 Fe 4.8 7.2 3.3 1.44 0.0008 7.3 0.0545 Mn 4.4 10.7 2.7 1.61 0.0016 10.7 0.0614 Elt. k-ratio Correc. Na 0.0019 2.3301 Mg 0.0054 1.7002 Sr 0.0025 1.3704 P 0.0018 1.1894 K 0.0002 0.9871 Cl 0.0010 1.0957 Ca 0.3674 1.0794 Ba 0.0002 1.5429 Fe 0.0004 1.2436 Mn 0.0005 1.2686 iteration : 3 Analysis no. 5 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4498 0.020408 0.4498 0.3967 Mg 0.9121 0.018189 0.9121 0.7610 Sr 0.3436 0.014379 0.3436 0.0795 P 0.2123 0.019621 0.2123 0.1390 K 0.0204 0.006376 0.0204 0.0106 Cl 0.1060 0.008543 0.1060 0.0606 Ca 39.6603 0.168012 39.6603 20.0670 Ba 0.0363 0.019640 0.0363 0.0054 Fe 0.0476 0.014740 0.0476 0.0173 Mn 0.0587 0.021257 0.0587 0.0217 C 11.2470 11.2470 18.9895 O 46.9059 46.9059 59.4517 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 6 x= -12963.0 y= 2572.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 41.8 3.5 3.6 11.53 0.0487 3.5 0.0284 Mg 210.8 1.5 2.5 83.70 0.1155 1.6 0.0109 Sr 46.0 2.3 14.3 3.22 0.0045 2.3 0.0392 P 24.7 4.5 2.4 10.49 0.0284 4.5 0.0387 K 9.6 7.2 5.1 1.87 0.0041 7.2 0.0177 Cl 11.6 5.4 2.2 5.26 0.0020 5.4 0.0219 Ca 4536.3 0.3 17.7 257.00 0.9911 0.4 0.0325 Ba 12.4 4.5 10.8 1.15 0.0010 4.5 0.0739 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0545 Mn 4.5 10.5 2.7 1.66 0.0018 10.5 0.0614 Elt. k-ratio Correc. Na 0.0024 2.3174 Mg 0.0084 1.6956 Sr 0.0028 1.3734 P 0.0044 1.1923 K 0.0004 0.9932 Cl 0.0011 1.1002 Ca 0.3597 1.0806 Ba 0.0003 1.5417 Fe 0.0000 1.2434 Mn 0.0005 1.2682 iteration : 3 Analysis no. 6 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5632 0.022346 0.5632 0.4966 Mg 1.4175 0.022653 1.4175 1.1823 Sr 0.3817 0.014802 0.3817 0.0883 P 0.5303 0.027743 0.5303 0.3471 K 0.0358 0.006878 0.0358 0.0185 Cl 0.1251 0.009052 0.1251 0.0715 Ca 38.8647 0.165731 38.8647 19.6573 Ba 0.0422 0.019723 0.0422 0.0062 Fe 0.0057 0.013520 0.0057 0.0021 Mn 0.0641 0.021477 0.0641 0.0236 C 11.0712 11.0712 18.6858 O 46.8987 46.8987 59.4207 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 7 x= -12963.0 y= 2576.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 33.9 3.8 3.6 9.35 0.0386 3.9 0.0283 Mg 236.9 1.5 2.5 94.06 0.1299 1.5 0.0109 Sr 41.5 2.5 14.3 2.91 0.0039 2.5 0.0392 P 36.6 3.7 2.4 15.58 0.0436 3.7 0.0387 K 10.0 7.1 5.1 1.95 0.0044 7.1 0.0178 Cl 14.7 4.8 2.2 6.68 0.0027 4.8 0.0219 Ca 4466.8 0.3 17.7 253.06 0.9758 0.4 0.0325 Ba 13.9 4.2 10.8 1.29 0.0019 4.3 0.0738 Fe 4.0 7.9 3.3 1.20 0.0004 7.9 0.0545 Mn 5.3 9.7 2.7 1.96 0.0025 9.7 0.0614 Elt. k-ratio Correc. Na 0.0019 2.3153 Mg 0.0094 1.6926 Sr 0.0024 1.3740 P 0.0068 1.1925 K 0.0004 0.9968 Cl 0.0015 1.1025 Ca 0.3541 1.0813 Ba 0.0005 1.5410 Fe 0.0002 1.2434 Mn 0.0007 1.2682 iteration : 3 Analysis no. 7 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4462 0.020265 0.4462 0.3928 Mg 1.5921 0.024011 1.5921 1.3257 Sr 0.3274 0.014234 0.3274 0.0756 P 0.8146 0.033413 0.8146 0.5322 K 0.0391 0.006997 0.0391 0.0202 Cl 0.1673 0.010052 0.1673 0.0955 Ca 38.2919 0.164074 38.2919 19.3354 Ba 0.0804 0.020332 0.0804 0.0118 Fe 0.0222 0.014010 0.0222 0.0080 Mn 0.0927 0.022637 0.0927 0.0341 C 11.0561 11.0561 18.6294 O 47.0701 47.0701 59.5390 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 8 x= -12962.0 y= 2580.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 39.8 3.5 3.6 10.97 0.0462 3.6 0.0283 Mg 250.6 1.4 2.5 99.50 0.1376 1.4 0.0109 Sr 45.3 2.3 14.3 3.17 0.0044 2.4 0.0392 P 45.0 3.3 2.4 19.13 0.0542 3.3 0.0388 K 8.6 7.6 5.1 1.68 0.0031 7.7 0.0179 Cl 18.4 4.3 2.2 8.36 0.0035 4.3 0.0220 Ca 4441.4 0.3 17.7 251.62 0.9710 0.4 0.0326 Ba 13.4 4.3 10.8 1.24 0.0016 4.3 0.0739 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0546 Mn 5.0 10.0 2.7 1.85 0.0023 10.0 0.0615 Elt. k-ratio Correc. Na 0.0023 2.3096 Mg 0.0100 1.6910 Sr 0.0027 1.3740 P 0.0085 1.1930 K 0.0003 0.9992 Cl 0.0020 1.1042 Ca 0.3524 1.0816 Ba 0.0004 1.5406 Fe 0.0001 1.2430 Mn 0.0006 1.2678 iteration : 3 Analysis no. 8 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5323 0.021786 0.5323 0.4694 Mg 1.6849 0.024716 1.6849 1.4053 Sr 0.3737 0.014733 0.3737 0.0865 P 1.0145 0.036939 1.0145 0.6640 K 0.0279 0.006685 0.0279 0.0145 Cl 0.2174 0.011127 0.2174 0.1243 Ca 38.1183 0.163622 38.1183 19.2795 Ba 0.0675 0.020136 0.0675 0.0100 Fe 0.0115 0.013702 0.0115 0.0042 Mn 0.0820 0.022221 0.0820 0.0303 C 10.9133 10.9133 18.4189 O 46.9566 46.9566 59.4933 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 9 x= -12961.0 y= 2584.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 39.1 3.6 3.6 10.78 0.0452 3.6 0.0283 Mg 259.8 1.4 2.5 103.18 0.1427 1.4 0.0109 Sr 44.1 2.4 14.3 3.09 0.0042 2.4 0.0392 P 38.9 3.6 2.4 16.53 0.0464 3.6 0.0388 K 10.1 7.0 5.1 1.97 0.0045 7.1 0.0179 Cl 18.3 4.3 2.2 8.32 0.0035 4.3 0.0220 Ca 4378.9 0.3 17.7 248.08 0.9568 0.4 0.0326 Ba 13.2 4.4 10.8 1.23 0.0015 4.4 0.0739 Fe 4.5 7.5 3.3 1.36 0.0007 7.5 0.0545 Mn 4.4 10.6 2.7 1.62 0.0017 10.7 0.0615 Elt. k-ratio Correc. Na 0.0023 2.3108 Mg 0.0103 1.6916 Sr 0.0026 1.3756 P 0.0073 1.1942 K 0.0004 1.0005 Cl 0.0020 1.1048 Ca 0.3472 1.0824 Ba 0.0004 1.5404 Fe 0.0003 1.2439 Mn 0.0005 1.2685 iteration : 3 Analysis no. 9 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5220 0.021607 0.5220 0.4576 Mg 1.7476 0.025183 1.7476 1.4490 Sr 0.3589 0.014585 0.3589 0.0825 P 0.8696 0.034442 0.8696 0.5658 K 0.0401 0.007048 0.0401 0.0207 Cl 0.2160 0.011099 0.2160 0.1228 Ca 37.5868 0.162059 37.5868 18.8990 Ba 0.0629 0.020050 0.0629 0.0092 Fe 0.0386 0.014494 0.0386 0.0139 Mn 0.0605 0.021338 0.0605 0.0222 C 11.1828 11.1828 18.7630 O 47.3142 47.3142 59.5942 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 10 x= -12960.0 y= 2588.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 35.5 3.8 3.6 9.77 0.0406 3.8 0.0283 Mg 255.9 1.4 2.5 101.60 0.1406 1.4 0.0109 Sr 41.9 2.4 14.3 2.93 0.0039 2.5 0.0392 P 43.4 3.4 2.4 18.45 0.0522 3.4 0.0388 K 9.3 7.3 5.1 1.81 0.0038 7.4 0.0178 Cl 20.7 4.0 2.2 9.40 0.0040 4.0 0.0220 Ca 4480.3 0.3 17.7 253.83 0.9795 0.4 0.0326 Ba 13.7 4.3 10.8 1.27 0.0018 4.3 0.0739 Fe 4.5 7.4 3.3 1.37 0.0007 7.4 0.0545 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0615 Elt. k-ratio Correc. Na 0.0020 2.3106 Mg 0.0102 1.6903 Sr 0.0024 1.3739 P 0.0082 1.1924 K 0.0003 0.9980 Cl 0.0022 1.1032 Ca 0.3555 1.0813 Ba 0.0005 1.5409 Fe 0.0003 1.2429 Mn 0.0004 1.2677 iteration : 3 Analysis no. 10 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4685 0.020660 0.4685 0.4140 Mg 1.7202 0.024975 1.7202 1.4381 Sr 0.3324 0.014296 0.3324 0.0771 P 0.9758 0.036273 0.9758 0.6401 K 0.0335 0.006845 0.0335 0.0174 Cl 0.2476 0.011713 0.2476 0.1419 Ca 38.4375 0.164544 38.4375 19.4862 Ba 0.0753 0.020265 0.0753 0.0111 Fe 0.0403 0.014536 0.0403 0.0146 Mn 0.0480 0.020802 0.0480 0.0178 C 10.8278 10.8278 18.3172 O 46.7933 46.7933 59.4244 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 11 x= -12959.0 y= 2593.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 36.9 3.7 3.6 10.16 0.0424 3.7 0.0283 Mg 254.3 1.4 2.5 100.97 0.1396 1.4 0.0109 Sr 44.9 2.4 14.3 3.15 0.0043 2.4 0.0392 P 42.2 3.4 2.4 17.96 0.0507 3.5 0.0388 K 9.3 7.3 5.1 1.81 0.0038 7.4 0.0179 Cl 17.8 4.3 2.2 8.11 0.0034 4.3 0.0220 Ca 4404.8 0.3 17.7 249.55 0.9627 0.4 0.0326 Ba 13.0 4.4 10.8 1.21 0.0013 4.4 0.0739 Fe 4.6 7.3 3.3 1.40 0.0007 7.4 0.0546 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0615 Elt. k-ratio Correc. Na 0.0021 2.3108 Mg 0.0101 1.6909 Sr 0.0027 1.3747 P 0.0080 1.1936 K 0.0003 1.0000 Cl 0.0019 1.1046 Ca 0.3494 1.0822 Ba 0.0004 1.5406 Fe 0.0004 1.2436 Mn 0.0004 1.2683 iteration : 3 Analysis no. 11 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4890 0.021027 0.4890 0.4296 Mg 1.7094 0.024896 1.7094 1.4204 Sr 0.3693 0.014688 0.3693 0.0851 P 0.9491 0.035831 0.9491 0.6189 K 0.0336 0.006857 0.0336 0.0174 Cl 0.2098 0.010973 0.2098 0.1195 Ca 37.8089 0.162715 37.8089 19.0516 Ba 0.0577 0.019972 0.0577 0.0085 Fe 0.0436 0.014634 0.0436 0.0158 Mn 0.0444 0.020652 0.0444 0.0163 C 11.0833 11.0833 18.6361 O 47.2019 47.2019 59.5808 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 12 x= -12958.0 y= 2597.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 38.6 3.6 3.6 10.64 0.0446 3.6 0.0283 Mg 280.4 1.3 2.5 111.35 0.1542 1.4 0.0109 Sr 44.8 2.4 14.3 3.14 0.0043 2.4 0.0393 P 41.5 3.5 2.4 17.64 0.0498 3.5 0.0389 K 8.7 7.6 5.1 1.70 0.0032 7.6 0.0179 Cl 18.7 4.2 2.2 8.49 0.0036 4.2 0.0220 Ca 4395.5 0.3 17.7 249.02 0.9612 0.4 0.0326 Ba 13.5 4.3 10.8 1.25 0.0016 4.3 0.0739 Fe 4.6 7.4 3.3 1.39 0.0007 7.4 0.0546 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0615 Elt. k-ratio Correc. Na 0.0022 2.3080 Mg 0.0112 1.6900 Sr 0.0027 1.3759 P 0.0078 1.1944 K 0.0003 1.0006 Cl 0.0020 1.1051 Ca 0.3488 1.0822 Ba 0.0005 1.5404 Fe 0.0003 1.2435 Mn 0.0003 1.2682 iteration : 3 Analysis no. 12 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5144 0.021468 0.5144 0.4522 Mg 1.8870 0.026195 1.8870 1.5690 Sr 0.3683 0.014694 0.3683 0.0849 P 0.9325 0.035567 0.9325 0.6084 K 0.0288 0.006720 0.0288 0.0149 Cl 0.2212 0.011210 0.2212 0.1261 Ca 37.7505 0.162572 37.7505 19.0345 Ba 0.0701 0.020180 0.0701 0.0103 Fe 0.0428 0.014617 0.0428 0.0155 Mn 0.0355 0.020269 0.0355 0.0131 C 11.0255 11.0255 18.5508 O 47.1236 47.1236 59.5204 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 13 x= -12957.0 y= 2601.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 37.3 3.7 3.6 10.29 0.0430 3.7 0.0283 Mg 276.8 1.3 2.5 109.90 0.1523 1.4 0.0109 Sr 46.6 2.3 14.3 3.26 0.0046 2.3 0.0393 P 44.9 3.3 2.4 19.11 0.0542 3.4 0.0389 K 11.3 6.7 5.1 2.21 0.0056 6.7 0.0179 Cl 21.5 3.9 2.2 9.77 0.0042 3.9 0.0220 Ca 4399.9 0.3 17.7 249.27 0.9625 0.4 0.0326 Ba 13.3 4.3 10.8 1.23 0.0015 4.3 0.0740 Fe 4.6 7.3 3.3 1.40 0.0007 7.4 0.0546 Mn 4.2 11.0 2.7 1.53 0.0014 11.0 0.0616 Elt. k-ratio Correc. Na 0.0021 2.3073 Mg 0.0110 1.6891 Sr 0.0028 1.3751 P 0.0085 1.1941 K 0.0005 1.0011 Cl 0.0023 1.1052 Ca 0.3493 1.0822 Ba 0.0004 1.5403 Fe 0.0004 1.2431 Mn 0.0004 1.2678 iteration : 3 Analysis no. 13 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4953 0.021132 0.4953 0.4361 Mg 1.8619 0.026012 1.8619 1.5509 Sr 0.3899 0.014915 0.3899 0.0901 P 1.0148 0.036971 1.0148 0.6633 K 0.0499 0.007335 0.0499 0.0258 Cl 0.2594 0.011954 0.2594 0.1481 Ca 37.7995 0.162732 37.7995 19.0929 Ba 0.0655 0.020112 0.0655 0.0097 Fe 0.0436 0.014641 0.0436 0.0158 Mn 0.0516 0.020971 0.0516 0.0190 C 10.9471 10.9471 18.4516 O 47.0215 47.0215 59.4967 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 14 x= -12956.0 y= 2605.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 29.6 4.1 3.6 8.15 0.0331 4.1 0.0283 Mg 264.1 1.4 2.5 104.89 0.1452 1.4 0.0109 Sr 42.0 2.4 14.3 2.94 0.0039 2.5 0.0393 P 70.9 2.7 2.4 30.18 0.0873 2.7 0.0389 K 11.3 6.7 5.1 2.21 0.0056 6.7 0.0182 Cl 30.1 3.3 2.2 13.67 0.0061 3.3 0.0222 Ca 4023.3 0.4 17.7 227.94 0.8795 0.4 0.0328 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0739 Fe 4.7 7.3 3.3 1.41 0.0008 7.3 0.0547 Mn 4.5 10.5 2.7 1.66 0.0018 10.5 0.0616 Elt. k-ratio Correc. Na 0.0017 2.3054 Mg 0.0105 1.6863 Sr 0.0024 1.3756 P 0.0137 1.1956 K 0.0005 1.0151 Cl 0.0034 1.1138 Ca 0.3192 1.0872 Ba 0.0000 1.5388 Fe 0.0004 1.2464 Mn 0.0005 1.2703 iteration : 3 Analysis no. 14 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3808 0.018981 0.3808 0.3273 Mg 1.7726 0.025338 1.7726 1.4410 Sr 0.3338 0.014328 0.3338 0.0753 P 1.6365 0.046341 1.6365 1.0439 K 0.0506 0.007435 0.0506 0.0256 Cl 0.3773 0.014059 0.3773 0.2103 Ca 34.7015 0.153728 34.7015 17.1070 Ba 0.0032 0.019055 0.0032 0.0005 Fe 0.0445 0.014697 0.0445 0.0157 Mn 0.0643 0.021535 0.0643 0.0231 C 11.8309 11.8309 19.4622 O 48.8039 48.8039 60.2681 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 15 x= -12955.0 y= 2609.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 28.9 4.2 3.6 7.95 0.0322 4.2 0.0284 Mg 169.9 1.7 2.5 67.45 0.0929 1.7 0.0109 Sr 39.1 2.5 14.3 2.74 0.0035 2.5 0.0393 P 60.2 2.9 2.4 25.60 0.0737 2.9 0.0389 K 14.8 5.8 5.1 2.90 0.0089 5.8 0.0182 Cl 34.2 3.1 2.2 15.53 0.0070 3.1 0.0222 Ca 3852.4 0.4 17.7 218.25 0.8424 0.4 0.0329 Ba 10.2 5.0 10.8 0.95 0.0000 5.0 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0549 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0618 Elt. k-ratio Correc. Na 0.0016 2.3160 Mg 0.0067 1.6924 Sr 0.0022 1.3742 P 0.0115 1.1949 K 0.0008 1.0181 Cl 0.0039 1.1143 Ca 0.3057 1.0896 Ba 0.0000 NaN Fe 0.0001 1.2493 Mn 0.0002 1.2728 iteration : 3 Analysis no. 15 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3725 0.018875 0.3725 0.3141 Mg 1.1386 0.020282 1.1386 0.9083 Sr 0.2990 0.013945 0.2990 0.0662 P 1.3798 0.042705 1.3798 0.8637 K 0.0800 0.008233 0.0800 0.0397 Cl 0.4333 0.014944 0.4333 0.2369 Ca 33.3093 0.149675 33.3093 16.1138 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0107 0.013756 0.0107 0.0037 Mn 0.0303 0.020115 0.0303 0.0107 C 12.8276 12.8276 20.7075 O 50.1188 50.1188 60.7354 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 16 x= -12955.0 y= 2614.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 12.1 6.4 3.6 3.32 0.0107 6.5 0.0285 Mg 114.8 2.1 2.5 45.59 0.0623 2.1 0.0109 Sr 36.5 2.6 14.3 2.55 0.0031 2.6 0.0391 P 39.9 3.5 2.4 16.96 0.0477 3.6 0.0387 K 13.1 6.2 5.1 2.56 0.0073 6.2 0.0179 Cl 40.8 2.9 2.2 18.54 0.0084 2.9 0.0220 Ca 4241.4 0.3 17.7 240.29 0.9269 0.4 0.0327 Ba 11.9 4.6 10.8 1.11 0.0007 4.6 0.0739 Fe 4.1 7.8 3.3 1.24 0.0004 7.8 0.0547 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0616 Elt. k-ratio Correc. Na 0.0005 2.3284 Mg 0.0045 1.6937 Sr 0.0019 1.3687 P 0.0075 1.1892 K 0.0006 1.0035 Cl 0.0047 1.1041 Ca 0.3364 1.0848 Ba 0.0002 1.5414 Fe 0.0002 1.2466 Mn 0.0003 1.2709 iteration : 3 Analysis no. 16 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1249 0.013138 0.1249 0.1076 Mg 0.7638 0.016642 0.7638 0.6225 Sr 0.2660 0.013527 0.2660 0.0601 P 0.8899 0.034729 0.8899 0.5692 K 0.0646 0.007741 0.0646 0.0327 Cl 0.5174 0.016084 0.5174 0.2891 Ca 36.4911 0.158933 36.4911 18.0352 Ba 0.0298 0.019525 0.0298 0.0043 Fe 0.0264 0.014176 0.0264 0.0094 Mn 0.0409 0.020540 0.0409 0.0148 C 12.1593 12.1593 20.0535 O 48.6258 48.6258 60.2017 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 17 x= -12954.0 y= 2618.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 19.6 5.0 3.6 5.40 0.0204 5.1 0.0285 Mg 128.5 2.0 2.5 51.01 0.0699 2.0 0.0109 Sr 35.9 2.6 14.3 2.51 0.0031 2.7 0.0392 P 46.9 3.3 2.4 19.94 0.0567 3.3 0.0388 K 14.0 6.0 5.1 2.74 0.0081 6.0 0.0181 Cl 33.6 3.1 2.2 15.29 0.0069 3.1 0.0221 Ca 3943.3 0.4 17.7 223.40 0.8620 0.4 0.0328 Ba 12.1 4.6 10.8 1.12 0.0008 4.6 0.0739 Fe 4.3 7.6 3.3 1.31 0.0006 7.6 0.0549 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0618 Elt. k-ratio Correc. Na 0.0010 2.3259 Mg 0.0051 1.6952 Sr 0.0019 1.3725 P 0.0089 1.1930 K 0.0007 1.0129 Cl 0.0038 1.1104 Ca 0.3128 1.0883 Ba 0.0002 1.5398 Fe 0.0003 1.2492 Mn 0.0003 1.2729 iteration : 3 Analysis no. 17 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2368 0.016001 0.2368 0.2000 Mg 0.8580 0.017634 0.8580 0.6856 Sr 0.2597 0.013491 0.2597 0.0576 P 1.0601 0.037700 1.0601 0.6647 K 0.0726 0.008010 0.0726 0.0361 Cl 0.4244 0.014776 0.4244 0.2325 Ca 34.0452 0.151812 34.0452 16.4960 Ba 0.0337 0.019582 0.0337 0.0048 Fe 0.0339 0.014428 0.0339 0.0118 Mn 0.0392 0.020506 0.0392 0.0139 C 12.9190 12.9190 20.8881 O 50.0175 50.0175 60.7092 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 18 x= -12953.0 y= 2622.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 20.3 5.0 3.6 5.60 0.0213 5.0 0.0285 Mg 165.0 1.7 2.5 65.53 0.0903 1.8 0.0109 Sr 39.0 2.5 14.3 2.73 0.0035 2.5 0.0392 P 52.5 3.1 2.4 22.34 0.0639 3.1 0.0388 K 15.0 5.8 5.1 2.93 0.0090 5.8 0.0180 Cl 30.4 3.3 2.2 13.82 0.0062 3.3 0.0221 Ca 4155.4 0.3 17.7 235.42 0.9093 0.4 0.0328 Ba 13.3 4.3 10.8 1.24 0.0015 4.3 0.0740 Fe 4.2 7.7 3.3 1.27 0.0005 7.7 0.0548 Mn 3.9 11.3 2.7 1.44 0.0012 11.3 0.0617 Elt. k-ratio Correc. Na 0.0011 2.3202 Mg 0.0065 1.6919 Sr 0.0022 1.3714 P 0.0100 1.1917 K 0.0008 1.0075 Cl 0.0034 1.1079 Ca 0.3300 1.0855 Ba 0.0004 1.5402 Fe 0.0002 1.2464 Mn 0.0003 1.2706 iteration : 3 Analysis no. 18 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2467 0.016215 0.2467 0.2124 Mg 1.1056 0.019986 1.1056 0.9004 Sr 0.2973 0.013909 0.2973 0.0672 P 1.1944 0.039845 1.1944 0.7633 K 0.0804 0.008181 0.0804 0.0407 Cl 0.3801 0.014069 0.3801 0.2122 Ca 35.8203 0.157037 35.8203 17.6898 Ba 0.0662 0.020132 0.0662 0.0095 Fe 0.0289 0.014264 0.0289 0.0102 Mn 0.0428 0.020641 0.0428 0.0154 C 12.0267 12.0267 19.8192 O 48.7106 48.7106 60.2596 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 19 x= -12952.0 y= 2626.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 16.9 5.4 3.6 4.66 0.0170 5.5 0.0286 Mg 121.6 2.0 2.5 48.27 0.0661 2.1 0.0109 Sr 36.6 2.6 14.3 2.56 0.0032 2.6 0.0392 P 48.4 3.2 2.4 20.60 0.0587 3.2 0.0388 K 14.2 5.9 5.1 2.77 0.0083 6.0 0.0181 Cl 37.6 3.0 2.2 17.10 0.0077 3.0 0.0221 Ca 4026.2 0.4 17.7 228.10 0.8808 0.4 0.0328 Ba 11.1 4.8 10.8 1.03 0.0002 4.8 0.0740 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0549 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0618 Elt. k-ratio Correc. Na 0.0008 2.3255 Mg 0.0048 1.6938 Sr 0.0020 1.3707 P 0.0092 1.1915 K 0.0007 1.0107 Cl 0.0043 1.1089 Ca 0.3196 1.0875 Ba 0.0001 1.5405 Fe 0.0001 1.2485 Mn 0.0002 1.2723 iteration : 3 Analysis no. 19 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1968 0.015043 0.1968 0.1673 Mg 0.8108 0.017148 0.8108 0.6518 Sr 0.2685 0.013584 0.2685 0.0599 P 1.0964 0.038280 1.0964 0.6916 K 0.0741 0.008040 0.0741 0.0370 Cl 0.4776 0.015564 0.4776 0.2632 Ca 34.7600 0.153951 34.7600 16.9450 Ba 0.0078 0.019167 0.0078 0.0011 Fe 0.0173 0.013947 0.0173 0.0061 Mn 0.0285 0.020031 0.0285 0.0101 C 12.6623 12.6623 20.5978 O 49.5999 49.5999 60.5691 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 20 x= -12951.0 y= 2630.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 16.7 5.5 3.6 4.60 0.0167 5.5 0.0285 Mg 144.5 1.9 2.5 57.40 0.0789 1.9 0.0109 Sr 39.6 2.5 14.3 2.78 0.0036 2.5 0.0391 P 50.2 3.2 2.4 21.36 0.0610 3.2 0.0387 K 15.6 5.7 5.1 3.05 0.0095 5.7 0.0180 Cl 29.5 3.4 2.2 13.41 0.0060 3.4 0.0220 Ca 4291.7 0.3 17.7 243.14 0.9390 0.4 0.0327 Ba 12.1 4.5 10.8 1.12 0.0008 4.6 0.0740 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0547 Mn 4.4 10.6 2.7 1.62 0.0017 10.7 0.0617 Elt. k-ratio Correc. Na 0.0008 2.3231 Mg 0.0057 1.6919 Sr 0.0022 1.3691 P 0.0096 1.1897 K 0.0008 1.0028 Cl 0.0033 1.1049 Ca 0.3408 1.0840 Ba 0.0002 1.5411 Fe 0.0002 1.2455 Mn 0.0005 1.2699 iteration : 3 Analysis no. 20 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1937 0.014953 0.1937 0.1681 Mg 0.9661 0.018686 0.9661 0.7933 Sr 0.3046 0.013968 0.3046 0.0694 P 1.1374 0.038907 1.1374 0.7329 K 0.0849 0.008262 0.0849 0.0434 Cl 0.3669 0.013833 0.3669 0.2066 Ca 36.9412 0.160291 36.9412 18.3942 Ba 0.0344 0.019619 0.0344 0.0050 Fe 0.0206 0.014010 0.0206 0.0074 Mn 0.0607 0.021392 0.0607 0.0220 C 11.7222 11.7222 19.4773 O 48.1673 48.1673 60.0805 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 21 x= -12950.0 y= 2634.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 25.3 4.4 3.6 6.96 0.0276 4.5 0.0285 Mg 174.5 1.7 2.5 69.28 0.0955 1.7 0.0109 Sr 34.2 2.7 14.3 2.39 0.0028 2.7 0.0394 P 48.8 3.2 2.4 20.77 0.0592 3.2 0.0390 K 14.7 5.8 5.1 2.88 0.0088 5.8 0.0183 Cl 41.0 2.8 2.2 18.63 0.0085 2.9 0.0223 Ca 3612.1 0.4 17.7 204.64 0.7897 0.5 0.0330 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 4.1 7.8 3.3 1.25 0.0005 7.8 0.0550 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0619 Elt. k-ratio Correc. Na 0.0014 2.3198 Mg 0.0069 1.6942 Sr 0.0017 1.3776 P 0.0093 1.1975 K 0.0008 1.0247 Cl 0.0047 1.1172 Ca 0.2866 1.0925 Ba 0.0000 NaN Fe 0.0002 1.2521 Mn 0.0003 1.2751 iteration : 3 Analysis no. 21 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3199 0.017819 0.3199 0.2646 Mg 1.1714 0.020584 1.1714 0.9164 Sr 0.2402 0.013315 0.2402 0.0521 P 1.1114 0.038624 1.1114 0.6823 K 0.0797 0.008266 0.0797 0.0388 Cl 0.5269 0.016332 0.5269 0.2826 Ca 31.3121 0.143761 31.3121 14.8554 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0273 0.014279 0.0273 0.0093 Mn 0.0357 0.020395 0.0357 0.0124 C 13.7542 13.7542 21.7748 O 51.4211 51.4211 61.1114 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 22 x= -12949.0 y= 2639.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 23.7 4.6 3.6 6.52 0.0256 4.6 0.0286 Mg 138.3 1.9 2.5 54.91 0.0754 1.9 0.0109 Sr 37.1 2.6 14.3 2.60 0.0032 2.6 0.0393 P 41.0 3.5 2.4 17.45 0.0493 3.5 0.0389 K 14.6 5.8 5.1 2.86 0.0087 5.9 0.0182 Cl 35.4 3.1 2.2 16.08 0.0073 3.1 0.0222 Ca 3911.9 0.4 17.7 221.63 0.8558 0.4 0.0329 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0549 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0619 Elt. k-ratio Correc. Na 0.0013 2.3247 Mg 0.0055 1.6957 Sr 0.0020 1.3737 P 0.0077 1.1940 K 0.0008 1.0136 Cl 0.0040 1.1106 Ca 0.3106 1.0887 Ba 0.0000 NaN Fe 0.0002 1.2496 Mn 0.0004 1.2732 iteration : 3 Analysis no. 22 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2969 0.017356 0.2969 0.2502 Mg 0.9259 0.018319 0.9259 0.7379 Sr 0.2746 0.013676 0.2746 0.0607 P 0.9222 0.035400 0.9222 0.5767 K 0.0781 0.008158 0.0781 0.0387 Cl 0.4482 0.015145 0.4482 0.2449 Ca 33.8149 0.151180 33.8149 16.3425 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0207 0.014060 0.0207 0.0072 Mn 0.0447 0.020764 0.0447 0.0158 C 13.0416 13.0416 21.0325 O 50.1323 50.1323 60.6929 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 23 x= -12948.0 y= 2643.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 23.7 4.6 3.6 6.52 0.0256 4.6 0.0286 Mg 131.7 1.9 2.5 52.29 0.0717 2.0 0.0109 Sr 37.6 2.6 14.3 2.63 0.0033 2.6 0.0393 P 42.2 3.4 2.4 17.94 0.0507 3.5 0.0389 K 15.9 5.6 5.1 3.11 0.0098 5.6 0.0181 Cl 31.6 3.2 2.2 14.35 0.0064 3.3 0.0221 Ca 4021.5 0.4 17.7 227.83 0.8799 0.4 0.0328 Ba 11.1 4.7 10.8 1.03 0.0002 4.8 0.0740 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0549 Mn 4.7 10.4 2.7 1.72 0.0019 10.4 0.0618 Elt. k-ratio Correc. Na 0.0013 2.3253 Mg 0.0052 1.6957 Sr 0.0020 1.3723 P 0.0080 1.1927 K 0.0009 1.0100 Cl 0.0036 1.1087 Ca 0.3193 1.0873 Ba 0.0001 1.5402 Fe 0.0001 1.2485 Mn 0.0005 1.2724 iteration : 3 Analysis no. 23 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2970 0.017360 0.2970 0.2522 Mg 0.8808 0.017873 0.8808 0.7076 Sr 0.2806 0.013733 0.2806 0.0625 P 0.9487 0.035837 0.9487 0.5980 K 0.0880 0.008384 0.0880 0.0440 Cl 0.3962 0.014331 0.3962 0.2182 Ca 34.7208 0.153836 34.7208 16.9144 Ba 0.0084 0.019180 0.0084 0.0012 Fe 0.0083 0.013678 0.0083 0.0029 Mn 0.0698 0.021814 0.0698 0.0248 C 12.6982 12.6982 20.6423 O 49.6032 49.6032 60.5320 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 24 x= -12947.0 y= 2647.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 17.5 5.3 3.6 4.81 0.0177 5.4 0.0286 Mg 103.2 2.2 2.5 41.00 0.0560 2.2 0.0109 Sr 32.7 2.8 14.3 2.29 0.0026 2.8 0.0393 P 39.3 3.6 2.4 16.70 0.0470 3.6 0.0389 K 16.1 5.6 5.1 3.15 0.0100 5.6 0.0182 Cl 35.1 3.1 2.2 15.94 0.0072 3.1 0.0222 Ca 3720.5 0.4 17.7 210.78 0.8137 0.5 0.0329 Ba 10.6 4.8 10.8 0.99 0.0000 4.9 0.0000 Fe 3.6 8.4 3.3 1.08 0.0002 8.4 0.0551 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0620 Elt. k-ratio Correc. Na 0.0009 2.3309 Mg 0.0041 1.6978 Sr 0.0016 1.3742 P 0.0074 1.1946 K 0.0009 1.0185 Cl 0.0040 1.1131 Ca 0.2953 1.0912 Ba 0.0000 NaN Fe 0.0001 1.2522 Mn 0.0004 1.2753 iteration : 3 Analysis no. 24 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2055 0.015283 0.2055 0.1703 Mg 0.6878 0.015845 0.6878 0.5391 Sr 0.2225 0.013087 0.2225 0.0484 P 0.8810 0.034684 0.8810 0.5418 K 0.0904 0.008495 0.0904 0.0441 Cl 0.4452 0.015118 0.4452 0.2392 Ca 32.2255 0.146492 32.2255 15.3166 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0091 0.013743 0.0091 0.0031 Mn 0.0466 0.020876 0.0466 0.0161 C 13.8325 13.8325 21.9386 O 51.3539 51.3539 61.1427 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 25 x= -12947.0 y= 2651.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 39.1 3.6 3.6 10.77 0.0453 3.6 0.0284 Mg 178.1 1.7 2.5 70.74 0.0976 1.7 0.0109 Sr 42.9 2.4 14.3 3.00 0.0041 2.4 0.0393 P 39.7 3.5 2.4 16.87 0.0475 3.6 0.0389 K 18.1 5.3 5.1 3.54 0.0118 5.3 0.0180 Cl 38.6 2.9 2.2 17.55 0.0080 2.9 0.0221 Ca 4226.4 0.3 17.7 239.44 0.9250 0.4 0.0327 Ba 12.2 4.5 10.8 1.13 0.0008 4.5 0.0740 Fe 3.8 8.1 3.3 1.15 0.0003 8.1 0.0548 Mn 5.0 10.0 2.7 1.85 0.0023 10.0 0.0617 Elt. k-ratio Correc. Na 0.0023 2.3159 Mg 0.0071 1.6944 Sr 0.0025 1.3726 P 0.0075 1.1925 K 0.0010 1.0055 Cl 0.0044 1.1058 Ca 0.3357 1.0845 Ba 0.0002 1.5402 Fe 0.0001 1.2454 Mn 0.0006 1.2698 iteration : 3 Analysis no. 25 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5233 0.021679 0.5233 0.4534 Mg 1.1968 0.020813 1.1968 0.9808 Sr 0.3443 0.014427 0.3443 0.0783 P 0.8890 0.034794 0.8890 0.5716 K 0.1056 0.008776 0.1056 0.0538 Cl 0.4899 0.015720 0.4899 0.2752 Ca 36.4074 0.158748 36.4074 18.0918 Ba 0.0364 0.019647 0.0364 0.0053 Fe 0.0165 0.013892 0.0165 0.0059 Mn 0.0822 0.022283 0.0822 0.0298 C 11.8033 11.8033 19.5725 O 48.1053 48.1053 59.8818 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 26 x= -12946.0 y= 2655.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 14.9 5.8 3.6 4.09 0.0143 5.8 0.0287 Mg 83.2 2.4 2.5 33.05 0.0448 2.5 0.0110 Sr 32.2 2.8 14.3 2.25 0.0025 2.8 0.0393 P 31.5 4.0 2.4 13.41 0.0372 4.0 0.0390 K 15.2 5.7 5.1 2.97 0.0092 5.8 0.0183 Cl 35.4 3.1 2.2 16.10 0.0073 3.1 0.0222 Ca 3561.5 0.4 17.7 201.77 0.7789 0.5 0.0330 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0740 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0552 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0621 Elt. k-ratio Correc. Na 0.0007 2.3357 Mg 0.0032 1.7002 Sr 0.0016 1.3755 P 0.0058 1.1961 K 0.0008 1.0224 Cl 0.0040 1.1149 Ca 0.2827 1.0931 Ba 0.0000 1.5392 Fe 0.0001 1.2542 Mn 0.0003 1.2770 iteration : 3 Analysis no. 26 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1672 0.014335 0.1672 0.1366 Mg 0.5519 0.014262 0.5519 0.4266 Sr 0.2158 0.013019 0.2158 0.0463 P 0.6968 0.031274 0.6968 0.4226 K 0.0833 0.008344 0.0833 0.0400 Cl 0.4504 0.015212 0.4504 0.2387 Ca 30.8987 0.142543 30.8987 14.4823 Ba 0.0039 0.019091 0.0039 0.0005 Fe 0.0149 0.013941 0.0149 0.0050 Mn 0.0394 0.020591 0.0394 0.0135 C 14.5325 14.5325 22.7294 O 52.3450 52.3450 61.4585 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 27 x= -12945.0 y= 2660.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 52.2 3.1 3.6 14.38 0.0620 3.1 0.0284 Mg 182.8 1.7 2.5 72.60 0.1002 1.7 0.0109 Sr 41.2 2.5 14.3 2.89 0.0038 2.5 0.0394 P 34.5 3.8 2.4 14.68 0.0410 3.8 0.0390 K 17.1 5.4 5.1 3.34 0.0109 5.4 0.0182 Cl 42.5 2.8 2.2 19.32 0.0088 2.8 0.0222 Ca 3934.2 0.4 17.7 222.89 0.8608 0.4 0.0328 Ba 10.3 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0549 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0618 Elt. k-ratio Correc. Na 0.0031 2.3137 Mg 0.0073 1.6976 Sr 0.0024 1.3767 P 0.0064 1.1962 K 0.0010 1.0142 Cl 0.0049 1.1107 Ca 0.3124 1.0883 Ba 0.0000 NaN Fe 0.0001 1.2485 Mn 0.0003 1.2722 iteration : 3 Analysis no. 27 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7162 0.024812 0.7162 0.6069 Mg 1.2312 0.021131 1.2312 0.9868 Sr 0.3257 0.014260 0.3257 0.0724 P 0.7686 0.032656 0.7686 0.4834 K 0.0983 0.008658 0.0983 0.0490 Cl 0.5448 0.016530 0.5448 0.2993 Ca 33.9962 0.151708 33.9962 16.5236 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0157 0.013902 0.0157 0.0055 Mn 0.0392 0.020513 0.0392 0.0139 C 12.7361 12.7361 20.6567 O 49.5280 49.5280 60.3025 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 28 x= -12944.0 y= 2664.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 26.4 4.3 3.6 7.28 0.0291 4.4 0.0286 Mg 92.2 2.3 2.5 36.63 0.0498 2.3 0.0110 Sr 37.3 2.6 14.3 2.61 0.0033 2.6 0.0393 P 29.2 4.1 2.4 12.43 0.0342 4.1 0.0389 K 16.9 5.4 5.1 3.31 0.0108 5.4 0.0182 Cl 41.1 2.8 2.2 18.70 0.0085 2.8 0.0221 Ca 3850.9 0.4 17.7 218.17 0.8425 0.4 0.0329 Ba 12.7 4.4 10.8 1.18 0.0012 4.5 0.0740 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0550 Mn 4.2 10.9 2.7 1.55 0.0015 10.9 0.0619 Elt. k-ratio Correc. Na 0.0015 2.3304 Mg 0.0036 1.7000 Sr 0.0020 1.3733 P 0.0054 1.1938 K 0.0010 1.0141 Cl 0.0047 1.1098 Ca 0.3057 1.0893 Ba 0.0003 1.5397 Fe 0.0001 1.2505 Mn 0.0004 1.2740 iteration : 3 Analysis no. 28 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3385 0.018263 0.3385 0.2832 Mg 0.6134 0.015003 0.6134 0.4854 Sr 0.2773 0.013704 0.2773 0.0609 P 0.6406 0.030120 0.6406 0.3978 K 0.0970 0.008628 0.0970 0.0477 Cl 0.5258 0.016261 0.5258 0.2853 Ca 33.3034 0.149667 33.3034 15.9810 Ba 0.0493 0.019854 0.0493 0.0069 Fe 0.0108 0.013776 0.0108 0.0037 Mn 0.0537 0.021164 0.0537 0.0188 C 13.5009 13.5009 21.6185 O 50.5892 50.5892 60.8109 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 29 x= -12943.0 y= 2668.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 32.3 3.9 3.6 8.91 0.0366 3.9 0.0285 Mg 137.0 1.9 2.5 54.41 0.0747 1.9 0.0109 Sr 39.4 2.5 14.3 2.76 0.0036 2.5 0.0392 P 37.6 3.6 2.4 15.98 0.0449 3.7 0.0388 K 19.6 5.0 5.1 3.84 0.0133 5.1 0.0180 Cl 41.8 2.8 2.2 19.01 0.0087 2.8 0.0220 Ca 4256.0 0.3 17.7 241.12 0.9316 0.4 0.0327 Ba 12.5 4.5 10.8 1.16 0.0010 4.5 0.0741 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0548 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0617 Elt. k-ratio Correc. Na 0.0018 2.3211 Mg 0.0054 1.6954 Sr 0.0022 1.3704 P 0.0070 1.1905 K 0.0012 1.0037 Cl 0.0048 1.1042 Ca 0.3381 1.0844 Ba 0.0003 1.5409 Fe 0.0000 1.2458 Mn 0.0004 1.2701 iteration : 3 Analysis no. 29 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4246 0.019917 0.4246 0.3675 Mg 0.9173 0.018235 0.9173 0.7511 Sr 0.3017 0.013951 0.3017 0.0685 P 0.8376 0.033842 0.8376 0.5381 K 0.1180 0.009051 0.1180 0.0601 Cl 0.5322 0.016304 0.5322 0.2987 Ca 36.6612 0.159499 36.6612 18.2033 Ba 0.0442 0.019787 0.0442 0.0064 Fe 0.0058 0.013575 0.0058 0.0021 Mn 0.0482 0.020871 0.0482 0.0174 C 11.9155 11.9155 19.7427 O 48.1939 48.1939 59.9440 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 30 x= -12942.0 y= 2672.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 18.6 5.2 3.6 5.11 0.0191 5.2 0.0286 Mg 112.9 2.1 2.5 44.83 0.0613 2.1 0.0110 Sr 24.4 3.2 14.3 1.71 0.0014 3.2 0.0395 P 35.0 3.8 2.4 14.90 0.0416 3.8 0.0391 K 14.5 5.9 5.1 2.83 0.0085 5.9 0.0186 Cl 42.8 2.8 2.2 19.45 0.0089 2.8 0.0224 Ca 3169.7 0.4 17.7 179.58 0.6928 0.5 0.0331 Ba 10.0 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0553 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0622 Elt. k-ratio Correc. Na 0.0010 2.3321 Mg 0.0044 1.7004 Sr 0.0009 1.3808 P 0.0065 1.2004 K 0.0008 1.0364 Cl 0.0049 1.1226 Ca 0.2514 1.0983 Ba 0.0000 NaN Fe 0.0001 1.2582 Mn 0.0001 1.2801 iteration : 2 Analysis no. 30 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2220 0.015689 0.2220 0.1767 Mg 0.7550 0.016594 0.7550 0.5684 Sr 0.1221 0.011914 0.1221 0.0255 P 0.7833 0.032995 0.7833 0.4628 K 0.0786 0.008310 0.0786 0.0368 Cl 0.5542 0.016758 0.5542 0.2861 Ca 27.6120 0.132632 27.6120 12.6071 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0117 0.013885 0.0117 0.0038 Mn 0.0142 0.019499 0.0142 0.0047 C 15.6426 15.6426 23.8327 O 54.2044 54.2044 61.9955 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 31 x= -12941.0 y= 2676.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 17.4 5.4 3.6 4.80 0.0176 5.4 0.0286 Mg 106.7 2.2 2.5 42.39 0.0579 2.2 0.0109 Sr 36.2 2.6 14.3 2.53 0.0031 2.6 0.0393 P 35.7 3.7 2.4 15.17 0.0424 3.8 0.0389 K 16.7 5.5 5.1 3.26 0.0106 5.5 0.0182 Cl 39.3 2.9 2.2 17.85 0.0081 2.9 0.0221 Ca 3878.7 0.4 17.7 219.74 0.8486 0.4 0.0329 Ba 13.0 4.4 10.8 1.21 0.0014 4.4 0.0740 Fe 4.0 7.9 3.3 1.21 0.0004 7.9 0.0550 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0619 Elt. k-ratio Correc. Na 0.0009 2.3299 Mg 0.0042 1.6971 Sr 0.0019 1.3728 P 0.0067 1.1933 K 0.0009 1.0138 Cl 0.0045 1.1100 Ca 0.3080 1.0890 Ba 0.0004 1.5398 Fe 0.0002 1.2502 Mn 0.0003 1.2737 iteration : 3 Analysis no. 31 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2047 0.015260 0.2047 0.1717 Mg 0.7115 0.016106 0.7115 0.5646 Sr 0.2636 0.013546 0.2636 0.0580 P 0.7942 0.033089 0.7942 0.4946 K 0.0949 0.008576 0.0949 0.0468 Cl 0.5007 0.015908 0.5007 0.2724 Ca 33.5367 0.150359 33.5367 16.1396 Ba 0.0591 0.020014 0.0591 0.0083 Fe 0.0232 0.014141 0.0232 0.0080 Mn 0.0339 0.020299 0.0339 0.0119 C 13.3307 13.3307 21.4080 O 50.4469 50.4469 60.8160 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 32 x= -12940.0 y= 2680.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 22.9 4.7 3.6 6.30 0.0246 4.7 0.0286 Mg 136.0 1.9 2.5 54.00 0.0742 1.9 0.0109 Sr 32.6 2.8 14.3 2.28 0.0026 2.8 0.0393 P 41.2 3.5 2.4 17.53 0.0495 3.5 0.0389 K 17.6 5.3 5.1 3.44 0.0114 5.3 0.0182 Cl 39.6 2.9 2.2 18.02 0.0082 2.9 0.0222 Ca 3790.8 0.4 17.7 214.76 0.8294 0.5 0.0329 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 4.3 7.7 3.3 1.29 0.0005 7.7 0.0550 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0620 Elt. k-ratio Correc. Na 0.0012 2.3253 Mg 0.0054 1.6961 Sr 0.0016 1.3747 P 0.0078 1.1946 K 0.0010 1.0175 Cl 0.0046 1.1125 Ca 0.3010 1.0904 Ba 0.0000 NaN Fe 0.0003 1.2510 Mn 0.0001 1.2743 iteration : 3 Analysis no. 32 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2852 0.017106 0.2852 0.2381 Mg 0.9106 0.018173 0.9106 0.7192 Sr 0.2211 0.013077 0.2211 0.0485 P 0.9277 0.035511 0.9277 0.5750 K 0.1027 0.008785 0.1027 0.0504 Cl 0.5069 0.016016 0.5069 0.2745 Ca 32.8194 0.148263 32.8194 15.7202 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0315 0.014392 0.0315 0.0108 Mn 0.0177 0.019580 0.0177 0.0062 C 13.4320 13.4320 21.4692 O 50.7452 50.7452 60.8879 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 33 x= -12939.0 y= 2685.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 12.2 6.4 3.6 3.36 0.0110 6.4 0.0287 Mg 81.3 2.5 2.5 32.30 0.0438 2.5 0.0110 Sr 35.3 2.7 14.3 2.47 0.0030 2.7 0.0394 P 44.1 3.4 2.4 18.77 0.0532 3.4 0.0391 K 14.3 5.9 5.1 2.80 0.0084 5.9 0.0186 Cl 39.3 2.9 2.2 17.85 0.0081 2.9 0.0224 Ca 3185.7 0.4 17.7 180.48 0.6964 0.5 0.0331 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0622 Elt. k-ratio Correc. Na 0.0005 2.3330 Mg 0.0032 1.6988 Sr 0.0018 1.3777 P 0.0083 1.1997 K 0.0007 1.0365 Cl 0.0045 1.1233 Ca 0.2527 1.0980 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2796 iteration : 2 Analysis no. 33 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1276 0.013250 0.1276 0.1018 Mg 0.5386 0.014092 0.5386 0.4064 Sr 0.2537 0.013475 0.2537 0.0531 P 1.0013 0.036855 1.0013 0.5928 K 0.0773 0.008281 0.0773 0.0363 Cl 0.5068 0.016102 0.5068 0.2622 Ca 27.7505 0.133060 27.7505 12.6980 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0196 0.019744 0.0196 0.0065 C 15.5562 15.5562 23.7529 O 54.1685 54.1685 62.0899 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 34 x= -12939.0 y= 2689.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 32.8 3.9 3.6 9.03 0.0372 3.9 0.0283 Mg 193.1 1.6 2.5 76.68 0.1059 1.6 0.0109 Sr 43.3 2.4 14.3 3.03 0.0041 2.4 0.0393 P 74.2 2.6 2.4 31.58 0.0916 2.6 0.0390 K 15.1 5.8 5.1 2.95 0.0091 5.8 0.0184 Cl 62.4 2.3 2.2 28.35 0.0132 2.3 0.0223 Ca 3643.7 0.4 17.7 206.43 0.7970 0.5 0.0330 Ba 11.8 4.6 10.8 1.10 0.0006 4.6 0.0739 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0550 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0619 Elt. k-ratio Correc. Na 0.0019 2.3062 Mg 0.0077 1.6885 Sr 0.0025 1.3748 P 0.0144 1.1966 K 0.0008 1.0286 Cl 0.0073 1.1196 Ca 0.2893 1.0922 Ba 0.0002 1.5372 Fe 0.0001 1.2497 Mn 0.0003 1.2729 iteration : 3 Analysis no. 34 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4285 0.019915 0.4285 0.3588 Mg 1.2945 0.021615 1.2945 1.0254 Sr 0.3503 0.014509 0.3503 0.0770 P 1.7187 0.047502 1.7187 1.0682 K 0.0830 0.008375 0.0830 0.0409 Cl 0.8196 0.020047 0.8196 0.4450 Ca 31.5915 0.144619 31.5915 15.1745 Ba 0.0266 0.019450 0.0266 0.0037 Fe 0.0157 0.013917 0.0157 0.0054 Mn 0.0393 0.020527 0.0393 0.0138 C 13.0683 13.0683 20.9465 O 50.5640 50.5640 60.8408 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 35 x= -12938.0 y= 2693.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 21.6 4.8 3.6 5.94 0.0229 4.8 0.0285 Mg 109.5 2.1 2.5 43.50 0.0595 2.2 0.0109 Sr 23.2 3.3 14.3 1.62 0.0013 3.3 0.0396 P 80.9 2.5 2.4 34.43 0.1002 2.5 0.0393 K 14.0 6.0 5.1 2.74 0.0081 6.0 0.0191 Cl 43.1 2.8 2.2 19.60 0.0089 2.8 0.0228 Ca 2422.1 0.5 17.7 137.22 0.5285 0.5 0.0334 Ba 7.0 6.0 10.8 0.65 0.0000 6.0 0.0000 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 2.9 13.1 2.7 1.07 0.0002 13.1 0.0625 Elt. k-ratio Correc. Na 0.0011 2.3229 Mg 0.0043 1.6979 Sr 0.0008 1.3849 P 0.0157 1.2067 K 0.0007 1.0667 Cl 0.0050 1.1418 Ca 0.1918 1.1082 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2848 iteration : 2 Analysis no. 35 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2656 0.016660 0.2656 0.2025 Mg 0.7310 0.016324 0.7310 0.5271 Sr 0.1082 0.011767 0.1082 0.0216 P 1.8950 0.050032 1.8950 1.0721 K 0.0765 0.008445 0.0765 0.0343 Cl 0.5684 0.017109 0.5684 0.2809 Ca 21.2555 0.112739 21.2555 9.2933 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0070 0.019233 0.0070 0.0022 C 17.3783 17.3783 25.3545 O 57.7146 57.7146 63.2114 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 36 x= -12937.0 y= 2697.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 18.6 5.2 3.6 5.11 0.0191 5.2 0.0285 Mg 94.8 2.3 2.5 37.64 0.0513 2.3 0.0109 Sr 25.0 3.2 14.3 1.75 0.0015 3.2 0.0395 P 93.8 2.3 2.4 39.93 0.1166 2.3 0.0392 K 12.7 6.3 5.1 2.48 0.0069 6.3 0.0190 Cl 42.0 2.8 2.2 19.08 0.0087 2.8 0.0227 Ca 2575.9 0.4 17.7 145.94 0.5624 0.5 0.0334 Ba 7.0 6.0 10.8 0.65 0.0000 6.0 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0555 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0624 Elt. k-ratio Correc. Na 0.0010 2.3222 Mg 0.0037 1.6960 Sr 0.0009 1.3814 P 0.0183 1.2040 K 0.0006 1.0621 Cl 0.0048 1.1398 Ca 0.2041 1.1061 Ba 0.0000 NaN Fe 0.0001 1.2623 Mn 0.0002 1.2831 iteration : 2 Analysis no. 36 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2211 0.015625 0.2211 0.1706 Mg 0.6296 0.015175 0.6296 0.4596 Sr 0.1294 0.012014 0.1294 0.0262 P 2.2014 0.053802 2.2014 1.2611 K 0.0650 0.008115 0.0650 0.0295 Cl 0.5517 0.016864 0.5517 0.2761 Ca 22.5744 0.116967 22.5744 9.9939 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0109 0.013908 0.0109 0.0035 Mn 0.0305 0.020291 0.0305 0.0099 C 16.7337 16.7337 24.7206 O 56.8524 56.8524 63.0490 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 37 x= -12936.0 y= 2701.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 36.8 3.7 3.6 10.15 0.0424 3.7 0.0283 Mg 189.6 1.6 2.5 75.29 0.1040 1.7 0.0109 Sr 46.2 2.3 14.3 3.24 0.0045 2.3 0.0395 P 95.7 2.3 2.4 40.71 0.1190 2.3 0.0392 K 14.8 5.8 5.1 2.90 0.0089 5.8 0.0188 Cl 48.6 2.6 2.2 22.07 0.0101 2.6 0.0226 Ca 3031.3 0.4 17.7 171.74 0.6625 0.5 0.0332 Ba 10.7 4.8 10.8 0.99 0.0000 4.8 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0552 Mn 3.9 11.3 2.7 1.44 0.0012 11.3 0.0621 Elt. k-ratio Correc. Na 0.0021 2.3032 Mg 0.0075 1.6894 Sr 0.0028 1.3798 P 0.0187 1.2032 K 0.0008 1.0493 Cl 0.0056 1.1334 Ca 0.2404 1.0999 Ba 0.0000 NaN Fe 0.0000 1.2553 Mn 0.0003 1.2773 iteration : 3 Analysis no. 37 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4875 0.020982 0.4875 0.3918 Mg 1.2715 0.021427 1.2715 0.9667 Sr 0.3868 0.014930 0.3868 0.0816 P 2.2445 0.054305 2.2445 1.3390 K 0.0825 0.008491 0.0825 0.0390 Cl 0.6393 0.017981 0.6393 0.3332 Ca 26.4430 0.129052 26.4430 12.1912 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0058 0.013681 0.0058 0.0019 Mn 0.0430 0.020756 0.0430 0.0145 C 14.7309 14.7309 22.6629 O 53.6651 53.6651 61.9781 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 38 x= -12935.0 y= 2706.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 20.6 4.9 3.6 5.68 0.0217 4.9 0.0286 Mg 85.5 2.4 2.5 33.94 0.0461 2.4 0.0110 Sr 20.5 3.5 14.3 1.44 0.0009 3.5 0.0397 P 78.5 2.5 2.4 33.41 0.0971 2.5 0.0394 K 13.2 6.2 5.1 2.58 0.0074 6.2 0.0192 Cl 46.4 2.7 2.2 21.10 0.0097 2.7 0.0228 Ca 2227.1 0.5 17.7 126.18 0.4857 0.5 0.0335 Ba 6.5 6.2 10.8 0.60 0.0000 6.2 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 2.5 14.3 2.7 0.90 0.0000 14.3 0.0000 Elt. k-ratio Correc. Na 0.0011 2.3263 Mg 0.0033 1.7000 Sr 0.0005 1.3861 P 0.0152 1.2081 K 0.0007 1.0736 Cl 0.0054 1.1450 Ca 0.1763 1.1108 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 38 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2519 0.016364 0.2519 0.1892 Mg 0.5674 0.014451 0.5674 0.4031 Sr 0.0760 0.011351 0.0760 0.0150 P 1.8392 0.049337 1.8392 1.0253 K 0.0701 0.008318 0.0701 0.0309 Cl 0.6160 0.017775 0.6160 0.3000 Ca 19.5783 0.107278 19.5783 8.4348 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 18.1376 18.1376 26.0752 O 58.8636 58.8635 63.5265 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 39 x= -12934.0 y= 2710.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 36.2 3.7 3.6 9.98 0.0416 3.7 0.0284 Mg 168.9 1.7 2.5 67.08 0.0925 1.7 0.0109 Sr 40.8 2.5 14.3 2.86 0.0038 2.5 0.0396 P 82.2 2.5 2.4 34.99 0.1018 2.5 0.0394 K 12.9 6.2 5.1 2.52 0.0071 6.2 0.0191 Cl 58.8 2.4 2.2 26.71 0.0124 2.4 0.0228 Ca 2510.9 0.4 17.7 142.25 0.5481 0.5 0.0334 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 2.9 9.3 3.3 0.88 0.0000 9.3 0.0000 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0623 Elt. k-ratio Correc. Na 0.0021 2.3082 Mg 0.0067 1.6937 Sr 0.0023 1.3854 P 0.0160 1.2085 K 0.0006 1.0662 Cl 0.0069 1.1416 Ca 0.1989 1.1067 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2823 iteration : 2 Analysis no. 39 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4797 0.020869 0.4797 0.3705 Mg 1.1338 0.020253 1.1338 0.8283 Sr 0.3223 0.014294 0.3223 0.0653 P 1.9293 0.050514 1.9293 1.1060 K 0.0670 0.008193 0.0670 0.0304 Cl 0.7857 0.019860 0.7857 0.3935 Ca 22.0131 0.115166 22.0131 9.7520 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0106 0.019367 0.0106 0.0034 C 16.6933 16.6933 24.6776 O 56.5652 56.5652 62.7729 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 40 x= -12933.0 y= 2714.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 25.4 4.4 3.6 7.00 0.0278 4.5 0.0285 Mg 98.3 2.3 2.5 39.03 0.0532 2.3 0.0110 Sr 24.8 3.2 14.3 1.73 0.0015 3.2 0.0396 P 86.0 2.4 2.4 36.60 0.1067 2.4 0.0394 K 14.2 5.9 5.1 2.78 0.0083 5.9 0.0192 Cl 50.3 2.6 2.2 22.86 0.0105 2.6 0.0228 Ca 2333.5 0.5 17.7 132.20 0.5092 0.5 0.0335 Ba 8.0 5.6 10.8 0.74 0.0000 5.6 0.0000 Fe 3.3 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 2.7 13.6 2.7 1.00 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0014 2.3207 Mg 0.0039 1.6980 Sr 0.0009 1.3847 P 0.0167 1.2072 K 0.0007 1.0708 Cl 0.0059 1.1439 Ca 0.1848 1.1094 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 40 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3224 0.017886 0.3224 0.2447 Mg 0.6543 0.015470 0.6543 0.4697 Sr 0.1273 0.012014 0.1273 0.0254 P 2.0191 0.051628 2.0191 1.1373 K 0.0790 0.008534 0.0790 0.0353 Cl 0.6694 0.018458 0.6694 0.3294 Ca 20.4989 0.110298 20.4989 8.9233 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.5774 17.5774 25.5327 O 58.0520 58.0520 63.3023 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 41 x= -12932.0 y= 2718.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 24.3 4.5 3.6 6.69 0.0264 4.6 0.0286 Mg 97.8 2.3 2.5 38.83 0.0529 2.3 0.0110 Sr 32.6 2.8 14.3 2.28 0.0026 2.8 0.0397 P 62.5 2.8 2.4 26.60 0.0767 2.8 0.0394 K 11.8 6.5 5.1 2.31 0.0061 6.5 0.0191 Cl 46.0 2.7 2.2 20.89 0.0096 2.7 0.0228 Ca 2379.6 0.5 17.7 134.82 0.5193 0.5 0.0335 Ba 8.9 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 2.7 9.7 3.3 0.81 0.0000 9.7 0.0000 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0625 Elt. k-ratio Correc. Na 0.0013 2.3257 Mg 0.0038 1.7004 Sr 0.0016 1.3860 P 0.0120 1.2086 K 0.0005 1.0672 Cl 0.0053 1.1412 Ca 0.1885 1.1084 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2853 iteration : 2 Analysis no. 41 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3061 0.017562 0.3061 0.2321 Mg 0.6518 0.015454 0.6518 0.4676 Sr 0.2230 0.013187 0.2230 0.0444 P 1.4535 0.044056 1.4535 0.8181 K 0.0580 0.007958 0.0580 0.0259 Cl 0.6076 0.017634 0.6076 0.2988 Ca 20.8892 0.111552 20.8892 9.0863 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0124 0.019500 0.0124 0.0039 C 17.7740 17.7740 25.7987 O 58.0244 58.0244 63.2244 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 42 x= -12931.0 y= 2722.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 36.3 3.7 3.6 10.01 0.0418 3.7 0.0285 Mg 132.8 1.9 2.5 52.72 0.0724 2.0 0.0109 Sr 37.7 2.6 14.3 2.64 0.0033 2.6 0.0395 P 52.9 3.1 2.4 22.49 0.0644 3.1 0.0391 K 17.0 5.4 5.1 3.33 0.0109 5.4 0.0186 Cl 50.2 2.6 2.2 22.81 0.0105 2.6 0.0224 Ca 3286.2 0.4 17.7 186.18 0.7186 0.5 0.0331 Ba 11.0 4.8 10.8 1.02 0.0001 4.8 0.0739 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0552 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0621 Elt. k-ratio Correc. Na 0.0021 2.3190 Mg 0.0052 1.6977 Sr 0.0021 1.3788 P 0.0101 1.2001 K 0.0010 1.0361 Cl 0.0058 1.1232 Ca 0.2608 1.0966 Ba 0.0000 1.5367 Fe 0.0001 1.2549 Mn 0.0003 1.2773 iteration : 3 Analysis no. 42 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4835 0.020995 0.4835 0.3913 Mg 0.8897 0.017975 0.8897 0.6811 Sr 0.2836 0.013820 0.2836 0.0602 P 1.2117 0.040272 1.2117 0.7279 K 0.1000 0.008837 0.1000 0.0476 Cl 0.6559 0.018107 0.6559 0.3443 Ca 28.5957 0.135626 28.5957 13.2759 Ba 0.0058 0.019098 0.0058 0.0008 Fe 0.0183 0.014052 0.0183 0.0061 Mn 0.0376 0.020521 0.0376 0.0127 C 14.7489 14.7489 22.8493 O 52.9694 52.9694 61.6027 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 43 x= -12931.0 y= 2726.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 19.2 5.1 3.6 5.28 0.0198 5.1 0.0288 Mg 60.5 2.9 2.5 24.03 0.0322 2.9 0.0110 Sr 29.0 2.9 14.3 2.03 0.0021 2.9 0.0395 P 27.2 4.3 2.4 11.55 0.0316 4.3 0.0392 K 14.5 5.9 5.1 2.83 0.0085 5.9 0.0186 Cl 35.6 3.1 2.2 16.17 0.0073 3.1 0.0224 Ca 3063.4 0.4 17.7 173.56 0.6697 0.5 0.0332 Ba 9.0 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.0 9.2 3.3 0.90 0.0000 9.2 0.0000 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0623 Elt. k-ratio Correc. Na 0.0010 2.3394 Mg 0.0023 1.7048 Sr 0.0013 1.3805 P 0.0050 1.2012 K 0.0008 1.0381 Cl 0.0041 1.1235 Ca 0.2430 1.0994 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2814 iteration : 3 Analysis no. 43 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2317 0.015957 0.2317 0.1825 Mg 0.3979 0.012240 0.3979 0.2963 Sr 0.1785 0.012617 0.1785 0.0369 P 0.5956 0.029305 0.5956 0.3481 K 0.0787 0.008328 0.0787 0.0365 Cl 0.4564 0.015369 0.4564 0.2330 Ca 26.7193 0.129909 26.7193 12.0687 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0395 0.020670 0.0395 0.0130 C 16.2564 16.2564 24.5023 O 55.0459 55.0459 62.2827 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 44 x= -12930.0 y= 2731.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 29.6 4.1 3.6 8.16 0.0332 4.1 0.0286 Mg 120.2 2.0 2.5 47.74 0.0654 2.1 0.0110 Sr 34.7 2.7 14.3 2.43 0.0029 2.7 0.0394 P 24.5 4.5 2.4 10.40 0.0282 4.5 0.0390 K 16.8 5.5 5.1 3.28 0.0107 5.5 0.0184 Cl 52.5 2.5 2.2 23.84 0.0110 2.5 0.0223 Ca 3535.2 0.4 17.7 200.28 0.7733 0.5 0.0330 Ba 10.2 4.9 10.8 0.95 0.0000 5.0 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 4.2 11.0 2.7 1.53 0.0014 11.0 0.0621 Elt. k-ratio Correc. Na 0.0017 2.3276 Mg 0.0047 1.7000 Sr 0.0018 1.3777 P 0.0044 1.1977 K 0.0009 1.0248 Cl 0.0061 1.1153 Ca 0.2807 1.0934 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0004 1.2766 iteration : 3 Analysis no. 44 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3858 0.019205 0.3858 0.3157 Mg 0.8050 0.017125 0.8050 0.6231 Sr 0.2465 0.013395 0.2465 0.0529 P 0.5292 0.027832 0.5292 0.3214 K 0.0968 0.008692 0.0968 0.0466 Cl 0.6821 0.018367 0.6821 0.3620 Ca 30.6884 0.141931 30.6884 14.4047 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0520 0.021137 0.0520 0.0178 C 14.4614 14.4614 22.6511 O 52.0527 52.0527 61.2046 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 45 x= -12929.0 y= 2735.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 20.7 4.9 3.6 5.71 0.0218 4.9 0.0287 Mg 69.3 2.7 2.5 27.51 0.0371 2.7 0.0110 Sr 23.1 3.3 14.3 1.61 0.0012 3.3 0.0396 P 27.3 4.3 2.4 11.60 0.0317 4.3 0.0392 K 14.3 5.9 5.1 2.80 0.0084 5.9 0.0188 Cl 56.8 2.4 2.2 25.80 0.0119 2.4 0.0225 Ca 2789.3 0.4 17.7 158.03 0.6092 0.5 0.0333 Ba 9.2 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.0 9.2 3.3 0.89 0.0000 9.2 0.0000 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0624 Elt. k-ratio Correc. Na 0.0011 2.3365 Mg 0.0027 1.7044 Sr 0.0008 1.3831 P 0.0050 1.2033 K 0.0007 1.0492 Cl 0.0066 1.1284 Ca 0.2211 1.1033 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2836 iteration : 2 Analysis no. 45 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2545 0.016470 0.2545 0.1969 Mg 0.4577 0.013066 0.4577 0.3350 Sr 0.1065 0.011732 0.1065 0.0216 P 0.5989 0.029398 0.5989 0.3439 K 0.0783 0.008382 0.0783 0.0356 Cl 0.7491 0.019303 0.7491 0.3758 Ca 24.3937 0.122703 24.3937 10.8262 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0015 0.018956 0.0015 0.0005 C 17.0819 17.0819 25.2977 O 56.2779 56.2779 62.5668 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 46 x= -12928.0 y= 2739.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 26.9 4.3 3.6 7.42 0.0297 4.3 0.0287 Mg 89.4 2.4 2.5 35.51 0.0483 2.4 0.0110 Sr 28.3 3.0 14.3 1.98 0.0020 3.0 0.0396 P 25.1 4.5 2.4 10.68 0.0290 4.5 0.0392 K 14.0 6.0 5.1 2.74 0.0081 6.0 0.0187 Cl 64.2 2.3 2.2 29.20 0.0136 2.3 0.0225 Ca 2903.1 0.4 17.7 164.47 0.6343 0.5 0.0333 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 2.9 9.2 3.3 0.89 0.0000 9.3 0.0000 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0623 Elt. k-ratio Correc. Na 0.0015 2.3316 Mg 0.0035 1.7032 Sr 0.0012 1.3827 P 0.0045 1.2030 K 0.0007 1.0462 Cl 0.0075 1.1265 Ca 0.2302 1.1017 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2821 iteration : 2 Analysis no. 46 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3462 0.018431 0.3462 0.2706 Mg 0.5956 0.014808 0.5956 0.4403 Sr 0.1706 0.012536 0.1706 0.0350 P 0.5471 0.028294 0.5471 0.3174 K 0.0751 0.008283 0.0751 0.0345 Cl 0.8504 0.020465 0.8504 0.4310 Ca 25.3612 0.125719 25.3612 11.3707 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0214 0.019867 0.0214 0.0070 C 16.6006 16.6006 24.8365 O 55.4318 55.4318 62.2568 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 47 x= -12927.0 y= 2743.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 38.0 3.6 3.6 10.46 0.0439 3.6 0.0286 Mg 118.8 2.0 2.5 47.18 0.0646 2.1 0.0110 Sr 31.9 2.8 14.3 2.23 0.0025 2.8 0.0398 P 27.8 4.2 2.4 11.81 0.0324 4.3 0.0394 K 13.7 6.0 5.1 2.68 0.0078 6.1 0.0191 Cl 57.5 2.4 2.2 26.13 0.0121 2.4 0.0227 Ca 2416.2 0.5 17.7 136.89 0.5272 0.5 0.0334 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0625 Elt. k-ratio Correc. Na 0.0022 2.3269 Mg 0.0047 1.7053 Sr 0.0015 1.3897 P 0.0051 1.2104 K 0.0007 1.0640 Cl 0.0067 1.1373 Ca 0.1913 1.1078 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2856 iteration : 2 Analysis no. 47 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5096 0.021500 0.5096 0.3860 Mg 0.7978 0.017075 0.7978 0.5717 Sr 0.2147 0.013116 0.2147 0.0427 P 0.6145 0.029823 0.6145 0.3455 K 0.0738 0.008356 0.0738 0.0329 Cl 0.7651 0.019576 0.7651 0.3759 Ca 21.1963 0.112530 21.1963 9.2107 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0197 0.019836 0.0197 0.0062 C 18.0021 18.0021 26.1039 O 57.8064 57.8064 62.9245 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 48 x= -12926.0 y= 2747.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 13.1 6.2 3.6 3.60 0.0120 6.2 0.0288 Mg 42.1 3.4 2.5 16.70 0.0220 3.5 0.0110 Sr 21.2 3.4 14.3 1.49 0.0010 3.4 0.0397 P 17.2 5.4 2.4 7.32 0.0189 5.4 0.0394 K 11.8 6.5 5.1 2.30 0.0061 6.5 0.0191 Cl 49.0 2.6 2.2 22.28 0.0102 2.6 0.0227 Ca 2309.8 0.5 17.7 130.86 0.5038 0.5 0.0335 Ba 8.3 5.5 10.8 0.77 0.0000 5.5 0.0000 Fe 2.8 9.4 3.3 0.86 0.0000 9.4 0.0000 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0626 Elt. k-ratio Correc. Na 0.0006 2.3459 Mg 0.0016 1.7088 Sr 0.0006 1.3881 P 0.0030 1.2087 K 0.0005 1.0647 Cl 0.0057 1.1368 Ca 0.1829 1.1094 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2885 iteration : 2 Analysis no. 48 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1410 0.013677 0.1410 0.1051 Mg 0.2718 0.010297 0.2718 0.1917 Sr 0.0847 0.011482 0.0847 0.0166 P 0.3588 0.023946 0.3588 0.1986 K 0.0574 0.007926 0.0574 0.0252 Cl 0.6476 0.018116 0.6476 0.3131 Ca 20.2861 0.109586 20.2861 8.6765 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0088 0.019374 0.0088 0.0027 C 18.9592 18.9592 27.0593 O 59.1846 59.1846 63.4111 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 49 x= -12925.0 y= 2752.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 27.2 4.3 3.6 7.49 0.0301 4.3 0.0286 Mg 87.3 2.4 2.5 34.68 0.0471 2.4 0.0110 Sr 30.8 2.8 14.3 2.15 0.0023 2.9 0.0395 P 26.7 4.3 2.4 11.36 0.0310 4.3 0.0392 K 14.8 5.8 5.1 2.89 0.0088 5.8 0.0187 Cl 64.2 2.3 2.2 29.18 0.0136 2.3 0.0225 Ca 2983.7 0.4 17.7 169.04 0.6520 0.5 0.0332 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.9 8.0 3.3 1.18 0.0003 8.0 0.0554 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0623 Elt. k-ratio Correc. Na 0.0015 2.3314 Mg 0.0034 1.7028 Sr 0.0014 1.3815 P 0.0049 1.2022 K 0.0008 1.0437 Cl 0.0075 1.1251 Ca 0.2366 1.1005 Ba 0.0000 NaN Fe 0.0002 1.2595 Mn 0.0003 1.2811 iteration : 3 Analysis no. 49 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3499 0.018504 0.3499 0.2753 Mg 0.5810 0.014630 0.5810 0.4324 Sr 0.1998 0.012879 0.1998 0.0412 P 0.5852 0.029095 0.5852 0.3417 K 0.0817 0.008435 0.0817 0.0378 Cl 0.8488 0.020435 0.8488 0.4330 Ca 26.0416 0.127817 26.0416 11.7515 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0200 0.014151 0.0200 0.0065 Mn 0.0341 0.020421 0.0341 0.0112 C 16.2995 16.2995 24.5441 O 54.9584 54.9584 62.1253 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 50 x= -12924.0 y= 2756.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 18.5 5.2 3.6 5.10 0.0190 5.2 0.0287 Mg 74.3 2.6 2.5 29.49 0.0399 2.6 0.0110 Sr 22.4 3.3 14.3 1.57 0.0011 3.4 0.0397 P 24.2 4.5 2.4 10.28 0.0278 4.6 0.0393 K 13.9 6.0 5.1 2.72 0.0080 6.0 0.0190 Cl 57.4 2.4 2.2 26.07 0.0121 2.4 0.0226 Ca 2539.6 0.4 17.7 143.88 0.5544 0.5 0.0334 Ba 7.6 5.7 10.8 0.71 0.0000 5.7 0.0000 Fe 3.1 8.9 3.3 0.95 0.0000 9.0 0.0000 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0625 Elt. k-ratio Correc. Na 0.0009 2.3380 Mg 0.0029 1.7054 Sr 0.0007 1.3862 P 0.0044 1.2064 K 0.0007 1.0579 Cl 0.0067 1.1331 Ca 0.2012 1.1065 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2858 iteration : 2 Analysis no. 50 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2219 0.015715 0.2219 0.1687 Mg 0.4923 0.013530 0.4923 0.3541 Sr 0.0983 0.011648 0.0983 0.0196 P 0.5258 0.027872 0.5258 0.2967 K 0.0751 0.008354 0.0751 0.0336 Cl 0.7606 0.019484 0.7606 0.3750 Ca 22.2624 0.115971 22.2624 9.7089 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0179 0.019758 0.0179 0.0057 C 17.9333 17.9333 26.0981 O 57.6126 57.6126 62.9398 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 51 x= -12923.0 y= 2760.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 44.5 3.4 3.6 12.26 0.0522 3.4 0.0285 Mg 149.1 1.8 2.5 59.22 0.0815 1.9 0.0110 Sr 39.6 2.5 14.3 2.77 0.0036 2.5 0.0396 P 28.0 4.2 2.4 11.92 0.0327 4.2 0.0393 K 15.3 5.7 5.1 3.00 0.0093 5.7 0.0187 Cl 64.7 2.3 2.2 29.41 0.0137 2.3 0.0225 Ca 3018.4 0.4 17.7 171.01 0.6596 0.5 0.0332 Ba 11.2 4.7 10.8 1.04 0.0003 4.7 0.0738 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0553 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0622 Elt. k-ratio Correc. Na 0.0026 2.3192 Mg 0.0059 1.7011 Sr 0.0022 1.3841 P 0.0051 1.2047 K 0.0008 1.0441 Cl 0.0076 1.1261 Ca 0.2394 1.0999 Ba 0.0001 1.5357 Fe 0.0001 1.2580 Mn 0.0001 1.2797 iteration : 3 Analysis no. 51 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6041 0.023066 0.6041 0.4787 Mg 1.0034 0.019097 1.0034 0.7522 Sr 0.3071 0.014118 0.3071 0.0639 P 0.6177 0.029808 0.6177 0.3633 K 0.0864 0.008554 0.0864 0.0402 Cl 0.8564 0.020529 0.8564 0.4401 Ca 26.3283 0.128688 26.3283 11.9686 Ba 0.0123 0.019193 0.0123 0.0016 Fe 0.0183 0.014084 0.0183 0.0060 Mn 0.0142 0.019495 0.0142 0.0047 C 15.8511 15.8511 24.0453 O 54.3008 54.3008 61.8353 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 52 x= -12923.0 y= 2764.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 37.6 3.6 3.6 10.37 0.0434 3.7 0.0286 Mg 120.8 2.0 2.5 47.97 0.0657 2.1 0.0110 Sr 34.6 2.7 14.3 2.42 0.0029 2.7 0.0396 P 26.1 4.4 2.4 11.11 0.0303 4.4 0.0393 K 16.1 5.6 5.1 3.16 0.0101 5.6 0.0188 Cl 69.2 2.2 2.2 31.44 0.0146 2.2 0.0225 Ca 2841.0 0.4 17.7 160.95 0.6205 0.5 0.0333 Ba 10.2 5.0 10.8 0.95 0.0000 5.0 0.0000 Fe 3.3 8.7 3.3 0.99 0.0000 8.7 0.0000 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0623 Elt. k-ratio Correc. Na 0.0022 2.3245 Mg 0.0048 1.7025 Sr 0.0018 1.3846 P 0.0047 1.2052 K 0.0009 1.0497 Cl 0.0081 1.1286 Ca 0.2252 1.1023 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2817 iteration : 3 Analysis no. 52 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5038 0.021383 0.5038 0.3935 Mg 0.8100 0.017187 0.8100 0.5985 Sr 0.2467 0.013446 0.2467 0.0506 P 0.5721 0.028856 0.5721 0.3317 K 0.0936 0.008766 0.0936 0.0430 Cl 0.9195 0.021252 0.9195 0.4658 Ca 24.8231 0.124025 24.8231 11.1219 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0395 0.020666 0.0395 0.0129 C 16.5838 16.5838 24.7946 O 55.4078 55.4078 62.1876 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 53 x= -12922.0 y= 2768.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 45.5 3.3 3.6 12.55 0.0535 3.3 0.0285 Mg 134.2 1.9 2.5 53.28 0.0731 2.0 0.0110 Sr 36.6 2.6 14.3 2.56 0.0032 2.6 0.0396 P 24.4 4.5 2.4 10.38 0.0281 4.5 0.0393 K 16.9 5.4 5.1 3.30 0.0107 5.5 0.0188 Cl 58.2 2.4 2.2 26.44 0.0122 2.4 0.0225 Ca 2876.6 0.4 17.7 162.97 0.6284 0.5 0.0333 Ba 10.8 4.8 10.8 1.00 0.0000 4.8 0.0738 Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0554 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0623 Elt. k-ratio Correc. Na 0.0027 2.3228 Mg 0.0053 1.7038 Sr 0.0020 1.3858 P 0.0044 1.2062 K 0.0010 1.0479 Cl 0.0068 1.1283 Ca 0.2280 1.1017 Ba 0.0000 1.5355 Fe 0.0001 1.2600 Mn 0.0002 1.2814 iteration : 3 Analysis no. 53 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6205 0.023355 0.6205 0.4859 Mg 0.9023 0.018133 0.9023 0.6683 Sr 0.2710 0.013730 0.2710 0.0557 P 0.5316 0.027994 0.5316 0.3089 K 0.0998 0.008906 0.0998 0.0460 Cl 0.7682 0.019528 0.7682 0.3900 Ca 25.1237 0.124958 25.1237 11.2837 Ba 0.0006 0.018991 0.0006 0.0001 Fe 0.0075 0.013781 0.0075 0.0024 Mn 0.0250 0.020017 0.0250 0.0082 C 16.4340 16.4340 24.6297 O 55.2157 55.2156 62.1211 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 54 x= -12921.0 y= 2772.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 27.9 4.2 3.6 7.69 0.0310 4.2 0.0287 Mg 78.8 2.5 2.5 31.28 0.0424 2.5 0.0110 Sr 24.2 3.2 14.3 1.69 0.0014 3.2 0.0396 P 24.6 4.5 2.4 10.45 0.0283 4.5 0.0393 K 16.7 5.5 5.1 3.27 0.0106 5.5 0.0189 Cl 65.0 2.3 2.2 29.55 0.0137 2.3 0.0226 Ca 2632.4 0.4 17.7 149.14 0.5747 0.5 0.0334 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0556 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0624 Elt. k-ratio Correc. Na 0.0015 2.3343 Mg 0.0031 1.7057 Sr 0.0009 1.3854 P 0.0044 1.2056 K 0.0009 1.0554 Cl 0.0076 1.1314 Ca 0.2086 1.1051 Ba 0.0000 NaN Fe 0.0001 1.2636 Mn 0.0004 1.2844 iteration : 2 Analysis no. 54 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3615 0.018751 0.3615 0.2772 Mg 0.5232 0.013927 0.5232 0.3796 Sr 0.1204 0.011927 0.1204 0.0242 P 0.5349 0.028059 0.5349 0.3045 K 0.0993 0.008939 0.0993 0.0448 Cl 0.8644 0.020669 0.8644 0.4299 Ca 23.0495 0.118460 23.0495 10.1401 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0184 0.014145 0.0184 0.0058 Mn 0.0451 0.020948 0.0451 0.0145 C 17.5086 17.5086 25.7027 O 56.8747 56.8747 62.6768 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 55 x= -12920.0 y= 2777.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 29.7 4.1 3.6 8.19 0.0333 4.1 0.0286 Mg 98.5 2.3 2.5 39.11 0.0533 2.3 0.0110 Sr 28.8 2.9 14.3 2.02 0.0021 3.0 0.0396 P 23.9 4.6 2.4 10.17 0.0275 4.6 0.0392 K 15.1 5.7 5.1 2.96 0.0091 5.8 0.0188 Cl 67.9 2.2 2.2 30.86 0.0144 2.2 0.0225 Ca 2866.7 0.4 17.7 162.41 0.6262 0.5 0.0333 Ba 10.8 4.8 10.8 1.00 0.0000 4.8 0.0738 Fe 3.3 8.7 3.3 0.99 0.0000 8.7 0.0000 Mn 4.3 10.8 2.7 1.59 0.0016 10.8 0.0623 Elt. k-ratio Correc. Na 0.0017 2.3304 Mg 0.0039 1.7034 Sr 0.0013 1.3835 P 0.0043 1.2038 K 0.0008 1.0478 Cl 0.0080 1.1272 Ca 0.2273 1.1020 Ba 0.0000 1.5360 Fe 0.0000 NaN Mn 0.0004 1.2821 iteration : 3 Analysis no. 55 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3876 0.019251 0.3876 0.3025 Mg 0.6576 0.015531 0.6576 0.4855 Sr 0.1767 0.012615 0.1767 0.0362 P 0.5185 0.027672 0.5185 0.3004 K 0.0850 0.008541 0.0850 0.0390 Cl 0.9010 0.021036 0.9010 0.4561 Ca 25.0449 0.124722 25.0449 11.2129 Ba 0.0006 0.018997 0.0006 0.0001 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0577 0.021454 0.0577 0.0188 C 16.6672 16.6672 24.9005 O 55.5033 55.5033 62.2481 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 56 x= -12919.0 y= 2781.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 37.5 3.6 3.6 10.33 0.0432 3.7 0.0286 Mg 113.2 2.1 2.5 44.93 0.0615 2.1 0.0110 Sr 32.5 2.8 14.3 2.27 0.0026 2.8 0.0396 P 24.8 4.5 2.4 10.55 0.0286 4.5 0.0393 K 19.6 5.1 5.1 3.83 0.0132 5.1 0.0188 Cl 56.4 2.4 2.2 25.63 0.0118 2.4 0.0225 Ca 2864.2 0.4 17.7 162.27 0.6255 0.5 0.0332 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0554 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0623 Elt. k-ratio Correc. Na 0.0022 2.3276 Mg 0.0044 1.7042 Sr 0.0016 1.3848 P 0.0045 1.2051 K 0.0012 1.0477 Cl 0.0066 1.1279 Ca 0.2270 1.1020 Ba 0.0000 NaN Fe 0.0000 1.2606 Mn 0.0003 1.2819 iteration : 3 Analysis no. 56 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5021 0.021369 0.5021 0.3922 Mg 0.7582 0.016647 0.7582 0.5601 Sr 0.2212 0.013152 0.2212 0.0453 P 0.5406 0.028174 0.5406 0.3134 K 0.1227 0.009436 0.1227 0.0564 Cl 0.7435 0.019228 0.7435 0.3766 Ca 25.0161 0.124618 25.0161 11.2064 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0033 0.013657 0.0033 0.0011 Mn 0.0414 0.020746 0.0414 0.0135 C 16.5879 16.5879 24.7964 O 55.4629 55.4629 62.2387 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 57 x= -12918.0 y= 2785.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 22.0 4.8 3.6 6.07 0.0235 4.8 0.0287 Mg 62.0 2.8 2.5 24.63 0.0331 2.9 0.0110 Sr 22.4 3.3 14.3 1.57 0.0011 3.4 0.0397 P 22.5 4.7 2.4 9.55 0.0256 4.7 0.0393 K 17.1 5.4 5.1 3.35 0.0110 5.4 0.0189 Cl 49.0 2.6 2.2 22.27 0.0102 2.6 0.0226 Ca 2549.4 0.4 17.7 144.43 0.5563 0.5 0.0334 Ba 7.4 5.8 10.8 0.68 0.0000 5.8 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0556 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0625 Elt. k-ratio Correc. Na 0.0012 2.3401 Mg 0.0024 1.7075 Sr 0.0007 1.3863 P 0.0040 1.2065 K 0.0010 1.0568 Cl 0.0057 1.1327 Ca 0.2019 1.1062 Ba 0.0000 NaN Fe 0.0001 1.2652 Mn 0.0002 1.2858 iteration : 2 Analysis no. 57 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2742 0.016929 0.2742 0.2084 Mg 0.4086 0.012400 0.4086 0.2937 Sr 0.0982 0.011645 0.0982 0.0196 P 0.4846 0.026944 0.4846 0.2734 K 0.1028 0.009030 0.1028 0.0459 Cl 0.6446 0.018040 0.6446 0.3177 Ca 22.3353 0.116180 22.3353 9.7377 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0109 0.013936 0.0109 0.0034 Mn 0.0288 0.020246 0.0288 0.0091 C 17.9576 17.9576 26.1252 O 57.6544 57.6544 62.9658 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 58 x= -12917.0 y= 2789.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 32.0 4.0 3.6 8.81 0.0362 4.0 0.0286 Mg 69.6 2.7 2.5 27.63 0.0372 2.7 0.0110 Sr 28.4 3.0 14.3 1.99 0.0020 3.0 0.0394 P 26.0 4.4 2.4 11.06 0.0301 4.4 0.0390 K 18.7 5.2 5.1 3.67 0.0124 5.2 0.0185 Cl 62.6 2.3 2.2 28.44 0.0132 2.3 0.0223 Ca 3282.0 0.4 17.7 185.94 0.7174 0.5 0.0331 Ba 9.8 5.0 10.8 0.91 0.0000 5.1 0.0000 Fe 3.8 8.1 3.3 1.15 0.0003 8.1 0.0553 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0622 Elt. k-ratio Correc. Na 0.0018 2.3319 Mg 0.0027 1.7037 Sr 0.0012 1.3781 P 0.0047 1.1983 K 0.0011 1.0332 Cl 0.0073 1.1190 Ca 0.2604 1.0968 Ba 0.0000 NaN Fe 0.0001 1.2567 Mn 0.0003 1.2789 iteration : 3 Analysis no. 58 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4213 0.019908 0.4213 0.3382 Mg 0.4594 0.013086 0.4594 0.3488 Sr 0.1705 0.012498 0.1705 0.0359 P 0.5663 0.028637 0.5663 0.3374 K 0.1139 0.009143 0.1139 0.0538 Cl 0.8217 0.020064 0.8217 0.4277 Ca 28.5560 0.135499 28.5560 13.1479 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0166 0.014017 0.0166 0.0055 Mn 0.0322 0.020300 0.0322 0.0108 C 15.3863 15.3863 23.6398 O 53.4556 53.4556 61.6542 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 59 x= -12916.0 y= 2793.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 25.9 4.4 3.6 7.13 0.0284 4.4 0.0287 Mg 81.5 2.5 2.5 32.37 0.0439 2.5 0.0110 Sr 27.5 3.0 14.3 1.92 0.0019 3.0 0.0395 P 24.6 4.5 2.4 10.47 0.0284 4.5 0.0391 K 16.8 5.4 5.1 3.29 0.0107 5.5 0.0185 Cl 51.2 2.5 2.2 23.27 0.0107 2.6 0.0224 Ca 3181.4 0.4 17.7 180.24 0.6953 0.5 0.0331 Ba 9.0 5.3 10.8 0.84 0.0000 5.3 0.0000 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0553 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0622 Elt. k-ratio Correc. Na 0.0014 2.3344 Mg 0.0032 1.7037 Sr 0.0012 1.3801 P 0.0044 1.2001 K 0.0009 1.0355 Cl 0.0060 1.1210 Ca 0.2523 1.0980 Ba 0.0000 NaN Fe 0.0001 1.2581 Mn 0.0003 1.2801 iteration : 3 Analysis no. 59 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3309 0.018123 0.3309 0.2633 Mg 0.5414 0.014145 0.5414 0.4075 Sr 0.1599 0.012382 0.1599 0.0334 P 0.5336 0.027953 0.5336 0.3152 K 0.0982 0.008789 0.0982 0.0460 Cl 0.6681 0.018238 0.6681 0.3447 Ca 27.7063 0.132912 27.7063 12.6464 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0117 0.013883 0.0117 0.0038 Mn 0.0359 0.020479 0.0359 0.0119 C 15.7690 15.7690 24.0182 O 54.1452 54.1452 61.9096 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 60 x= -12915.0 y= 2798.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 24.8 4.5 3.6 6.82 0.0270 4.5 0.0287 Mg 70.5 2.7 2.5 27.98 0.0377 2.7 0.0110 Sr 24.5 3.2 14.3 1.71 0.0014 3.2 0.0396 P 23.1 4.7 2.4 9.81 0.0264 4.7 0.0392 K 18.6 5.2 5.1 3.65 0.0123 5.2 0.0188 Cl 52.6 2.5 2.2 23.89 0.0110 2.5 0.0225 Ca 2772.9 0.4 17.7 157.10 0.6055 0.5 0.0333 Ba 9.8 5.0 10.8 0.91 0.0000 5.1 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0555 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0624 Elt. k-ratio Correc. Na 0.0013 2.3369 Mg 0.0027 1.7059 Sr 0.0009 1.3840 P 0.0041 1.2042 K 0.0011 1.0493 Cl 0.0061 1.1285 Ca 0.2197 1.1034 Ba 0.0000 NaN Fe 0.0001 1.2626 Mn 0.0001 1.2837 iteration : 2 Analysis no. 60 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3148 0.017798 0.3148 0.2433 Mg 0.4662 0.013186 0.4662 0.3407 Sr 0.1239 0.011960 0.1239 0.0251 P 0.4981 0.027221 0.4981 0.2857 K 0.1148 0.009266 0.1148 0.0522 Cl 0.6913 0.018594 0.6913 0.3463 Ca 24.2466 0.122228 24.2466 10.7458 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0109 0.013909 0.0109 0.0035 Mn 0.0088 0.019298 0.0088 0.0028 C 17.1632 17.1632 25.3826 O 56.3613 56.3613 62.5719 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 61 x= -12915.0 y= 2802.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 45.0 3.3 3.6 12.41 0.0529 3.4 0.0285 Mg 139.1 1.9 2.5 55.23 0.0759 1.9 0.0110 Sr 36.5 2.6 14.3 2.56 0.0032 2.6 0.0396 P 23.0 4.7 2.4 9.77 0.0263 4.7 0.0392 K 20.0 5.0 5.1 3.92 0.0136 5.0 0.0186 Cl 66.0 2.2 2.2 29.98 0.0139 2.2 0.0224 Ca 3150.6 0.4 17.7 178.49 0.6885 0.5 0.0331 Ba 11.7 4.6 10.8 1.09 0.0006 4.6 0.0739 Fe 3.7 8.2 3.3 1.13 0.0002 8.2 0.0553 Mn 2.9 13.2 2.7 1.05 0.0001 13.2 0.0622 Elt. k-ratio Correc. Na 0.0026 2.3209 Mg 0.0055 1.7020 Sr 0.0020 1.3828 P 0.0041 1.2029 K 0.0012 1.0391 Cl 0.0078 1.1227 Ca 0.2499 1.0983 Ba 0.0002 1.5365 Fe 0.0001 1.2570 Mn 0.0000 1.2789 iteration : 3 Analysis no. 61 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6125 0.023212 0.6125 0.4893 Mg 0.9348 0.018441 0.9348 0.7064 Sr 0.2700 0.013696 0.2700 0.0566 P 0.4952 0.027137 0.4952 0.2936 K 0.1255 0.009444 0.1255 0.0590 Cl 0.8710 0.020657 0.8710 0.4512 Ca 27.4422 0.132099 27.4422 12.5751 Ba 0.0246 0.019405 0.0246 0.0033 Fe 0.0141 0.013946 0.0141 0.0047 Mn 0.0051 0.019056 0.0051 0.0017 C 15.5272 15.5272 23.7429 O 53.6777 53.6777 61.6162 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 62 x= -12914.0 y= 2806.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 35.7 3.7 3.6 9.83 0.0409 3.8 0.0286 Mg 112.7 2.1 2.5 44.73 0.0612 2.1 0.0110 Sr 36.7 2.6 14.3 2.57 0.0032 2.6 0.0395 P 23.4 4.6 2.4 9.96 0.0268 4.6 0.0392 K 19.5 5.1 5.1 3.82 0.0132 5.1 0.0187 Cl 64.5 2.3 2.2 29.30 0.0136 2.3 0.0224 Ca 3015.6 0.4 17.7 170.85 0.6588 0.5 0.0332 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.1 9.0 3.3 0.94 0.0000 9.0 0.0000 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0622 Elt. k-ratio Correc. Na 0.0020 2.3261 Mg 0.0044 1.7023 Sr 0.0020 1.3826 P 0.0042 1.2034 K 0.0012 1.0431 Cl 0.0076 1.1249 Ca 0.2391 1.1001 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2804 iteration : 3 Analysis no. 62 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4751 0.020876 0.4751 0.3752 Mg 0.7540 0.016592 0.7540 0.5633 Sr 0.2718 0.013713 0.2718 0.0563 P 0.5062 0.027390 0.5062 0.2967 K 0.1218 0.009385 0.1218 0.0566 Cl 0.8520 0.020465 0.8520 0.4364 Ca 26.3016 0.128601 26.3016 11.9160 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0304 0.020242 0.0304 0.0101 C 16.0965 16.0965 24.3347 O 54.5906 54.5906 61.9547 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 63 x= -12913.0 y= 2810.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 35.2 3.8 3.6 9.69 0.0403 3.8 0.0286 Mg 101.4 2.2 2.5 40.28 0.0550 2.2 0.0110 Sr 32.5 2.8 14.3 2.28 0.0026 2.8 0.0395 P 19.3 5.1 2.4 8.21 0.0216 5.1 0.0392 K 22.0 4.8 5.1 4.31 0.0154 4.8 0.0187 Cl 60.7 2.3 2.2 27.59 0.0128 2.3 0.0224 Ca 3031.9 0.4 17.7 171.77 0.6624 0.5 0.0332 Ba 9.6 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.0 9.2 3.3 0.90 0.0000 9.2 0.0000 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0622 Elt. k-ratio Correc. Na 0.0020 2.3292 Mg 0.0040 1.7039 Sr 0.0016 1.3826 P 0.0034 1.2028 K 0.0014 1.0416 Cl 0.0071 1.1238 Ca 0.2404 1.0999 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2808 iteration : 3 Analysis no. 63 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4683 0.020770 0.4683 0.3696 Mg 0.6779 0.015764 0.6779 0.5061 Sr 0.2212 0.013135 0.2212 0.0458 P 0.4074 0.025083 0.4074 0.2387 K 0.1427 0.009838 0.1427 0.0662 Cl 0.7997 0.019856 0.7997 0.4093 Ca 26.4430 0.129042 26.4430 11.9701 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0268 0.020086 0.0268 0.0089 C 16.1629 16.1629 24.4149 O 54.6499 54.6499 61.9705 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 64 x= -12912.0 y= 2814.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 45.9 3.3 3.6 12.66 0.0540 3.3 0.0285 Mg 129.4 2.0 2.5 51.37 0.0705 2.0 0.0110 Sr 36.6 2.6 14.3 2.56 0.0032 2.6 0.0395 P 23.3 4.6 2.4 9.89 0.0266 4.6 0.0392 K 22.9 4.7 5.1 4.49 0.0163 4.7 0.0186 Cl 62.5 2.3 2.2 28.39 0.0132 2.3 0.0224 Ca 3215.3 0.4 17.7 182.16 0.7027 0.5 0.0331 Ba 11.7 4.6 10.8 1.08 0.0005 4.6 0.0739 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0552 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0621 Elt. k-ratio Correc. Na 0.0027 2.3220 Mg 0.0051 1.7026 Sr 0.0020 1.3819 P 0.0042 1.2020 K 0.0014 1.0366 Cl 0.0073 1.1214 Ca 0.2550 1.0974 Ba 0.0002 1.5368 Fe 0.0001 1.2563 Mn 0.0001 1.2785 iteration : 3 Analysis no. 64 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6261 0.023440 0.6261 0.5023 Mg 0.8686 0.017787 0.8686 0.6592 Sr 0.2705 0.013693 0.2705 0.0569 P 0.5020 0.027279 0.5020 0.2989 K 0.1496 0.009954 0.1496 0.0706 Cl 0.8221 0.020092 0.8221 0.4277 Ca 27.9874 0.133761 27.9874 12.8793 Ba 0.0233 0.019387 0.0233 0.0031 Fe 0.0158 0.013988 0.0158 0.0052 Mn 0.0123 0.019388 0.0123 0.0041 C 15.3392 15.3392 23.5549 O 53.3829 53.3829 61.5377 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 65 x= -12911.0 y= 2818.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 30.2 4.1 3.6 8.31 0.0339 4.1 0.0287 Mg 83.7 2.4 2.5 33.25 0.0451 2.5 0.0110 Sr 25.2 3.1 14.3 1.76 0.0015 3.2 0.0395 P 23.1 4.7 2.4 9.81 0.0264 4.7 0.0392 K 23.3 4.6 5.1 4.56 0.0166 4.6 0.0187 Cl 53.5 2.5 2.2 24.30 0.0112 2.5 0.0224 Ca 2998.7 0.4 17.7 169.89 0.6552 0.5 0.0332 Ba 7.7 5.7 10.8 0.71 0.0000 5.7 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0554 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0623 Elt. k-ratio Correc. Na 0.0017 2.3338 Mg 0.0033 1.7051 Sr 0.0010 1.3824 P 0.0041 1.2021 K 0.0015 1.0418 Cl 0.0062 1.1242 Ca 0.2378 1.1004 Ba 0.0000 NaN Fe 0.0000 1.2599 Mn 0.0004 1.2815 iteration : 3 Analysis no. 65 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3948 0.019409 0.3948 0.3104 Mg 0.5570 0.014345 0.5570 0.4141 Sr 0.1319 0.012051 0.1319 0.0272 P 0.4973 0.027175 0.4973 0.2901 K 0.1533 0.010067 0.1533 0.0709 Cl 0.7010 0.018678 0.7010 0.3573 Ca 26.1651 0.128192 26.1651 11.7974 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0025 0.013627 0.0025 0.0008 Mn 0.0450 0.020900 0.0450 0.0148 C 16.3336 16.3336 24.5751 O 55.0185 55.0185 62.1418 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 66 x= -12910.0 y= 2823.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 31.8 4.0 3.6 8.75 0.0359 4.0 0.0286 Mg 111.0 2.1 2.5 44.10 0.0603 2.1 0.0110 Sr 37.2 2.6 14.3 2.60 0.0032 2.6 0.0394 P 22.0 4.8 2.4 9.34 0.0250 4.8 0.0390 K 22.2 4.7 5.1 4.35 0.0156 4.8 0.0183 Cl 57.8 2.4 2.2 26.28 0.0122 2.4 0.0222 Ca 3585.4 0.4 17.7 203.13 0.7841 0.5 0.0330 Ba 12.1 4.5 10.8 1.12 0.0008 4.6 0.0740 Fe 4.1 7.8 3.3 1.24 0.0004 7.8 0.0551 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0620 Elt. k-ratio Correc. Na 0.0018 2.3273 Mg 0.0044 1.7005 Sr 0.0020 1.3768 P 0.0039 1.1971 K 0.0014 1.0236 Cl 0.0068 1.1140 Ca 0.2846 1.0927 Ba 0.0002 1.5385 Fe 0.0002 1.2529 Mn 0.0002 1.2758 iteration : 3 Analysis no. 66 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4175 0.019813 0.4175 0.3432 Mg 0.7423 0.016458 0.7423 0.5772 Sr 0.2765 0.013722 0.2765 0.0596 P 0.4689 0.026464 0.4689 0.2861 K 0.1419 0.009705 0.1419 0.0686 Cl 0.7539 0.019225 0.7539 0.4018 Ca 31.0951 0.143125 31.0951 14.6609 Ba 0.0344 0.019594 0.0344 0.0047 Fe 0.0265 0.014268 0.0265 0.0090 Mn 0.0303 0.020173 0.0303 0.0104 C 14.3087 14.3087 22.5122 O 51.7040 51.7040 61.0663 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 67 x= -12909.0 y= 2827.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 43.1 3.4 3.6 11.87 0.0504 3.4 0.0285 Mg 131.7 1.9 2.5 52.31 0.0718 2.0 0.0110 Sr 37.3 2.6 14.3 2.61 0.0033 2.6 0.0395 P 23.6 4.6 2.4 10.04 0.0271 4.6 0.0392 K 22.4 4.7 5.1 4.38 0.0158 4.7 0.0186 Cl 70.2 2.2 2.2 31.93 0.0149 2.2 0.0224 Ca 3218.9 0.4 17.7 182.36 0.7036 0.5 0.0331 Ba 11.7 4.6 10.8 1.09 0.0006 4.6 0.0739 Fe 3.7 8.2 3.3 1.13 0.0002 8.2 0.0552 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0621 Elt. k-ratio Correc. Na 0.0025 2.3215 Mg 0.0052 1.7014 Sr 0.0020 1.3814 P 0.0042 1.2016 K 0.0014 1.0371 Cl 0.0083 1.1213 Ca 0.2554 1.0974 Ba 0.0002 1.5366 Fe 0.0001 1.2560 Mn 0.0003 1.2782 iteration : 3 Analysis no. 67 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5839 0.022743 0.5839 0.4690 Mg 0.8843 0.017939 0.8843 0.6719 Sr 0.2789 0.013785 0.2789 0.0588 P 0.5103 0.027463 0.5103 0.3043 K 0.1451 0.009861 0.1451 0.0685 Cl 0.9282 0.021274 0.9282 0.4835 Ca 28.0214 0.133870 28.0214 12.9118 Ba 0.0240 0.019399 0.0240 0.0032 Fe 0.0141 0.013937 0.0141 0.0047 Mn 0.0412 0.020690 0.0412 0.0139 C 15.2961 15.2961 23.5195 O 53.2726 53.2726 61.4909 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 68 x= -12908.0 y= 2831.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 40.9 3.5 3.6 11.28 0.0476 3.5 0.0286 Mg 111.7 2.1 2.5 44.38 0.0607 2.1 0.0110 Sr 36.0 2.6 14.3 2.52 0.0031 2.6 0.0394 P 23.1 4.7 2.4 9.81 0.0264 4.7 0.0390 K 27.8 4.2 5.1 5.44 0.0207 4.3 0.0184 Cl 66.3 2.2 2.2 30.14 0.0140 2.2 0.0223 Ca 3465.9 0.4 17.7 196.36 0.7579 0.5 0.0330 Ba 10.0 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0551 Mn 4.7 10.4 2.7 1.72 0.0019 10.4 0.0621 Elt. k-ratio Correc. Na 0.0024 2.3242 Mg 0.0044 1.7014 Sr 0.0019 1.3780 P 0.0041 1.1982 K 0.0018 1.0284 Cl 0.0078 1.1162 Ca 0.2751 1.0944 Ba 0.0000 NaN Fe 0.0000 1.2538 Mn 0.0005 1.2765 iteration : 3 Analysis no. 68 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5527 0.022233 0.5527 0.4513 Mg 0.7476 0.016522 0.7476 0.5774 Sr 0.2631 0.013583 0.2631 0.0564 P 0.4957 0.027091 0.4957 0.3004 K 0.1889 0.010702 0.1889 0.0907 Cl 0.8706 0.020591 0.8706 0.4609 Ca 30.1032 0.140170 30.1032 14.0983 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0033 0.013588 0.0033 0.0011 Mn 0.0701 0.021890 0.0701 0.0239 C 14.5874 14.5874 22.7970 O 52.1174 52.1174 61.1426 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 69 x= -12907.0 y= 2835.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 18.0 5.3 3.6 4.95 0.0183 5.3 0.0287 Mg 86.1 2.4 2.5 34.20 0.0465 2.4 0.0110 Sr 30.8 2.8 14.3 2.16 0.0024 2.9 0.0395 P 22.4 4.7 2.4 9.51 0.0255 4.7 0.0392 K 22.7 4.7 5.1 4.45 0.0161 4.7 0.0186 Cl 54.6 2.5 2.2 24.81 0.0115 2.5 0.0224 Ca 3027.3 0.4 17.7 171.51 0.6615 0.5 0.0332 Ba 9.3 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0554 Mn 4.3 10.8 2.7 1.57 0.0015 10.8 0.0623 Elt. k-ratio Correc. Na 0.0009 2.3354 Mg 0.0034 1.7023 Sr 0.0015 1.3812 P 0.0040 1.2018 K 0.0014 1.0410 Cl 0.0064 1.1237 Ca 0.2401 1.1000 Ba 0.0000 NaN Fe 0.0000 1.2595 Mn 0.0004 1.2812 iteration : 2 Analysis no. 69 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2134 0.015496 0.2134 0.1681 Mg 0.5725 0.014524 0.5725 0.4265 Sr 0.2006 0.012884 0.2006 0.0415 P 0.4804 0.026790 0.4804 0.2808 K 0.1485 0.009961 0.1485 0.0688 Cl 0.7163 0.018861 0.7163 0.3658 Ca 26.4080 0.128942 26.4080 11.9303 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013597 0.0017 0.0005 Mn 0.0558 0.021361 0.0558 0.0184 C 16.2837 16.2837 24.5481 O 54.9190 54.9190 62.1511 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 70 x= -12907.0 y= 2839.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 36.5 3.7 3.6 10.05 0.0419 3.7 0.0286 Mg 140.3 1.9 2.5 55.71 0.0765 1.9 0.0110 Sr 33.4 2.7 14.3 2.34 0.0027 2.7 0.0396 P 24.3 4.5 2.4 10.32 0.0279 4.6 0.0392 K 24.6 4.5 5.1 4.81 0.0178 4.5 0.0187 Cl 57.1 2.4 2.2 25.97 0.0120 2.4 0.0224 Ca 3028.3 0.4 17.7 171.56 0.6617 0.5 0.0332 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.6 8.4 3.3 1.08 0.0002 8.4 0.0553 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0622 Elt. k-ratio Correc. Na 0.0021 2.3246 Mg 0.0055 1.7018 Sr 0.0017 1.3840 P 0.0044 1.2039 K 0.0016 1.0425 Cl 0.0067 1.1250 Ca 0.2401 1.0999 Ba 0.0000 NaN Fe 0.0001 1.2586 Mn 0.0003 1.2803 iteration : 3 Analysis no. 70 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4867 0.021079 0.4867 0.3850 Mg 0.9430 0.018520 0.9430 0.7056 Sr 0.2320 0.013273 0.2320 0.0482 P 0.5269 0.027860 0.5269 0.3094 K 0.1644 0.010303 0.1644 0.0765 Cl 0.7517 0.019301 0.7517 0.3856 Ca 26.4125 0.128949 26.4125 11.9845 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0092 0.013815 0.0092 0.0030 Mn 0.0341 0.020404 0.0341 0.0113 C 15.9669 15.9669 24.1757 O 54.4726 54.4726 61.9153 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 71 x= -12906.0 y= 2844.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 24.7 4.5 3.6 6.81 0.0269 4.5 0.0287 Mg 74.4 2.6 2.5 29.53 0.0399 2.6 0.0110 Sr 25.0 3.2 14.3 1.75 0.0015 3.2 0.0396 P 23.7 4.6 2.4 10.06 0.0272 4.6 0.0393 K 21.5 4.8 5.1 4.21 0.0150 4.8 0.0188 Cl 62.5 2.3 2.2 28.39 0.0132 2.3 0.0225 Ca 2777.9 0.4 17.7 157.38 0.6070 0.5 0.0333 Ba 9.2 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0624 Elt. k-ratio Correc. Na 0.0013 2.3348 Mg 0.0029 1.7047 Sr 0.0009 1.3835 P 0.0043 1.2037 K 0.0013 1.0500 Cl 0.0073 1.1283 Ca 0.2203 1.1034 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2834 iteration : 2 Analysis no. 71 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3140 0.017777 0.3140 0.2431 Mg 0.4929 0.013537 0.4929 0.3610 Sr 0.1300 0.012040 0.1300 0.0264 P 0.5127 0.027551 0.5127 0.2946 K 0.1393 0.009822 0.1393 0.0634 Cl 0.8277 0.020227 0.8277 0.4155 Ca 24.3057 0.122445 24.3057 10.7931 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0233 0.019975 0.0233 0.0075 C 17.0797 17.0797 25.3085 O 56.1748 56.1748 62.4869 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 72 x= -12905.0 y= 2848.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 41.0 3.5 3.6 11.31 0.0478 3.5 0.0285 Mg 127.6 2.0 2.5 50.68 0.0695 2.0 0.0110 Sr 42.0 2.4 14.3 2.94 0.0039 2.5 0.0394 P 25.2 4.4 2.4 10.72 0.0291 4.5 0.0391 K 25.9 4.4 5.1 5.07 0.0190 4.4 0.0184 Cl 85.4 2.0 2.2 38.83 0.0182 2.0 0.0223 Ca 3506.6 0.4 17.7 198.66 0.7671 0.5 0.0330 Ba 11.8 4.6 10.8 1.10 0.0006 4.6 0.0740 Fe 3.1 9.0 3.3 0.94 0.0000 9.0 0.0000 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0620 Elt. k-ratio Correc. Na 0.0024 2.3182 Mg 0.0050 1.6980 Sr 0.0024 1.3769 P 0.0046 1.1978 K 0.0017 1.0293 Cl 0.0101 1.1159 Ca 0.2784 1.0939 Ba 0.0002 1.5376 Fe 0.0000 NaN Mn 0.0003 1.2754 iteration : 3 Analysis no. 72 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5529 0.022207 0.5529 0.4544 Mg 0.8547 0.017627 0.8547 0.6644 Sr 0.3346 0.014361 0.3346 0.0722 P 0.5472 0.028226 0.5472 0.3338 K 0.1732 0.010398 0.1732 0.0837 Cl 1.1303 0.023314 1.1303 0.6024 Ca 30.4538 0.141237 30.4538 14.3558 Ba 0.0266 0.019461 0.0266 0.0037 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0358 0.020415 0.0358 0.0123 C 14.3051 14.3051 22.5022 O 51.5857 51.5857 60.9152 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 73 x= -12904.0 y= 2852.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 51.6 3.1 3.6 14.23 0.0613 3.1 0.0284 Mg 157.7 1.8 2.5 62.62 0.0862 1.8 0.0110 Sr 42.0 2.4 14.3 2.94 0.0039 2.5 0.0395 P 26.2 4.4 2.4 11.13 0.0303 4.4 0.0391 K 28.8 4.2 5.1 5.65 0.0217 4.2 0.0185 Cl 82.8 2.0 2.2 37.62 0.0176 2.0 0.0223 Ca 3408.8 0.4 17.7 193.12 0.7455 0.5 0.0331 Ba 11.3 4.7 10.8 1.05 0.0003 4.7 0.0739 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0551 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0620 Elt. k-ratio Correc. Na 0.0031 2.3132 Mg 0.0062 1.6985 Sr 0.0024 1.3797 P 0.0048 1.2001 K 0.0019 1.0329 Cl 0.0098 1.1184 Ca 0.2705 1.0951 Ba 0.0001 1.5370 Fe 0.0000 1.2532 Mn 0.0003 1.2759 iteration : 3 Analysis no. 73 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7081 0.024687 0.7081 0.5790 Mg 1.0604 0.019615 1.0604 0.8201 Sr 0.3358 0.014394 0.3358 0.0720 P 0.5709 0.028764 0.5709 0.3465 K 0.1985 0.010922 0.1985 0.0954 Cl 1.0963 0.022999 1.0963 0.5812 Ca 29.6275 0.138745 29.6275 13.8953 Ba 0.0130 0.019221 0.0130 0.0018 Fe 0.0041 0.013608 0.0041 0.0014 Mn 0.0322 0.020258 0.0322 0.0110 C 14.4581 14.4581 22.6273 O 51.8951 51.8951 60.9690 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 74 x= -12903.0 y= 2856.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 18.5 5.2 3.6 5.09 0.0189 5.2 0.0288 Mg 54.1 3.0 2.5 21.47 0.0287 3.1 0.0110 Sr 16.5 3.9 14.3 1.15 0.0003 3.9 0.0397 P 19.2 5.1 2.4 8.17 0.0215 5.1 0.0394 K 22.9 4.7 5.1 4.49 0.0163 4.7 0.0190 Cl 50.8 2.6 2.2 23.08 0.0106 2.6 0.0227 Ca 2378.7 0.5 17.7 134.76 0.5192 0.5 0.0335 Ba 4.3 7.6 10.8 0.40 0.0000 7.6 0.0000 Fe 2.9 9.2 3.3 0.89 0.0000 9.3 0.0000 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0626 Elt. k-ratio Correc. Na 0.0009 2.3430 Mg 0.0021 1.7086 Sr 0.0002 1.3880 P 0.0034 1.2077 K 0.0014 1.0625 Cl 0.0059 1.1353 Ca 0.1884 1.1087 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2877 iteration : 2 Analysis no. 74 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2217 0.015735 0.2217 0.1663 Mg 0.3544 0.011617 0.3544 0.2515 Sr 0.0265 0.010683 0.0265 0.0052 P 0.4069 0.025140 0.4069 0.2266 K 0.1534 0.010209 0.1534 0.0677 Cl 0.6714 0.018411 0.6714 0.3267 Ca 20.8898 0.111573 20.8898 8.9903 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0106 0.019456 0.0106 0.0033 C 18.6131 18.6131 26.7306 O 58.6522 58.6522 63.2317 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 75 x= -12902.0 y= 2860.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 30.4 4.1 3.6 8.37 0.0342 4.1 0.0286 Mg 114.5 2.1 2.5 45.47 0.0623 2.1 0.0110 Sr 41.0 2.5 14.3 2.87 0.0038 2.5 0.0394 P 27.8 4.2 2.4 11.81 0.0324 4.3 0.0391 K 27.1 4.3 5.1 5.31 0.0201 4.3 0.0185 Cl 66.5 2.2 2.2 30.21 0.0141 2.2 0.0223 Ca 3465.7 0.4 17.7 196.34 0.7584 0.5 0.0331 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0552 Mn 3.9 11.3 2.7 1.44 0.0012 11.3 0.0621 Elt. k-ratio Correc. Na 0.0017 2.3242 Mg 0.0045 1.6984 Sr 0.0023 1.3768 P 0.0051 1.1980 K 0.0018 1.0290 Cl 0.0078 1.1168 Ca 0.2752 1.0944 Ba 0.0000 NaN Fe 0.0001 1.2536 Mn 0.0003 1.2763 iteration : 3 Analysis no. 75 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3965 0.019402 0.3965 0.3240 Mg 0.7656 0.016704 0.7656 0.5917 Sr 0.3229 0.014239 0.3229 0.0692 P 0.6086 0.029536 0.6086 0.3691 K 0.1837 0.010608 0.1837 0.0883 Cl 0.8738 0.020640 0.8738 0.4630 Ca 30.1214 0.140258 30.1214 14.1185 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0108 0.013821 0.0108 0.0036 Mn 0.0430 0.020753 0.0430 0.0147 C 14.5478 14.5478 22.7542 O 52.1259 52.1259 61.2036 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 76 x= -12901.0 y= 2864.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 35.5 3.7 3.6 9.79 0.0408 3.8 0.0286 Mg 92.3 2.3 2.5 36.65 0.0500 2.3 0.0110 Sr 34.5 2.7 14.3 2.42 0.0029 2.7 0.0396 P 24.9 4.5 2.4 10.60 0.0288 4.5 0.0392 K 25.7 4.4 5.1 5.04 0.0189 4.4 0.0187 Cl 87.2 2.0 2.2 39.63 0.0186 2.0 0.0225 Ca 3104.0 0.4 17.7 175.85 0.6795 0.5 0.0333 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 2.9 9.3 3.3 0.88 0.0000 9.3 0.0000 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0624 Elt. k-ratio Correc. Na 0.0020 2.3245 Mg 0.0036 1.7010 Sr 0.0018 1.3795 P 0.0045 1.2004 K 0.0017 1.0415 Cl 0.0104 1.1224 Ca 0.2466 1.0992 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2794 iteration : 3 Analysis no. 76 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4735 0.020861 0.4735 0.3771 Mg 0.6152 0.015042 0.6152 0.4635 Sr 0.2453 0.013410 0.2453 0.0513 P 0.5420 0.028171 0.5420 0.3204 K 0.1743 0.010511 0.1743 0.0816 Cl 1.1627 0.023720 1.1627 0.6005 Ca 27.1080 0.131182 27.1080 12.3850 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0196 0.019773 0.0196 0.0065 C 15.7590 15.7590 24.0258 O 53.9004 53.9004 61.6881 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 77 x= -12900.0 y= 2869.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 32.4 3.9 3.6 8.93 0.0368 3.9 0.0286 Mg 98.9 2.2 2.5 39.27 0.0536 2.3 0.0110 Sr 35.7 2.6 14.3 2.50 0.0030 2.7 0.0395 P 27.4 4.3 2.4 11.66 0.0320 4.3 0.0392 K 25.7 4.4 5.1 5.03 0.0188 4.4 0.0187 Cl 94.6 1.9 2.2 42.99 0.0202 1.9 0.0225 Ca 3090.2 0.4 17.7 175.07 0.6763 0.5 0.0333 Ba 11.5 4.7 10.8 1.07 0.0004 4.7 0.0740 Fe 3.6 8.3 3.3 1.09 0.0002 8.3 0.0554 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0623 Elt. k-ratio Correc. Na 0.0018 2.3232 Mg 0.0039 1.6995 Sr 0.0019 1.3792 P 0.0050 1.2004 K 0.0017 1.0429 Cl 0.0113 1.1229 Ca 0.2454 1.0993 Ba 0.0001 1.5363 Fe 0.0001 1.2571 Mn 0.0003 1.2791 iteration : 3 Analysis no. 77 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4271 0.019992 0.4271 0.3404 Mg 0.6597 0.015549 0.6597 0.4975 Sr 0.2598 0.013569 0.2598 0.0543 P 0.6019 0.029441 0.6019 0.3561 K 0.1740 0.010513 0.1740 0.0816 Cl 1.2638 0.024693 1.2638 0.6533 Ca 26.9818 0.130779 26.9818 12.3374 Ba 0.0188 0.019335 0.0188 0.0025 Fe 0.0100 0.013845 0.0100 0.0033 Mn 0.0395 0.020655 0.0395 0.0132 C 15.7245 15.7245 23.9926 O 53.8392 53.8392 61.6679 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 78 x= -12899.0 y= 2873.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 39.2 3.6 3.6 10.80 0.0455 3.6 0.0286 Mg 114.3 2.1 2.5 45.39 0.0622 2.1 0.0110 Sr 44.0 2.4 14.3 3.08 0.0042 2.4 0.0395 P 29.1 4.1 2.4 12.36 0.0341 4.2 0.0392 K 31.9 4.0 5.1 6.25 0.0245 4.0 0.0186 Cl 78.2 2.1 2.2 35.54 0.0166 2.1 0.0224 Ca 3271.5 0.4 17.7 185.35 0.7162 0.5 0.0332 Ba 10.7 4.8 10.8 0.99 0.0000 4.8 0.0000 Fe 3.9 8.0 3.3 1.17 0.0003 8.0 0.0553 Mn 4.2 11.0 2.7 1.53 0.0014 11.0 0.0622 Elt. k-ratio Correc. Na 0.0023 2.3204 Mg 0.0045 1.6992 Sr 0.0026 1.3784 P 0.0053 1.2001 K 0.0022 1.0366 Cl 0.0093 1.1205 Ca 0.2599 1.0968 Ba 0.0000 NaN Fe 0.0002 1.2548 Mn 0.0004 1.2772 iteration : 3 Analysis no. 78 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5266 0.021780 0.5266 0.4257 Mg 0.7651 0.016710 0.7651 0.5851 Sr 0.3602 0.014656 0.3602 0.0764 P 0.6414 0.030251 0.6414 0.3849 K 0.2252 0.011461 0.2252 0.1070 Cl 1.0373 0.022437 1.0373 0.5438 Ca 28.5095 0.135429 28.5095 13.2208 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0191 0.014092 0.0191 0.0064 Mn 0.0521 0.021172 0.0521 0.0176 C 15.0288 15.0288 23.2564 O 52.8346 52.8346 61.3758 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 79 x= -12899.0 y= 2877.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 34.1 3.8 3.6 9.39 0.0389 3.8 0.0286 Mg 104.6 2.2 2.5 41.55 0.0568 2.2 0.0110 Sr 36.0 2.6 14.3 2.52 0.0031 2.6 0.0396 P 28.1 4.2 2.4 11.94 0.0328 4.2 0.0393 K 27.4 4.3 5.1 5.36 0.0204 4.3 0.0188 Cl 82.6 2.0 2.2 37.55 0.0176 2.0 0.0225 Ca 3031.9 0.4 17.7 171.77 0.6635 0.5 0.0333 Ba 10.2 4.9 10.8 0.95 0.0000 5.0 0.0000 Fe 3.5 8.4 3.3 1.06 0.0001 8.5 0.0555 Mn 2.9 13.1 2.7 1.07 0.0002 13.1 0.0624 Elt. k-ratio Correc. Na 0.0019 2.3233 Mg 0.0041 1.7001 Sr 0.0019 1.3805 P 0.0051 1.2017 K 0.0018 1.0442 Cl 0.0098 1.1244 Ca 0.2408 1.1002 Ba 0.0000 NaN Fe 0.0001 1.2580 Mn 0.0001 1.2798 iteration : 3 Analysis no. 79 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4516 0.020452 0.4516 0.3581 Mg 0.6995 0.016000 0.6995 0.5247 Sr 0.2634 0.013621 0.2634 0.0548 P 0.6182 0.029800 0.6182 0.3639 K 0.1887 0.010816 0.1887 0.0880 Cl 1.1018 0.023136 1.1018 0.5666 Ca 26.4914 0.129279 26.4914 12.0510 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0067 0.013755 0.0067 0.0022 Mn 0.0069 0.019186 0.0069 0.0023 C 15.9212 15.9212 24.1680 O 54.2507 54.2507 61.8204 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 80 x= -12898.0 y= 2881.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 44.3 3.4 3.6 12.20 0.0520 3.4 0.0284 Mg 147.4 1.8 2.5 58.53 0.0806 1.9 0.0110 Sr 41.5 2.5 14.3 2.91 0.0039 2.5 0.0395 P 33.6 3.9 2.4 14.30 0.0399 3.9 0.0392 K 28.0 4.2 5.1 5.48 0.0209 4.2 0.0187 Cl 108.3 1.8 2.2 49.22 0.0232 1.8 0.0224 Ca 3241.5 0.4 17.7 183.64 0.7094 0.5 0.0332 Ba 10.6 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 3.5 8.4 3.3 1.06 0.0001 8.5 0.0553 Mn 2.9 13.2 2.7 1.05 0.0001 13.2 0.0622 Elt. k-ratio Correc. Na 0.0026 2.3109 Mg 0.0058 1.6954 Sr 0.0024 1.3787 P 0.0063 1.1999 K 0.0019 1.0406 Cl 0.0129 1.1216 Ca 0.2574 1.0976 Ba 0.0000 NaN Fe 0.0001 1.2544 Mn 0.0000 1.2768 iteration : 3 Analysis no. 80 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5996 0.022959 0.5996 0.4858 Mg 0.9891 0.018939 0.9891 0.7580 Sr 0.3296 0.014330 0.3296 0.0701 P 0.7503 0.032386 0.7503 0.4512 K 0.1930 0.010874 0.1930 0.0920 Cl 1.4493 0.026366 1.4493 0.7615 Ca 28.2565 0.134662 28.2565 13.1321 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0067 0.013710 0.0067 0.0022 Mn 0.0051 0.019047 0.0051 0.0017 C 14.8835 14.8835 23.0817 O 52.5375 52.5375 61.1638 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 81 x= -12897.0 y= 2885.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 24.6 4.5 3.6 6.77 0.0268 4.5 0.0287 Mg 65.5 2.8 2.5 26.00 0.0350 2.8 0.0110 Sr 31.0 2.8 14.3 2.17 0.0024 2.9 0.0397 P 28.6 4.2 2.4 12.17 0.0335 4.2 0.0393 K 28.4 4.2 5.1 5.57 0.0213 4.2 0.0189 Cl 70.5 2.2 2.2 32.06 0.0150 2.2 0.0226 Ca 2735.6 0.4 17.7 154.98 0.5985 0.5 0.0334 Ba 9.0 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0557 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0626 Elt. k-ratio Correc. Na 0.0013 2.3322 Mg 0.0025 1.7031 Sr 0.0015 1.3822 P 0.0053 1.2037 K 0.0019 1.0527 Cl 0.0083 1.1294 Ca 0.2172 1.1040 Ba 0.0000 NaN Fe 0.0000 1.2620 Mn 0.0001 1.2831 iteration : 2 Analysis no. 81 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3118 0.017733 0.3118 0.2414 Mg 0.4320 0.012723 0.4320 0.3163 Sr 0.2030 0.012939 0.2030 0.0412 P 0.6327 0.030131 0.6327 0.3635 K 0.1992 0.011083 0.1992 0.0907 Cl 0.9408 0.021513 0.9408 0.4722 Ca 23.9776 0.121478 23.9776 10.6458 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0050 0.013751 0.0050 0.0016 Mn 0.0106 0.019410 0.0106 0.0034 C 17.0938 17.0938 25.3256 O 56.1934 56.1934 62.4983 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 82 x= -12896.0 y= 2890.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 48.1 3.2 3.6 13.25 0.0568 3.2 0.0285 Mg 128.1 2.0 2.5 50.88 0.0699 2.0 0.0110 Sr 38.3 2.6 14.3 2.68 0.0034 2.6 0.0396 P 33.5 3.9 2.4 14.24 0.0397 3.9 0.0393 K 28.1 4.2 5.1 5.51 0.0210 4.2 0.0188 Cl 85.2 2.0 2.2 38.71 0.0182 2.0 0.0225 Ca 3045.4 0.4 17.7 172.53 0.6662 0.5 0.0333 Ba 10.0 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0554 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0623 Elt. k-ratio Correc. Na 0.0028 2.3162 Mg 0.0051 1.7001 Sr 0.0021 1.3815 P 0.0062 1.2025 K 0.0019 1.0451 Cl 0.0101 1.1253 Ca 0.2418 1.0999 Ba 0.0000 NaN Fe 0.0001 1.2571 Mn 0.0002 1.2789 iteration : 3 Analysis no. 82 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6572 0.023922 0.6572 0.5236 Mg 0.8599 0.017698 0.8599 0.6480 Sr 0.2920 0.013943 0.2920 0.0610 P 0.7483 0.032388 0.7483 0.4425 K 0.1951 0.010946 0.1951 0.0914 Cl 1.1371 0.023492 1.1371 0.5874 Ca 26.5939 0.129573 26.5939 12.1530 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0133 0.013940 0.0133 0.0044 Mn 0.0196 0.019755 0.0196 0.0065 C 15.6268 15.6268 23.8297 O 53.8567 53.8567 61.6524 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 83 x= -12895.0 y= 2894.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 39.1 3.6 3.6 10.77 0.0454 3.6 0.0285 Mg 133.1 1.9 2.5 52.86 0.0727 2.0 0.0110 Sr 39.9 2.5 14.3 2.79 0.0036 2.5 0.0396 P 35.8 3.7 2.4 15.21 0.0427 3.8 0.0393 K 30.3 4.1 5.1 5.93 0.0230 4.1 0.0188 Cl 90.5 1.9 2.2 41.14 0.0193 1.9 0.0225 Ca 3007.2 0.4 17.7 170.37 0.6584 0.5 0.0333 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0555 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0624 Elt. k-ratio Correc. Na 0.0023 2.3164 Mg 0.0053 1.6977 Sr 0.0023 1.3810 P 0.0067 1.2025 K 0.0020 1.0469 Cl 0.0108 1.1261 Ca 0.2389 1.1004 Ba 0.0000 NaN Fe 0.0002 1.2572 Mn 0.0002 1.2790 iteration : 3 Analysis no. 83 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5245 0.021727 0.5245 0.4172 Mg 0.8936 0.018030 0.8936 0.6724 Sr 0.3112 0.014159 0.3112 0.0650 P 0.8043 0.033454 0.8043 0.4749 K 0.2139 0.011325 0.2139 0.1000 Cl 1.2120 0.024242 1.2120 0.6252 Ca 26.2918 0.128682 26.2918 11.9964 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0208 0.014175 0.0208 0.0068 Mn 0.0232 0.019937 0.0232 0.0077 C 15.7086 15.7086 23.9176 O 53.9960 53.9960 61.7167 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 84 x= -12894.0 y= 2898.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 40.2 3.5 3.6 11.08 0.0468 3.5 0.0286 Mg 100.9 2.2 2.5 40.08 0.0548 2.2 0.0110 Sr 34.3 2.7 14.3 2.40 0.0028 2.7 0.0396 P 35.7 3.7 2.4 15.19 0.0426 3.8 0.0393 K 30.4 4.1 5.1 5.95 0.0231 4.1 0.0188 Cl 75.6 2.1 2.2 34.38 0.0161 2.1 0.0225 Ca 3013.4 0.4 17.7 170.72 0.6596 0.5 0.0333 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0555 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0624 Elt. k-ratio Correc. Na 0.0023 2.3217 Mg 0.0040 1.7010 Sr 0.0018 1.3806 P 0.0067 1.2017 K 0.0021 1.0450 Cl 0.0090 1.1255 Ca 0.2394 1.1004 Ba 0.0000 NaN Fe 0.0001 1.2580 Mn 0.0000 1.2798 iteration : 3 Analysis no. 84 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5427 0.022070 0.5427 0.4303 Mg 0.6747 0.015728 0.6747 0.5060 Sr 0.2428 0.013391 0.2428 0.0505 P 0.8025 0.033406 0.8025 0.4723 K 0.2143 0.011319 0.2143 0.0999 Cl 1.0075 0.022183 1.0075 0.5181 Ca 26.3420 0.128832 26.3420 11.9812 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0133 0.013960 0.0133 0.0044 Mn 0.0015 0.018932 0.0015 0.0005 C 15.8584 15.8584 24.0691 O 54.3003 54.3003 61.8677 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 85 x= -12893.0 y= 2902.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 50.5 3.1 3.6 13.93 0.0600 3.2 0.0286 Mg 114.7 2.1 2.5 45.55 0.0625 2.1 0.0110 Sr 35.7 2.6 14.3 2.50 0.0030 2.7 0.0396 P 37.1 3.7 2.4 15.79 0.0444 3.7 0.0393 K 33.4 3.9 5.1 6.55 0.0259 3.9 0.0188 Cl 79.5 2.0 2.2 36.11 0.0169 2.0 0.0225 Ca 3067.9 0.4 17.7 173.81 0.6720 0.5 0.0333 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0555 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0624 Elt. k-ratio Correc. Na 0.0030 2.3172 Mg 0.0045 1.7013 Sr 0.0019 1.3808 P 0.0070 1.2017 K 0.0023 1.0439 Cl 0.0094 1.1248 Ca 0.2439 1.0995 Ba 0.0000 NaN Fe 0.0001 1.2568 Mn 0.0003 1.2788 iteration : 3 Analysis no. 85 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6946 0.024532 0.6946 0.5544 Mg 0.7695 0.016775 0.7695 0.5810 Sr 0.2600 0.013594 0.2600 0.0544 P 0.8366 0.034043 0.8366 0.4956 K 0.2401 0.011793 0.2401 0.1127 Cl 1.0597 0.022722 1.0597 0.5485 Ca 26.8154 0.130308 26.8154 12.2769 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0125 0.013929 0.0125 0.0041 Mn 0.0377 0.020589 0.0377 0.0126 C 15.5200 15.5200 23.7108 O 53.7540 53.7540 61.6490 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 86 x= -12892.0 y= 2906.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 24.4 4.5 3.6 6.73 0.0266 4.5 0.0287 Mg 59.2 2.9 2.5 23.51 0.0316 2.9 0.0110 Sr 27.0 3.0 14.3 1.89 0.0018 3.1 0.0396 P 44.2 3.4 2.4 18.81 0.0535 3.4 0.0393 K 30.0 4.1 5.1 5.88 0.0228 4.1 0.0189 Cl 74.8 2.1 2.2 34.00 0.0159 2.1 0.0226 Ca 2788.4 0.4 17.7 157.98 0.6104 0.5 0.0334 Ba 8.0 5.6 10.8 0.74 0.0000 5.6 0.0000 Fe 4.1 7.8 3.3 1.23 0.0004 7.8 0.0556 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0626 Elt. k-ratio Correc. Na 0.0013 2.3296 Mg 0.0023 1.7013 Sr 0.0011 1.3801 P 0.0084 1.2016 K 0.0020 1.0523 Cl 0.0089 1.1295 Ca 0.2215 1.1034 Ba 0.0000 NaN Fe 0.0002 1.2609 Mn 0.0001 1.2821 iteration : 2 Analysis no. 86 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3094 0.017675 0.3094 0.2411 Mg 0.3889 0.012110 0.3889 0.2866 Sr 0.1542 0.012337 0.1542 0.0315 P 1.0074 0.037034 1.0074 0.5827 K 0.2129 0.011347 0.2129 0.0976 Cl 1.0001 0.022152 1.0001 0.5053 Ca 24.4428 0.122964 24.4428 10.9251 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0259 0.014368 0.0259 0.0083 Mn 0.0160 0.019659 0.0160 0.0052 C 16.6917 16.6917 24.8955 O 55.7506 55.7506 62.4211 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 87 x= -12891.0 y= 2910.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 50.4 3.1 3.6 13.88 0.0599 3.2 0.0285 Mg 144.4 1.9 2.5 57.36 0.0790 1.9 0.0110 Sr 39.6 2.5 14.3 2.77 0.0036 2.5 0.0396 P 47.5 3.2 2.4 20.22 0.0577 3.3 0.0393 K 31.5 4.0 5.1 6.18 0.0242 4.0 0.0188 Cl 81.8 2.0 2.2 37.16 0.0174 2.0 0.0225 Ca 3103.8 0.4 17.7 175.84 0.6799 0.5 0.0333 Ba 10.3 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0554 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0624 Elt. k-ratio Correc. Na 0.0030 2.3108 Mg 0.0057 1.6975 Sr 0.0022 1.3804 P 0.0090 1.2018 K 0.0021 1.0444 Cl 0.0097 1.1258 Ca 0.2468 1.0991 Ba 0.0000 NaN Fe 0.0000 1.2558 Mn 0.0001 1.2778 iteration : 3 Analysis no. 87 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6905 0.024431 0.6905 0.5545 Mg 0.9713 0.018793 0.9713 0.7378 Sr 0.3076 0.014120 0.3076 0.0648 P 1.0872 0.038363 1.0872 0.6480 K 0.2241 0.011503 0.2241 0.1058 Cl 1.0922 0.023064 1.0922 0.5687 Ca 27.1227 0.131257 27.1227 12.4929 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0058 0.013717 0.0058 0.0019 Mn 0.0178 0.019679 0.0178 0.0060 C 15.1485 15.1485 23.2835 O 53.3322 53.3322 61.5361 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 88 x= -12891.0 y= 2915.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 15.1 5.7 3.6 4.16 0.0147 5.8 0.0288 Mg 49.4 3.2 2.5 19.60 0.0261 3.2 0.0110 Sr 22.0 3.4 14.3 1.54 0.0011 3.4 0.0397 P 34.5 3.8 2.4 14.66 0.0410 3.8 0.0394 K 24.9 4.5 5.1 4.88 0.0181 4.5 0.0190 Cl 68.5 2.2 2.2 31.12 0.0145 2.2 0.0227 Ca 2580.6 0.4 17.7 146.20 0.5648 0.5 0.0335 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0558 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0627 Elt. k-ratio Correc. Na 0.0007 2.3368 Mg 0.0019 1.7033 Sr 0.0007 1.3828 P 0.0064 1.2038 K 0.0016 1.0578 Cl 0.0081 1.1324 Ca 0.2050 1.1062 Ba 0.0000 NaN Fe 0.0000 1.2642 Mn 0.0001 1.2849 iteration : 2 Analysis no. 88 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1715 0.014477 0.1715 0.1311 Mg 0.3218 0.011107 0.3218 0.2327 Sr 0.0943 0.011595 0.0943 0.0189 P 0.7743 0.032927 0.7743 0.4395 K 0.1703 0.010543 0.1703 0.0765 Cl 0.9153 0.021273 0.9153 0.4539 Ca 22.6719 0.117391 22.6719 9.9438 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013683 0.0017 0.0005 Mn 0.0106 0.019453 0.0106 0.0034 C 17.6565 17.6565 25.8415 O 57.2118 57.2118 62.8581 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 89 x= -12890.0 y= 2919.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 35.3 3.8 3.6 9.72 0.0405 3.8 0.0286 Mg 122.0 2.0 2.5 48.45 0.0666 2.0 0.0110 Sr 32.6 2.8 14.3 2.28 0.0026 2.8 0.0396 P 43.5 3.4 2.4 18.51 0.0526 3.4 0.0393 K 33.1 3.9 5.1 6.48 0.0256 3.9 0.0187 Cl 76.8 2.1 2.2 34.90 0.0163 2.1 0.0225 Ca 3128.3 0.4 17.7 177.23 0.6854 0.5 0.0333 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 4.0 7.9 3.3 1.20 0.0004 7.9 0.0555 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0624 Elt. k-ratio Correc. Na 0.0020 2.3192 Mg 0.0048 1.6978 Sr 0.0016 1.3794 P 0.0082 1.2002 K 0.0023 1.0420 Cl 0.0091 1.1241 Ca 0.2487 1.0990 Ba 0.0000 NaN Fe 0.0002 1.2565 Mn 0.0001 1.2785 iteration : 3 Analysis no. 89 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4690 0.020761 0.4690 0.3758 Mg 0.8180 0.017268 0.8180 0.6200 Sr 0.2221 0.013149 0.2221 0.0467 P 0.9895 0.036710 0.9895 0.5885 K 0.2367 0.011719 0.2367 0.1115 Cl 1.0224 0.022331 1.0224 0.5313 Ca 27.3339 0.131909 27.3339 12.5636 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0225 0.014222 0.0225 0.0074 Mn 0.0178 0.019689 0.0178 0.0060 C 15.3121 15.3121 23.4853 O 53.5559 53.5559 61.6638 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 90 x= -12889.0 y= 2923.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 43.9 3.4 3.6 12.09 0.0515 3.4 0.0286 Mg 129.3 2.0 2.5 51.33 0.0706 2.0 0.0110 Sr 41.4 2.5 14.3 2.90 0.0039 2.5 0.0397 P 40.1 3.5 2.4 17.04 0.0482 3.5 0.0394 K 31.0 4.0 5.1 6.07 0.0237 4.0 0.0189 Cl 82.1 2.0 2.2 37.31 0.0175 2.0 0.0226 Ca 2946.7 0.4 17.7 166.94 0.6455 0.5 0.0334 Ba 11.5 4.7 10.8 1.07 0.0005 4.7 0.0741 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0555 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0625 Elt. k-ratio Correc. Na 0.0026 2.3154 Mg 0.0051 1.6988 Sr 0.0024 1.3817 P 0.0076 1.2035 K 0.0021 1.0488 Cl 0.0097 1.1278 Ca 0.2343 1.1010 Ba 0.0001 1.5351 Fe 0.0001 1.2577 Mn 0.0001 1.2794 iteration : 3 Analysis no. 90 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5957 0.022941 0.5957 0.4722 Mg 0.8684 0.017791 0.8684 0.6511 Sr 0.3293 0.014367 0.3293 0.0685 P 0.9093 0.035381 0.9093 0.5349 K 0.2204 0.011466 0.2204 0.1027 Cl 1.0991 0.023159 1.0991 0.5649 Ca 25.7932 0.127170 25.7932 11.7268 Ba 0.0201 0.019366 0.0201 0.0027 Fe 0.0159 0.014043 0.0159 0.0052 Mn 0.0124 0.019456 0.0124 0.0041 C 15.8338 15.8338 24.0220 O 54.3023 54.3023 61.8448 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 91 x= -12888.0 y= 2927.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 42.9 3.4 3.6 11.83 0.0503 3.4 0.0286 Mg 110.0 2.1 2.5 43.70 0.0599 2.2 0.0110 Sr 32.8 2.8 14.3 2.29 0.0026 2.8 0.0397 P 40.4 3.5 2.4 17.19 0.0486 3.5 0.0393 K 33.2 3.9 5.1 6.51 0.0258 3.9 0.0189 Cl 88.7 1.9 2.2 40.33 0.0190 1.9 0.0226 Ca 2953.5 0.4 17.7 167.33 0.6470 0.5 0.0334 Ba 10.2 4.9 10.8 0.95 0.0000 4.9 0.0000 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0556 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0625 Elt. k-ratio Correc. Na 0.0025 2.3181 Mg 0.0043 1.6998 Sr 0.0016 1.3808 P 0.0076 1.2018 K 0.0023 1.0484 Cl 0.0106 1.1269 Ca 0.2348 1.1012 Ba 0.0000 NaN Fe 0.0001 1.2580 Mn 0.0002 1.2797 iteration : 3 Analysis no. 91 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5823 0.022732 0.5823 0.4613 Mg 0.7372 0.016422 0.7372 0.5523 Sr 0.2245 0.013190 0.2245 0.0467 P 0.9164 0.035478 0.9164 0.5388 K 0.2395 0.011816 0.2395 0.1116 Cl 1.1894 0.024041 1.1894 0.6110 Ca 25.8553 0.127371 25.8553 11.7478 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0175 0.014095 0.0175 0.0057 Mn 0.0269 0.020125 0.0269 0.0089 C 15.8789 15.8789 24.0755 O 54.3320 54.3320 61.8404 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 92 x= -12887.0 y= 2931.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 56.0 3.0 3.6 15.44 0.0671 3.0 0.0285 Mg 138.6 1.9 2.5 55.05 0.0759 1.9 0.0110 Sr 39.0 2.5 14.3 2.73 0.0035 2.5 0.0398 P 37.3 3.7 2.4 15.87 0.0447 3.7 0.0395 K 34.2 3.8 5.1 6.71 0.0267 3.8 0.0189 Cl 80.9 2.0 2.2 36.75 0.0172 2.0 0.0226 Ca 2870.0 0.4 17.7 162.60 0.6288 0.5 0.0334 Ba 10.5 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0556 Mn 2.7 13.6 2.7 1.00 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0034 2.3126 Mg 0.0055 1.7009 Sr 0.0022 1.3839 P 0.0070 1.2050 K 0.0024 1.0512 Cl 0.0096 1.1292 Ca 0.2282 1.1021 Ba 0.0000 NaN Fe 0.0001 1.2585 Mn 0.0000 NaN iteration : 3 Analysis no. 92 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7751 0.025737 0.7751 0.6112 Mg 0.9341 0.018457 0.9341 0.6967 Sr 0.3013 0.014084 0.3013 0.0623 P 0.8443 0.034248 0.8443 0.4941 K 0.2488 0.012008 0.2488 0.1154 Cl 1.0838 0.023023 1.0838 0.5542 Ca 25.1507 0.125196 25.1507 11.3757 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0084 0.013832 0.0084 0.0027 Mn 0.0000 0.000000 0.0000 0.0000 C 16.0402 16.0402 24.2096 O 54.6134 54.6134 61.8781 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 93 x= -12886.0 y= 2936.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 21.7 4.8 3.6 5.97 0.0231 4.8 0.0287 Mg 90.4 2.3 2.5 35.91 0.0490 2.4 0.0110 Sr 23.3 3.3 14.3 1.63 0.0013 3.3 0.0398 P 46.3 3.3 2.4 19.70 0.0562 3.3 0.0395 K 27.8 4.2 5.1 5.44 0.0208 4.3 0.0192 Cl 76.0 2.1 2.2 34.54 0.0162 2.1 0.0228 Ca 2451.8 0.5 17.7 138.90 0.5366 0.5 0.0336 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.0 9.2 3.3 0.90 0.0000 9.2 0.0000 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0628 Elt. k-ratio Correc. Na 0.0012 2.3274 Mg 0.0035 1.7004 Sr 0.0008 1.3848 P 0.0088 1.2059 K 0.0018 1.0647 Cl 0.0090 1.1366 Ca 0.1947 1.1079 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2850 iteration : 2 Analysis no. 93 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2684 0.016773 0.2684 0.2045 Mg 0.6030 0.014904 0.6030 0.4346 Sr 0.1100 0.011819 0.1100 0.0220 P 1.0624 0.038035 1.0624 0.6008 K 0.1961 0.011111 0.1961 0.0879 Cl 1.0232 0.022476 1.0232 0.5056 Ca 21.5741 0.113897 21.5741 9.4288 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0088 0.019375 0.0088 0.0028 C 17.6975 17.6975 25.8098 O 57.4565 57.4565 62.9033 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 94 x= -12885.0 y= 2940.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 51.4 3.1 3.6 14.16 0.0612 3.1 0.0286 Mg 129.0 2.0 2.5 51.23 0.0705 2.0 0.0110 Sr 32.8 2.8 14.3 2.29 0.0026 2.8 0.0400 P 44.4 3.4 2.4 18.87 0.0537 3.4 0.0398 K 22.7 4.7 5.1 4.44 0.0161 4.7 0.0196 Cl 94.8 1.9 2.2 43.08 0.0203 1.9 0.0230 Ca 1904.8 0.5 17.7 107.91 0.4159 0.6 0.0338 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 2.8 13.3 2.7 1.03 0.0001 13.4 0.0629 Elt. k-ratio Correc. Na 0.0031 2.3140 Mg 0.0051 1.7033 Sr 0.0016 1.3929 P 0.0084 1.2147 K 0.0014 1.0871 Cl 0.0113 1.1487 Ca 0.1510 1.1149 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2882 iteration : 2 Analysis no. 94 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7065 0.024705 0.7065 0.5217 Mg 0.8692 0.017823 0.8692 0.6070 Sr 0.2265 0.013308 0.2265 0.0439 P 1.0226 0.037519 1.0226 0.5604 K 0.1551 0.010422 0.1551 0.0674 Cl 1.2975 0.025323 1.2975 0.6212 Ca 16.8303 0.098171 16.8303 7.1279 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0033 0.019163 0.0033 0.0010 C 19.1720 19.1720 27.0949 O 59.7169 59.7169 63.3546 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 95 x= -12884.0 y= 2944.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 11.5 6.6 3.6 3.17 0.0101 6.6 0.0290 Mg 7.7 8.1 2.5 3.06 0.0029 8.1 0.0111 Sr 11.2 4.7 14.3 0.78 0.0000 4.7 0.0000 P 1.7 17.4 2.4 0.70 0.0000 17.4 0.0000 K 4.5 10.6 5.1 0.87 0.0000 10.6 0.0000 Cl 158.0 1.5 2.2 71.82 0.0342 1.5 0.0238 Ca 22.9 4.7 17.7 1.30 0.0012 4.7 0.0346 Ba 6.6 6.1 10.8 0.61 0.0000 6.2 0.0000 Fe 1.5 12.8 3.3 0.46 0.0000 12.8 0.0000 Mn 1.1 21.3 2.7 0.41 0.0000 21.3 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3466 Mg 0.0002 1.7152 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0190 1.1848 Ca 0.0004 1.1424 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 95 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1182 0.013066 0.1182 0.0765 Mg 0.0359 0.004948 0.0359 0.0219 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 2.2526 0.033693 2.2526 0.9451 Ca 0.0480 0.013015 0.0480 0.0178 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7369 26.7369 33.1111 O 70.8085 70.8085 65.8276 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 96 x= -12883.0 y= 2948.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 13.2 6.1 3.6 3.64 0.0123 6.2 0.0291 Mg 10.4 6.9 2.5 4.13 0.0044 6.9 0.0112 Sr 12.2 4.5 14.3 0.85 0.0000 4.5 0.0000 P 1.2 20.4 2.4 0.51 0.0000 20.4 0.0000 K 4.8 10.2 5.1 0.94 0.0000 10.2 0.0000 Cl 69.2 2.2 2.2 31.44 0.0147 2.2 0.0238 Ca 20.8 4.9 17.7 1.18 0.0007 4.9 0.0346 Ba 6.6 6.2 10.8 0.61 0.0000 6.2 0.0000 Fe 1.7 12.0 3.3 0.52 0.0000 12.0 0.0000 Mn 1.7 17.1 2.7 0.63 0.0000 17.2 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3599 Mg 0.0003 1.7235 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0082 1.1875 Ca 0.0002 1.1416 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 96 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1445 0.013858 0.1445 0.0928 Mg 0.0548 0.005590 0.0548 0.0333 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.9703 0.022426 0.9703 0.4041 Ca 0.0283 0.012654 0.0283 0.0104 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9971 26.9971 33.1904 O 71.8049 71.8049 66.2689 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 97 x= -12883.0 y= 2952.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 8.5 7.7 3.6 2.33 0.0062 7.7 0.0292 Mg 11.8 6.5 2.5 4.67 0.0051 6.5 0.0112 Sr 10.5 4.9 14.3 0.73 0.0000 4.9 0.0000 P 1.8 16.6 2.4 0.77 0.0000 16.7 0.0000 K 5.8 9.3 5.1 1.14 0.0006 9.3 0.0210 Cl 55.0 2.5 2.2 24.98 0.0116 2.5 0.0238 Ca 23.4 4.6 17.7 1.33 0.0013 4.6 0.0346 Ba 6.3 6.3 10.8 0.59 0.0000 6.3 0.0000 Fe 1.7 12.0 3.3 0.52 0.0000 12.0 0.0000 Mn 1.2 20.4 2.7 0.44 0.0000 20.4 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3631 Mg 0.0004 1.7239 Sr 0.0000 NaN P 0.0000 NaN K 0.0001 1.1674 Cl 0.0064 1.1878 Ca 0.0005 1.1415 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 97 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0729 0.011751 0.0729 0.0468 Mg 0.0642 0.005878 0.0642 0.0390 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0066 0.007008 0.0066 0.0025 Cl 0.7647 0.020061 0.7647 0.3181 Ca 0.0525 0.013084 0.0525 0.0193 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0513 27.0513 33.2168 O 71.9878 71.9878 66.3575 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 98 x= -12882.0 y= 2956.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 10.8 6.8 3.6 2.98 0.0092 6.8 0.0291 Mg 11.4 6.6 2.5 4.51 0.0049 6.6 0.0111 Sr 9.9 5.0 14.3 0.69 0.0000 5.0 0.0000 P 1.6 17.9 2.4 0.66 0.0000 18.0 0.0000 K 5.1 9.9 5.1 1.00 0.0000 9.9 NaN Cl 99.2 1.8 2.2 45.08 0.0213 1.8 0.0238 Ca 20.5 4.9 17.7 1.16 0.0006 4.9 0.0346 Ba 6.9 6.0 10.8 0.64 0.0000 6.0 0.0000 Fe 2.1 11.0 3.3 0.63 0.0000 11.0 0.0000 Mn 1.1 21.8 2.7 0.39 0.0000 21.8 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3556 Mg 0.0004 1.7203 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0118 1.1866 Ca 0.0002 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 98 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1081 0.012809 0.1081 0.0696 Mg 0.0613 0.005783 0.0613 0.0373 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.4044 0.026759 1.4044 0.5863 Ca 0.0260 0.012619 0.0260 0.0096 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9167 26.9167 33.1695 O 71.4834 71.4834 66.1276 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 99 x= -12881.0 y= 2961.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 12.1 6.4 3.6 3.32 0.0108 6.5 0.0292 Mg 12.4 6.4 2.5 4.90 0.0055 6.4 0.0112 Sr 12.3 4.5 14.3 0.86 0.0000 4.5 0.0000 P 1.5 18.6 2.4 0.62 0.0000 18.6 0.0000 K 4.6 10.4 5.1 0.90 0.0000 10.4 0.0000 Cl 46.4 2.7 2.2 21.10 0.0097 2.7 0.0238 Ca 22.1 4.8 17.7 1.25 0.0010 4.8 0.0346 Ba 6.5 6.2 10.8 0.60 0.0000 6.2 0.0000 Fe 1.7 12.2 3.3 0.51 0.0000 12.2 0.0000 Mn 1.8 16.6 2.7 0.66 0.0000 16.7 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3635 Mg 0.0004 1.7253 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0054 1.1882 Ca 0.0004 1.1414 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 99 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1274 0.013401 0.1274 0.0817 Mg 0.0685 0.006007 0.0685 0.0415 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.6413 0.018504 0.6413 0.2666 Ca 0.0402 0.012870 0.0402 0.0148 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0623 27.0623 33.2105 O 72.0604 72.0604 66.3849 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 100 x= -12880.0 y= 2965.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 14.1 6.0 3.6 3.87 0.0134 6.0 0.0289 Mg 13.2 6.2 2.5 5.22 0.0059 6.2 0.0111 Sr 11.1 4.7 14.3 0.78 0.0000 4.7 0.0000 P 2.0 15.8 2.4 0.85 0.0000 15.8 0.0000 K 6.4 8.9 5.1 1.25 0.0011 8.9 0.0211 Cl 166.1 1.4 2.2 75.51 0.0359 1.4 0.0238 Ca 23.0 4.7 17.7 1.30 0.0012 4.7 0.0346 Ba 7.0 6.0 10.8 0.65 0.0000 6.0 0.0000 Fe 1.8 11.7 3.3 0.55 0.0000 11.7 0.0000 Mn 1.8 16.9 2.7 0.65 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3441 Mg 0.0004 1.7146 Sr 0.0000 NaN P 0.0000 NaN K 0.0001 1.1698 Cl 0.0200 1.1846 Ca 0.0004 1.1424 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 100 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1563 0.014114 0.1563 0.1013 Mg 0.0736 0.006128 0.0736 0.0451 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0119 0.007199 0.0119 0.0045 Cl 2.3697 0.034548 2.3697 0.9953 Ca 0.0485 0.013025 0.0485 0.0180 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.6770 26.6770 33.0725 O 70.6631 70.6631 65.7633 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 101 x= -12879.0 y= 2969.0 z= -278. carb2 trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 12.4 6.3 3.6 3.42 0.0112 6.4 0.0291 Mg 8.6 7.6 2.5 3.40 0.0034 7.7 0.0112 Sr 11.1 4.7 14.3 0.78 0.0000 4.8 0.0000 P 2.0 16.0 2.4 0.83 0.0000 16.0 0.0000 K 5.3 9.7 5.1 1.04 0.0002 9.7 0.0210 Cl 66.0 2.2 2.2 30.02 0.0140 2.2 0.0238 Ca 15.0 5.8 17.7 0.85 0.0000 5.8 0.0000 Ba 6.1 6.4 10.8 0.57 0.0000 6.4 0.0000 Fe 2.1 10.9 3.3 0.64 0.0000 10.9 0.0000 Mn 2.0 16.0 2.7 0.72 0.0000 16.0 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3608 Mg 0.0002 1.7238 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1680 Cl 0.0078 1.1876 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 101 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1325 0.013533 0.1325 0.0851 Mg 0.0420 0.005176 0.0420 0.0255 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0019 0.006850 0.0019 0.0007 Cl 0.9253 0.021934 0.9253 0.3852 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0271 27.0271 33.2092 O 71.8712 71.8712 66.2943 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 102 x= -13501.0 y= 2612.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 4.1 11.1 3.6 1.12 0.0005 11.1 0.0292 Mg 6.7 8.7 2.5 2.64 0.0023 8.7 0.0112 Sr 13.2 4.4 14.3 0.92 0.0000 4.4 0.0000 P 1.2 20.8 2.4 0.49 0.0000 20.9 0.0000 K 3.8 11.5 5.1 0.75 0.0000 11.5 0.0000 Cl 59.5 2.4 2.2 27.04 0.0126 2.4 0.0238 Ca 28.6 4.2 17.7 1.62 0.0024 4.2 0.0346 Ba 7.3 5.9 10.8 0.68 0.0000 5.9 0.0000 Fe 2.8 9.4 3.3 0.85 0.0000 9.5 0.0000 Mn 1.8 16.9 2.7 0.65 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0000 2.3640 Mg 0.0002 1.7229 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0070 1.1875 Ca 0.0009 1.1415 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 102 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0064 0.009373 0.0064 0.0041 Mg 0.0287 0.004708 0.0287 0.0174 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.8304 0.020847 0.8304 0.3455 Ca 0.1000 0.013894 0.1000 0.0368 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0619 27.0619 33.2375 O 71.9725 71.9725 66.3586 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 103 x= -13499.0 y= 2616.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 40.1 3.5 3.6 11.06 0.0468 3.5 0.0287 Mg 160.9 1.8 2.5 63.90 0.0883 1.8 0.0110 Sr 42.7 2.4 14.3 2.99 0.0041 2.4 0.0395 P 12.1 6.4 2.4 5.15 0.0125 6.4 0.0390 K 7.9 8.0 5.1 1.54 0.0025 8.0 0.0179 Cl 13.7 4.9 2.2 6.21 0.0025 4.9 0.0220 Ca 4472.7 0.3 17.7 253.40 0.9823 0.4 0.0328 Ba 13.3 4.3 10.8 1.24 0.0016 4.3 0.0745 Fe 4.1 7.8 3.3 1.24 0.0005 7.8 0.0550 Mn 4.3 10.8 2.7 1.57 0.0015 10.8 0.0620 Elt. k-ratio Correc. Na 0.0023 2.3257 Mg 0.0064 1.7001 Sr 0.0025 1.3730 P 0.0020 1.1917 K 0.0002 0.9921 Cl 0.0014 1.0986 Ca 0.3565 1.0809 Ba 0.0004 1.5420 Fe 0.0002 1.2445 Mn 0.0004 1.2692 iteration : 3 Analysis no. 103 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5429 0.022113 0.5429 0.4750 Mg 1.0866 0.019894 1.0866 0.8993 Sr 0.3440 0.014461 0.3440 0.0790 P 0.2330 0.020338 0.2330 0.1513 K 0.0222 0.006493 0.0222 0.0114 Cl 0.1538 0.009757 0.1538 0.0873 Ca 38.5330 0.165040 38.5330 19.3400 Ba 0.0672 0.020234 0.0672 0.0098 Fe 0.0264 0.014218 0.0264 0.0095 Mn 0.0555 0.021230 0.0555 0.0203 C 11.5397 11.5397 19.3271 O 47.3959 47.3959 59.5900 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 104 x= -13498.0 y= 2621.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 52.3 3.1 3.6 14.41 0.0623 3.1 0.0286 Mg 196.1 1.6 2.5 77.85 0.1079 1.6 0.0110 Sr 43.6 2.4 14.3 3.05 0.0042 2.4 0.0395 P 20.5 4.9 2.4 8.72 0.0232 4.9 0.0391 K 8.4 7.7 5.1 1.65 0.0030 7.7 0.0179 Cl 13.3 5.0 2.2 6.03 0.0024 5.0 0.0221 Ca 4419.9 0.3 17.7 250.41 0.9708 0.4 0.0328 Ba 13.0 4.4 10.8 1.21 0.0014 4.4 0.0745 Fe 3.8 8.1 3.3 1.15 0.0003 8.1 0.0550 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0620 Elt. k-ratio Correc. Na 0.0031 2.3174 Mg 0.0078 1.6990 Sr 0.0026 1.3748 P 0.0036 1.1933 K 0.0003 0.9954 Cl 0.0014 1.1012 Ca 0.3523 1.0816 Ba 0.0004 1.5415 Fe 0.0001 1.2444 Mn 0.0002 1.2691 iteration : 3 Analysis no. 104 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7213 0.024958 0.7213 0.6310 Mg 1.3270 0.021989 1.3270 1.0982 Sr 0.3551 0.014594 0.3551 0.0815 P 0.4343 0.025659 0.4343 0.2820 K 0.0267 0.006653 0.0267 0.0137 Cl 0.1488 0.009657 0.1488 0.0844 Ca 38.1073 0.163823 38.1073 19.1237 Ba 0.0587 0.020093 0.0587 0.0086 Fe 0.0165 0.013928 0.0165 0.0060 Mn 0.0213 0.019727 0.0213 0.0078 C 11.4160 11.4160 19.1174 O 47.3671 47.3671 59.5457 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 105 x= -13496.0 y= 2625.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 39.2 3.6 3.6 10.81 0.0456 3.6 0.0285 Mg 259.6 1.4 2.5 103.08 0.1433 1.4 0.0110 Sr 43.7 2.4 14.3 3.06 0.0042 2.4 0.0396 P 33.5 3.9 2.4 14.24 0.0398 3.9 0.0391 K 9.1 7.4 5.1 1.77 0.0036 7.4 0.0180 Cl 14.8 4.7 2.2 6.71 0.0028 4.8 0.0221 Ca 4412.1 0.3 17.7 249.96 0.9690 0.4 0.0328 Ba 13.9 4.2 10.8 1.29 0.0019 4.3 0.0744 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0550 Mn 5.2 9.8 2.7 1.90 0.0024 9.9 0.0620 Elt. k-ratio Correc. Na 0.0023 2.3120 Mg 0.0104 1.6924 Sr 0.0026 1.3757 P 0.0062 1.1940 K 0.0003 0.9980 Cl 0.0015 1.1033 Ca 0.3517 1.0816 Ba 0.0005 1.5407 Fe 0.0001 1.2435 Mn 0.0007 1.2682 iteration : 3 Analysis no. 105 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5264 0.021753 0.5264 0.4627 Mg 1.7556 0.025309 1.7556 1.4598 Sr 0.3568 0.014619 0.3568 0.0823 P 0.7446 0.032225 0.7446 0.4858 K 0.0321 0.006829 0.0321 0.0166 Cl 0.1693 0.010134 0.1693 0.0965 Ca 38.0369 0.163612 38.0369 19.1803 Ba 0.0808 0.020438 0.0808 0.0119 Fe 0.0107 0.013744 0.0107 0.0039 Mn 0.0878 0.022546 0.0878 0.0323 C 11.0918 11.0918 18.6638 O 47.1073 47.1073 59.5041 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 106 x= -13495.0 y= 2629.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 38.1 3.6 3.6 10.49 0.0441 3.6 0.0285 Mg 288.8 1.3 2.5 114.70 0.1596 1.4 0.0109 Sr 45.1 2.4 14.3 3.16 0.0044 2.4 0.0396 P 42.4 3.4 2.4 18.04 0.0512 3.4 0.0391 K 9.9 7.1 5.1 1.93 0.0044 7.1 0.0180 Cl 16.9 4.4 2.2 7.67 0.0032 4.4 0.0222 Ca 4392.6 0.3 17.7 248.86 0.9646 0.4 0.0328 Ba 12.9 4.4 10.8 1.20 0.0013 4.4 0.0744 Fe 4.5 7.5 3.3 1.36 0.0007 7.5 0.0549 Mn 4.7 10.4 2.7 1.72 0.0019 10.4 0.0620 Elt. k-ratio Correc. Na 0.0022 2.3074 Mg 0.0116 1.6894 Sr 0.0027 1.3761 P 0.0080 1.1945 K 0.0004 1.0003 Cl 0.0018 1.1050 Ca 0.3501 1.0820 Ba 0.0004 1.5404 Fe 0.0003 1.2432 Mn 0.0006 1.2679 iteration : 3 Analysis no. 106 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5083 0.021411 0.5083 0.4477 Mg 1.9518 0.026706 1.9518 1.6259 Sr 0.3729 0.014790 0.3729 0.0862 P 0.9593 0.036114 0.9593 0.6270 K 0.0386 0.007035 0.0386 0.0200 Cl 0.1978 0.010759 0.1978 0.1130 Ca 37.8786 0.163158 37.8786 19.1349 Ba 0.0554 0.020023 0.0554 0.0082 Fe 0.0388 0.014559 0.0388 0.0141 Mn 0.0698 0.021809 0.0698 0.0257 C 10.9267 10.9267 18.4191 O 47.0019 47.0019 59.4782 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 107 x= -13493.0 y= 2633.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 39.5 3.6 3.6 10.89 0.0460 3.6 0.0285 Mg 264.8 1.4 2.5 105.15 0.1462 1.4 0.0110 Sr 44.9 2.4 14.3 3.15 0.0044 2.4 0.0396 P 47.3 3.2 2.4 20.13 0.0575 3.3 0.0391 K 11.9 6.5 5.1 2.33 0.0062 6.5 0.0181 Cl 22.3 3.9 2.2 10.14 0.0044 3.9 0.0222 Ca 4314.5 0.3 17.7 244.44 0.9476 0.4 0.0329 Ba 13.8 4.3 10.8 1.28 0.0019 4.3 0.0744 Fe 4.2 7.7 3.3 1.27 0.0005 7.7 0.0550 Mn 4.8 10.2 2.7 1.75 0.0020 10.3 0.0620 Elt. k-ratio Correc. Na 0.0023 2.3076 Mg 0.0106 1.6901 Sr 0.0027 1.3754 P 0.0090 1.1943 K 0.0006 1.0032 Cl 0.0025 1.1064 Ca 0.3439 1.0829 Ba 0.0005 1.5399 Fe 0.0002 1.2437 Mn 0.0006 1.2683 iteration : 3 Analysis no. 107 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5299 0.021792 0.5299 0.4644 Mg 1.7890 0.025541 1.7890 1.4832 Sr 0.3710 0.014766 0.3710 0.0853 P 1.0767 0.038082 1.0767 0.7004 K 0.0555 0.007526 0.0555 0.0286 Cl 0.2715 0.012218 0.2715 0.1543 Ca 37.2424 0.161327 37.2424 18.7240 Ba 0.0795 0.020409 0.0795 0.0117 Fe 0.0297 0.014308 0.0297 0.0107 Mn 0.0734 0.021968 0.0734 0.0269 C 11.1360 11.1360 18.6827 O 47.3454 47.3454 59.6277 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 108 x= -13492.0 y= 2638.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 34.7 3.8 3.6 9.55 0.0398 3.8 0.0286 Mg 208.3 1.5 2.5 82.73 0.1147 1.6 0.0110 Sr 44.5 2.4 14.3 3.12 0.0043 2.4 0.0394 P 49.7 3.2 2.4 21.15 0.0606 3.2 0.0390 K 14.2 5.9 5.1 2.78 0.0083 5.9 0.0181 Cl 34.4 3.1 2.2 15.64 0.0071 3.1 0.0222 Ca 4348.5 0.3 17.7 246.36 0.9551 0.4 0.0328 Ba 14.0 4.2 10.8 1.30 0.0020 4.2 0.0744 Fe 4.6 7.3 3.3 1.40 0.0007 7.4 0.0550 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0620 Elt. k-ratio Correc. Na 0.0020 2.3117 Mg 0.0083 1.6908 Sr 0.0027 1.3717 P 0.0095 1.1916 K 0.0007 1.0026 Cl 0.0039 1.1050 Ca 0.3466 1.0827 Ba 0.0006 1.5402 Fe 0.0004 1.2435 Mn 0.0004 1.2681 iteration : 3 Analysis no. 108 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4591 0.020551 0.4591 0.4030 Mg 1.4045 0.022577 1.4045 1.1664 Sr 0.3649 0.014673 0.3649 0.0841 P 1.1316 0.038924 1.1316 0.7374 K 0.0742 0.008015 0.0742 0.0383 Cl 0.4345 0.014925 0.4345 0.2474 Ca 37.5298 0.162169 37.5298 18.9004 Ba 0.0853 0.020508 0.0853 0.0125 Fe 0.0438 0.014705 0.0438 0.0158 Mn 0.0500 0.020985 0.0500 0.0184 C 11.1549 11.1549 18.7461 O 47.2675 47.2675 59.6302 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 109 x= -13490.0 y= 2642.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 48.7 3.2 3.6 13.42 0.0577 3.2 0.0285 Mg 207.8 1.5 2.5 82.51 0.1144 1.6 0.0110 Sr 43.7 2.4 14.3 3.06 0.0042 2.4 0.0395 P 46.9 3.3 2.4 19.96 0.0570 3.3 0.0391 K 15.1 5.7 5.1 2.96 0.0092 5.8 0.0181 Cl 35.6 3.1 2.2 16.19 0.0073 3.1 0.0222 Ca 4200.0 0.3 17.7 237.95 0.9224 0.4 0.0329 Ba 13.3 4.3 10.8 1.24 0.0016 4.3 0.0744 Fe 3.9 8.0 3.3 1.18 0.0003 8.0 0.0550 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0620 Elt. k-ratio Correc. Na 0.0029 2.3093 Mg 0.0083 1.6937 Sr 0.0026 1.3741 P 0.0089 1.1937 K 0.0008 1.0070 Cl 0.0041 1.1075 Ca 0.3348 1.0845 Ba 0.0004 1.5397 Fe 0.0002 1.2449 Mn 0.0004 1.2693 iteration : 3 Analysis no. 109 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6656 0.024046 0.6656 0.5780 Mg 1.4032 0.022586 1.4032 1.1525 Sr 0.3562 0.014601 0.3562 0.0811 P 1.0666 0.037908 1.0666 0.6874 K 0.0819 0.008237 0.0819 0.0418 Cl 0.4517 0.015204 0.4517 0.2544 Ca 36.3058 0.158622 36.3058 18.0837 Ba 0.0671 0.020209 0.0671 0.0098 Fe 0.0198 0.014033 0.0198 0.0071 Mn 0.0501 0.021006 0.0501 0.0182 C 11.5981 11.5981 19.2774 O 47.9339 47.9339 59.8085 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 110 x= -13489.0 y= 2646.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 44.7 3.3 3.6 12.31 0.0526 3.4 0.0286 Mg 201.1 1.6 2.5 79.86 0.1107 1.6 0.0110 Sr 43.7 2.4 14.3 3.06 0.0042 2.4 0.0395 P 41.6 3.5 2.4 17.68 0.0501 3.5 0.0391 K 15.1 5.8 5.1 2.95 0.0091 5.8 0.0182 Cl 42.5 2.8 2.2 19.32 0.0088 2.8 0.0222 Ca 4137.1 0.3 17.7 234.39 0.9085 0.4 0.0329 Ba 13.2 4.3 10.8 1.23 0.0015 4.4 0.0744 Fe 4.3 7.7 3.3 1.29 0.0005 7.7 0.0551 Mn 4.6 10.5 2.7 1.68 0.0018 10.5 0.0621 Elt. k-ratio Correc. Na 0.0026 2.3116 Mg 0.0080 1.6940 Sr 0.0026 1.3744 P 0.0079 1.1941 K 0.0008 1.0087 Cl 0.0049 1.1078 Ca 0.3297 1.0853 Ba 0.0004 1.5394 Fe 0.0003 1.2456 Mn 0.0005 1.2698 iteration : 3 Analysis no. 110 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6071 0.023117 0.6071 0.5243 Mg 1.3579 0.022216 1.3579 1.1093 Sr 0.3565 0.014608 0.3565 0.0808 P 0.9388 0.035759 0.9388 0.6018 K 0.0817 0.008241 0.0817 0.0415 Cl 0.5452 0.016545 0.5452 0.3054 Ca 35.7851 0.157105 35.7851 17.7279 Ba 0.0645 0.020164 0.0645 0.0093 Fe 0.0314 0.014379 0.0314 0.0112 Mn 0.0663 0.021699 0.0663 0.0240 C 11.8901 11.8901 19.6558 O 48.2754 48.2753 59.9088 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 111 x= -13487.0 y= 2650.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 46.0 3.3 3.6 12.68 0.0543 3.3 0.0285 Mg 219.6 1.5 2.5 87.22 0.1211 1.5 0.0110 Sr 44.7 2.4 14.3 3.13 0.0043 2.4 0.0395 P 44.4 3.4 2.4 18.87 0.0537 3.4 0.0391 K 16.8 5.5 5.1 3.28 0.0107 5.5 0.0181 Cl 34.4 3.1 2.2 15.66 0.0071 3.1 0.0222 Ca 4346.3 0.3 17.7 246.24 0.9547 0.4 0.0329 Ba 13.4 4.3 10.8 1.24 0.0016 4.3 0.0744 Fe 4.3 7.6 3.3 1.31 0.0006 7.6 0.0550 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0620 Elt. k-ratio Correc. Na 0.0027 2.3088 Mg 0.0088 1.6924 Sr 0.0027 1.3731 P 0.0084 1.1925 K 0.0009 1.0025 Cl 0.0039 1.1048 Ca 0.3465 1.0828 Ba 0.0004 1.5403 Fe 0.0003 1.2435 Mn 0.0003 1.2682 iteration : 3 Analysis no. 111 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6263 0.023415 0.6263 0.5498 Mg 1.4832 0.023222 1.4832 1.2316 Sr 0.3680 0.014718 0.3680 0.0848 P 1.0046 0.036857 1.0046 0.6546 K 0.0950 0.008530 0.0950 0.0491 Cl 0.4349 0.014931 0.4349 0.2476 Ca 37.5158 0.162134 37.5158 18.8912 Ba 0.0678 0.020228 0.0678 0.0100 Fe 0.0339 0.014426 0.0339 0.0122 Mn 0.0339 0.020282 0.0339 0.0124 C 11.1492 11.1492 18.7342 O 47.1876 47.1876 59.5226 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 112 x= -13485.0 y= 2655.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 13.5 6.1 3.6 3.71 0.0126 6.1 0.0289 Mg 85.9 2.4 2.5 34.12 0.0465 2.4 0.0110 Sr 25.4 3.1 14.3 1.78 0.0016 3.1 0.0396 P 39.0 3.6 2.4 16.58 0.0468 3.6 0.0392 K 14.2 5.9 5.1 2.77 0.0083 6.0 0.0185 Cl 30.5 3.3 2.2 13.88 0.0062 3.3 0.0224 Ca 3366.7 0.4 17.7 190.74 0.7387 0.5 0.0332 Ba 8.7 5.4 10.8 0.81 0.0000 5.4 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0556 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0625 Elt. k-ratio Correc. Na 0.0006 2.3360 Mg 0.0034 1.7004 Sr 0.0010 1.3774 P 0.0073 1.1975 K 0.0007 1.0284 Cl 0.0035 1.1189 Ca 0.2681 1.0956 Ba 0.0000 NaN Fe 0.0000 1.2563 Mn 0.0002 1.2787 iteration : 3 Analysis no. 112 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1469 0.013829 0.1469 0.1185 Mg 0.5725 0.014542 0.5725 0.4368 Sr 0.1347 0.012085 0.1347 0.0285 P 0.8791 0.034766 0.8791 0.5262 K 0.0757 0.008212 0.0757 0.0359 Cl 0.3871 0.014290 0.3871 0.2025 Ca 29.3701 0.138132 29.3701 13.5864 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0033 0.013662 0.0033 0.0011 Mn 0.0305 0.020291 0.0305 0.0103 C 15.0509 15.0509 23.2331 O 53.3491 53.3491 61.8208 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 113 x= -13484.0 y= 2659.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 13.1 6.2 3.6 3.61 0.0121 6.2 0.0287 Mg 146.7 1.8 2.5 58.27 0.0804 1.9 0.0110 Sr 38.7 2.5 14.3 2.71 0.0035 2.6 0.0395 P 42.7 3.4 2.4 18.15 0.0516 3.4 0.0391 K 15.6 5.7 5.1 3.06 0.0096 5.7 0.0182 Cl 26.3 3.6 2.2 11.97 0.0053 3.6 0.0222 Ca 4062.4 0.4 17.7 230.15 0.8921 0.4 0.0330 Ba 12.3 4.5 10.8 1.14 0.0009 4.5 0.0745 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0552 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0622 Elt. k-ratio Correc. Na 0.0006 2.3261 Mg 0.0058 1.6933 Sr 0.0022 1.3720 P 0.0081 1.1924 K 0.0009 1.0081 Cl 0.0029 1.1080 Ca 0.3238 1.0866 Ba 0.0003 1.5405 Fe 0.0001 1.2480 Mn 0.0003 1.2720 iteration : 3 Analysis no. 113 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1411 0.013629 0.1411 0.1203 Mg 0.9857 0.018918 0.9857 0.7949 Sr 0.2952 0.013930 0.2952 0.0660 P 0.9639 0.036166 0.9639 0.6099 K 0.0861 0.008348 0.0861 0.0432 Cl 0.3265 0.013209 0.3265 0.1805 Ca 35.1795 0.155358 35.1795 17.2031 Ba 0.0404 0.019786 0.0404 0.0058 Fe 0.0174 0.013996 0.0174 0.0061 Mn 0.0376 0.020503 0.0376 0.0134 C 12.5325 12.5325 20.4504 O 49.3941 49.3941 60.5064 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 114 x= -13482.0 y= 2663.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 16.0 5.6 3.6 4.41 0.0159 5.6 0.0287 Mg 172.9 1.7 2.5 68.67 0.0950 1.7 0.0110 Sr 37.4 2.6 14.3 2.62 0.0033 2.6 0.0395 P 43.1 3.4 2.4 18.32 0.0521 3.4 0.0391 K 15.2 5.7 5.1 2.98 0.0093 5.7 0.0182 Cl 33.7 3.1 2.2 15.34 0.0069 3.1 0.0223 Ca 3969.4 0.4 17.7 224.88 0.8716 0.4 0.0330 Ba 10.8 4.8 10.8 1.00 0.0000 4.8 NaN Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0552 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0622 Elt. k-ratio Correc. Na 0.0008 2.3223 Mg 0.0069 1.6920 Sr 0.0020 1.3738 P 0.0082 1.1938 K 0.0008 1.0119 Cl 0.0039 1.1100 Ca 0.3163 1.0879 Ba 0.0000 NaN Fe 0.0001 1.2488 Mn 0.0003 1.2726 iteration : 3 Analysis no. 114 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1839 0.014744 0.1839 0.1560 Mg 1.1639 0.020545 1.1639 0.9335 Sr 0.2795 0.013771 0.2795 0.0622 P 0.9746 0.036371 0.9746 0.6134 K 0.0832 0.008299 0.0832 0.0415 Cl 0.4275 0.014856 0.4275 0.2350 Ca 34.4136 0.153125 34.4136 16.7377 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0075 0.013706 0.0075 0.0026 Mn 0.0412 0.020671 0.0412 0.0146 C 12.7211 12.7211 20.6461 O 49.7041 49.7041 60.5575 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 115 x= -13481.0 y= 2667.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 14.7 5.8 3.6 4.05 0.0142 5.8 0.0288 Mg 127.5 2.0 2.5 50.62 0.0697 2.0 0.0110 Sr 33.7 2.7 14.3 2.36 0.0028 2.7 0.0396 P 44.3 3.4 2.4 18.85 0.0537 3.4 0.0392 K 16.0 5.6 5.1 3.14 0.0100 5.6 0.0184 Cl 30.2 3.3 2.2 13.73 0.0061 3.3 0.0224 Ca 3684.6 0.4 17.7 208.75 0.8089 0.5 0.0331 Ba 7.6 5.7 10.8 0.70 0.0000 5.7 0.0000 Fe 4.0 7.9 3.3 1.21 0.0004 7.9 0.0554 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0624 Elt. k-ratio Correc. Na 0.0007 2.3287 Mg 0.0050 1.6959 Sr 0.0017 1.3750 P 0.0084 1.1955 K 0.0009 1.0198 Cl 0.0034 1.1144 Ca 0.2936 1.0914 Ba 0.0000 NaN Fe 0.0002 1.2521 Mn 0.0003 1.2753 iteration : 3 Analysis no. 115 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1651 0.014286 0.1651 0.1368 Mg 0.8555 0.017653 0.8555 0.6705 Sr 0.2347 0.013274 0.2347 0.0510 P 1.0061 0.036936 1.0061 0.6187 K 0.0905 0.008528 0.0905 0.0441 Cl 0.3811 0.014163 0.3811 0.2048 Ca 32.0410 0.146127 32.0410 15.2280 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0233 0.014215 0.0233 0.0079 Mn 0.0395 0.020638 0.0395 0.0137 C 13.7708 13.7708 21.8395 O 51.3925 51.3925 61.1850 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 116 x= -13479.0 y= 2672.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 14.0 6.0 3.6 3.86 0.0133 6.0 0.0287 Mg 149.5 1.8 2.5 59.38 0.0820 1.9 0.0110 Sr 30.7 2.9 14.3 2.15 0.0023 2.9 0.0396 P 44.4 3.4 2.4 18.87 0.0537 3.4 0.0392 K 14.0 6.0 5.1 2.75 0.0082 6.0 0.0184 Cl 34.2 3.1 2.2 15.56 0.0070 3.1 0.0224 Ca 3665.0 0.4 17.7 207.64 0.8045 0.5 0.0331 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 4.0 7.9 3.3 1.20 0.0004 7.9 0.0554 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0624 Elt. k-ratio Correc. Na 0.0007 2.3268 Mg 0.0059 1.6947 Sr 0.0014 1.3761 P 0.0084 1.1959 K 0.0007 1.0208 Cl 0.0039 1.1149 Ca 0.2920 1.0918 Ba 0.0000 NaN Fe 0.0002 1.2523 Mn 0.0003 1.2754 iteration : 3 Analysis no. 116 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1545 0.013997 0.1545 0.1279 Mg 1.0058 0.019118 1.0058 0.7877 Sr 0.1988 0.012861 0.1988 0.0432 P 1.0076 0.036967 1.0076 0.6192 K 0.0739 0.008120 0.0739 0.0360 Cl 0.4362 0.015028 0.4362 0.2342 Ca 31.8770 0.145639 31.8770 15.1386 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0225 0.014192 0.0225 0.0077 Mn 0.0359 0.020480 0.0359 0.0124 C 13.7753 13.7753 21.8302 O 51.4126 51.4126 61.1629 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 117 x= -13478.0 y= 2676.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 13.7 6.0 3.6 3.76 0.0129 6.1 0.0288 Mg 102.2 2.2 2.5 40.58 0.0556 2.2 0.0110 Sr 28.1 3.0 14.3 1.97 0.0020 3.0 0.0396 P 40.3 3.5 2.4 17.15 0.0486 3.5 0.0392 K 14.2 5.9 5.1 2.77 0.0083 6.0 0.0185 Cl 36.1 3.0 2.2 16.41 0.0074 3.0 0.0224 Ca 3480.6 0.4 17.7 197.19 0.7638 0.5 0.0332 Ba 10.2 4.9 10.8 0.95 0.0000 5.0 0.0000 Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0555 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0625 Elt. k-ratio Correc. Na 0.0006 2.3327 Mg 0.0040 1.6983 Sr 0.0012 1.3764 P 0.0076 1.1966 K 0.0007 1.0257 Cl 0.0041 1.1171 Ca 0.2772 1.0941 Ba 0.0000 NaN Fe 0.0001 1.2547 Mn 0.0003 1.2774 iteration : 3 Analysis no. 117 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1497 0.013892 0.1497 0.1219 Mg 0.6834 0.015828 0.6834 0.5265 Sr 0.1679 0.012491 0.1679 0.0359 P 0.9109 0.035316 0.9109 0.5507 K 0.0755 0.008191 0.0755 0.0362 Cl 0.4625 0.015440 0.4625 0.2443 Ca 30.3308 0.141025 30.3308 14.1721 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0075 0.013772 0.0075 0.0025 Mn 0.0341 0.020432 0.0341 0.0116 C 14.5836 14.5836 22.7386 O 52.5940 52.5940 61.5596 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 118 x= -13476.0 y= 2680.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 15.6 5.7 3.6 4.29 0.0153 5.7 0.0287 Mg 126.2 2.0 2.5 50.12 0.0690 2.0 0.0110 Sr 33.7 2.7 14.3 2.36 0.0028 2.7 0.0395 P 44.5 3.3 2.4 18.94 0.0539 3.4 0.0392 K 16.0 5.6 5.1 3.14 0.0100 5.6 0.0184 Cl 37.3 3.0 2.2 16.94 0.0077 3.0 0.0223 Ca 3731.9 0.4 17.7 211.43 0.8192 0.5 0.0331 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0553 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0623 Elt. k-ratio Correc. Na 0.0008 2.3271 Mg 0.0050 1.6951 Sr 0.0017 1.3741 P 0.0085 1.1947 K 0.0009 1.0189 Cl 0.0043 1.1135 Ca 0.2973 1.0910 Ba 0.0000 NaN Fe 0.0001 1.2516 Mn 0.0002 1.2748 iteration : 3 Analysis no. 118 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1776 0.014603 0.1776 0.1477 Mg 0.8464 0.017555 0.8464 0.6659 Sr 0.2348 0.013267 0.2348 0.0512 P 1.0100 0.036986 1.0100 0.6236 K 0.0904 0.008519 0.0904 0.0442 Cl 0.4769 0.015623 0.4769 0.2572 Ca 32.4366 0.147300 32.4366 15.4758 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0083 0.013762 0.0083 0.0028 Mn 0.0232 0.019903 0.0232 0.0081 C 13.6075 13.6075 21.6644 O 51.0883 51.0883 61.0590 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 119 x= -13475.0 y= 2684.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 16.0 5.6 3.6 4.41 0.0159 5.6 0.0288 Mg 110.1 2.1 2.5 43.72 0.0600 2.2 0.0110 Sr 26.7 3.1 14.3 1.87 0.0018 3.1 0.0397 P 41.1 3.5 2.4 17.49 0.0496 3.5 0.0393 K 17.1 5.4 5.1 3.34 0.0110 5.4 0.0186 Cl 37.5 3.0 2.2 17.07 0.0078 3.0 0.0225 Ca 3296.1 0.4 17.7 186.74 0.7231 0.5 0.0333 Ba 8.0 5.6 10.8 0.75 0.0000 5.6 0.0000 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0556 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0625 Elt. k-ratio Correc. Na 0.0008 2.3316 Mg 0.0043 1.6989 Sr 0.0011 1.3787 P 0.0078 1.1987 K 0.0010 1.0321 Cl 0.0043 1.1207 Ca 0.2624 1.0965 Ba 0.0000 NaN Fe 0.0002 1.2565 Mn 0.0001 1.2788 iteration : 3 Analysis no. 119 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1847 0.014803 0.1847 0.1486 Mg 0.7378 0.016432 0.7378 0.5615 Sr 0.1509 0.012298 0.1509 0.0319 P 0.9317 0.035713 0.9317 0.5564 K 0.1003 0.008842 0.1003 0.0475 Cl 0.4836 0.015777 0.4836 0.2523 Ca 28.7754 0.136336 28.7754 13.2798 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0209 0.014190 0.0209 0.0069 Mn 0.0160 0.019632 0.0160 0.0054 C 15.1216 15.1216 23.2872 O 53.4771 53.4771 61.8226 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 120 x= -13473.0 y= 2689.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.6 5.3 3.6 4.84 0.0179 5.3 0.0287 Mg 136.2 1.9 2.5 54.08 0.0745 1.9 0.0110 Sr 39.9 2.5 14.3 2.79 0.0036 2.5 0.0395 P 39.3 3.6 2.4 16.73 0.0473 3.6 0.0392 K 16.9 5.4 5.1 3.30 0.0108 5.5 0.0183 Cl 34.7 3.1 2.2 15.79 0.0071 3.1 0.0223 Ca 3792.6 0.4 17.7 214.86 0.8326 0.5 0.0331 Ba 12.5 4.5 10.8 1.17 0.0011 4.5 0.0744 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0553 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0623 Elt. k-ratio Correc. Na 0.0009 2.3265 Mg 0.0054 1.6954 Sr 0.0023 1.3744 P 0.0074 1.1952 K 0.0010 1.0168 Cl 0.0040 1.1124 Ca 0.3021 1.0898 Ba 0.0003 1.5391 Fe 0.0002 1.2505 Mn 0.0004 1.2739 iteration : 3 Analysis no. 120 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2073 0.015345 0.2073 0.1734 Mg 0.9147 0.018241 0.9147 0.7235 Sr 0.3099 0.014109 0.3099 0.0680 P 0.8858 0.034847 0.8858 0.5498 K 0.0972 0.008671 0.0972 0.0478 Cl 0.4419 0.015094 0.4419 0.2397 Ca 32.9287 0.148733 32.9287 15.7954 Ba 0.0462 0.019864 0.0462 0.0065 Fe 0.0208 0.014120 0.0208 0.0071 Mn 0.0503 0.021082 0.0503 0.0176 C 13.4084 13.4084 21.4626 O 50.6888 50.6888 60.9086 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 121 x= -13471.0 y= 2693.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 18.5 5.2 3.6 5.09 0.0190 5.2 0.0289 Mg 72.5 2.6 2.5 28.80 0.0390 2.6 0.0110 Sr 20.3 3.5 14.3 1.42 0.0009 3.5 0.0397 P 40.0 3.5 2.4 17.00 0.0481 3.6 0.0393 K 16.7 5.5 5.1 3.26 0.0106 5.5 0.0187 Cl 32.0 3.2 2.2 14.55 0.0065 3.2 0.0226 Ca 3069.8 0.4 17.7 173.91 0.6732 0.5 0.0334 Ba 7.1 5.9 10.8 0.66 0.0000 5.9 0.0000 Fe 4.1 7.8 3.3 1.24 0.0005 7.8 0.0557 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0626 Elt. k-ratio Correc. Na 0.0009 2.3378 Mg 0.0028 1.7037 Sr 0.0005 1.3804 P 0.0075 1.2002 K 0.0009 1.0383 Cl 0.0036 1.1242 Ca 0.2443 1.0993 Ba 0.0000 NaN Fe 0.0002 1.2594 Mn 0.0004 1.2811 iteration : 2 Analysis no. 121 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2218 0.015748 0.2218 0.1752 Mg 0.4814 0.013404 0.4814 0.3597 Sr 0.0735 0.011311 0.0735 0.0152 P 0.9052 0.035273 0.9052 0.5307 K 0.0976 0.008815 0.0976 0.0453 Cl 0.4092 0.014679 0.4092 0.2096 Ca 26.8590 0.130492 26.8590 12.1684 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0268 0.014394 0.0268 0.0087 Mn 0.0451 0.020970 0.0451 0.0149 C 16.0016 16.0016 24.1911 O 54.8788 54.8788 62.2812 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 122 x= -13470.0 y= 2697.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 13.4 6.1 3.6 3.69 0.0125 6.1 0.0288 Mg 99.3 2.2 2.5 39.45 0.0540 2.3 0.0110 Sr 31.6 2.8 14.3 2.21 0.0025 2.8 0.0396 P 36.9 3.7 2.4 15.70 0.0442 3.7 0.0392 K 14.7 5.8 5.1 2.88 0.0088 5.8 0.0184 Cl 36.3 3.0 2.2 16.49 0.0075 3.0 0.0224 Ca 3570.4 0.4 17.7 202.28 0.7837 0.5 0.0332 Ba 10.0 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0554 Mn 4.5 10.5 2.7 1.66 0.0018 10.5 0.0624 Elt. k-ratio Correc. Na 0.0006 2.3335 Mg 0.0039 1.6985 Sr 0.0015 1.3755 P 0.0069 1.1959 K 0.0008 1.0225 Cl 0.0042 1.1152 Ca 0.2844 1.0928 Ba 0.0000 NaN Fe 0.0002 1.2536 Mn 0.0005 1.2765 iteration : 3 Analysis no. 122 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1460 0.013796 0.1460 0.1197 Mg 0.6639 0.015609 0.6639 0.5149 Sr 0.2096 0.012985 0.2096 0.0451 P 0.8289 0.033837 0.8289 0.5045 K 0.0799 0.008282 0.0799 0.0385 Cl 0.4640 0.015448 0.4640 0.2467 Ca 31.0828 0.143271 31.0828 14.6190 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0208 0.014159 0.0208 0.0070 Mn 0.0649 0.021743 0.0649 0.0223 C 14.3272 14.3272 22.4857 O 52.1120 52.1120 61.3966 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 123 x= -13468.0 y= 2701.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 25.2 4.4 3.6 6.95 0.0277 4.5 0.0287 Mg 146.8 1.8 2.5 58.29 0.0804 1.9 0.0110 Sr 39.8 2.5 14.3 2.79 0.0036 2.5 0.0395 P 43.5 3.4 2.4 18.51 0.0526 3.4 0.0391 K 16.7 5.5 5.1 3.27 0.0106 5.5 0.0183 Cl 42.7 2.8 2.2 19.43 0.0089 2.8 0.0223 Ca 3869.7 0.4 17.7 219.23 0.8496 0.4 0.0330 Ba 11.1 4.8 10.8 1.03 0.0002 4.8 0.0744 Fe 4.1 7.8 3.3 1.23 0.0004 7.9 0.0552 Mn 4.4 10.6 2.7 1.62 0.0017 10.7 0.0622 Elt. k-ratio Correc. Na 0.0014 2.3218 Mg 0.0058 1.6945 Sr 0.0022 1.3737 P 0.0083 1.1944 K 0.0009 1.0157 Cl 0.0050 1.1115 Ca 0.3083 1.0890 Ba 0.0001 1.5393 Fe 0.0002 1.2493 Mn 0.0005 1.2729 iteration : 3 Analysis no. 123 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3206 0.017889 0.3206 0.2703 Mg 0.9868 0.018935 0.9868 0.7869 Sr 0.3089 0.014093 0.3089 0.0683 P 0.9858 0.036572 0.9858 0.6168 K 0.0959 0.008633 0.0959 0.0475 Cl 0.5503 0.016645 0.5503 0.3008 Ca 33.5790 0.150664 33.5790 16.2373 Ba 0.0078 0.019227 0.0078 0.0011 Fe 0.0249 0.014230 0.0249 0.0086 Mn 0.0611 0.021527 0.0611 0.0215 C 13.0075 13.0075 20.9888 O 50.0715 50.0715 60.6520 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 124 x= -13467.0 y= 2706.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 12.8 6.2 3.6 3.53 0.0118 6.3 0.0289 Mg 57.4 2.9 2.5 22.80 0.0306 3.0 0.0110 Sr 26.6 3.1 14.3 1.86 0.0018 3.1 0.0396 P 40.1 3.5 2.4 17.07 0.0483 3.5 0.0393 K 12.7 6.3 5.1 2.49 0.0070 6.3 0.0186 Cl 35.9 3.0 2.2 16.31 0.0074 3.0 0.0225 Ca 3226.4 0.4 17.7 182.79 0.7077 0.5 0.0333 Ba 6.7 6.1 10.8 0.62 0.0000 6.1 0.0000 Fe 3.3 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 2.7 13.6 2.7 1.00 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3376 Mg 0.0022 1.7015 Sr 0.0011 1.3772 P 0.0076 1.1981 K 0.0006 1.0333 Cl 0.0041 1.1213 Ca 0.2569 1.0975 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 124 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1373 0.013572 0.1373 0.1095 Mg 0.3770 0.011946 0.3770 0.2846 Sr 0.1492 0.012266 0.1492 0.0312 P 0.9072 0.035273 0.9072 0.5373 K 0.0639 0.007934 0.0639 0.0300 Cl 0.4610 0.015449 0.4610 0.2386 Ca 28.1883 0.134557 28.1883 12.9025 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 15.5721 15.5721 23.7848 O 54.1440 54.1440 62.0816 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 125 x= -13465.0 y= 2710.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 28.4 4.2 3.6 7.83 0.0318 4.2 0.0286 Mg 163.6 1.7 2.5 64.97 0.0898 1.8 0.0110 Sr 36.4 2.6 14.3 2.55 0.0032 2.6 0.0396 P 49.2 3.2 2.4 20.92 0.0599 3.2 0.0392 K 18.0 5.3 5.1 3.52 0.0118 5.3 0.0184 Cl 44.3 2.7 2.2 20.14 0.0092 2.7 0.0224 Ca 3713.1 0.4 17.7 210.36 0.8149 0.5 0.0331 Ba 10.8 4.8 10.8 1.01 0.0000 4.8 0.0744 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0553 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0623 Elt. k-ratio Correc. Na 0.0016 2.3184 Mg 0.0065 1.6940 Sr 0.0020 1.3757 P 0.0094 1.1960 K 0.0010 1.0215 Cl 0.0051 1.1151 Ca 0.2957 1.0912 Ba 0.0000 1.5388 Fe 0.0001 1.2508 Mn 0.0002 1.2741 iteration : 3 Analysis no. 125 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3676 0.018833 0.3676 0.3068 Mg 1.1013 0.019994 1.1013 0.8693 Sr 0.2684 0.013659 0.2684 0.0588 P 1.1225 0.038855 1.1225 0.6953 K 0.1068 0.008926 0.1068 0.0524 Cl 0.5733 0.016985 0.5733 0.3102 Ca 32.2711 0.146796 32.2711 15.4482 Ba 0.0020 0.019117 0.0020 0.0003 Fe 0.0150 0.013950 0.0150 0.0051 Mn 0.0286 0.020131 0.0286 0.0100 C 13.3737 13.3737 21.3630 O 50.7699 50.7699 60.8806 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 126 x= -13464.0 y= 2714.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 13.3 6.1 3.6 3.65 0.0123 6.2 0.0288 Mg 83.4 2.4 2.5 33.13 0.0451 2.5 0.0110 Sr 24.7 3.2 14.3 1.73 0.0015 3.2 0.0396 P 47.0 3.3 2.4 19.98 0.0571 3.3 0.0393 K 14.3 5.9 5.1 2.79 0.0084 5.9 0.0187 Cl 39.1 2.9 2.2 17.78 0.0081 2.9 0.0225 Ca 3128.9 0.4 17.7 177.27 0.6861 0.5 0.0333 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0556 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0626 Elt. k-ratio Correc. Na 0.0006 2.3338 Mg 0.0033 1.6998 Sr 0.0009 1.3787 P 0.0089 1.1993 K 0.0007 1.0379 Cl 0.0045 1.1240 Ca 0.2490 1.0987 Ba 0.0000 NaN Fe 0.0001 1.2584 Mn 0.0001 1.2803 iteration : 2 Analysis no. 126 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1437 0.013733 0.1437 0.1142 Mg 0.5551 0.014324 0.5551 0.4172 Sr 0.1260 0.011983 0.1260 0.0263 P 1.0728 0.038105 1.0728 0.6327 K 0.0773 0.008308 0.0773 0.0361 Cl 0.5065 0.016132 0.5065 0.2610 Ca 27.3597 0.132025 27.3597 12.4710 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0084 0.013835 0.0084 0.0027 Mn 0.0124 0.019484 0.0124 0.0041 C 15.6882 15.6882 23.8622 O 54.4501 54.4501 62.1723 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 127 x= -13462.0 y= 2718.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 15.3 5.7 3.6 4.20 0.0149 5.7 0.0287 Mg 111.3 2.1 2.5 44.22 0.0607 2.1 0.0110 Sr 34.6 2.7 14.3 2.42 0.0029 2.7 0.0395 P 59.4 2.9 2.4 25.28 0.0730 2.9 0.0391 K 14.9 5.8 5.1 2.92 0.0090 5.8 0.0184 Cl 44.7 2.7 2.2 20.34 0.0093 2.7 0.0224 Ca 3640.0 0.4 17.7 206.22 0.7988 0.5 0.0331 Ba 10.7 4.8 10.8 0.99 0.0000 4.8 0.0000 Fe 3.5 8.4 3.3 1.06 0.0001 8.5 0.0553 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0623 Elt. k-ratio Correc. Na 0.0007 2.3247 Mg 0.0044 1.6937 Sr 0.0018 1.3729 P 0.0114 1.1943 K 0.0008 1.0238 Cl 0.0052 1.1164 Ca 0.2899 1.0922 Ba 0.0000 NaN Fe 0.0001 1.2518 Mn 0.0004 1.2749 iteration : 3 Analysis no. 127 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1729 0.014471 0.1729 0.1434 Mg 0.7440 0.016472 0.7440 0.5834 Sr 0.2452 0.013375 0.2452 0.0533 P 1.3666 0.042585 1.3666 0.8409 K 0.0816 0.008332 0.0816 0.0398 Cl 0.5799 0.017086 0.5799 0.3117 Ca 31.6642 0.145001 31.6642 15.0570 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0067 0.013712 0.0067 0.0023 Mn 0.0503 0.021098 0.0503 0.0175 C 13.6964 13.6964 21.7332 O 51.3923 51.3923 61.2176 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 128 x= -13461.0 y= 2723.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 21.4 4.8 3.6 5.89 0.0227 4.9 0.0286 Mg 121.2 2.0 2.5 48.11 0.0661 2.1 0.0110 Sr 43.4 2.4 14.3 3.04 0.0042 2.4 0.0395 P 79.7 2.5 2.4 33.92 0.0990 2.5 0.0392 K 15.7 5.6 5.1 3.07 0.0097 5.7 0.0185 Cl 46.8 2.7 2.2 21.27 0.0098 2.7 0.0225 Ca 3546.8 0.4 17.7 200.94 0.7783 0.5 0.0332 Ba 12.9 4.4 10.8 1.20 0.0013 4.4 0.0743 Fe 3.9 8.0 3.3 1.18 0.0003 8.0 0.0553 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0623 Elt. k-ratio Correc. Na 0.0011 2.3163 Mg 0.0048 1.6912 Sr 0.0026 1.3724 P 0.0155 1.1956 K 0.0009 1.0296 Cl 0.0054 1.1208 Ca 0.2825 1.0931 Ba 0.0004 1.5372 Fe 0.0002 1.2512 Mn 0.0002 1.2742 iteration : 3 Analysis no. 128 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2628 0.016601 0.2628 0.2178 Mg 0.8098 0.017156 0.8098 0.6350 Sr 0.3524 0.014548 0.3524 0.0767 P 1.8548 0.049359 1.8548 1.1414 K 0.0884 0.008536 0.0884 0.0431 Cl 0.6100 0.017522 0.6100 0.3279 Ca 30.8756 0.142637 30.8756 14.6826 Ba 0.0546 0.019975 0.0546 0.0076 Fe 0.0199 0.014103 0.0199 0.0068 Mn 0.0286 0.020135 0.0286 0.0099 C 13.5725 13.5725 21.5376 O 51.4706 51.4706 61.3136 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 129 x= -13459.0 y= 2727.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 20.5 4.9 3.6 5.65 0.0216 5.0 0.0287 Mg 96.4 2.3 2.5 38.28 0.0523 2.3 0.0110 Sr 24.5 3.2 14.3 1.71 0.0015 3.2 0.0398 P 80.2 2.5 2.4 34.14 0.0996 2.5 0.0395 K 14.2 5.9 5.1 2.78 0.0083 5.9 0.0191 Cl 38.6 2.9 2.2 17.55 0.0080 2.9 0.0228 Ca 2632.1 0.4 17.7 149.12 0.5767 0.5 0.0335 Ba 6.7 6.1 10.8 0.62 0.0000 6.1 0.0000 Fe 4.0 7.9 3.3 1.21 0.0004 7.9 0.0558 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0627 Elt. k-ratio Correc. Na 0.0011 2.3253 Mg 0.0038 1.6983 Sr 0.0009 1.3822 P 0.0156 1.2041 K 0.0007 1.0584 Cl 0.0044 1.1372 Ca 0.2093 1.1051 Ba 0.0000 NaN Fe 0.0002 1.2620 Mn 0.0004 1.2829 iteration : 2 Analysis no. 129 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2512 0.016379 0.2512 0.1943 Mg 0.6435 0.015373 0.6435 0.4708 Sr 0.1242 0.011988 0.1242 0.0252 P 1.8804 0.049876 1.8804 1.0797 K 0.0784 0.008462 0.0784 0.0356 Cl 0.5056 0.016224 0.5056 0.2536 Ca 23.1268 0.118862 23.1268 10.2616 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0235 0.014325 0.0235 0.0075 Mn 0.0506 0.021233 0.0506 0.0164 C 16.7016 16.7016 24.7289 O 56.6143 56.6143 62.9265 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 130 x= -13457.0 y= 2731.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 30.3 4.1 3.6 8.34 0.0341 4.1 0.0285 Mg 143.6 1.9 2.5 57.04 0.0787 1.9 0.0109 Sr 41.7 2.4 14.3 2.92 0.0039 2.5 0.0395 P 106.2 2.2 2.4 45.18 0.1328 2.2 0.0392 K 16.7 5.5 5.1 3.26 0.0106 5.5 0.0187 Cl 60.2 2.4 2.2 27.36 0.0127 2.4 0.0226 Ca 3301.0 0.4 17.7 187.01 0.7240 0.5 0.0333 Ba 11.4 4.7 10.8 1.06 0.0004 4.7 0.0742 Fe 3.1 8.9 3.3 0.95 0.0000 9.0 0.0000 Mn 3.9 11.3 2.7 1.44 0.0012 11.3 0.0623 Elt. k-ratio Correc. Na 0.0017 2.3052 Mg 0.0057 1.6877 Sr 0.0024 1.3735 P 0.0208 1.1972 K 0.0009 1.0412 Cl 0.0071 1.1280 Ca 0.2628 1.0966 Ba 0.0001 1.5356 Fe 0.0000 NaN Mn 0.0003 1.2750 iteration : 3 Analysis no. 130 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3928 0.019265 0.3928 0.3223 Mg 0.9612 0.018650 0.9612 0.7460 Sr 0.3321 0.014339 0.3321 0.0715 P 2.4925 0.057165 2.4925 1.5181 K 0.0978 0.008837 0.0978 0.0472 Cl 0.7986 0.019918 0.7986 0.4249 Ca 28.8138 0.136447 28.8138 13.5621 Ba 0.0169 0.019329 0.0169 0.0023 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0431 0.020785 0.0431 0.0148 C 13.8217 13.8217 21.7088 O 52.2296 52.2296 61.5819 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 131 x= -13456.0 y= 2735.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 15.0 5.8 3.6 4.12 0.0145 5.8 0.0287 Mg 84.2 2.4 2.5 33.45 0.0455 2.5 0.0110 Sr 22.3 3.3 14.3 1.56 0.0011 3.4 0.0398 P 95.0 2.3 2.4 40.42 0.1185 2.3 0.0395 K 13.4 6.1 5.1 2.62 0.0076 6.1 0.0192 Cl 44.6 2.7 2.2 20.29 0.0093 2.7 0.0229 Ca 2394.7 0.5 17.7 135.67 0.5242 0.5 0.0336 Ba 7.9 5.6 10.8 0.73 0.0000 5.6 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0628 Elt. k-ratio Correc. Na 0.0007 2.3237 Mg 0.0033 1.6963 Sr 0.0007 1.3824 P 0.0186 1.2052 K 0.0007 1.0684 Cl 0.0052 1.1430 Ca 0.1902 1.1085 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2848 iteration : 2 Analysis no. 131 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1684 0.014348 0.1684 0.1284 Mg 0.5594 0.014361 0.5594 0.4033 Sr 0.0971 0.011637 0.0971 0.0194 P 2.2383 0.054362 2.2383 1.2664 K 0.0717 0.008350 0.0717 0.0321 Cl 0.5923 0.017473 0.5923 0.2927 Ca 21.0883 0.112342 21.0883 9.2202 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0179 0.019804 0.0179 0.0057 C 17.3371 17.3371 25.2944 O 57.8296 57.8296 63.3373 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 132 x= -13454.0 y= 2740.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 29.2 4.1 3.6 8.05 0.0328 4.2 0.0285 Mg 139.1 1.9 2.5 55.23 0.0761 1.9 0.0110 Sr 34.3 2.7 14.3 2.40 0.0028 2.7 0.0397 P 106.0 2.2 2.4 45.12 0.1326 2.2 0.0394 K 13.6 6.1 5.1 2.67 0.0078 6.1 0.0190 Cl 59.5 2.4 2.2 27.06 0.0126 2.4 0.0228 Ca 2786.8 0.4 17.7 157.88 0.6106 0.5 0.0335 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0625 Elt. k-ratio Correc. Na 0.0016 2.3081 Mg 0.0055 1.6905 Sr 0.0018 1.3791 P 0.0208 1.2024 K 0.0007 1.0577 Cl 0.0070 1.1374 Ca 0.2216 1.1033 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2796 iteration : 2 Analysis no. 132 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3778 0.018985 0.3778 0.2984 Mg 0.9317 0.018380 0.9317 0.6960 Sr 0.2426 0.013392 0.2426 0.0503 P 2.4997 0.057371 2.4997 1.4653 K 0.0731 0.008322 0.0731 0.0340 Cl 0.7960 0.019976 0.7960 0.4076 Ca 24.4494 0.123025 24.4494 11.0755 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0414 0.020782 0.0414 0.0137 C 15.5459 15.5459 23.4995 O 55.0424 55.0424 62.4599 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 133 x= -13453.0 y= 2744.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 14.5 5.9 3.6 4.00 0.0139 5.9 0.0287 Mg 71.4 2.6 2.5 28.36 0.0384 2.7 0.0110 Sr 24.3 3.2 14.3 1.70 0.0014 3.2 0.0397 P 88.1 2.4 2.4 37.48 0.1096 2.4 0.0395 K 12.1 6.4 5.1 2.36 0.0064 6.4 0.0192 Cl 48.2 2.6 2.2 21.92 0.0101 2.6 0.0229 Ca 2372.9 0.5 17.7 134.44 0.5193 0.5 0.0336 Ba 8.4 5.5 10.8 0.78 0.0000 5.5 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0559 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0628 Elt. k-ratio Correc. Na 0.0007 2.3261 Mg 0.0028 1.6975 Sr 0.0009 1.3825 P 0.0172 1.2055 K 0.0006 1.0687 Cl 0.0056 1.1427 Ca 0.1885 1.1087 Ba 0.0000 NaN Fe 0.0000 1.2647 Mn 0.0003 1.2850 iteration : 2 Analysis no. 133 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1619 0.014186 0.1619 0.1231 Mg 0.4720 0.013252 0.4720 0.3394 Sr 0.1223 0.011964 0.1223 0.0244 P 2.0718 0.052328 2.0718 1.1691 K 0.0604 0.008052 0.0604 0.0270 Cl 0.6418 0.018123 0.6418 0.3164 Ca 20.8968 0.111714 20.8968 9.1129 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0025 0.013723 0.0025 0.0008 Mn 0.0361 0.020628 0.0361 0.0115 C 17.5340 17.5340 25.5156 O 58.0002 58.0002 63.3598 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 134 x= -13451.0 y= 2748.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 26.9 4.3 3.6 7.40 0.0298 4.3 0.0286 Mg 138.0 1.9 2.5 54.81 0.0755 1.9 0.0110 Sr 34.2 2.7 14.3 2.40 0.0028 2.7 0.0398 P 92.0 2.3 2.4 39.16 0.1147 2.3 0.0395 K 10.9 6.8 5.1 2.14 0.0053 6.8 0.0193 Cl 63.4 2.3 2.2 28.82 0.0134 2.3 0.0229 Ca 2432.1 0.5 17.7 137.79 0.5324 0.5 0.0336 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0558 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0627 Elt. k-ratio Correc. Na 0.0015 2.3119 Mg 0.0055 1.6931 Sr 0.0018 1.3837 P 0.0180 1.2070 K 0.0005 1.0691 Cl 0.0075 1.1431 Ca 0.1932 1.1079 Ba 0.0000 NaN Fe 0.0001 1.2625 Mn 0.0001 1.2831 iteration : 2 Analysis no. 134 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3436 0.018316 0.3436 0.2640 Mg 0.9259 0.018337 0.9259 0.6730 Sr 0.2431 0.013434 0.2431 0.0490 P 2.1703 0.053578 2.1703 1.2377 K 0.0504 0.007780 0.0504 0.0228 Cl 0.8539 0.020699 0.8539 0.4255 Ca 21.4070 0.113364 21.4070 9.4349 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0117 0.013980 0.0117 0.0037 Mn 0.0142 0.019609 0.0142 0.0046 C 16.9293 16.9293 24.8982 O 57.0504 57.0504 62.9866 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 135 x= -13450.0 y= 2752.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 35.9 3.7 3.6 9.89 0.0413 3.8 0.0285 Mg 158.7 1.8 2.5 63.00 0.0870 1.8 0.0110 Sr 36.9 2.6 14.3 2.58 0.0032 2.6 0.0398 P 95.0 2.3 2.4 40.44 0.1185 2.3 0.0396 K 14.1 5.9 5.1 2.76 0.0083 6.0 0.0193 Cl 57.5 2.4 2.2 26.13 0.0121 2.4 0.0230 Ca 2395.4 0.5 17.7 135.71 0.5243 0.5 0.0336 Ba 10.0 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 2.7 13.7 2.7 0.98 0.0000 13.7 0.0000 Elt. k-ratio Correc. Na 0.0021 2.3071 Mg 0.0063 1.6932 Sr 0.0020 1.3853 P 0.0186 1.2086 K 0.0007 1.0708 Cl 0.0067 1.1447 Ca 0.1903 1.1083 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 135 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4758 0.020830 0.4758 0.3653 Mg 1.0668 0.019674 1.0668 0.7747 Sr 0.2754 0.013811 0.2754 0.0555 P 2.2457 0.054526 2.2457 1.2797 K 0.0784 0.008537 0.0784 0.0354 Cl 0.7725 0.019765 0.7725 0.3846 Ca 21.0884 0.112330 21.0884 9.2866 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.8982 16.8982 24.8314 O 57.0988 57.0988 62.9868 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 136 x= -13448.0 y= 2757.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 19.2 5.1 3.6 5.29 0.0200 5.1 0.0286 Mg 102.0 2.2 2.5 40.52 0.0555 2.2 0.0110 Sr 29.9 2.9 14.3 2.09 0.0022 2.9 0.0399 P 75.0 2.6 2.4 31.92 0.0929 2.6 0.0397 K 12.6 6.3 5.1 2.47 0.0069 6.3 0.0195 Cl 82.8 2.0 2.2 37.63 0.0177 2.0 0.0231 Ca 1984.6 0.5 17.7 112.44 0.4337 0.6 0.0338 Ba 8.4 5.5 10.8 0.78 0.0000 5.5 0.0000 Fe 3.0 9.2 3.3 0.89 0.0000 9.2 0.0000 Mn 2.6 14.0 2.7 0.94 0.0000 14.0 0.0000 Elt. k-ratio Correc. Na 0.0010 2.3194 Mg 0.0040 1.6964 Sr 0.0014 1.3873 P 0.0146 1.2107 K 0.0006 1.0849 Cl 0.0098 1.1495 Ca 0.1574 1.1141 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 136 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2312 0.015885 0.2312 0.1717 Mg 0.6813 0.015794 0.6813 0.4785 Sr 0.1903 0.012842 0.1903 0.0371 P 1.7641 0.048479 1.7641 0.9722 K 0.0662 0.008305 0.0662 0.0289 Cl 1.1308 0.023718 1.1308 0.5445 Ca 17.5372 0.100604 17.5372 7.4693 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 18.7756 18.7756 26.6848 O 59.6234 59.6234 63.6131 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 137 x= -13447.0 y= 2761.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 34.5 3.8 3.6 9.51 0.0396 3.8 0.0285 Mg 148.5 1.8 2.5 58.97 0.0814 1.9 0.0110 Sr 37.7 2.6 14.3 2.64 0.0033 2.6 0.0399 P 84.9 2.4 2.4 36.14 0.1056 2.4 0.0397 K 11.5 6.6 5.1 2.25 0.0059 6.6 0.0195 Cl 70.6 2.2 2.2 32.09 0.0150 2.2 0.0231 Ca 2050.1 0.5 17.7 116.15 0.4482 0.6 0.0338 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 2.5 10.0 3.3 0.76 0.0000 10.0 0.0000 Mn 2.6 14.0 2.7 0.94 0.0000 14.0 0.0000 Elt. k-ratio Correc. Na 0.0020 2.3093 Mg 0.0059 1.6951 Sr 0.0021 1.3887 P 0.0166 1.2124 K 0.0005 1.0833 Cl 0.0083 1.1504 Ca 0.1626 1.1129 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 137 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4563 0.020486 0.4563 0.3418 Mg 0.9985 0.019047 0.9985 0.7074 Sr 0.2865 0.013961 0.2865 0.0563 P 2.0072 0.051670 2.0072 1.1158 K 0.0564 0.008029 0.0564 0.0248 Cl 0.9606 0.021954 0.9606 0.4665 Ca 18.1005 0.102490 18.1005 7.7762 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 18.1902 18.1902 26.0772 O 58.9437 58.9437 63.4339 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 138 x= -13445.0 y= 2765.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 26.0 4.4 3.6 7.17 0.0287 4.4 0.0286 Mg 123.3 2.0 2.5 48.97 0.0673 2.0 0.0110 Sr 33.9 2.7 14.3 2.37 0.0028 2.7 0.0399 P 78.7 2.5 2.4 33.50 0.0977 2.5 0.0397 K 9.3 7.3 5.1 1.82 0.0039 7.3 0.0195 Cl 69.8 2.2 2.2 31.74 0.0148 2.2 0.0231 Ca 2016.1 0.5 17.7 114.22 0.4407 0.6 0.0338 Ba 9.0 5.3 10.8 0.84 0.0000 5.3 0.0000 Fe 3.1 8.9 3.3 0.95 0.0000 9.0 0.0000 Mn 2.9 13.1 2.7 1.07 0.0002 13.1 0.0629 Elt. k-ratio Correc. Na 0.0014 2.3161 Mg 0.0049 1.6965 Sr 0.0017 1.3884 P 0.0153 1.2119 K 0.0003 1.0836 Cl 0.0083 1.1500 Ca 0.1599 1.1134 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2871 iteration : 2 Analysis no. 138 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3317 0.018090 0.3317 0.2470 Mg 0.8270 0.017362 0.8270 0.5827 Sr 0.2397 0.013430 0.2397 0.0468 P 1.8558 0.049715 1.8558 1.0260 K 0.0370 0.007480 0.0370 0.0162 Cl 0.9495 0.021831 0.9495 0.4586 Ca 17.8068 0.101505 17.8068 7.6079 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0070 0.019330 0.0070 0.0022 C 18.5419 18.5419 26.4352 O 59.4036 59.4036 63.5773 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 139 x= -13443.0 y= 2769.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 33.8 3.8 3.6 9.31 0.0386 3.9 0.0285 Mg 167.1 1.7 2.5 66.34 0.0917 1.8 0.0110 Sr 40.7 2.5 14.3 2.85 0.0038 2.5 0.0398 P 91.6 2.3 2.4 38.99 0.1142 2.4 0.0396 K 11.5 6.6 5.1 2.25 0.0059 6.6 0.0193 Cl 64.6 2.3 2.2 29.38 0.0137 2.3 0.0229 Ca 2411.0 0.5 17.7 136.59 0.5277 0.5 0.0336 Ba 10.4 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.1 9.0 3.3 0.92 0.0000 9.1 0.0000 Mn 2.9 13.1 2.7 1.07 0.0002 13.1 0.0627 Elt. k-ratio Correc. Na 0.0019 2.3060 Mg 0.0066 1.6920 Sr 0.0023 1.3851 P 0.0179 1.2088 K 0.0005 1.0706 Cl 0.0076 1.1442 Ca 0.1915 1.1080 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2827 iteration : 2 Analysis no. 139 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4446 0.020253 0.4446 0.3419 Mg 1.1235 0.020182 1.1235 0.8172 Sr 0.3223 0.014325 0.3223 0.0650 P 2.1636 0.053534 2.1636 1.2349 K 0.0557 0.007935 0.0557 0.0252 Cl 0.8719 0.020913 0.8719 0.4348 Ca 21.2216 0.112759 21.2216 9.3607 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0070 0.019262 0.0070 0.0022 C 16.8533 16.8533 24.8065 O 56.9365 56.9365 62.9115 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 140 x= -13442.0 y= 2774.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.6 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.6 15.0 Na 12.9 6.2 3.6 3.54 0.0118 6.2 0.0288 Mg 122.8 2.0 2.5 48.77 0.0671 2.0 0.0110 Sr 36.9 2.6 14.3 2.59 0.0032 2.6 0.0396 P 26.8 4.3 2.4 11.41 0.0313 4.3 0.0393 K 14.0 6.0 5.1 2.75 0.0082 6.0 0.0185 Cl 53.4 2.5 2.2 24.27 0.0112 2.5 0.0224 Ca 3435.0 0.4 17.7 194.61 0.7536 0.5 0.0332 Ba 11.2 4.7 10.8 1.04 0.0003 4.7 0.0743 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0555 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0624 Elt. k-ratio Correc. Na 0.0006 2.3302 Mg 0.0049 1.6970 Sr 0.0020 1.3776 P 0.0049 1.1983 K 0.0007 1.0280 Cl 0.0062 1.1171 Ca 0.2735 1.0946 Ba 0.0001 1.5383 Fe 0.0001 1.2547 Mn 0.0002 1.2773 iteration : 3 Analysis no. 140 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1375 0.013547 0.1375 0.1118 Mg 0.8238 0.017331 0.8238 0.6334 Sr 0.2748 0.013745 0.2748 0.0586 P 0.5875 0.029144 0.5875 0.3544 K 0.0744 0.008175 0.0744 0.0356 Cl 0.6980 0.018612 0.6980 0.3679 Ca 29.9367 0.139823 29.9367 13.9567 Ba 0.0117 0.019276 0.0117 0.0016 Fe 0.0108 0.013869 0.0108 0.0036 Mn 0.0305 0.020264 0.0305 0.0104 C 14.7898 14.7898 23.0086 O 52.6242 52.6242 61.4574 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 141 x= -13440.0 y= 2778.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 27.1 4.3 3.6 7.46 0.0300 4.3 0.0288 Mg 109.9 2.1 2.5 43.66 0.0599 2.2 0.0110 Sr 34.0 2.7 14.3 2.38 0.0028 2.7 0.0396 P 26.5 4.3 2.4 11.28 0.0309 4.4 0.0392 K 14.8 5.8 5.1 2.89 0.0089 5.8 0.0184 Cl 56.2 2.4 2.2 25.54 0.0118 2.4 0.0224 Ca 3561.0 0.4 17.7 201.75 0.7815 0.5 0.0332 Ba 11.5 4.7 10.8 1.07 0.0005 4.7 0.0744 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0554 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0624 Elt. k-ratio Correc. Na 0.0015 2.3283 Mg 0.0043 1.6997 Sr 0.0017 1.3766 P 0.0048 1.1967 K 0.0008 1.0239 Cl 0.0066 1.1146 Ca 0.2836 1.0929 Ba 0.0001 1.5387 Fe 0.0001 1.2533 Mn 0.0003 1.2762 iteration : 3 Analysis no. 141 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3491 0.018510 0.3491 0.2865 Mg 0.7370 0.016426 0.7370 0.5721 Sr 0.2395 0.013339 0.2395 0.0516 P 0.5796 0.028957 0.5796 0.3531 K 0.0804 0.008303 0.0804 0.0388 Cl 0.7347 0.019037 0.7347 0.3910 Ca 30.9977 0.143006 30.9977 14.5923 Ba 0.0202 0.019426 0.0202 0.0028 Fe 0.0183 0.014079 0.0183 0.0062 Mn 0.0359 0.020490 0.0359 0.0123 C 14.3457 14.3457 22.5354 O 51.8620 51.8620 61.1579 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 142 x= -13439.0 y= 2782.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 52.6 3.1 3.6 14.50 0.0628 3.1 0.0287 Mg 140.7 1.9 2.5 55.88 0.0771 1.9 0.0110 Sr 36.6 2.6 14.3 2.56 0.0032 2.6 0.0398 P 30.6 4.0 2.4 13.00 0.0361 4.1 0.0395 K 15.2 5.7 5.1 2.97 0.0092 5.8 0.0188 Cl 59.7 2.4 2.2 27.12 0.0126 2.4 0.0226 Ca 3062.6 0.4 17.7 173.51 0.6718 0.5 0.0334 Ba 11.1 4.7 10.8 1.03 0.0002 4.8 0.0743 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0556 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0626 Elt. k-ratio Correc. Na 0.0031 2.3185 Mg 0.0056 1.7030 Sr 0.0020 1.3838 P 0.0057 1.2040 K 0.0008 1.0420 Cl 0.0070 1.1253 Ca 0.2438 1.0991 Ba 0.0001 1.5360 Fe 0.0000 1.2575 Mn 0.0003 1.2793 iteration : 3 Analysis no. 142 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7272 0.025063 0.7272 0.5786 Mg 0.9504 0.018635 0.9504 0.7152 Sr 0.2722 0.013771 0.2722 0.0568 P 0.6812 0.031151 0.6812 0.4023 K 0.0852 0.008537 0.0852 0.0399 Cl 0.7897 0.019794 0.7897 0.4074 Ca 26.7984 0.130307 26.7984 12.2295 Ba 0.0084 0.019203 0.0084 0.0011 Fe 0.0017 0.013628 0.0017 0.0005 Mn 0.0360 0.020549 0.0360 0.0120 C 15.6356 15.6356 23.8101 O 54.0138 54.0138 61.7466 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 143 x= -13437.0 y= 2786.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 26.8 4.3 3.6 7.39 0.0297 4.3 0.0288 Mg 96.3 2.3 2.5 38.24 0.0523 2.3 0.0110 Sr 30.1 2.9 14.3 2.11 0.0023 2.9 0.0398 P 32.2 3.9 2.4 13.68 0.0381 4.0 0.0395 K 14.4 5.9 5.1 2.81 0.0085 5.9 0.0189 Cl 59.1 2.4 2.2 26.85 0.0125 2.4 0.0226 Ca 2904.6 0.4 17.7 164.56 0.6372 0.5 0.0335 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 2.5 14.1 2.7 0.92 0.0000 14.1 0.0000 Elt. k-ratio Correc. Na 0.0015 2.3294 Mg 0.0038 1.7019 Sr 0.0014 1.3823 P 0.0060 1.2031 K 0.0008 1.0463 Cl 0.0069 1.1272 Ca 0.2313 1.1015 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 143 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3458 0.018456 0.3458 0.2709 Mg 0.6446 0.015409 0.6446 0.4776 Sr 0.1928 0.012844 0.1928 0.0396 P 0.7196 0.031897 0.7196 0.4184 K 0.0788 0.008404 0.0788 0.0363 Cl 0.7831 0.019738 0.7831 0.3978 Ca 25.4732 0.126249 25.4732 11.4452 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.4413 16.4413 24.6504 O 55.3207 55.3207 62.2639 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 144 x= -13436.0 y= 2791.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 36.2 3.7 3.6 9.97 0.0417 3.7 0.0288 Mg 124.1 2.0 2.5 49.27 0.0678 2.0 0.0111 Sr 34.1 2.7 14.3 2.39 0.0028 2.7 0.0400 P 29.6 4.1 2.4 12.58 0.0348 4.1 0.0397 K 13.8 6.0 5.1 2.71 0.0080 6.0 0.0192 Cl 62.8 2.3 2.2 28.54 0.0133 2.3 0.0228 Ca 2458.9 0.5 17.7 139.31 0.5389 0.5 0.0336 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.0 9.1 3.3 0.91 0.0000 9.1 0.0000 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0629 Elt. k-ratio Correc. Na 0.0021 2.3252 Mg 0.0049 1.7037 Sr 0.0017 1.3887 P 0.0055 1.2097 K 0.0007 1.0628 Cl 0.0074 1.1364 Ca 0.1956 1.1071 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2848 iteration : 2 Analysis no. 144 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4845 0.021096 0.4845 0.3689 Mg 0.8365 0.017505 0.8365 0.6024 Sr 0.2424 0.013474 0.2424 0.0484 P 0.6605 0.030825 0.6605 0.3732 K 0.0753 0.008415 0.0753 0.0337 Cl 0.8414 0.020503 0.8414 0.4154 Ca 21.6501 0.114172 21.6501 9.4551 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0362 0.020646 0.0362 0.0115 C 17.7604 17.7604 25.8824 O 57.4127 57.4127 62.8089 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 145 x= -13434.0 y= 2795.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.0 5.4 3.6 4.69 0.0172 5.4 0.0289 Mg 59.2 2.9 2.5 23.51 0.0316 2.9 0.0111 Sr 24.1 3.2 14.3 1.69 0.0014 3.2 0.0399 P 26.1 4.4 2.4 11.11 0.0304 4.4 0.0396 K 12.0 6.4 5.1 2.35 0.0063 6.5 0.0191 Cl 68.8 2.2 2.2 31.27 0.0146 2.2 0.0228 Ca 2529.1 0.4 17.7 143.28 0.5544 0.5 0.0336 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 2.9 9.4 3.3 0.86 0.0000 9.4 0.0000 Mn 2.7 13.6 2.7 1.00 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3372 Mg 0.0023 1.7044 Sr 0.0009 1.3847 P 0.0048 1.2055 K 0.0006 1.0589 Cl 0.0081 1.1330 Ca 0.2012 1.1066 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 145 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2003 0.015228 0.2003 0.1524 Mg 0.3904 0.012158 0.3904 0.2810 Sr 0.1196 0.011958 0.1196 0.0239 P 0.5748 0.028992 0.5748 0.3246 K 0.0595 0.007975 0.0595 0.0266 Cl 0.9222 0.021375 0.9222 0.4550 Ca 22.2657 0.116169 22.2657 9.7179 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.9259 17.9259 26.1074 O 57.5417 57.5417 62.9112 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 146 x= -13433.0 y= 2799.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 39.9 3.5 3.6 10.99 0.0465 3.6 0.0287 Mg 129.6 2.0 2.5 51.45 0.0709 2.0 0.0111 Sr 36.7 2.6 14.3 2.57 0.0032 2.6 0.0399 P 29.8 4.1 2.4 12.68 0.0351 4.1 0.0396 K 14.8 5.8 5.1 2.90 0.0089 5.8 0.0190 Cl 71.0 2.2 2.2 32.29 0.0151 2.2 0.0227 Ca 2690.1 0.4 17.7 152.41 0.5899 0.5 0.0335 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.6 8.3 3.3 1.09 0.0002 8.3 0.0558 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0628 Elt. k-ratio Correc. Na 0.0023 2.3220 Mg 0.0051 1.7022 Sr 0.0020 1.3861 P 0.0055 1.2071 K 0.0008 1.0553 Cl 0.0084 1.1319 Ca 0.2141 1.1041 Ba 0.0000 NaN Fe 0.0001 1.2614 Mn 0.0003 1.2825 iteration : 3 Analysis no. 146 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5389 0.022037 0.5389 0.4176 Mg 0.8736 0.017875 0.8736 0.6404 Sr 0.2737 0.013809 0.2737 0.0557 P 0.6651 0.030881 0.6651 0.3826 K 0.0834 0.008575 0.0834 0.0380 Cl 0.9521 0.021688 0.9521 0.4784 Ca 23.6362 0.120496 23.6362 10.5065 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0101 0.013931 0.0101 0.0032 Mn 0.0361 0.020608 0.0361 0.0117 C 16.9226 16.9226 25.1012 O 56.0082 56.0082 62.3648 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 147 x= -13431.0 y= 2803.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 23.1 4.6 3.6 6.37 0.0250 4.7 0.0289 Mg 77.9 2.5 2.5 30.94 0.0421 2.6 0.0111 Sr 23.2 3.3 14.3 1.62 0.0013 3.3 0.0399 P 30.1 4.1 2.4 12.79 0.0355 4.1 0.0395 K 15.7 5.6 5.1 3.08 0.0097 5.7 0.0190 Cl 53.1 2.5 2.2 24.13 0.0112 2.5 0.0227 Ca 2686.9 0.4 17.7 152.23 0.5893 0.5 0.0336 Ba 8.5 5.4 10.8 0.79 0.0000 5.4 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0629 Elt. k-ratio Correc. Na 0.0012 2.3351 Mg 0.0030 1.7046 Sr 0.0008 1.3845 P 0.0056 1.2047 K 0.0009 1.0526 Cl 0.0062 1.1307 Ca 0.2139 1.1044 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2842 iteration : 2 Analysis no. 147 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2914 0.017335 0.2914 0.2242 Mg 0.5194 0.013906 0.5194 0.3781 Sr 0.1086 0.011815 0.1086 0.0219 P 0.6700 0.030948 0.6700 0.3827 K 0.0909 0.008747 0.0909 0.0411 Cl 0.7032 0.018809 0.7032 0.3510 Ca 23.6197 0.120465 23.6197 10.4274 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0125 0.019564 0.0125 0.0040 C 17.2925 17.2925 25.4747 O 56.6919 56.6919 62.6948 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 148 x= -13429.0 y= 2808.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 28.0 4.2 3.6 7.71 0.0312 4.2 0.0288 Mg 107.6 2.2 2.5 42.75 0.0587 2.2 0.0110 Sr 32.8 2.8 14.3 2.30 0.0026 2.8 0.0398 P 27.2 4.3 2.4 11.58 0.0318 4.3 0.0395 K 14.2 5.9 5.1 2.77 0.0083 6.0 0.0189 Cl 71.0 2.2 2.2 32.28 0.0151 2.2 0.0226 Ca 2944.9 0.4 17.7 166.84 0.6462 0.5 0.0335 Ba 10.6 4.8 10.8 0.99 0.0000 4.9 0.0000 Fe 3.6 8.3 3.3 1.09 0.0002 8.3 0.0558 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0627 Elt. k-ratio Correc. Na 0.0016 2.3273 Mg 0.0042 1.7009 Sr 0.0016 1.3822 P 0.0050 1.2029 K 0.0007 1.0456 Cl 0.0084 1.1260 Ca 0.2345 1.1010 Ba 0.0000 NaN Fe 0.0001 1.2595 Mn 0.0001 1.2810 iteration : 2 Analysis no. 148 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3627 0.018791 0.3627 0.2853 Mg 0.7224 0.016281 0.7224 0.5375 Sr 0.2260 0.013236 0.2260 0.0466 P 0.6001 0.029488 0.6001 0.3503 K 0.0771 0.008356 0.0771 0.0356 Cl 0.9467 0.021572 0.9467 0.4829 Ca 25.8191 0.127325 25.8191 11.6485 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0100 0.013911 0.0100 0.0033 Mn 0.0142 0.019598 0.0142 0.0047 C 16.2893 16.2893 24.5234 O 54.9323 54.9323 62.0820 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 149 x= -13428.0 y= 2812.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.8 3.5 3.6 11.25 0.0477 3.5 0.0287 Mg 142.5 1.9 2.5 56.58 0.0781 1.9 0.0110 Sr 35.9 2.6 14.3 2.51 0.0031 2.7 0.0399 P 29.2 4.1 2.4 12.41 0.0343 4.2 0.0396 K 15.8 5.6 5.1 3.10 0.0098 5.6 0.0190 Cl 67.9 2.2 2.2 30.86 0.0144 2.2 0.0227 Ca 2709.1 0.4 17.7 153.48 0.5941 0.5 0.0335 Ba 10.6 4.9 10.8 0.99 0.0000 4.9 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0558 Mn 2.7 13.6 2.7 1.00 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0024 2.3206 Mg 0.0057 1.7017 Sr 0.0019 1.3867 P 0.0054 1.2074 K 0.0009 1.0546 Cl 0.0080 1.1317 Ca 0.2156 1.1039 Ba 0.0000 NaN Fe 0.0000 1.2614 Mn 0.0000 NaN iteration : 3 Analysis no. 149 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5527 0.022266 0.5527 0.4287 Mg 0.9621 0.018746 0.9621 0.7060 Sr 0.2640 0.013705 0.2640 0.0537 P 0.6495 0.030569 0.6495 0.3740 K 0.0919 0.008782 0.0919 0.0419 Cl 0.9085 0.021211 0.9085 0.4570 Ca 23.8009 0.121019 23.8009 10.5905 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013676 0.0017 0.0005 Mn 0.0000 0.000000 0.0000 0.0000 C 16.8495 16.8495 25.0184 O 55.9191 55.9191 62.3292 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 150 x= -13426.0 y= 2816.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 42.1 3.4 3.6 11.59 0.0493 3.5 0.0287 Mg 132.4 1.9 2.5 52.59 0.0725 2.0 0.0111 Sr 35.6 2.6 14.3 2.49 0.0030 2.7 0.0399 P 29.7 4.1 2.4 12.62 0.0349 4.1 0.0396 K 15.8 5.6 5.1 3.10 0.0098 5.6 0.0189 Cl 58.8 2.4 2.2 26.72 0.0124 2.4 0.0227 Ca 2853.6 0.4 17.7 161.67 0.6259 0.5 0.0335 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 2.9 9.3 3.3 0.87 0.0000 9.3 0.0000 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0627 Elt. k-ratio Correc. Na 0.0025 2.3227 Mg 0.0052 1.7028 Sr 0.0019 1.3852 P 0.0055 1.2058 K 0.0009 1.0487 Cl 0.0069 1.1289 Ca 0.2271 1.1019 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0004 1.2813 iteration : 3 Analysis no. 150 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5717 0.022598 0.5717 0.4476 Mg 0.8934 0.018075 0.8934 0.6617 Sr 0.2601 0.013647 0.2601 0.0534 P 0.6606 0.030768 0.6606 0.3839 K 0.0914 0.008731 0.0914 0.0421 Cl 0.7805 0.019722 0.7805 0.3963 Ca 25.0269 0.124841 25.0269 11.2399 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0488 0.021141 0.0488 0.0160 C 16.4105 16.4105 24.5939 O 55.2563 55.2563 62.1653 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 151 x= -13425.0 y= 2820.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 37.6 3.6 3.6 10.35 0.0435 3.7 0.0287 Mg 118.2 2.1 2.5 46.94 0.0645 2.1 0.0110 Sr 32.0 2.8 14.3 2.24 0.0025 2.8 0.0398 P 28.9 4.2 2.4 12.30 0.0340 4.2 0.0395 K 16.8 5.5 5.1 3.28 0.0107 5.5 0.0189 Cl 67.1 2.2 2.2 30.50 0.0142 2.2 0.0226 Ca 2895.6 0.4 17.7 164.05 0.6350 0.5 0.0334 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0557 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0627 Elt. k-ratio Correc. Na 0.0022 2.3244 Mg 0.0047 1.7023 Sr 0.0016 1.3838 P 0.0053 1.2041 K 0.0009 1.0474 Cl 0.0079 1.1275 Ca 0.2305 1.1016 Ba 0.0000 NaN Fe 0.0001 1.2598 Mn 0.0001 1.2813 iteration : 3 Analysis no. 151 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5050 0.021453 0.5050 0.3962 Mg 0.7952 0.017066 0.7952 0.5902 Sr 0.2161 0.013127 0.2161 0.0445 P 0.6414 0.030352 0.6414 0.3736 K 0.0993 0.008916 0.0993 0.0458 Cl 0.8937 0.021000 0.8937 0.4547 Ca 25.3857 0.125957 25.3857 11.4251 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0075 0.013832 0.0075 0.0024 Mn 0.0179 0.019761 0.0179 0.0059 C 16.3503 16.3503 24.5553 O 55.0878 55.0878 62.1063 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 152 x= -13423.0 y= 2825.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 22.8 4.7 3.6 6.27 0.0245 4.7 0.0288 Mg 92.9 2.3 2.5 36.90 0.0504 2.3 0.0110 Sr 26.3 3.1 14.3 1.84 0.0017 3.1 0.0398 P 29.2 4.1 2.4 12.43 0.0344 4.1 0.0395 K 14.7 5.8 5.1 2.87 0.0088 5.8 0.0190 Cl 66.0 2.2 2.2 30.00 0.0140 2.2 0.0227 Ca 2732.1 0.4 17.7 154.79 0.5990 0.5 0.0335 Ba 9.3 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0559 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0628 Elt. k-ratio Correc. Na 0.0012 2.3317 Mg 0.0037 1.7025 Sr 0.0011 1.3840 P 0.0054 1.2044 K 0.0008 1.0523 Cl 0.0078 1.1299 Ca 0.2174 1.1038 Ba 0.0000 NaN Fe 0.0001 1.2623 Mn 0.0001 1.2833 iteration : 2 Analysis no. 152 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2856 0.017187 0.2856 0.2209 Mg 0.6217 0.015142 0.6217 0.4549 Sr 0.1463 0.012286 0.1463 0.0297 P 0.6489 0.030510 0.6489 0.3726 K 0.0818 0.008515 0.0818 0.0372 Cl 0.8806 0.020880 0.8806 0.4417 Ca 23.9960 0.121629 23.9960 10.6469 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0076 0.013861 0.0076 0.0024 Mn 0.0143 0.019627 0.0143 0.0046 C 17.0679 17.0679 25.2704 O 56.2494 56.2494 62.5188 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 153 x= -13422.0 y= 2829.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 35.6 3.7 3.6 9.80 0.0410 3.8 0.0287 Mg 122.4 2.0 2.5 48.61 0.0669 2.0 0.0110 Sr 33.3 2.7 14.3 2.33 0.0027 2.8 0.0399 P 26.3 4.4 2.4 11.17 0.0306 4.4 0.0395 K 16.7 5.5 5.1 3.26 0.0106 5.5 0.0190 Cl 71.8 2.2 2.2 32.64 0.0153 2.2 0.0227 Ca 2800.6 0.4 17.7 158.67 0.6143 0.5 0.0335 Ba 10.6 4.8 10.8 0.99 0.0000 4.9 0.0000 Fe 3.3 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0628 Elt. k-ratio Correc. Na 0.0020 2.3243 Mg 0.0048 1.7020 Sr 0.0017 1.3848 P 0.0048 1.2053 K 0.0009 1.0509 Cl 0.0085 1.1291 Ca 0.2229 1.1028 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2820 iteration : 3 Analysis no. 153 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4754 0.020927 0.4754 0.3706 Mg 0.8243 0.017371 0.8243 0.6079 Sr 0.2316 0.013320 0.2316 0.0474 P 0.5782 0.029060 0.5782 0.3346 K 0.0988 0.008928 0.0988 0.0453 Cl 0.9603 0.021747 0.9603 0.4855 Ca 24.5851 0.123482 24.5851 10.9940 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0233 0.020030 0.0233 0.0076 C 16.6751 16.6751 24.8829 O 55.5478 55.5478 62.2243 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 154 x= -13420.0 y= 2833.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.5 3.5 3.6 11.15 0.0473 3.5 0.0287 Mg 119.2 2.0 2.5 47.32 0.0651 2.1 0.0111 Sr 31.0 2.8 14.3 2.17 0.0024 2.9 0.0399 P 28.9 4.2 2.4 12.30 0.0340 4.2 0.0395 K 18.1 5.3 5.1 3.55 0.0119 5.3 0.0189 Cl 65.5 2.3 2.2 29.77 0.0139 2.3 0.0226 Ca 2891.8 0.4 17.7 163.83 0.6344 0.5 0.0335 Ba 10.6 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0558 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0627 Elt. k-ratio Correc. Na 0.0024 2.3241 Mg 0.0047 1.7030 Sr 0.0015 1.3841 P 0.0053 1.2043 K 0.0011 1.0474 Cl 0.0077 1.1275 Ca 0.2302 1.1016 Ba 0.0000 NaN Fe 0.0001 1.2598 Mn 0.0001 1.2813 iteration : 3 Analysis no. 154 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5483 0.022211 0.5483 0.4302 Mg 0.8024 0.017148 0.8024 0.5955 Sr 0.2041 0.012992 0.2041 0.0420 P 0.6418 0.030368 0.6418 0.3737 K 0.1109 0.009192 0.1109 0.0511 Cl 0.8721 0.020764 0.8721 0.4437 Ca 25.3626 0.125904 25.3626 11.4135 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0134 0.014014 0.0134 0.0043 Mn 0.0142 0.019601 0.0142 0.0047 C 16.3436 16.3436 24.5427 O 55.0866 55.0866 62.0986 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 155 x= -13419.0 y= 2837.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 29.9 4.1 3.6 8.24 0.0337 4.1 0.0288 Mg 75.4 2.6 2.5 29.95 0.0407 2.6 0.0111 Sr 26.1 3.1 14.3 1.83 0.0017 3.1 0.0398 P 26.5 4.3 2.4 11.26 0.0308 4.4 0.0394 K 18.1 5.3 5.1 3.55 0.0119 5.3 0.0188 Cl 58.8 2.4 2.2 26.71 0.0124 2.4 0.0226 Ca 2987.2 0.4 17.7 169.24 0.6553 0.5 0.0334 Ba 8.9 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0558 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0627 Elt. k-ratio Correc. Na 0.0017 2.3329 Mg 0.0029 1.7045 Sr 0.0010 1.3815 P 0.0048 1.2016 K 0.0011 1.0424 Cl 0.0069 1.1245 Ca 0.2378 1.1004 Ba 0.0000 NaN Fe 0.0001 1.2597 Mn 0.0002 1.2814 iteration : 2 Analysis no. 155 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3926 0.019410 0.3926 0.3088 Mg 0.5019 0.013678 0.5019 0.3734 Sr 0.1437 0.012235 0.1437 0.0296 P 0.5811 0.029066 0.5811 0.3393 K 0.1103 0.009146 0.1103 0.0510 Cl 0.7770 0.019639 0.7770 0.3963 Ca 26.1722 0.128404 26.1722 11.8079 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0176 0.014135 0.0176 0.0057 Mn 0.0197 0.019849 0.0197 0.0065 C 16.3020 16.3020 24.5428 O 54.9819 54.9819 62.1387 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 156 x= -13417.0 y= 2842.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 30.5 4.0 3.6 8.41 0.0345 4.1 0.0288 Mg 86.9 2.4 2.5 34.52 0.0471 2.4 0.0110 Sr 29.6 2.9 14.3 2.07 0.0022 2.9 0.0397 P 27.2 4.3 2.4 11.55 0.0317 4.3 0.0393 K 17.2 5.4 5.1 3.37 0.0111 5.4 0.0187 Cl 65.6 2.3 2.2 29.82 0.0139 2.3 0.0225 Ca 3217.6 0.4 17.7 182.29 0.7062 0.5 0.0333 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0744 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0626 Elt. k-ratio Correc. Na 0.0017 2.3293 Mg 0.0034 1.7020 Sr 0.0013 1.3790 P 0.0050 1.1992 K 0.0010 1.0355 Cl 0.0077 1.1204 Ca 0.2563 1.0975 Ba 0.0000 1.5376 Fe 0.0000 NaN Mn 0.0002 1.2792 iteration : 3 Analysis no. 156 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4009 0.019553 0.4009 0.3210 Mg 0.5803 0.014647 0.5803 0.4394 Sr 0.1859 0.012735 0.1859 0.0391 P 0.5968 0.029365 0.5968 0.3547 K 0.1020 0.008907 0.1020 0.0480 Cl 0.8678 0.020644 0.8678 0.4505 Ca 28.1279 0.134398 28.1279 12.9170 Ba 0.0026 0.019128 0.0026 0.0003 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0197 0.019816 0.0197 0.0066 C 15.4822 15.4822 23.7250 O 53.6339 53.6339 61.6984 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 157 x= -13415.0 y= 2846.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.5 4.0 3.6 8.69 0.0358 4.0 0.0288 Mg 100.6 2.2 2.5 39.97 0.0548 2.3 0.0111 Sr 25.1 3.2 14.3 1.76 0.0015 3.2 0.0398 P 27.0 4.3 2.4 11.49 0.0316 4.3 0.0395 K 18.5 5.2 5.1 3.62 0.0123 5.2 0.0189 Cl 67.5 2.2 2.2 30.70 0.0143 2.2 0.0226 Ca 2845.4 0.4 17.7 161.20 0.6242 0.5 0.0335 Ba 8.2 5.5 10.8 0.77 0.0000 5.5 0.0000 Fe 2.9 9.2 3.3 0.89 0.0000 9.3 0.0000 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0628 Elt. k-ratio Correc. Na 0.0018 2.3292 Mg 0.0040 1.7033 Sr 0.0010 1.3837 P 0.0049 1.2035 K 0.0011 1.0483 Cl 0.0080 1.1275 Ca 0.2265 1.1023 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2822 iteration : 2 Analysis no. 157 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4159 0.019844 0.4159 0.3246 Mg 0.6752 0.015765 0.6752 0.4984 Sr 0.1323 0.012111 0.1323 0.0271 P 0.5955 0.029399 0.5955 0.3449 K 0.1140 0.009269 0.1140 0.0523 Cl 0.9001 0.021076 0.9001 0.4555 Ca 24.9699 0.124688 24.9699 11.1767 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0361 0.020603 0.0361 0.0118 C 16.6421 16.6421 24.8573 O 55.5190 55.5190 62.2515 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 158 x= -13414.0 y= 2850.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 25.2 4.4 3.6 6.95 0.0277 4.5 0.0289 Mg 84.5 2.4 2.5 33.57 0.0458 2.5 0.0111 Sr 25.3 3.1 14.3 1.77 0.0016 3.2 0.0398 P 23.0 4.7 2.4 9.79 0.0264 4.7 0.0395 K 17.9 5.3 5.1 3.51 0.0117 5.3 0.0189 Cl 63.0 2.3 2.2 28.64 0.0133 2.3 0.0226 Ca 2803.7 0.4 17.7 158.84 0.6149 0.5 0.0335 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0559 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0628 Elt. k-ratio Correc. Na 0.0014 2.3337 Mg 0.0033 1.7042 Sr 0.0010 1.3837 P 0.0041 1.2037 K 0.0010 1.0488 Cl 0.0074 1.1277 Ca 0.2232 1.1029 Ba 0.0000 NaN Fe 0.0000 1.2618 Mn 0.0002 1.2830 iteration : 2 Analysis no. 158 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3225 0.017993 0.3225 0.2504 Mg 0.5645 0.014466 0.5645 0.4145 Sr 0.1348 0.012141 0.1348 0.0274 P 0.4989 0.027301 0.4989 0.2875 K 0.1093 0.009163 0.1093 0.0499 Cl 0.8377 0.020376 0.8377 0.4217 Ca 24.6124 0.123569 24.6124 10.9595 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0025 0.013705 0.0025 0.0008 Mn 0.0270 0.020208 0.0270 0.0088 C 16.9396 16.9396 25.1702 O 55.9507 55.9507 62.4094 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 159 x= -13412.0 y= 2854.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 24.5 4.5 3.6 6.74 0.0267 4.5 0.0289 Mg 89.5 2.4 2.5 35.55 0.0485 2.4 0.0111 Sr 25.8 3.1 14.3 1.80 0.0016 3.1 0.0398 P 25.0 4.5 2.4 10.64 0.0290 4.5 0.0395 K 20.9 4.9 5.1 4.10 0.0145 4.9 0.0189 Cl 60.9 2.3 2.2 27.68 0.0129 2.3 0.0226 Ca 2878.2 0.4 17.7 163.06 0.6313 0.5 0.0335 Ba 8.8 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 4.1 7.8 3.3 1.25 0.0005 7.8 0.0558 Mn 4.2 10.9 2.7 1.55 0.0015 10.9 0.0627 Elt. k-ratio Correc. Na 0.0013 2.3337 Mg 0.0035 1.7037 Sr 0.0010 1.3830 P 0.0045 1.2030 K 0.0013 1.0463 Cl 0.0072 1.1265 Ca 0.2291 1.1018 Ba 0.0000 NaN Fe 0.0002 1.2607 Mn 0.0004 1.2821 iteration : 2 Analysis no. 159 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3113 0.017754 0.3113 0.2431 Mg 0.5988 0.014878 0.5988 0.4424 Sr 0.1399 0.012199 0.1399 0.0287 P 0.5468 0.028351 0.5468 0.3170 K 0.1346 0.009721 0.1346 0.0618 Cl 0.8078 0.020019 0.8078 0.4091 Ca 25.2438 0.125529 25.2438 11.3102 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0277 0.014442 0.0277 0.0089 Mn 0.0543 0.021388 0.0543 0.0177 C 16.6351 16.6351 24.8709 O 55.5001 55.5001 62.2901 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 160 x= -13411.0 y= 2859.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 33.2 3.9 3.6 9.15 0.0380 3.9 0.0288 Mg 102.6 2.2 2.5 40.76 0.0559 2.2 0.0111 Sr 30.9 2.8 14.3 2.16 0.0024 2.9 0.0398 P 23.7 4.6 2.4 10.06 0.0273 4.6 0.0395 K 20.1 5.0 5.1 3.94 0.0138 5.0 0.0188 Cl 58.4 2.4 2.2 26.53 0.0123 2.4 0.0226 Ca 2949.6 0.4 17.7 167.11 0.6473 0.5 0.0335 Ba 9.2 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0558 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0627 Elt. k-ratio Correc. Na 0.0019 2.3294 Mg 0.0040 1.7037 Sr 0.0015 1.3832 P 0.0043 1.2034 K 0.0012 1.0441 Cl 0.0069 1.1256 Ca 0.2349 1.1008 Ba 0.0000 NaN Fe 0.0001 1.2597 Mn 0.0002 1.2813 iteration : 3 Analysis no. 160 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4414 0.020330 0.4414 0.3468 Mg 0.6892 0.015927 0.6892 0.5122 Sr 0.2024 0.012968 0.2024 0.0417 P 0.5146 0.027653 0.5146 0.3001 K 0.1275 0.009552 0.1275 0.0589 Cl 0.7725 0.019601 0.7725 0.3936 Ca 25.8599 0.127453 25.8599 11.6544 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0117 0.013966 0.0117 0.0038 Mn 0.0270 0.020187 0.0270 0.0089 C 16.3360 16.3360 24.5674 O 55.0177 55.0177 62.1121 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 161 x= -13409.0 y= 2863.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 23.9 4.6 3.6 6.58 0.0260 4.6 0.0289 Mg 69.2 2.7 2.5 27.49 0.0372 2.7 0.0111 Sr 34.2 2.7 14.3 2.39 0.0028 2.7 0.0397 P 23.9 4.6 2.4 10.17 0.0276 4.6 0.0394 K 19.7 5.0 5.1 3.86 0.0134 5.0 0.0187 Cl 59.9 2.4 2.2 27.22 0.0127 2.4 0.0225 Ca 3137.7 0.4 17.7 177.76 0.6887 0.5 0.0334 Ba 10.2 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0557 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0626 Elt. k-ratio Correc. Na 0.0013 2.3336 Mg 0.0027 1.7026 Sr 0.0018 1.3790 P 0.0043 1.2002 K 0.0012 1.0374 Cl 0.0070 1.1215 Ca 0.2499 1.0984 Ba 0.0000 NaN Fe 0.0000 1.2580 Mn 0.0003 1.2799 iteration : 3 Analysis no. 161 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3023 0.017563 0.3023 0.2403 Mg 0.4588 0.013103 0.4588 0.3450 Sr 0.2416 0.013390 0.2416 0.0504 P 0.5191 0.027707 0.5191 0.3063 K 0.1233 0.009413 0.1233 0.0576 Cl 0.7906 0.019774 0.7906 0.4076 Ca 27.4538 0.132348 27.4538 12.5190 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0059 0.013767 0.0059 0.0019 Mn 0.0324 0.020406 0.0324 0.0108 C 15.8650 15.8650 24.1410 O 54.2071 54.2071 61.9201 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 162 x= -13408.0 y= 2867.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 37.0 3.7 3.6 10.20 0.0428 3.7 0.0287 Mg 113.8 2.1 2.5 45.19 0.0621 2.1 0.0110 Sr 38.5 2.5 14.3 2.70 0.0035 2.6 0.0396 P 27.3 4.3 2.4 11.60 0.0319 4.3 0.0393 K 23.9 4.6 5.1 4.68 0.0172 4.6 0.0185 Cl 63.8 2.3 2.2 28.98 0.0135 2.3 0.0224 Ca 3595.0 0.4 17.7 203.67 0.7895 0.5 0.0332 Ba 10.8 4.8 10.8 1.00 0.0000 4.8 0.0744 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0554 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0624 Elt. k-ratio Correc. Na 0.0021 2.3234 Mg 0.0045 1.6995 Sr 0.0021 1.3761 P 0.0050 1.1966 K 0.0015 1.0241 Cl 0.0075 1.1142 Ca 0.2865 1.0926 Ba 0.0000 1.5385 Fe 0.0001 1.2523 Mn 0.0004 1.2753 iteration : 3 Analysis no. 162 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4967 0.021303 0.4967 0.4099 Mg 0.7639 0.016721 0.7639 0.5963 Sr 0.2935 0.013950 0.2935 0.0636 P 0.5980 0.029353 0.5980 0.3663 K 0.1563 0.010042 0.1563 0.0759 Cl 0.8380 0.020249 0.8380 0.4484 Ca 31.3056 0.143963 31.3056 14.8186 Ba 0.0013 0.019118 0.0013 0.0002 Fe 0.0108 0.013853 0.0108 0.0037 Mn 0.0486 0.021042 0.0486 0.0168 C 14.0899 14.0899 22.2557 O 51.3974 51.3974 60.9448 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 163 x= -13406.0 y= 2871.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 52.9 3.1 3.6 14.57 0.0632 3.1 0.0286 Mg 158.5 1.8 2.5 62.92 0.0870 1.8 0.0110 Sr 40.4 2.5 14.3 2.83 0.0037 2.5 0.0398 P 25.9 4.4 2.4 11.02 0.0302 4.4 0.0395 K 22.9 4.7 5.1 4.49 0.0163 4.7 0.0187 Cl 66.3 2.2 2.2 30.15 0.0141 2.2 0.0226 Ca 3183.6 0.4 17.7 180.37 0.6989 0.5 0.0334 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0744 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0556 Mn 2.9 13.2 2.7 1.05 0.0001 13.2 0.0626 Elt. k-ratio Correc. Na 0.0032 2.3156 Mg 0.0063 1.7010 Sr 0.0023 1.3830 P 0.0047 1.2032 K 0.0014 1.0385 Cl 0.0078 1.1227 Ca 0.2536 1.0977 Ba 0.0000 1.5364 Fe 0.0001 1.2559 Mn 0.0000 1.2781 iteration : 3 Analysis no. 163 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7303 0.025101 0.7303 0.5869 Mg 1.0716 0.019774 1.0716 0.8145 Sr 0.3182 0.014276 0.3182 0.0671 P 0.5688 0.028831 0.5688 0.3392 K 0.1505 0.010016 0.1505 0.0711 Cl 0.8798 0.020805 0.8798 0.4585 Ca 27.8410 0.133526 27.8410 12.8324 Ba 0.0026 0.019118 0.0026 0.0004 Fe 0.0159 0.014046 0.0159 0.0052 Mn 0.0051 0.019128 0.0051 0.0017 C 15.2041 15.2041 23.3846 O 53.2119 53.2119 61.4384 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 164 x= -13405.0 y= 2876.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.2 5.4 3.6 4.73 0.0174 5.4 0.0289 Mg 68.7 2.7 2.5 27.29 0.0369 2.7 0.0111 Sr 24.9 3.2 14.3 1.75 0.0015 3.2 0.0398 P 22.1 4.8 2.4 9.38 0.0252 4.8 0.0395 K 16.8 5.4 5.1 3.29 0.0107 5.5 0.0189 Cl 69.1 2.2 2.2 31.40 0.0147 2.2 0.0227 Ca 2783.2 0.4 17.7 157.68 0.6106 0.5 0.0335 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.0 9.2 3.3 0.90 0.0000 9.2 0.0000 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0628 Elt. k-ratio Correc. Na 0.0009 2.3365 Mg 0.0027 1.7034 Sr 0.0009 1.3826 P 0.0040 1.2030 K 0.0010 1.0495 Cl 0.0082 1.1276 Ca 0.2216 1.1032 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2834 iteration : 2 Analysis no. 164 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2025 0.015281 0.2025 0.1568 Mg 0.4557 0.013066 0.4557 0.3338 Sr 0.1298 0.012073 0.1298 0.0264 P 0.4758 0.026772 0.4758 0.2735 K 0.1000 0.008950 0.1000 0.0455 Cl 0.9216 0.021316 0.9216 0.4628 Ca 24.4477 0.123074 24.4477 10.8611 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0216 0.019973 0.0216 0.0070 C 17.1001 17.1001 25.3504 O 56.1453 56.1453 62.4826 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 165 x= -13403.0 y= 2880.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 28.5 4.2 3.6 7.84 0.0319 4.2 0.0288 Mg 98.6 2.2 2.5 39.17 0.0536 2.3 0.0110 Sr 33.4 2.7 14.3 2.34 0.0027 2.7 0.0397 P 25.2 4.4 2.4 10.72 0.0293 4.5 0.0393 K 24.6 4.5 5.1 4.81 0.0179 4.5 0.0186 Cl 74.5 2.1 2.2 33.85 0.0159 2.1 0.0224 Ca 3419.7 0.4 17.7 193.74 0.7511 0.5 0.0333 Ba 10.6 4.8 10.8 0.99 0.0000 4.9 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0556 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0625 Elt. k-ratio Correc. Na 0.0016 2.3265 Mg 0.0039 1.6992 Sr 0.0017 1.3766 P 0.0046 1.1971 K 0.0016 1.0298 Cl 0.0088 1.1164 Ca 0.2726 1.0951 Ba 0.0000 NaN Fe 0.0000 1.2545 Mn 0.0002 1.2771 iteration : 3 Analysis no. 165 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3701 0.018938 0.3701 0.3012 Mg 0.6600 0.015576 0.6600 0.5080 Sr 0.2322 0.013267 0.2322 0.0496 P 0.5492 0.028328 0.5492 0.3317 K 0.1631 0.010224 0.1631 0.0781 Cl 0.9862 0.021898 0.9862 0.5204 Ca 29.8520 0.139643 29.8520 13.9340 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013605 0.0017 0.0006 Mn 0.0196 0.019794 0.0196 0.0067 C 14.7691 14.7691 23.0041 O 52.3968 52.3968 61.2657 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 166 x= -13401.0 y= 2884.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 18.2 5.2 3.6 5.02 0.0187 5.3 0.0289 Mg 68.4 2.7 2.5 27.17 0.0368 2.7 0.0111 Sr 23.1 3.3 14.3 1.62 0.0013 3.3 0.0399 P 22.2 4.7 2.4 9.43 0.0254 4.8 0.0396 K 20.3 5.0 5.1 3.98 0.0140 5.0 0.0191 Cl 61.4 2.3 2.2 27.89 0.0130 2.3 0.0228 Ca 2527.6 0.4 17.7 143.20 0.5543 0.5 0.0336 Ba 7.2 5.9 10.8 0.67 0.0000 5.9 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0560 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0630 Elt. k-ratio Correc. Na 0.0009 2.3383 Mg 0.0027 1.7054 Sr 0.0008 1.3858 P 0.0040 1.2061 K 0.0012 1.0581 Cl 0.0072 1.1327 Ca 0.2012 1.1065 Ba 0.0000 NaN Fe 0.0000 1.2650 Mn 0.0002 1.2856 iteration : 2 Analysis no. 166 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2184 0.015680 0.2184 0.1661 Mg 0.4542 0.013056 0.4542 0.3268 Sr 0.1078 0.011817 0.1078 0.0215 P 0.4796 0.026904 0.4796 0.2708 K 0.1310 0.009722 0.1310 0.0586 Cl 0.8192 0.020217 0.8192 0.4041 Ca 22.2587 0.116158 22.2587 9.7119 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013799 0.0042 0.0013 Mn 0.0307 0.020425 0.0307 0.0098 C 17.9423 17.9423 26.1235 O 57.5539 57.5539 62.9056 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 167 x= -13400.0 y= 2888.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 28.9 4.2 3.6 7.95 0.0324 4.2 0.0288 Mg 90.6 2.3 2.5 35.99 0.0492 2.4 0.0111 Sr 35.1 2.7 14.3 2.46 0.0030 2.7 0.0397 P 24.8 4.5 2.4 10.53 0.0287 4.5 0.0394 K 24.5 4.5 5.1 4.80 0.0178 4.5 0.0186 Cl 64.2 2.3 2.2 29.18 0.0136 2.3 0.0225 Ca 3296.0 0.4 17.7 186.73 0.7240 0.5 0.0333 Ba 10.3 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 4.0 7.9 3.3 1.22 0.0004 7.9 0.0556 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0626 Elt. k-ratio Correc. Na 0.0016 2.3291 Mg 0.0036 1.7011 Sr 0.0018 1.3781 P 0.0045 1.1989 K 0.0016 1.0329 Cl 0.0076 1.1188 Ca 0.2627 1.0964 Ba 0.0000 NaN Fe 0.0002 1.2559 Mn 0.0002 1.2782 iteration : 3 Analysis no. 167 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3765 0.019082 0.3765 0.3035 Mg 0.6058 0.014955 0.6058 0.4618 Sr 0.2534 0.013524 0.2534 0.0536 P 0.5393 0.028141 0.5393 0.3226 K 0.1633 0.010249 0.1633 0.0774 Cl 0.8480 0.020414 0.8480 0.4431 Ca 28.8083 0.136493 28.8083 13.3169 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0242 0.014298 0.0242 0.0080 Mn 0.0233 0.019980 0.0233 0.0079 C 15.2091 15.2091 23.4606 O 53.1488 53.1488 61.5447 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 168 x= -13398.0 y= 2893.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 34.5 3.8 3.6 9.51 0.0396 3.8 0.0288 Mg 114.9 2.1 2.5 45.63 0.0627 2.1 0.0110 Sr 40.8 2.5 14.3 2.86 0.0038 2.5 0.0397 P 24.5 4.5 2.4 10.43 0.0284 4.5 0.0394 K 22.9 4.7 5.1 4.49 0.0163 4.7 0.0186 Cl 71.0 2.2 2.2 32.28 0.0151 2.2 0.0225 Ca 3408.1 0.4 17.7 193.09 0.7488 0.5 0.0333 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.5 8.4 3.3 1.06 0.0001 8.5 0.0556 Mn 4.4 10.7 2.7 1.61 0.0016 10.7 0.0625 Elt. k-ratio Correc. Na 0.0020 2.3236 Mg 0.0045 1.6994 Sr 0.0023 1.3777 P 0.0044 1.1987 K 0.0015 1.0304 Cl 0.0084 1.1173 Ca 0.2718 1.0949 Ba 0.0000 NaN Fe 0.0001 1.2540 Mn 0.0005 1.2766 iteration : 3 Analysis no. 168 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4598 0.020645 0.4598 0.3746 Mg 0.7719 0.016813 0.7719 0.5948 Sr 0.3226 0.014287 0.3226 0.0690 P 0.5332 0.028007 0.5332 0.3224 K 0.1494 0.009943 0.1494 0.0716 Cl 0.9399 0.021415 0.9399 0.4965 Ca 29.7537 0.139345 29.7537 13.9033 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0067 0.013756 0.0067 0.0022 Mn 0.0595 0.021542 0.0595 0.0203 C 14.7022 14.7022 22.9249 O 52.3010 52.3010 61.2204 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 169 x= -13397.0 y= 2897.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 29.3 4.1 3.6 8.07 0.0329 4.1 0.0288 Mg 81.3 2.5 2.5 32.28 0.0440 2.5 0.0111 Sr 32.9 2.8 14.3 2.30 0.0027 2.8 0.0397 P 25.1 4.5 2.4 10.68 0.0291 4.5 0.0394 K 24.4 4.5 5.1 4.78 0.0177 4.5 0.0187 Cl 65.3 2.3 2.2 29.70 0.0139 2.3 0.0225 Ca 3165.7 0.4 17.7 179.35 0.6953 0.5 0.0334 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 2.9 9.2 3.3 0.89 0.0000 9.3 0.0000 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0627 Elt. k-ratio Correc. Na 0.0016 2.3300 Mg 0.0032 1.7021 Sr 0.0016 1.3791 P 0.0046 1.1999 K 0.0016 1.0372 Cl 0.0077 1.1211 Ca 0.2523 1.0982 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2794 iteration : 3 Analysis no. 169 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3827 0.019209 0.3827 0.3054 Mg 0.5418 0.014181 0.5418 0.4090 Sr 0.2259 0.013216 0.2259 0.0473 P 0.5482 0.028350 0.5482 0.3247 K 0.1631 0.010274 0.1631 0.0765 Cl 0.8653 0.020632 0.8653 0.4478 Ca 27.7091 0.133159 27.7091 12.6832 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0251 0.020083 0.0251 0.0084 C 15.6630 15.6630 23.9237 O 53.8756 53.8756 61.7741 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 170 x= -13395.0 y= 2901.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 36.5 3.7 3.6 10.06 0.0422 3.7 0.0288 Mg 109.4 2.1 2.5 43.44 0.0597 2.2 0.0110 Sr 33.7 2.7 14.3 2.36 0.0028 2.7 0.0398 P 28.0 4.2 2.4 11.92 0.0328 4.2 0.0394 K 23.8 4.6 5.1 4.66 0.0171 4.6 0.0187 Cl 68.4 2.2 2.2 31.09 0.0145 2.2 0.0225 Ca 3164.4 0.4 17.7 179.27 0.6948 0.5 0.0334 Ba 9.3 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0557 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0626 Elt. k-ratio Correc. Na 0.0021 2.3243 Mg 0.0043 1.7011 Sr 0.0017 1.3803 P 0.0052 1.2007 K 0.0015 1.0383 Cl 0.0081 1.1220 Ca 0.2522 1.0982 Ba 0.0000 NaN Fe 0.0000 1.2569 Mn 0.0001 1.2790 iteration : 3 Analysis no. 170 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4897 0.021189 0.4897 0.3917 Mg 0.7347 0.016418 0.7347 0.5559 Sr 0.2367 0.013348 0.2367 0.0497 P 0.6184 0.029844 0.6184 0.3671 K 0.1577 0.010169 0.1577 0.0742 Cl 0.9079 0.021111 0.9079 0.4709 Ca 27.6922 0.133097 27.6922 12.7048 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0033 0.013684 0.0033 0.0011 Mn 0.0124 0.019488 0.0124 0.0042 C 15.4915 15.4915 23.7166 O 53.6553 53.6553 61.6640 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 171 x= -13394.0 y= 2905.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 24.6 4.5 3.6 6.78 0.0269 4.5 0.0288 Mg 86.9 2.4 2.5 34.52 0.0471 2.4 0.0110 Sr 35.3 2.7 14.3 2.47 0.0030 2.7 0.0397 P 24.2 4.5 2.4 10.30 0.0280 4.6 0.0394 K 25.3 4.4 5.1 4.96 0.0186 4.5 0.0187 Cl 67.4 2.2 2.2 30.64 0.0143 2.2 0.0225 Ca 3271.0 0.4 17.7 185.32 0.7185 0.5 0.0334 Ba 10.6 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0557 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0626 Elt. k-ratio Correc. Na 0.0013 2.3300 Mg 0.0034 1.7005 Sr 0.0019 1.3778 P 0.0044 1.1988 K 0.0016 1.0339 Cl 0.0080 1.1191 Ca 0.2608 1.0968 Ba 0.0000 NaN Fe 0.0001 1.2561 Mn 0.0003 1.2784 iteration : 3 Analysis no. 171 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3132 0.017786 0.3132 0.2520 Mg 0.5802 0.014645 0.5802 0.4414 Sr 0.2555 0.013546 0.2555 0.0539 P 0.5261 0.027851 0.5261 0.3141 K 0.1701 0.010397 0.1701 0.0805 Cl 0.8920 0.020910 0.8920 0.4653 Ca 28.6004 0.135869 28.6004 13.1952 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0117 0.013931 0.0117 0.0039 Mn 0.0342 0.020474 0.0342 0.0115 C 15.3199 15.3199 23.5859 O 53.2966 53.2966 61.5964 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 172 x= -13392.0 y= 2910.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 37.5 3.6 3.6 10.33 0.0434 3.7 0.0287 Mg 128.6 2.0 2.5 51.07 0.0704 2.0 0.0110 Sr 45.2 2.3 14.3 3.17 0.0044 2.4 0.0397 P 27.0 4.3 2.4 11.49 0.0316 4.3 0.0394 K 25.6 4.4 5.1 5.02 0.0188 4.4 0.0186 Cl 65.7 2.3 2.2 29.86 0.0139 2.3 0.0225 Ca 3451.0 0.4 17.7 195.51 0.7582 0.5 0.0333 Ba 10.5 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0555 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0625 Elt. k-ratio Correc. Na 0.0022 2.3207 Mg 0.0051 1.6985 Sr 0.0027 1.3777 P 0.0050 1.1991 K 0.0017 1.0294 Cl 0.0078 1.1173 Ca 0.2752 1.0943 Ba 0.0000 NaN Fe 0.0001 1.2532 Mn 0.0004 1.2760 iteration : 3 Analysis no. 172 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5031 0.021411 0.5031 0.4117 Mg 0.8656 0.017780 0.8656 0.6700 Sr 0.3761 0.014853 0.3761 0.0807 P 0.5936 0.029306 0.5936 0.3605 K 0.1719 0.010403 0.1719 0.0827 Cl 0.8673 0.020616 0.8673 0.4602 Ca 30.1115 0.140415 30.1115 14.1331 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0108 0.013873 0.0108 0.0037 Mn 0.0450 0.020910 0.0450 0.0154 C 14.4639 14.4639 22.6536 O 51.9912 51.9912 61.1284 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 173 x= -13391.0 y= 2914.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 34.6 3.8 3.6 9.54 0.0398 3.8 0.0288 Mg 97.3 2.3 2.5 38.65 0.0529 2.3 0.0111 Sr 36.2 2.6 14.3 2.54 0.0031 2.6 0.0398 P 28.0 4.2 2.4 11.89 0.0328 4.2 0.0395 K 26.3 4.4 5.1 5.15 0.0194 4.4 0.0188 Cl 62.9 2.3 2.2 28.57 0.0133 2.3 0.0226 Ca 3050.3 0.4 17.7 172.81 0.6698 0.5 0.0334 Ba 9.8 5.1 10.8 0.91 0.0000 5.1 0.0000 Fe 3.1 9.0 3.3 0.92 0.0000 9.1 0.0000 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0627 Elt. k-ratio Correc. Na 0.0020 2.3264 Mg 0.0038 1.7020 Sr 0.0019 1.3809 P 0.0051 1.2020 K 0.0017 1.0417 Cl 0.0074 1.1241 Ca 0.2431 1.0996 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2800 iteration : 3 Analysis no. 173 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4619 0.020698 0.4619 0.3663 Mg 0.6523 0.015503 0.6523 0.4893 Sr 0.2671 0.013700 0.2671 0.0556 P 0.6180 0.029857 0.6180 0.3637 K 0.1795 0.010639 0.1795 0.0837 Cl 0.8337 0.020302 0.8337 0.4287 Ca 26.7278 0.130150 26.7278 12.1570 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0197 0.019843 0.0197 0.0065 C 15.9049 15.9049 24.1403 O 54.3352 54.3352 61.9090 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 174 x= -13389.0 y= 2918.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 41.3 3.5 3.6 11.37 0.0483 3.5 0.0287 Mg 122.2 2.0 2.5 48.51 0.0668 2.0 0.0110 Sr 38.7 2.5 14.3 2.71 0.0035 2.6 0.0398 P 30.8 4.0 2.4 13.09 0.0364 4.0 0.0394 K 28.7 4.2 5.1 5.62 0.0216 4.2 0.0187 Cl 73.9 2.1 2.2 33.58 0.0157 2.1 0.0225 Ca 3245.0 0.4 17.7 183.84 0.7127 0.5 0.0334 Ba 11.4 4.7 10.8 1.06 0.0004 4.7 0.0744 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0556 Mn 4.2 11.0 2.7 1.53 0.0014 11.0 0.0626 Elt. k-ratio Correc. Na 0.0024 2.3199 Mg 0.0048 1.6998 Sr 0.0021 1.3794 P 0.0057 1.2003 K 0.0019 1.0368 Cl 0.0088 1.1210 Ca 0.2587 1.0970 Ba 0.0001 1.5367 Fe 0.0000 1.2552 Mn 0.0004 1.2775 iteration : 3 Analysis no. 174 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5595 0.022385 0.5595 0.4516 Mg 0.8219 0.017339 0.8219 0.6275 Sr 0.2966 0.014016 0.2966 0.0628 P 0.6846 0.031179 0.6846 0.4101 K 0.1989 0.010989 0.1989 0.0944 Cl 0.9822 0.021904 0.9822 0.5141 Ca 28.3748 0.135174 28.3748 13.1375 Ba 0.0163 0.019361 0.0163 0.0022 Fe 0.0008 0.013590 0.0008 0.0003 Mn 0.0523 0.021248 0.0523 0.0177 C 15.0577 15.0577 23.2641 O 52.9545 52.9545 61.4176 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 175 x= -13387.0 y= 2922.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 36.3 3.7 3.6 10.01 0.0420 3.7 0.0288 Mg 90.7 2.3 2.5 36.03 0.0493 2.4 0.0111 Sr 33.2 2.7 14.3 2.32 0.0027 2.8 0.0399 P 29.4 4.1 2.4 12.51 0.0347 4.1 0.0396 K 27.6 4.3 5.1 5.40 0.0206 4.3 0.0190 Cl 71.0 2.2 2.2 32.26 0.0151 2.2 0.0227 Ca 2786.9 0.4 17.7 157.89 0.6116 0.5 0.0335 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0559 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0628 Elt. k-ratio Correc. Na 0.0021 2.3262 Mg 0.0036 1.7031 Sr 0.0017 1.3831 P 0.0054 1.2043 K 0.0018 1.0513 Cl 0.0084 1.1290 Ca 0.2220 1.1031 Ba 0.0000 NaN Fe 0.0000 1.2608 Mn 0.0001 1.2821 iteration : 2 Analysis no. 175 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4872 0.021158 0.4872 0.3795 Mg 0.6073 0.014983 0.6073 0.4475 Sr 0.2303 0.013298 0.2303 0.0471 P 0.6543 0.030632 0.6543 0.3783 K 0.1923 0.010960 0.1923 0.0881 Cl 0.9493 0.021635 0.9493 0.4795 Ca 24.4860 0.123206 24.4860 10.9410 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0008 0.013653 0.0008 0.0003 Mn 0.0143 0.019625 0.0143 0.0046 C 16.7342 16.7342 24.9513 O 55.6441 55.6441 62.2828 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 176 x= -13386.0 y= 2927.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 25.6 4.4 3.6 7.06 0.0282 4.4 0.0288 Mg 81.9 2.5 2.5 32.53 0.0443 2.5 0.0111 Sr 30.0 2.9 14.3 2.10 0.0022 2.9 0.0398 P 36.8 3.7 2.4 15.66 0.0441 3.7 0.0395 K 27.2 4.3 5.1 5.32 0.0203 4.3 0.0189 Cl 70.5 2.2 2.2 32.03 0.0150 2.2 0.0226 Ca 2957.2 0.4 17.7 167.54 0.6492 0.5 0.0335 Ba 9.1 5.2 10.8 0.84 0.0000 5.3 0.0000 Fe 3.7 8.2 3.3 1.13 0.0002 8.2 0.0558 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0628 Elt. k-ratio Correc. Na 0.0014 2.3284 Mg 0.0032 1.7007 Sr 0.0014 1.3800 P 0.0069 1.2011 K 0.0018 1.0456 Cl 0.0083 1.1260 Ca 0.2356 1.1010 Ba 0.0000 NaN Fe 0.0001 1.2591 Mn 0.0002 1.2808 iteration : 2 Analysis no. 176 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3280 0.018090 0.3280 0.2585 Mg 0.5459 0.014225 0.5459 0.4070 Sr 0.1914 0.012816 0.1914 0.0396 P 0.8311 0.033981 0.8311 0.4863 K 0.1879 0.010833 0.1879 0.0871 Cl 0.9398 0.021502 0.9398 0.4804 Ca 25.9422 0.127741 25.9422 11.7303 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0142 0.014040 0.0142 0.0046 Mn 0.0215 0.019940 0.0215 0.0071 C 16.1627 16.1627 24.3874 O 54.8354 54.8354 62.1117 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 177 x= -13384.0 y= 2931.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.0 4.0 3.6 8.53 0.0351 4.0 0.0288 Mg 106.4 2.2 2.5 42.25 0.0580 2.2 0.0110 Sr 36.1 2.6 14.3 2.53 0.0031 2.6 0.0397 P 36.7 3.7 2.4 15.62 0.0440 3.7 0.0394 K 29.0 4.1 5.1 5.69 0.0220 4.2 0.0188 Cl 78.8 2.1 2.2 35.82 0.0168 2.1 0.0226 Ca 3142.7 0.4 17.7 178.05 0.6902 0.5 0.0334 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0557 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0626 Elt. k-ratio Correc. Na 0.0018 2.3223 Mg 0.0042 1.6983 Sr 0.0019 1.3786 P 0.0069 1.2000 K 0.0019 1.0407 Cl 0.0094 1.1229 Ca 0.2505 1.0986 Ba 0.0000 NaN Fe 0.0001 1.2565 Mn 0.0001 1.2786 iteration : 3 Analysis no. 177 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4068 0.019640 0.4068 0.3259 Mg 0.7131 0.016170 0.7131 0.5403 Sr 0.2654 0.013665 0.2654 0.0558 P 0.8279 0.033905 0.8279 0.4923 K 0.2027 0.011089 0.2027 0.0955 Cl 1.0519 0.022653 1.0519 0.5464 Ca 27.5195 0.132589 27.5195 12.6453 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0184 0.014135 0.0184 0.0061 Mn 0.0160 0.019655 0.0160 0.0054 C 15.4058 15.4058 23.6221 O 53.5726 53.5727 61.6651 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 178 x= -13383.0 y= 2935.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 35.2 3.8 3.6 9.69 0.0405 3.8 0.0287 Mg 110.5 2.1 2.5 43.88 0.0603 2.1 0.0110 Sr 34.5 2.7 14.3 2.41 0.0029 2.7 0.0398 P 39.2 3.6 2.4 16.68 0.0472 3.6 0.0395 K 25.2 4.4 5.1 4.94 0.0185 4.5 0.0190 Cl 74.5 2.1 2.2 33.87 0.0159 2.1 0.0227 Ca 2846.7 0.4 17.7 161.28 0.6248 0.5 0.0335 Ba 10.0 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0558 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0628 Elt. k-ratio Correc. Na 0.0020 2.3216 Mg 0.0044 1.7000 Sr 0.0018 1.3822 P 0.0074 1.2036 K 0.0016 1.0507 Cl 0.0088 1.1291 Ca 0.2268 1.1024 Ba 0.0000 NaN Fe 0.0000 1.2596 Mn 0.0001 1.2810 iteration : 2 Analysis no. 178 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4692 0.020806 0.4692 0.3681 Mg 0.7420 0.016495 0.7420 0.5506 Sr 0.2463 0.013476 0.2463 0.0507 P 0.8908 0.035098 0.8908 0.5187 K 0.1721 0.010549 0.1721 0.0794 Cl 0.9982 0.022158 0.9982 0.5078 Ca 24.9981 0.124807 24.9981 11.2488 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0050 0.013768 0.0050 0.0016 Mn 0.0124 0.019525 0.0124 0.0041 C 16.3267 16.3267 24.5159 O 55.1392 55.1392 62.1543 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 179 x= -13381.0 y= 2939.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.3 4.0 3.6 8.62 0.0355 4.0 0.0288 Mg 111.9 2.1 2.5 44.42 0.0610 2.1 0.0110 Sr 33.9 2.7 14.3 2.37 0.0028 2.7 0.0397 P 37.1 3.7 2.4 15.79 0.0445 3.7 0.0394 K 27.2 4.3 5.1 5.33 0.0203 4.3 0.0188 Cl 77.9 2.1 2.2 35.42 0.0166 2.1 0.0226 Ca 3136.1 0.4 17.7 177.67 0.6887 0.5 0.0334 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 4.2 7.7 3.3 1.28 0.0005 7.7 0.0557 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0626 Elt. k-ratio Correc. Na 0.0018 2.3225 Mg 0.0044 1.6985 Sr 0.0017 1.3791 P 0.0070 1.2001 K 0.0018 1.0408 Cl 0.0093 1.1231 Ca 0.2499 1.0986 Ba 0.0000 NaN Fe 0.0002 1.2566 Mn 0.0002 1.2786 iteration : 3 Analysis no. 179 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4112 0.019727 0.4112 0.3293 Mg 0.7506 0.016579 0.7506 0.5685 Sr 0.2381 0.013357 0.2381 0.0500 P 0.8375 0.034082 0.8375 0.4978 K 0.1874 0.010791 0.1874 0.0882 Cl 1.0396 0.022527 1.0396 0.5398 Ca 27.4605 0.132403 27.4605 12.6123 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0309 0.014501 0.0309 0.0102 Mn 0.0269 0.020152 0.0269 0.0090 C 15.4118 15.4118 23.6205 O 53.6054 53.6054 61.6744 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 180 x= -13380.0 y= 2944.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 24.0 4.6 3.6 6.62 0.0262 4.6 0.0289 Mg 65.2 2.8 2.5 25.88 0.0350 2.8 0.0111 Sr 24.8 3.2 14.3 1.73 0.0015 3.2 0.0399 P 38.8 3.6 2.4 16.51 0.0467 3.6 0.0396 K 29.3 4.1 5.1 5.75 0.0222 4.1 0.0192 Cl 72.2 2.1 2.2 32.84 0.0154 2.1 0.0228 Ca 2506.3 0.4 17.7 141.99 0.5497 0.5 0.0337 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0630 Elt. k-ratio Correc. Na 0.0013 2.3311 Mg 0.0025 1.7029 Sr 0.0009 1.3839 P 0.0073 1.2052 K 0.0020 1.0615 Cl 0.0086 1.1345 Ca 0.1995 1.1071 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2848 iteration : 2 Analysis no. 180 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3044 0.017604 0.3044 0.2324 Mg 0.4313 0.012733 0.4313 0.3114 Sr 0.1279 0.012062 0.1279 0.0256 P 0.8823 0.034972 0.8823 0.4999 K 0.2093 0.011360 0.2093 0.0939 Cl 0.9715 0.021930 0.9715 0.4809 Ca 22.0834 0.115615 22.0834 9.6697 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0106 0.019497 0.0106 0.0034 C 17.6803 17.6803 25.8334 O 57.2990 57.2990 62.8494 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 181 x= -13378.0 y= 2948.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 24.0 4.6 3.6 6.60 0.0261 4.6 0.0288 Mg 86.0 2.4 2.5 34.14 0.0466 2.4 0.0111 Sr 30.9 2.8 14.3 2.16 0.0024 2.9 0.0398 P 35.7 3.7 2.4 15.19 0.0427 3.8 0.0395 K 24.8 4.5 5.1 4.85 0.0181 4.5 0.0190 Cl 78.7 2.1 2.2 35.76 0.0168 2.1 0.0227 Ca 2844.8 0.4 17.7 161.17 0.6247 0.5 0.0336 Ba 8.8 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0559 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0628 Elt. k-ratio Correc. Na 0.0013 2.3273 Mg 0.0034 1.6999 Sr 0.0015 1.3809 P 0.0067 1.2022 K 0.0016 1.0500 Cl 0.0094 1.1280 Ca 0.2267 1.1025 Ba 0.0000 NaN Fe 0.0000 1.2602 Mn 0.0001 1.2816 iteration : 2 Analysis no. 181 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3033 0.017568 0.3033 0.2374 Mg 0.5738 0.014569 0.5738 0.4247 Sr 0.2023 0.012958 0.2023 0.0415 P 0.8057 0.033540 0.8057 0.4679 K 0.1682 0.010469 0.1682 0.0774 Cl 1.0553 0.022747 1.0553 0.5355 Ca 24.9974 0.124834 24.9974 11.2200 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0008 0.013653 0.0008 0.0003 Mn 0.0106 0.019458 0.0106 0.0035 C 16.5229 16.5229 24.7475 O 55.3597 55.3597 62.2444 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 182 x= -13377.0 y= 2952.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 38.0 3.6 3.6 10.46 0.0441 3.6 0.0287 Mg 133.6 1.9 2.5 53.04 0.0732 2.0 0.0110 Sr 41.1 2.5 14.3 2.88 0.0038 2.5 0.0397 P 40.7 3.5 2.4 17.32 0.0491 3.5 0.0394 K 30.1 4.1 5.1 5.90 0.0230 4.1 0.0188 Cl 89.2 1.9 2.2 40.54 0.0191 1.9 0.0226 Ca 3175.9 0.4 17.7 179.93 0.6976 0.5 0.0334 Ba 11.9 4.6 10.8 1.11 0.0007 4.6 0.0744 Fe 3.6 8.3 3.3 1.09 0.0002 8.3 0.0556 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0626 Elt. k-ratio Correc. Na 0.0022 2.3149 Mg 0.0053 1.6962 Sr 0.0024 1.3787 P 0.0077 1.2004 K 0.0020 1.0414 Cl 0.0106 1.1232 Ca 0.2532 1.0980 Ba 0.0002 1.5360 Fe 0.0001 1.2551 Mn 0.0003 1.2773 iteration : 3 Analysis no. 182 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5094 0.021493 0.5094 0.4109 Mg 0.8986 0.018099 0.8986 0.6856 Sr 0.3263 0.014336 0.3263 0.0691 P 0.9247 0.035645 0.9247 0.5536 K 0.2121 0.011276 0.2121 0.1006 Cl 1.1948 0.024082 1.1948 0.6249 Ca 27.7988 0.133438 27.7988 12.8613 Ba 0.0299 0.019584 0.0299 0.0040 Fe 0.0100 0.013871 0.0100 0.0033 Mn 0.0323 0.020378 0.0323 0.0109 C 15.0520 15.0520 23.2381 O 53.0111 53.0111 61.4377 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 183 x= -13375.0 y= 2956.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.8 5.3 3.6 4.91 0.0182 5.3 0.0289 Mg 82.3 2.5 2.5 32.69 0.0446 2.5 0.0111 Sr 24.6 3.2 14.3 1.72 0.0015 3.2 0.0399 P 35.8 3.7 2.4 15.24 0.0429 3.7 0.0396 K 27.3 4.3 5.1 5.35 0.0204 4.3 0.0192 Cl 66.8 2.2 2.2 30.38 0.0142 2.2 0.0228 Ca 2504.2 0.4 17.7 141.87 0.5493 0.5 0.0337 Ba 8.1 5.5 10.8 0.76 0.0000 5.6 0.0000 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0560 Mn 2.8 13.3 2.7 1.03 0.0001 13.4 0.0630 Elt. k-ratio Correc. Na 0.0009 2.3326 Mg 0.0032 1.7021 Sr 0.0009 1.3849 P 0.0067 1.2059 K 0.0018 1.0610 Cl 0.0079 1.1345 Ca 0.1993 1.1070 Ba 0.0000 NaN Fe 0.0002 1.2644 Mn 0.0000 1.2850 iteration : 2 Analysis no. 183 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2120 0.015502 0.2120 0.1616 Mg 0.5492 0.014274 0.5492 0.3961 Sr 0.1261 0.012049 0.1261 0.0252 P 0.8103 0.033675 0.8103 0.4586 K 0.1919 0.011019 0.1919 0.0861 Cl 0.8967 0.021116 0.8967 0.4434 Ca 22.0674 0.115567 22.0674 9.6529 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0210 0.014301 0.0210 0.0066 Mn 0.0033 0.019158 0.0033 0.0011 C 17.7294 17.7294 25.8792 O 57.3928 57.3928 62.8891 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 184 x= -13373.0 y= 2961.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 38.5 3.6 3.6 10.60 0.0447 3.6 0.0287 Mg 109.4 2.1 2.5 43.44 0.0597 2.2 0.0110 Sr 30.5 2.9 14.3 2.14 0.0023 2.9 0.0398 P 54.3 3.0 2.4 23.11 0.0666 3.0 0.0394 K 31.1 4.0 5.1 6.10 0.0239 4.0 0.0189 Cl 77.7 2.1 2.2 35.32 0.0166 2.1 0.0227 Ca 3022.2 0.4 17.7 171.22 0.6637 0.5 0.0335 Ba 9.0 5.3 10.8 0.84 0.0000 5.3 0.0000 Fe 4.0 7.9 3.3 1.20 0.0004 8.0 0.0557 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0627 Elt. k-ratio Correc. Na 0.0022 2.3176 Mg 0.0043 1.6980 Sr 0.0014 1.3792 P 0.0104 1.2004 K 0.0021 1.0462 Cl 0.0092 1.1268 Ca 0.2409 1.1003 Ba 0.0000 NaN Fe 0.0002 1.2572 Mn 0.0001 1.2790 iteration : 2 Analysis no. 184 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5174 0.021649 0.5174 0.4124 Mg 0.7337 0.016395 0.7337 0.5531 Sr 0.1977 0.012887 0.1977 0.0413 P 1.2526 0.041013 1.2526 0.7410 K 0.2216 0.011488 0.2216 0.1039 Cl 1.0404 0.022576 1.0404 0.5377 Ca 26.5004 0.129471 26.5004 12.1148 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0217 0.014242 0.0217 0.0071 Mn 0.0142 0.019580 0.0142 0.0047 C 15.4968 15.4968 23.6403 O 54.0034 54.0034 61.8436 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 185 x= -13372.0 y= 2965.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 30.2 4.1 3.6 8.31 0.0341 4.1 0.0288 Mg 94.0 2.3 2.5 37.34 0.0512 2.3 0.0110 Sr 39.1 2.5 14.3 2.74 0.0035 2.5 0.0398 P 54.4 3.0 2.4 23.15 0.0668 3.0 0.0395 K 29.7 4.1 5.1 5.82 0.0226 4.1 0.0189 Cl 80.1 2.0 2.2 36.39 0.0171 2.0 0.0227 Ca 3010.1 0.4 17.7 170.53 0.6618 0.5 0.0335 Ba 11.2 4.7 10.8 1.04 0.0002 4.7 0.0745 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0558 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0628 Elt. k-ratio Correc. Na 0.0017 2.3194 Mg 0.0037 1.6966 Sr 0.0022 1.3777 P 0.0105 1.2004 K 0.0020 1.0467 Cl 0.0095 1.1271 Ca 0.2402 1.1002 Ba 0.0001 1.5355 Fe 0.0001 1.2570 Mn 0.0003 1.2788 iteration : 3 Analysis no. 185 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3948 0.019409 0.3948 0.3146 Mg 0.6284 0.015211 0.6284 0.4736 Sr 0.3018 0.014075 0.3018 0.0631 P 1.2565 0.041099 1.2565 0.7431 K 0.2101 0.011282 0.2101 0.0984 Cl 1.0741 0.022939 1.0741 0.5549 Ca 26.4234 0.129282 26.4234 12.0760 Ba 0.0104 0.019274 0.0104 0.0014 Fe 0.0159 0.014083 0.0159 0.0052 Mn 0.0342 0.020507 0.0342 0.0114 C 15.5714 15.5714 23.7470 O 54.0790 54.0790 61.9113 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 186 x= -13370.0 y= 2969.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.4 3.5 3.6 11.13 0.0472 3.5 0.0286 Mg 126.3 2.0 2.5 50.14 0.0691 2.0 0.0110 Sr 38.1 2.6 14.3 2.67 0.0034 2.6 0.0397 P 55.8 3.0 2.4 23.73 0.0684 3.0 0.0394 K 32.1 3.9 5.1 6.29 0.0248 4.0 0.0189 Cl 96.8 1.9 2.2 44.02 0.0208 1.9 0.0226 Ca 3075.4 0.4 17.7 174.23 0.6754 0.5 0.0334 Ba 11.2 4.7 10.8 1.04 0.0003 4.7 0.0744 Fe 3.1 9.0 3.3 0.93 0.0000 9.0 0.0000 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0626 Elt. k-ratio Correc. Na 0.0024 2.3111 Mg 0.0050 1.6947 Sr 0.0021 1.3780 P 0.0107 1.2000 K 0.0022 1.0465 Cl 0.0116 1.1262 Ca 0.2451 1.0996 Ba 0.0001 1.5355 Fe 0.0000 NaN Mn 0.0002 1.2777 iteration : 3 Analysis no. 186 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5441 0.022075 0.5441 0.4370 Mg 0.8477 0.017579 0.8477 0.6441 Sr 0.2896 0.013930 0.2896 0.0610 P 1.2871 0.041533 1.2871 0.7674 K 0.2302 0.011649 0.2302 0.1087 Cl 1.3031 0.025145 1.3031 0.6787 Ca 26.9513 0.130855 26.9513 12.4171 Ba 0.0111 0.019260 0.0111 0.0015 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0269 0.020139 0.0269 0.0090 C 15.1534 15.1534 23.2969 O 53.3554 53.3554 61.5785 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 187 x= -13369.0 y= 2973.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.6 4.0 3.6 8.71 0.0360 4.0 0.0288 Mg 81.0 2.5 2.5 32.18 0.0439 2.5 0.0111 Sr 31.3 2.8 14.3 2.19 0.0024 2.8 0.0399 P 49.2 3.2 2.4 20.94 0.0601 3.2 0.0396 K 31.3 4.0 5.1 6.14 0.0241 4.0 0.0190 Cl 72.3 2.1 2.2 32.87 0.0154 2.1 0.0228 Ca 2817.0 0.4 17.7 159.60 0.6193 0.5 0.0336 Ba 8.9 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0560 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0629 Elt. k-ratio Correc. Na 0.0018 2.3238 Mg 0.0032 1.7001 Sr 0.0015 1.3804 P 0.0094 1.2022 K 0.0021 1.0518 Cl 0.0086 1.1299 Ca 0.2247 1.1028 Ba 0.0000 NaN Fe 0.0001 1.2598 Mn 0.0002 1.2812 iteration : 2 Analysis no. 187 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4174 0.019871 0.4174 0.3270 Mg 0.5404 0.014166 0.5404 0.4005 Sr 0.2070 0.013022 0.2070 0.0426 P 1.1331 0.039198 1.1331 0.6589 K 0.2249 0.011600 0.2249 0.1036 Cl 0.9700 0.021885 0.9700 0.4928 Ca 24.7855 0.124222 24.7855 11.1388 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0109 0.013970 0.0109 0.0035 Mn 0.0197 0.019895 0.0197 0.0065 C 16.3633 16.3633 24.5393 O 55.3278 55.3278 62.2866 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 188 x= -13367.0 y= 2978.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 26.8 4.3 3.6 7.39 0.0298 4.3 0.0289 Mg 74.4 2.6 2.5 29.55 0.0401 2.6 0.0111 Sr 22.3 3.3 14.3 1.56 0.0011 3.4 0.0400 P 40.8 3.5 2.4 17.36 0.0493 3.5 0.0396 K 33.4 3.9 5.1 6.54 0.0259 3.9 0.0192 Cl 62.8 2.3 2.2 28.54 0.0133 2.3 0.0229 Ca 2392.8 0.5 17.7 135.56 0.5246 0.5 0.0337 Ba 7.7 5.7 10.8 0.71 0.0000 5.7 0.0000 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0561 Mn 2.7 13.6 2.7 1.00 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0015 2.3310 Mg 0.0029 1.7041 Sr 0.0007 1.3861 P 0.0077 1.2069 K 0.0023 1.0652 Cl 0.0074 1.1371 Ca 0.1904 1.1085 Ba 0.0000 NaN Fe 0.0001 1.2655 Mn 0.0000 NaN iteration : 2 Analysis no. 188 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3463 0.018483 0.3463 0.2623 Mg 0.4953 0.013598 0.4953 0.3549 Sr 0.0981 0.011695 0.0981 0.0195 P 0.9322 0.035882 0.9322 0.5241 K 0.2452 0.012057 0.2452 0.1092 Cl 0.8425 0.020530 0.8425 0.4139 Ca 21.1058 0.112471 21.1058 9.1704 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0135 0.014087 0.0135 0.0042 Mn 0.0000 0.000000 0.0000 0.0000 C 18.0021 18.0021 26.1011 O 57.9190 57.9190 63.0404 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 189 x= -13366.0 y= 2982.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.4 3.5 3.6 11.14 0.0473 3.5 0.0287 Mg 120.8 2.0 2.5 47.95 0.0661 2.1 0.0110 Sr 37.2 2.6 14.3 2.60 0.0033 2.6 0.0398 P 37.1 3.7 2.4 15.77 0.0445 3.7 0.0395 K 30.8 4.0 5.1 6.03 0.0236 4.0 0.0188 Cl 81.5 2.0 2.2 37.05 0.0174 2.0 0.0226 Ca 3173.8 0.4 17.7 179.81 0.6976 0.5 0.0334 Ba 11.5 4.7 10.8 1.07 0.0004 4.7 0.0745 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0627 Elt. k-ratio Correc. Na 0.0024 2.3178 Mg 0.0048 1.6985 Sr 0.0020 1.3792 P 0.0070 1.2002 K 0.0021 1.0402 Cl 0.0097 1.1227 Ca 0.2532 1.0981 Ba 0.0001 1.5364 Fe 0.0000 NaN Mn 0.0002 1.2779 iteration : 3 Analysis no. 189 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5468 0.022167 0.5468 0.4399 Mg 0.8123 0.017240 0.8123 0.6182 Sr 0.2785 0.013823 0.2785 0.0588 P 0.8371 0.034091 0.8371 0.4999 K 0.2175 0.011374 0.2175 0.1029 Cl 1.0895 0.023041 1.0895 0.5684 Ca 27.7992 0.133470 27.7992 12.8291 Ba 0.0189 0.019417 0.0189 0.0025 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0251 0.020074 0.0251 0.0085 C 15.1772 15.1772 23.3726 O 53.1979 53.1979 61.4992 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 190 x= -13364.0 y= 2986.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 43.3 3.4 3.6 11.94 0.0509 3.4 0.0287 Mg 124.3 2.0 2.5 49.35 0.0680 2.0 0.0110 Sr 33.9 2.7 14.3 2.37 0.0028 2.7 0.0398 P 42.4 3.4 2.4 18.02 0.0512 3.4 0.0395 K 33.8 3.8 5.1 6.62 0.0263 3.9 0.0190 Cl 85.4 2.0 2.2 38.81 0.0183 2.0 0.0227 Ca 2844.0 0.4 17.7 161.12 0.6242 0.5 0.0335 Ba 9.4 5.1 10.8 0.88 0.0000 5.2 0.0000 Fe 4.2 7.7 3.3 1.28 0.0005 7.7 0.0558 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0627 Elt. k-ratio Correc. Na 0.0025 2.3169 Mg 0.0049 1.6996 Sr 0.0017 1.3825 P 0.0080 1.2035 K 0.0023 1.0521 Cl 0.0102 1.1293 Ca 0.2265 1.1024 Ba 0.0000 NaN Fe 0.0002 1.2588 Mn 0.0003 1.2803 iteration : 3 Analysis no. 190 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5893 0.022871 0.5893 0.4639 Mg 0.8364 0.017489 0.8364 0.6229 Sr 0.2390 0.013394 0.2390 0.0494 P 0.9669 0.036429 0.9669 0.5650 K 0.2456 0.011971 0.2456 0.1137 Cl 1.1487 0.023697 1.1487 0.5864 Ca 24.9749 0.124736 24.9749 11.2783 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0310 0.014528 0.0310 0.0100 Mn 0.0379 0.020666 0.0379 0.0125 C 16.1293 16.1293 24.3055 O 54.8010 54.8010 61.9923 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 191 x= -13363.0 y= 2990.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 42.4 3.4 3.6 11.69 0.0499 3.5 0.0287 Mg 128.9 2.0 2.5 51.17 0.0706 2.0 0.0111 Sr 35.8 2.6 14.3 2.51 0.0031 2.7 0.0400 P 40.5 3.5 2.4 17.21 0.0489 3.5 0.0397 K 32.4 3.9 5.1 6.35 0.0251 3.9 0.0191 Cl 82.7 2.0 2.2 37.60 0.0177 2.0 0.0228 Ca 2785.9 0.4 17.7 157.83 0.6122 0.5 0.0336 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0559 Mn 2.9 13.2 2.7 1.05 0.0001 13.2 0.0629 Elt. k-ratio Correc. Na 0.0025 2.3164 Mg 0.0051 1.6994 Sr 0.0019 1.3833 P 0.0077 1.2046 K 0.0022 1.0538 Cl 0.0099 1.1305 Ca 0.2222 1.1032 Ba 0.0000 NaN Fe 0.0001 1.2596 Mn 0.0000 1.2809 iteration : 2 Analysis no. 191 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5766 0.022673 0.5766 0.4518 Mg 0.8690 0.017832 0.8690 0.6442 Sr 0.2627 0.013685 0.2627 0.0540 P 0.9230 0.035709 0.9230 0.5369 K 0.2347 0.011794 0.2347 0.1082 Cl 1.1143 0.023383 1.1143 0.5663 Ca 24.5108 0.123348 24.5108 11.0184 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0159 0.014113 0.0159 0.0051 Mn 0.0052 0.019206 0.0052 0.0017 C 16.3439 16.3439 24.5169 O 55.1438 55.1438 62.0964 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 192 x= -13361.0 y= 2995.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.1 5.4 3.6 4.71 0.0173 5.4 0.0289 Mg 68.4 2.7 2.5 27.17 0.0368 2.7 0.0111 Sr 32.1 2.8 14.3 2.25 0.0025 2.8 0.0399 P 45.5 3.3 2.4 19.34 0.0553 3.3 0.0396 K 26.5 4.3 5.1 5.20 0.0197 4.4 0.0191 Cl 75.2 2.1 2.2 34.20 0.0161 2.1 0.0228 Ca 2723.3 0.4 17.7 154.28 0.5984 0.5 0.0336 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 2.9 9.3 3.3 0.88 0.0000 9.3 0.0000 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0630 Elt. k-ratio Correc. Na 0.0009 2.3289 Mg 0.0027 1.6990 Sr 0.0016 1.3802 P 0.0087 1.2026 K 0.0017 1.0546 Cl 0.0089 1.1311 Ca 0.2172 1.1041 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2825 iteration : 2 Analysis no. 192 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2014 0.015239 0.2014 0.1564 Mg 0.4532 0.013027 0.4532 0.3329 Sr 0.2170 0.013136 0.2170 0.0442 P 1.0425 0.037719 1.0425 0.6009 K 0.1841 0.010830 0.1841 0.0841 Cl 1.0115 0.022334 1.0115 0.5094 Ca 23.9787 0.121687 23.9787 10.6814 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0179 0.019827 0.0179 0.0058 C 16.8528 16.8528 25.0509 O 56.0408 56.0408 62.5340 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 193 x= -13359.0 y= 2999.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 24.3 4.5 3.6 6.70 0.0266 4.5 0.0288 Mg 91.1 2.3 2.5 36.17 0.0495 2.4 0.0110 Sr 29.8 2.9 14.3 2.08 0.0022 2.9 0.0399 P 57.3 3.0 2.4 24.39 0.0705 3.0 0.0396 K 24.0 4.6 5.1 4.70 0.0173 4.6 0.0192 Cl 88.9 1.9 2.2 40.42 0.0191 1.9 0.0228 Ca 2638.6 0.4 17.7 149.49 0.5795 0.5 0.0337 Ba 10.3 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0629 Elt. k-ratio Correc. Na 0.0013 2.3210 Mg 0.0036 1.6969 Sr 0.0014 1.3810 P 0.0110 1.2032 K 0.0015 1.0599 Cl 0.0106 1.1340 Ca 0.2103 1.1054 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2824 iteration : 2 Analysis no. 193 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3079 0.017642 0.3079 0.2387 Mg 0.6081 0.014972 0.6081 0.4460 Sr 0.1887 0.012803 0.1887 0.0384 P 1.3294 0.042253 1.3294 0.7651 K 0.1629 0.010430 0.1629 0.0743 Cl 1.2037 0.024301 1.2037 0.6052 Ca 23.2471 0.119370 23.2471 10.3393 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0106 0.019481 0.0106 0.0034 C 16.8216 16.8216 24.9653 O 56.1200 56.1200 62.5243 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 194 x= -13358.0 y= 3003.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 16.4 5.5 3.6 4.51 0.0164 5.5 0.0291 Mg 29.7 4.1 2.5 11.78 0.0152 4.1 0.0112 Sr 14.1 4.2 14.3 0.98 0.0000 4.2 0.0000 P 20.5 4.9 2.4 8.72 0.0233 4.9 0.0404 K 8.8 7.5 5.1 1.73 0.0034 7.5 0.0206 Cl 89.2 1.9 2.2 40.56 0.0191 1.9 0.0237 Ca 600.4 0.9 17.7 34.02 0.1289 1.0 0.0346 Ba 7.0 6.0 10.8 0.65 0.0000 6.0 0.0000 Fe 2.7 9.7 3.3 0.81 0.0000 9.7 0.0000 Mn 2.0 15.8 2.7 0.74 0.0000 15.8 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3460 Mg 0.0011 1.7148 Sr 0.0000 NaN P 0.0037 1.2276 K 0.0003 1.1396 Cl 0.0107 1.1739 Ca 0.0468 1.1333 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 194 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1917 0.015075 0.1917 0.1284 Mg 0.1884 0.008826 0.1884 0.1194 Sr 0.0000 0.000000 0.0000 0.0000 P 0.4483 0.026484 0.4483 0.2228 K 0.0344 0.007754 0.0344 0.0136 Cl 1.2513 0.025216 1.2513 0.5434 Ca 5.3034 0.052507 5.3034 2.0372 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 24.5540 24.5540 31.4742 O 68.0286 68.0286 65.4612 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 195 x= -13356.0 y= 3007.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.6 5.3 3.6 4.84 0.0179 5.3 0.0293 Mg 11.1 6.7 2.5 4.41 0.0048 6.7 0.0112 Sr 10.9 4.8 14.3 0.77 0.0000 4.8 0.0000 P 3.3 12.4 2.4 1.38 0.0012 12.4 0.0407 K 5.7 9.4 5.1 1.11 0.0005 9.4 0.0211 Cl 64.0 2.3 2.2 29.07 0.0136 2.3 0.0239 Ca 55.5 3.0 17.7 3.14 0.0084 3.0 0.0348 Ba 6.5 6.2 10.8 0.60 0.0000 6.2 0.0000 Fe 1.8 11.9 3.3 0.54 0.0000 11.9 0.0000 Mn 1.6 17.9 2.7 0.57 0.0000 18.0 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3590 Mg 0.0003 1.7243 Sr 0.0000 NaN P 0.0002 1.2370 K 0.0000 1.1659 Cl 0.0076 1.1868 Ca 0.0030 1.1410 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 195 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2109 0.015609 0.2109 0.1358 Mg 0.0599 0.005764 0.0599 0.0365 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0224 0.013168 0.0224 0.0107 K 0.0052 0.006976 0.0052 0.0020 Cl 0.8978 0.021656 0.8978 0.3748 Ca 0.3464 0.017541 0.3464 0.1279 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8485 26.8485 33.0799 O 71.6088 71.6088 66.2325 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 196 x= -13355.0 y= 3012.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 9.4 7.3 3.6 2.59 0.0074 7.3 0.0293 Mg 9.1 7.4 2.5 3.59 0.0037 7.4 0.0112 Sr 11.8 4.6 14.3 0.83 0.0000 4.6 0.0000 P 1.9 16.4 2.4 0.79 0.0000 16.4 0.0000 K 5.2 9.8 5.1 1.02 0.0001 9.8 0.0211 Cl 65.4 2.3 2.2 29.71 0.0139 2.3 0.0239 Ca 21.5 4.8 17.7 1.22 0.0009 4.8 0.0348 Ba 6.6 6.1 10.8 0.62 0.0000 6.1 0.0000 Fe 1.9 11.4 3.3 0.58 0.0000 11.4 0.0000 Mn 1.4 19.2 2.7 0.50 0.0000 19.2 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3615 Mg 0.0003 1.7232 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1678 Cl 0.0077 1.1875 Ca 0.0003 1.1416 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 196 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0875 0.012242 0.0875 0.0562 Mg 0.0456 0.005309 0.0456 0.0277 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0010 0.006839 0.0010 0.0004 Cl 0.9187 0.021899 0.9187 0.3825 Ca 0.0353 0.012825 0.0353 0.0130 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0302 27.0302 33.2142 O 71.8817 71.8817 66.3061 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 197 x= -13353.0 y= 3016.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 10.7 6.8 3.6 2.94 0.0090 6.9 0.0292 Mg 10.6 6.9 2.5 4.19 0.0045 6.9 0.0112 Sr 11.0 4.8 14.3 0.77 0.0000 4.8 0.0000 P 1.5 18.2 2.4 0.64 0.0000 18.3 0.0000 K 3.4 12.1 5.1 0.67 0.0000 12.1 0.0000 Cl 121.3 1.7 2.2 55.11 0.0262 1.7 0.0239 Ca 22.8 4.7 17.7 1.29 0.0011 4.7 0.0348 Ba 6.1 6.4 10.8 0.57 0.0000 6.4 0.0000 Fe 1.9 11.5 3.3 0.58 0.0000 11.5 0.0000 Mn 1.7 17.1 2.7 0.63 0.0000 17.2 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3522 Mg 0.0003 1.7182 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0146 1.1859 Ca 0.0004 1.1421 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 197 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1061 0.012768 0.1061 0.0684 Mg 0.0559 0.005627 0.0559 0.0341 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.7290 0.029651 1.7290 0.7233 Ca 0.0472 0.013042 0.0472 0.0175 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8432 26.8432 33.1442 O 71.2186 71.2185 66.0125 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 198 x= -13352.0 y= 3020.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 10.7 6.8 3.6 2.94 0.0090 6.9 0.0292 Mg 11.3 6.6 2.5 4.49 0.0049 6.7 0.0112 Sr 10.8 4.8 14.3 0.75 0.0000 4.8 0.0000 P 2.1 15.6 2.4 0.87 0.0000 15.6 0.0000 K 4.6 10.4 5.1 0.90 0.0000 10.4 0.0000 Cl 105.7 1.8 2.2 48.04 0.0228 1.8 0.0239 Ca 22.4 4.7 17.7 1.27 0.0010 4.7 0.0348 Ba 6.2 6.3 10.8 0.58 0.0000 6.3 0.0000 Fe 1.5 13.0 3.3 0.45 0.0000 13.0 0.0000 Mn 2.0 15.8 2.7 0.74 0.0000 15.8 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3546 Mg 0.0004 1.7196 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0127 1.1864 Ca 0.0004 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 198 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1062 0.012781 0.1062 0.0684 Mg 0.0612 0.005791 0.0612 0.0373 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.5036 0.027706 1.5036 0.6282 Ca 0.0431 0.012968 0.0431 0.0159 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8900 26.8900 33.1590 O 71.3959 71.3959 66.0913 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 199 x= -13350.0 y= 3024.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 12.3 6.4 3.6 3.38 0.0111 6.4 0.0292 Mg 7.9 8.0 2.5 3.12 0.0030 8.0 0.0112 Sr 10.5 4.9 14.3 0.74 0.0000 4.9 0.0000 P 1.9 16.4 2.4 0.79 0.0000 16.4 0.0000 K 5.0 10.0 5.1 0.97 0.0000 10.1 0.0000 Cl 113.2 1.7 2.2 51.44 0.0244 1.7 0.0239 Ca 17.9 5.3 17.7 1.01 0.0001 5.3 0.0348 Ba 7.1 5.9 10.8 0.66 0.0000 5.9 0.0000 Fe 1.9 11.4 3.3 0.58 0.0000 11.4 0.0000 Mn 1.7 17.1 2.7 0.63 0.0000 17.2 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3534 Mg 0.0002 1.7194 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0136 1.1862 Ca 0.0000 1.1420 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 199 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1303 0.013469 0.1303 0.0839 Mg 0.0371 0.005013 0.0371 0.0226 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.6116 0.028650 1.6116 0.6735 Ca 0.0023 0.012222 0.0023 0.0008 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8848 26.8848 33.1635 O 71.3339 71.3339 66.0556 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 200 x= -13349.0 y= 3029.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 15.5 5.7 3.6 4.27 0.0153 5.7 0.0293 Mg 8.2 7.8 2.5 3.24 0.0032 7.8 0.0112 Sr 9.7 5.1 14.3 0.68 0.0000 5.1 0.0000 P 2.1 15.4 2.4 0.89 0.0000 15.4 0.0000 K 5.3 9.7 5.1 1.03 0.0001 9.8 0.0211 Cl 83.6 2.0 2.2 37.99 0.0179 2.0 0.0239 Ca 20.4 4.9 17.7 1.16 0.0006 5.0 0.0348 Ba 7.1 5.9 10.8 0.66 0.0000 6.0 0.0000 Fe 1.7 12.1 3.3 0.52 0.0000 12.1 0.0000 Mn 1.7 17.1 2.7 0.63 0.0000 17.2 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3572 Mg 0.0002 1.7227 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1682 Cl 0.0100 1.1871 Ca 0.0002 1.1417 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 200 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1797 0.014820 0.1797 0.1156 Mg 0.0393 0.005096 0.0393 0.0239 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0014 0.006859 0.0014 0.0005 Cl 1.1833 0.024693 1.1833 0.4935 Ca 0.0252 0.012646 0.0252 0.0093 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9469 26.9469 33.1709 O 71.6241 71.6241 66.1863 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 201 x= -13347.0 y= 3033.0 z= -280. carb2 trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 12.8 6.2 3.6 3.53 0.0118 6.3 0.0293 Mg 6.5 8.8 2.5 2.56 0.0022 8.8 0.0112 Sr 10.7 4.8 14.3 0.75 0.0000 4.8 0.0000 P 1.8 16.9 2.4 0.74 0.0000 16.9 0.0000 K 5.0 10.0 5.1 0.97 0.0000 10.1 0.0000 Cl 66.0 2.2 2.2 30.02 0.0140 2.2 0.0239 Ca 14.7 5.8 17.7 0.83 0.0000 5.8 0.0000 Ba 6.3 6.3 10.8 0.58 0.0000 6.3 0.0000 Fe 1.9 11.5 3.3 0.57 0.0000 11.6 0.0000 Mn 1.3 19.6 2.7 0.48 0.0000 19.6 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3608 Mg 0.0002 1.7240 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0078 1.1876 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 201 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1391 0.013750 0.1391 0.0893 Mg 0.0274 0.004676 0.0274 0.0167 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.9285 0.022011 0.9285 0.3865 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0312 27.0312 33.2132 O 71.8738 71.8738 66.2944 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 202 x= -14195.0 y= 2682.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 11.9 6.5 3.6 3.28 0.0106 6.5 0.0292 Mg 32.6 3.9 2.5 12.93 0.0168 3.9 0.0112 Sr 20.0 3.5 14.3 1.40 0.0008 3.5 0.0406 P 4.3 10.8 2.4 1.81 0.0024 10.9 0.0404 K 6.8 8.6 5.1 1.32 0.0015 8.6 0.0203 Cl 60.1 2.4 2.2 27.30 0.0127 2.4 0.0235 Ca 900.3 0.7 17.7 51.01 0.1952 0.8 0.0344 Ba 8.7 5.3 10.8 0.81 0.0000 5.4 0.0000 Fe 6.2 6.3 3.3 1.89 0.0017 6.3 0.0570 Mn 2.1 15.4 2.7 0.78 0.0000 15.4 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3546 Mg 0.0012 1.7175 Sr 0.0005 1.4047 P 0.0004 1.2263 K 0.0001 1.1233 Cl 0.0071 1.1662 Ca 0.0708 1.1283 Ba 0.0000 NaN Fe 0.0008 1.2842 Mn 0.0000 NaN iteration : 2 Analysis no. 202 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1250 0.013325 0.1250 0.0850 Mg 0.2088 0.009228 0.2088 0.1342 Sr 0.0710 0.011486 0.0710 0.0127 P 0.0469 0.014168 0.0469 0.0236 K 0.0151 0.007054 0.0151 0.0060 Cl 0.8261 0.020630 0.8261 0.3641 Ca 7.9934 0.064911 7.9934 3.1165 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.1001 0.016700 0.1001 0.0280 Mn 0.0000 0.000000 0.0000 0.0000 C 23.8312 23.8312 31.0052 O 66.7823 66.7823 65.2245 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 203 x= -14194.0 y= 2686.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 56.2 3.0 3.6 15.48 0.0676 3.0 0.0288 Mg 206.6 1.6 2.5 82.03 0.1141 1.6 0.0111 Sr 42.4 2.4 14.3 2.97 0.0040 2.4 0.0398 P 14.0 6.0 2.4 5.96 0.0150 6.0 0.0393 K 8.5 7.7 5.1 1.67 0.0031 7.7 0.0180 Cl 12.4 5.2 2.2 5.64 0.0022 5.2 0.0222 Ca 4381.4 0.3 17.7 248.22 0.9655 0.4 0.0330 Ba 13.9 4.2 10.8 1.29 0.0019 4.2 0.0749 Fe 3.9 8.0 3.3 1.17 0.0003 8.0 0.0553 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0624 Elt. k-ratio Correc. Na 0.0034 2.3175 Mg 0.0083 1.7005 Sr 0.0025 1.3765 P 0.0023 1.1943 K 0.0003 0.9955 Cl 0.0012 1.1011 Ca 0.3504 1.0817 Ba 0.0005 1.5412 Fe 0.0002 1.2446 Mn 0.0004 1.2692 iteration : 3 Analysis no. 203 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7818 0.025919 0.7818 0.6826 Mg 1.4051 0.022682 1.4051 1.1604 Sr 0.3424 0.014510 0.3424 0.0784 P 0.2799 0.021766 0.2799 0.1814 K 0.0276 0.006701 0.0276 0.0142 Cl 0.1376 0.009413 0.1376 0.0779 Ca 37.9034 0.163395 37.9034 18.9827 Ba 0.0824 0.020536 0.0824 0.0120 Fe 0.0191 0.014051 0.0191 0.0069 Mn 0.0466 0.020918 0.0466 0.0170 C 11.5219 11.5219 19.2553 O 47.4521 47.4521 59.5311 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 204 x= -14194.0 y= 2691.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 51.6 3.1 3.6 14.23 0.0617 3.1 0.0288 Mg 228.8 1.5 2.5 90.86 0.1266 1.5 0.0111 Sr 41.5 2.5 14.3 2.91 0.0039 2.5 0.0398 P 19.8 5.0 2.4 8.40 0.0223 5.0 0.0393 K 9.0 7.5 5.1 1.75 0.0035 7.5 0.0180 Cl 13.6 4.9 2.2 6.18 0.0025 5.0 0.0222 Ca 4380.6 0.3 17.7 248.18 0.9654 0.4 0.0330 Ba 12.9 4.4 10.8 1.20 0.0013 4.4 0.0749 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0553 Mn 4.7 10.4 2.7 1.72 0.0019 10.4 0.0624 Elt. k-ratio Correc. Na 0.0031 2.3155 Mg 0.0092 1.6979 Sr 0.0024 1.3766 P 0.0035 1.1943 K 0.0003 0.9965 Cl 0.0014 1.1019 Ca 0.3504 1.0818 Ba 0.0004 1.5411 Fe 0.0002 1.2444 Mn 0.0006 1.2690 iteration : 3 Analysis no. 204 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7135 0.024875 0.7135 0.6240 Mg 1.5559 0.023872 1.5559 1.2872 Sr 0.3315 0.014395 0.3315 0.0761 P 0.4181 0.025339 0.4181 0.2715 K 0.0313 0.006818 0.0313 0.0161 Cl 0.1539 0.009800 0.1539 0.0873 Ca 37.9038 0.163406 37.9038 19.0159 Ba 0.0562 0.020115 0.0562 0.0082 Fe 0.0207 0.014098 0.0207 0.0075 Mn 0.0701 0.021906 0.0701 0.0257 C 11.3901 11.3901 19.0683 O 47.3547 47.3547 59.5123 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 205 x= -14193.0 y= 2695.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.6 3.5 3.6 11.20 0.0476 3.5 0.0287 Mg 247.5 1.4 2.5 98.30 0.1370 1.5 0.0110 Sr 41.7 2.4 14.3 2.92 0.0039 2.5 0.0397 P 35.0 3.8 2.4 14.90 0.0419 3.8 0.0393 K 10.6 6.9 5.1 2.07 0.0050 6.9 0.0181 Cl 22.1 3.9 2.2 10.06 0.0044 3.9 0.0223 Ca 4363.0 0.3 17.7 247.18 0.9613 0.4 0.0330 Ba 13.3 4.3 10.8 1.23 0.0015 4.3 0.0748 Fe 4.0 7.9 3.3 1.21 0.0004 7.9 0.0553 Mn 3.9 11.3 2.7 1.44 0.0012 11.3 0.0623 Elt. k-ratio Correc. Na 0.0024 2.3114 Mg 0.0099 1.6925 Sr 0.0024 1.3752 P 0.0066 1.1936 K 0.0004 0.9996 Cl 0.0024 1.1038 Ca 0.3489 1.0823 Ba 0.0004 1.5408 Fe 0.0002 1.2440 Mn 0.0003 1.2686 iteration : 3 Analysis no. 205 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5488 0.022179 0.5488 0.4813 Mg 1.6791 0.024778 1.6791 1.3928 Sr 0.3336 0.014404 0.3336 0.0768 P 0.7840 0.033024 0.7840 0.5103 K 0.0445 0.007218 0.0445 0.0229 Cl 0.2695 0.012186 0.2695 0.1533 Ca 37.7600 0.162993 37.7600 18.9939 Ba 0.0654 0.020255 0.0654 0.0096 Fe 0.0232 0.014163 0.0232 0.0084 Mn 0.0430 0.020748 0.0430 0.0158 C 11.1976 11.1976 18.7956 O 47.2514 47.2514 59.5395 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 206 x= -14192.0 y= 2700.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 51.1 3.1 3.6 14.08 0.0610 3.1 0.0286 Mg 239.3 1.4 2.5 95.04 0.1324 1.5 0.0110 Sr 44.1 2.4 14.3 3.09 0.0043 2.4 0.0397 P 43.9 3.4 2.4 18.68 0.0533 3.4 0.0393 K 12.0 6.5 5.1 2.34 0.0063 6.5 0.0182 Cl 26.8 3.5 2.2 12.18 0.0054 3.5 0.0223 Ca 4256.9 0.3 17.7 241.17 0.9377 0.4 0.0330 Ba 13.3 4.3 10.8 1.24 0.0016 4.3 0.0748 Fe 4.4 7.6 3.3 1.32 0.0006 7.6 0.0553 Mn 4.4 10.6 2.7 1.62 0.0017 10.7 0.0623 Elt. k-ratio Correc. Na 0.0030 2.3076 Mg 0.0096 1.6934 Sr 0.0026 1.3755 P 0.0084 1.1945 K 0.0006 1.0044 Cl 0.0030 1.1066 Ca 0.3403 1.0835 Ba 0.0004 1.5398 Fe 0.0003 1.2442 Mn 0.0005 1.2687 iteration : 3 Analysis no. 206 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7027 0.024656 0.7027 0.6134 Mg 1.6235 0.024359 1.6235 1.3406 Sr 0.3628 0.014714 0.3628 0.0831 P 0.9984 0.036844 0.9984 0.6469 K 0.0561 0.007569 0.0561 0.0288 Cl 0.3334 0.013340 0.3334 0.1888 Ca 36.8737 0.160412 36.8737 18.4649 Ba 0.0673 0.020271 0.0673 0.0098 Fe 0.0348 0.014500 0.0348 0.0125 Mn 0.0610 0.021518 0.0610 0.0223 C 11.3328 11.3328 18.9372 O 47.5535 47.5535 59.6516 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 207 x= -14191.0 y= 2704.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 51.1 3.1 3.6 14.09 0.0611 3.1 0.0287 Mg 217.2 1.5 2.5 86.25 0.1201 1.5 0.0110 Sr 44.2 2.4 14.3 3.09 0.0043 2.4 0.0398 P 39.7 3.5 2.4 16.90 0.0479 3.6 0.0394 K 14.5 5.9 5.1 2.84 0.0087 5.9 0.0183 Cl 36.1 3.0 2.2 16.40 0.0075 3.0 0.0224 Ca 4081.1 0.3 17.7 231.21 0.8993 0.4 0.0331 Ba 12.9 4.4 10.8 1.20 0.0013 4.4 0.0748 Fe 4.2 7.8 3.3 1.26 0.0005 7.8 0.0554 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0624 Elt. k-ratio Correc. Na 0.0030 2.3094 Mg 0.0087 1.6948 Sr 0.0026 1.3762 P 0.0075 1.1956 K 0.0008 1.0096 Cl 0.0042 1.1089 Ca 0.3264 1.0858 Ba 0.0004 1.5393 Fe 0.0002 1.2461 Mn 0.0003 1.2702 iteration : 3 Analysis no. 207 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7043 0.024699 0.7043 0.6063 Mg 1.4736 0.023202 1.4736 1.1999 Sr 0.3637 0.014735 0.3637 0.0822 P 0.8987 0.035148 0.8987 0.5742 K 0.0775 0.008163 0.0775 0.0392 Cl 0.4602 0.015370 0.4602 0.2569 Ca 35.4360 0.156258 35.4360 17.4977 Ba 0.0562 0.020094 0.0562 0.0081 Fe 0.0282 0.014338 0.0282 0.0100 Mn 0.0413 0.020703 0.0413 0.0149 C 11.9899 11.9899 19.7560 O 48.4705 48.4705 59.9546 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 208 x= -14191.0 y= 2709.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 55.3 3.0 3.6 15.25 0.0665 3.0 0.0287 Mg 212.6 1.5 2.5 84.44 0.1175 1.6 0.0111 Sr 43.4 2.4 14.3 3.04 0.0042 2.4 0.0398 P 45.0 3.3 2.4 19.13 0.0547 3.3 0.0394 K 15.7 5.6 5.1 3.08 0.0098 5.7 0.0183 Cl 36.6 3.0 2.2 16.64 0.0076 3.0 0.0224 Ca 4093.5 0.3 17.7 231.91 0.9020 0.4 0.0331 Ba 13.1 4.4 10.8 1.22 0.0014 4.4 0.0748 Fe 4.0 7.9 3.3 1.22 0.0004 7.9 0.0554 Mn 5.0 10.0 2.7 1.83 0.0022 10.1 0.0624 Elt. k-ratio Correc. Na 0.0033 2.3082 Mg 0.0085 1.6952 Sr 0.0026 1.3758 P 0.0086 1.1951 K 0.0009 1.0098 Cl 0.0042 1.1091 Ca 0.3273 1.0856 Ba 0.0004 1.5391 Fe 0.0002 1.2457 Mn 0.0006 1.2698 iteration : 3 Analysis no. 208 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7661 0.025630 0.7661 0.6612 Mg 1.4426 0.022954 1.4426 1.1776 Sr 0.3545 0.014633 0.3545 0.0803 P 1.0246 0.037304 1.0246 0.6563 K 0.0874 0.008411 0.0874 0.0443 Cl 0.4675 0.015479 0.4675 0.2616 Ca 35.5339 0.156536 35.5339 17.5910 Ba 0.0614 0.020174 0.0614 0.0089 Fe 0.0241 0.014211 0.0241 0.0086 Mn 0.0810 0.022364 0.0810 0.0293 C 11.8491 11.8491 19.5741 O 48.3078 48.3078 59.9067 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 209 x= -14190.0 y= 2713.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 23.5 4.6 3.6 6.48 0.0256 4.6 0.0290 Mg 68.5 2.7 2.5 27.21 0.0369 2.7 0.0111 Sr 23.7 3.2 14.3 1.66 0.0013 3.3 0.0399 P 42.0 3.4 2.4 17.87 0.0509 3.5 0.0395 K 16.0 5.6 5.1 3.14 0.0100 5.6 0.0188 Cl 34.8 3.1 2.2 15.82 0.0072 3.1 0.0227 Ca 3139.5 0.4 17.7 177.87 0.6910 0.5 0.0335 Ba 9.3 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0559 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0629 Elt. k-ratio Correc. Na 0.0013 2.3349 Mg 0.0027 1.7033 Sr 0.0008 1.3791 P 0.0080 1.1994 K 0.0009 1.0362 Cl 0.0040 1.1230 Ca 0.2508 1.0983 Ba 0.0000 NaN Fe 0.0001 1.2583 Mn 0.0002 1.2803 iteration : 3 Analysis no. 209 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2981 0.017507 0.2981 0.2370 Mg 0.4554 0.013078 0.4554 0.3425 Sr 0.1146 0.011878 0.1146 0.0239 P 0.9571 0.036232 0.9571 0.5649 K 0.0922 0.008694 0.0922 0.0431 Cl 0.4487 0.015306 0.4487 0.2313 Ca 27.5412 0.132740 27.5412 12.5606 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0084 0.013884 0.0084 0.0027 Mn 0.0307 0.020385 0.0307 0.0102 C 15.6841 15.6841 23.8691 O 54.3697 54.3697 62.1147 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 210 x= -14189.0 y= 2718.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 13.5 6.1 3.6 3.71 0.0126 6.1 0.0289 Mg 99.9 2.2 2.5 39.67 0.0545 2.3 0.0111 Sr 37.1 2.6 14.3 2.60 0.0033 2.6 0.0397 P 45.1 3.3 2.4 19.19 0.0549 3.3 0.0393 K 12.6 6.3 5.1 2.46 0.0069 6.3 0.0184 Cl 42.8 2.8 2.2 19.48 0.0089 2.8 0.0224 Ca 3741.5 0.4 17.7 211.97 0.8241 0.5 0.0333 Ba 12.4 4.5 10.8 1.15 0.0010 4.5 0.0748 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0556 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0626 Elt. k-ratio Correc. Na 0.0006 2.3291 Mg 0.0039 1.6956 Sr 0.0020 1.3724 P 0.0086 1.1937 K 0.0006 1.0185 Cl 0.0050 1.1129 Ca 0.2991 1.0904 Ba 0.0003 1.5392 Fe 0.0001 1.2510 Mn 0.0004 1.2743 iteration : 3 Analysis no. 210 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1469 0.013835 0.1469 0.1225 Mg 0.6687 0.015677 0.6687 0.5273 Sr 0.2769 0.013766 0.2769 0.0606 P 1.0271 0.037324 1.0271 0.6354 K 0.0619 0.007813 0.0619 0.0304 Cl 0.5542 0.016741 0.5542 0.2995 Ca 32.6143 0.147980 32.6143 15.5937 Ba 0.0418 0.019858 0.0418 0.0058 Fe 0.0158 0.014027 0.0158 0.0054 Mn 0.0505 0.021162 0.0505 0.0176 C 13.5751 13.5751 21.6587 O 50.9667 50.9667 61.0431 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 211 x= -14188.0 y= 2722.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 10.2 7.0 3.6 2.81 0.0085 7.0 0.0289 Mg 122.7 2.0 2.5 48.73 0.0672 2.0 0.0110 Sr 30.7 2.9 14.3 2.15 0.0023 2.9 0.0397 P 54.1 3.0 2.4 23.00 0.0664 3.1 0.0393 K 14.9 5.8 5.1 2.91 0.0090 5.8 0.0185 Cl 46.7 2.7 2.2 21.22 0.0098 2.7 0.0225 Ca 3760.8 0.4 17.7 213.06 0.8284 0.5 0.0333 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0626 Elt. k-ratio Correc. Na 0.0004 2.3257 Mg 0.0049 1.6926 Sr 0.0014 1.3722 P 0.0104 1.1928 K 0.0008 1.0190 Cl 0.0054 1.1133 Ca 0.3007 1.0907 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2742 iteration : 3 Analysis no. 211 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0982 0.012427 0.0982 0.0821 Mg 0.8240 0.017342 0.8240 0.6516 Sr 0.1986 0.012865 0.1986 0.0436 P 1.2413 0.040745 1.2413 0.7702 K 0.0811 0.008313 0.0811 0.0399 Cl 0.6067 0.017450 0.6067 0.3289 Ca 32.7912 0.148528 32.7912 15.7243 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0414 0.020770 0.0414 0.0145 C 13.3506 13.3506 21.3630 O 50.7668 50.7668 60.9820 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 212 x= -14188.0 y= 2727.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 21.2 4.9 3.6 5.85 0.0226 4.9 0.0289 Mg 96.7 2.3 2.5 38.40 0.0527 2.3 0.0111 Sr 31.7 2.8 14.3 2.22 0.0025 2.8 0.0397 P 57.0 3.0 2.4 24.26 0.0701 3.0 0.0394 K 15.2 5.7 5.1 2.97 0.0092 5.8 0.0186 Cl 41.2 2.8 2.2 18.73 0.0086 2.8 0.0226 Ca 3447.3 0.4 17.7 195.31 0.7589 0.5 0.0334 Ba 12.0 4.6 10.8 1.11 0.0007 4.6 0.0747 Fe 4.5 7.5 3.3 1.36 0.0007 7.5 0.0557 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0627 Elt. k-ratio Correc. Na 0.0011 2.3269 Mg 0.0038 1.6973 Sr 0.0015 1.3751 P 0.0110 1.1963 K 0.0008 1.0288 Cl 0.0048 1.1194 Ca 0.2754 1.0943 Ba 0.0002 1.5379 Fe 0.0003 1.2537 Mn 0.0002 1.2764 iteration : 3 Analysis no. 212 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2626 0.016681 0.2626 0.2147 Mg 0.6472 0.015437 0.6472 0.5006 Sr 0.2120 0.013043 0.2120 0.0455 P 1.3155 0.041934 1.3155 0.7983 K 0.0844 0.008453 0.0844 0.0406 Cl 0.5349 0.016525 0.5349 0.2836 Ca 30.1363 0.140583 30.1363 14.1333 Ba 0.0320 0.019675 0.0320 0.0044 Fe 0.0393 0.014734 0.0393 0.0132 Mn 0.0306 0.020318 0.0306 0.0105 C 14.3276 14.3276 22.4221 O 52.3776 52.3776 61.5333 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 213 x= -14187.0 y= 2731.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 30.0 4.1 3.6 8.27 0.0339 4.1 0.0287 Mg 214.3 1.5 2.5 85.09 0.1185 1.6 0.0110 Sr 43.0 2.4 14.3 3.01 0.0041 2.4 0.0397 P 62.6 2.8 2.4 26.62 0.0773 2.8 0.0394 K 17.3 5.4 5.1 3.38 0.0112 5.4 0.0184 Cl 45.9 2.7 2.2 20.84 0.0096 2.7 0.0225 Ca 3895.9 0.4 17.7 220.72 0.8582 0.4 0.0332 Ba 12.2 4.5 10.8 1.13 0.0009 4.5 0.0747 Fe 3.9 8.0 3.3 1.17 0.0003 8.0 0.0554 Mn 4.2 10.9 2.7 1.55 0.0015 10.9 0.0625 Elt. k-ratio Correc. Na 0.0017 2.3087 Mg 0.0086 1.6887 Sr 0.0025 1.3745 P 0.0121 1.1951 K 0.0010 1.0180 Cl 0.0053 1.1139 Ca 0.3115 1.0885 Ba 0.0002 1.5385 Fe 0.0002 1.2474 Mn 0.0004 1.2712 iteration : 3 Analysis no. 213 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3911 0.019290 0.3911 0.3333 Mg 1.4483 0.022956 1.4483 1.1676 Sr 0.3484 0.014558 0.3484 0.0779 P 1.4480 0.043869 1.4480 0.9160 K 0.1010 0.008790 0.1010 0.0506 Cl 0.5956 0.017307 0.5956 0.3292 Ca 33.9034 0.151781 33.9034 16.5748 Ba 0.0379 0.019783 0.0379 0.0054 Fe 0.0191 0.014084 0.0191 0.0067 Mn 0.0540 0.021263 0.0540 0.0192 C 12.3312 12.3312 20.1168 O 49.3222 49.3222 60.4025 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 214 x= -14186.0 y= 2736.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 11.3 6.7 3.6 3.10 0.0098 6.7 0.0289 Mg 91.1 2.3 2.5 36.19 0.0496 2.4 0.0111 Sr 33.2 2.7 14.3 2.32 0.0027 2.8 0.0397 P 56.9 3.0 2.4 24.20 0.0700 3.0 0.0394 K 13.0 6.2 5.1 2.55 0.0073 6.2 0.0187 Cl 40.2 2.9 2.2 18.28 0.0084 2.9 0.0226 Ca 3404.2 0.4 17.7 192.86 0.7495 0.5 0.0334 Ba 8.7 5.3 10.8 0.81 0.0000 5.4 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0558 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0628 Elt. k-ratio Correc. Na 0.0005 2.3292 Mg 0.0036 1.6957 Sr 0.0017 1.3746 P 0.0110 1.1964 K 0.0006 1.0299 Cl 0.0047 1.1201 Ca 0.2720 1.0950 Ba 0.0000 NaN Fe 0.0000 1.2546 Mn 0.0003 1.2772 iteration : 3 Analysis no. 214 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1140 0.012911 0.1140 0.0928 Mg 0.6086 0.014980 0.6086 0.4685 Sr 0.2296 0.013247 0.2296 0.0490 P 1.3123 0.041891 1.3123 0.7926 K 0.0664 0.008001 0.0664 0.0318 Cl 0.5216 0.016346 0.5216 0.2752 Ca 29.7835 0.139541 29.7835 13.9022 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0033 0.013689 0.0033 0.0011 Mn 0.0360 0.020577 0.0360 0.0123 C 14.5599 14.5599 22.6784 O 52.7646 52.7646 61.6961 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 215 x= -14185.0 y= 2740.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 14.7 5.8 3.6 4.04 0.0142 5.9 0.0289 Mg 122.1 2.0 2.5 48.47 0.0669 2.0 0.0110 Sr 31.6 2.8 14.3 2.22 0.0025 2.8 0.0398 P 58.6 2.9 2.4 24.92 0.0721 2.9 0.0394 K 14.1 6.0 5.1 2.75 0.0082 6.0 0.0187 Cl 44.7 2.7 2.2 20.31 0.0094 2.7 0.0226 Ca 3422.1 0.4 17.7 193.87 0.7534 0.5 0.0334 Ba 10.4 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0557 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0628 Elt. k-ratio Correc. Na 0.0007 2.3248 Mg 0.0048 1.6943 Sr 0.0015 1.3756 P 0.0113 1.1968 K 0.0007 1.0303 Cl 0.0052 1.1202 Ca 0.2734 1.0948 Ba 0.0000 NaN Fe 0.0001 1.2540 Mn 0.0003 1.2767 iteration : 3 Analysis no. 215 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1646 0.014289 0.1646 0.1344 Mg 0.8203 0.017312 0.8203 0.6336 Sr 0.2109 0.013036 0.2109 0.0452 P 1.3537 0.042518 1.3537 0.8205 K 0.0753 0.008233 0.0753 0.0361 Cl 0.5830 0.017192 0.5830 0.3087 Ca 29.9357 0.140001 29.9357 14.0223 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0109 0.013911 0.0109 0.0037 Mn 0.0378 0.020649 0.0378 0.0129 C 14.3484 14.3484 22.4275 O 52.4594 52.4594 61.5550 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 216 x= -14185.0 y= 2745.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 11.3 6.6 3.6 3.12 0.0099 6.7 0.0289 Mg 104.6 2.2 2.5 41.53 0.0571 2.2 0.0111 Sr 27.7 3.0 14.3 1.94 0.0019 3.0 0.0399 P 49.1 3.2 2.4 20.90 0.0600 3.2 0.0396 K 14.3 5.9 5.1 2.79 0.0084 5.9 0.0189 Cl 46.6 2.7 2.2 21.19 0.0098 2.7 0.0227 Ca 3020.5 0.4 17.7 171.12 0.6646 0.5 0.0336 Ba 9.4 5.1 10.8 0.88 0.0000 5.2 0.0000 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0560 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0629 Elt. k-ratio Correc. Na 0.0005 2.3307 Mg 0.0041 1.6977 Sr 0.0012 1.3798 P 0.0094 1.2008 K 0.0007 1.0424 Cl 0.0054 1.1264 Ca 0.2412 1.0999 Ba 0.0000 NaN Fe 0.0001 1.2588 Mn 0.0003 1.2805 iteration : 2 Analysis no. 216 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1149 0.012940 0.1149 0.0909 Mg 0.7019 0.016059 0.7019 0.5253 Sr 0.1637 0.012501 0.1637 0.0340 P 1.1298 0.039130 1.1298 0.6635 K 0.0779 0.008374 0.0779 0.0362 Cl 0.6129 0.017643 0.6129 0.3145 Ca 26.5282 0.129634 26.5282 12.0395 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0134 0.014039 0.0134 0.0044 Mn 0.0343 0.020550 0.0343 0.0114 C 15.8698 15.8698 24.0336 O 54.7531 54.7531 62.2468 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 217 x= -14184.0 y= 2749.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 33.9 3.8 3.6 9.35 0.0389 3.9 0.0287 Mg 152.9 1.8 2.5 60.72 0.0841 1.8 0.0110 Sr 37.6 2.6 14.3 2.63 0.0033 2.6 0.0397 P 54.0 3.0 2.4 22.96 0.0662 3.1 0.0394 K 17.8 5.3 5.1 3.49 0.0117 5.3 0.0185 Cl 53.8 2.5 2.2 24.43 0.0113 2.5 0.0225 Ca 3720.7 0.4 17.7 210.79 0.8192 0.5 0.0333 Ba 10.7 4.8 10.8 1.00 0.0000 4.8 0.0000 Fe 3.3 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0626 Elt. k-ratio Correc. Na 0.0019 2.3153 Mg 0.0061 1.6937 Sr 0.0021 1.3745 P 0.0104 1.1952 K 0.0010 1.0222 Cl 0.0063 1.1151 Ca 0.2973 1.0910 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2735 iteration : 3 Analysis no. 217 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4500 0.020441 0.4500 0.3769 Mg 1.0311 0.019377 1.0311 0.8168 Sr 0.2832 0.013849 0.2832 0.0622 P 1.2407 0.040769 1.2407 0.7712 K 0.1059 0.008931 0.1059 0.0522 Cl 0.7040 0.018698 0.7040 0.3823 Ca 32.4354 0.147442 32.4354 15.5805 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0359 0.020509 0.0359 0.0126 C 13.2096 13.2096 21.1739 O 50.5041 50.5041 60.7714 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 218 x= -14183.0 y= 2753.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 29.2 4.1 3.6 8.04 0.0328 4.2 0.0288 Mg 122.1 2.0 2.5 48.47 0.0669 2.0 0.0111 Sr 33.4 2.7 14.3 2.34 0.0027 2.8 0.0397 P 48.6 3.2 2.4 20.66 0.0593 3.2 0.0394 K 17.4 5.4 5.1 3.41 0.0113 5.4 0.0185 Cl 44.6 2.7 2.2 20.29 0.0093 2.7 0.0225 Ca 3657.7 0.4 17.7 207.22 0.8055 0.5 0.0333 Ba 12.0 4.6 10.8 1.12 0.0008 4.6 0.0748 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0556 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0626 Elt. k-ratio Correc. Na 0.0016 2.3226 Mg 0.0048 1.6968 Sr 0.0017 1.3748 P 0.0093 1.1952 K 0.0010 1.0221 Cl 0.0052 1.1151 Ca 0.2923 1.0916 Ba 0.0002 1.5388 Fe 0.0000 1.2515 Mn 0.0002 1.2747 iteration : 3 Analysis no. 218 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3807 0.019156 0.3807 0.3162 Mg 0.8214 0.017336 0.8214 0.6452 Sr 0.2317 0.013271 0.2317 0.0505 P 1.1112 0.038729 1.1112 0.6849 K 0.1026 0.008854 0.1026 0.0501 Cl 0.5798 0.017105 0.5798 0.3122 Ca 31.9105 0.145890 31.9105 15.2005 Ba 0.0327 0.019698 0.0327 0.0045 Fe 0.0050 0.013705 0.0050 0.0017 Mn 0.0305 0.020292 0.0305 0.0106 C 13.6456 13.6456 21.6903 O 51.1483 51.1483 61.0331 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 219 x= -14182.0 y= 2758.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 18.9 5.1 3.6 5.21 0.0196 5.2 0.0290 Mg 71.3 2.6 2.5 28.32 0.0385 2.7 0.0111 Sr 24.2 3.2 14.3 1.70 0.0014 3.2 0.0398 P 35.8 3.7 2.4 15.24 0.0429 3.7 0.0394 K 14.7 5.8 5.1 2.88 0.0088 5.8 0.0186 Cl 42.3 2.8 2.2 19.23 0.0088 2.8 0.0226 Ca 3323.9 0.4 17.7 188.31 0.7315 0.5 0.0334 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 4.0 7.9 3.3 1.21 0.0004 7.9 0.0558 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0628 Elt. k-ratio Correc. Na 0.0010 2.3358 Mg 0.0028 1.7020 Sr 0.0009 1.3773 P 0.0067 1.1973 K 0.0008 1.0300 Cl 0.0049 1.1188 Ca 0.2655 1.0960 Ba 0.0000 NaN Fe 0.0002 1.2565 Mn 0.0003 1.2788 iteration : 3 Analysis no. 219 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2291 0.015944 0.2291 0.1844 Mg 0.4742 0.013322 0.4742 0.3611 Sr 0.1211 0.011943 0.1211 0.0256 P 0.8058 0.033487 0.8058 0.4815 K 0.0807 0.008367 0.0807 0.0382 Cl 0.5496 0.016724 0.5496 0.2869 Ca 29.0957 0.137451 29.0957 13.4354 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0234 0.014307 0.0234 0.0078 Mn 0.0324 0.020436 0.0324 0.0109 C 15.1765 15.1765 23.3853 O 53.4116 53.4116 61.7829 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 220 x= -14182.0 y= 2762.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.2 4.0 3.6 8.60 0.0355 4.0 0.0288 Mg 135.8 1.9 2.5 53.92 0.0745 1.9 0.0111 Sr 35.6 2.6 14.3 2.50 0.0031 2.7 0.0398 P 41.6 3.5 2.4 17.68 0.0503 3.5 0.0394 K 20.1 5.0 5.1 3.93 0.0138 5.0 0.0185 Cl 45.1 2.7 2.2 20.51 0.0094 2.7 0.0225 Ca 3624.4 0.4 17.7 205.34 0.7982 0.5 0.0333 Ba 11.2 4.7 10.8 1.04 0.0002 4.7 0.0748 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0556 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0627 Elt. k-ratio Correc. Na 0.0018 2.3218 Mg 0.0054 1.6970 Sr 0.0019 1.3761 P 0.0079 1.1965 K 0.0012 1.0229 Cl 0.0053 1.1153 Ca 0.2897 1.0921 Ba 0.0001 1.5387 Fe 0.0000 1.2520 Mn 0.0002 1.2751 iteration : 3 Analysis no. 220 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4112 0.019746 0.4112 0.3405 Mg 0.9158 0.018292 0.9158 0.7173 Sr 0.2597 0.013601 0.2597 0.0564 P 0.9439 0.035952 0.9439 0.5801 K 0.1248 0.009371 0.1248 0.0608 Cl 0.5863 0.017195 0.5863 0.3148 Ca 31.6348 0.145076 31.6348 15.0258 Ba 0.0104 0.019328 0.0104 0.0014 Fe 0.0033 0.013660 0.0033 0.0011 Mn 0.0215 0.019889 0.0215 0.0074 C 13.7944 13.7944 21.8637 O 51.2938 51.2938 61.0305 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 221 x= -14181.0 y= 2767.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 37.9 3.6 3.6 10.44 0.0440 3.7 0.0289 Mg 114.1 2.1 2.5 45.29 0.0624 2.1 0.0111 Sr 29.7 2.9 14.3 2.08 0.0022 2.9 0.0398 P 38.7 3.6 2.4 16.45 0.0466 3.6 0.0395 K 16.5 5.5 5.1 3.24 0.0105 5.5 0.0186 Cl 50.6 2.6 2.2 23.01 0.0107 2.6 0.0225 Ca 3445.3 0.4 17.7 195.19 0.7585 0.5 0.0334 Ba 10.5 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0557 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0628 Elt. k-ratio Correc. Na 0.0022 2.3238 Mg 0.0045 1.7004 Sr 0.0014 1.3778 P 0.0073 1.1976 K 0.0009 1.0282 Cl 0.0059 1.1178 Ca 0.2753 1.0944 Ba 0.0000 NaN Fe 0.0000 1.2542 Mn 0.0001 1.2769 iteration : 3 Analysis no. 221 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5108 0.021588 0.5108 0.4169 Mg 0.7681 0.016793 0.7681 0.5929 Sr 0.1872 0.012769 0.1872 0.0401 P 0.8748 0.034753 0.8748 0.5299 K 0.0957 0.008727 0.0957 0.0459 Cl 0.6630 0.018213 0.6630 0.3509 Ca 30.1257 0.140562 30.1257 14.1025 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013632 0.0017 0.0006 Mn 0.0179 0.019750 0.0179 0.0061 C 14.4659 14.4659 22.5971 O 52.2894 52.2894 61.3172 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 222 x= -14180.0 y= 2771.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 49.8 3.2 3.6 13.72 0.0593 3.2 0.0288 Mg 163.7 1.7 2.5 65.01 0.0902 1.8 0.0111 Sr 35.3 2.7 14.3 2.47 0.0030 2.7 0.0399 P 38.7 3.6 2.4 16.45 0.0466 3.6 0.0395 K 17.4 5.4 5.1 3.41 0.0113 5.4 0.0186 Cl 48.3 2.6 2.2 21.93 0.0101 2.6 0.0225 Ca 3519.4 0.4 17.7 199.39 0.7748 0.5 0.0333 Ba 11.8 4.6 10.8 1.10 0.0006 4.6 0.0747 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0557 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0627 Elt. k-ratio Correc. Na 0.0030 2.3160 Mg 0.0065 1.6995 Sr 0.0019 1.3797 P 0.0073 1.1992 K 0.0010 1.0268 Cl 0.0056 1.1176 Ca 0.2812 1.0931 Ba 0.0002 1.5377 Fe 0.0001 1.2525 Mn 0.0003 1.2753 iteration : 3 Analysis no. 222 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6861 0.024451 0.6861 0.5652 Mg 1.1093 0.020133 1.1093 0.8644 Sr 0.2566 0.013593 0.2566 0.0555 P 0.8759 0.034795 0.8759 0.5355 K 0.1031 0.008894 0.1031 0.0499 Cl 0.6304 0.017793 0.6304 0.3367 Ca 30.7382 0.142378 30.7382 14.5244 Ba 0.0268 0.019585 0.0268 0.0037 Fe 0.0134 0.013966 0.0134 0.0045 Mn 0.0414 0.020782 0.0414 0.0143 C 13.9739 13.9739 22.0337 O 51.5450 51.5450 61.0122 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 223 x= -14179.0 y= 2776.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 39.2 3.6 3.6 10.80 0.0457 3.6 0.0288 Mg 117.3 2.1 2.5 46.58 0.0642 2.1 0.0111 Sr 40.8 2.5 14.3 2.86 0.0038 2.5 0.0399 P 35.8 3.7 2.4 15.21 0.0429 3.8 0.0395 K 15.6 5.7 5.1 3.05 0.0096 5.7 0.0187 Cl 51.0 2.6 2.2 23.16 0.0107 2.6 0.0226 Ca 3344.7 0.4 17.7 189.49 0.7363 0.5 0.0334 Ba 11.5 4.7 10.8 1.07 0.0004 4.7 0.0747 Fe 3.0 9.2 3.3 0.89 0.0000 9.2 0.0000 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0628 Elt. k-ratio Correc. Na 0.0023 2.3223 Mg 0.0046 1.7003 Sr 0.0023 1.3787 P 0.0067 1.2000 K 0.0009 1.0319 Cl 0.0060 1.1201 Ca 0.2672 1.0954 Ba 0.0001 1.5373 Fe 0.0000 NaN Mn 0.0002 1.2771 iteration : 3 Analysis no. 223 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5299 0.021915 0.5299 0.4299 Mg 0.7905 0.017031 0.7905 0.6066 Sr 0.3232 0.014324 0.3232 0.0688 P 0.8065 0.033548 0.8065 0.4857 K 0.0880 0.008563 0.0880 0.0420 Cl 0.6689 0.018309 0.6689 0.3519 Ca 29.2692 0.137970 29.2692 13.6218 Ba 0.0189 0.019452 0.0189 0.0026 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0306 0.020332 0.0306 0.0104 C 14.7662 14.7662 22.9319 O 52.7081 52.7081 61.4483 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 224 x= -14179.0 y= 2780.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 49.6 3.2 3.6 13.68 0.0592 3.2 0.0287 Mg 163.6 1.7 2.5 64.95 0.0901 1.8 0.0111 Sr 39.8 2.5 14.3 2.79 0.0037 2.5 0.0398 P 45.3 3.3 2.4 19.28 0.0551 3.3 0.0394 K 19.6 5.1 5.1 3.83 0.0133 5.1 0.0185 Cl 49.0 2.6 2.2 22.25 0.0103 2.6 0.0225 Ca 3689.5 0.4 17.7 209.03 0.8126 0.5 0.0333 Ba 10.2 5.0 10.8 0.95 0.0000 5.0 0.0000 Fe 4.0 7.9 3.3 1.22 0.0004 7.9 0.0556 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0626 Elt. k-ratio Correc. Na 0.0030 2.3134 Mg 0.0065 1.6972 Sr 0.0023 1.3769 P 0.0086 1.1972 K 0.0012 1.0224 Cl 0.0057 1.1153 Ca 0.2949 1.0911 Ba 0.0000 NaN Fe 0.0002 1.2503 Mn 0.0003 1.2736 iteration : 3 Analysis no. 224 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6831 0.024392 0.6831 0.5709 Mg 1.1070 0.020100 1.1070 0.8750 Sr 0.3106 0.014173 0.3106 0.0681 P 1.0348 0.037509 1.0348 0.6418 K 0.1206 0.009273 0.1206 0.0593 Cl 0.6387 0.017882 0.6387 0.3461 Ca 32.1763 0.146677 32.1763 15.4231 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0242 0.014264 0.0242 0.0083 Mn 0.0377 0.020597 0.0377 0.0132 C 13.3083 13.3083 21.2866 O 50.5587 50.5587 60.7076 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 225 x= -14178.0 y= 2785.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 57.7 2.9 3.6 15.90 0.0695 3.0 0.0288 Mg 147.2 1.8 2.5 58.47 0.0809 1.9 0.0111 Sr 34.7 2.7 14.3 2.43 0.0029 2.7 0.0399 P 39.0 3.6 2.4 16.58 0.0470 3.6 0.0395 K 17.9 5.3 5.1 3.50 0.0117 5.3 0.0186 Cl 39.7 2.9 2.2 18.04 0.0082 2.9 0.0226 Ca 3452.8 0.4 17.7 195.62 0.7599 0.5 0.0334 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0627 Elt. k-ratio Correc. Na 0.0035 2.3168 Mg 0.0059 1.7023 Sr 0.0018 1.3804 P 0.0074 1.2000 K 0.0010 1.0282 Cl 0.0046 1.1189 Ca 0.2758 1.0940 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2762 iteration : 3 Analysis no. 225 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.8037 0.026234 0.8037 0.6579 Mg 0.9974 0.019108 0.9974 0.7723 Sr 0.2488 0.013507 0.2488 0.0534 P 0.8835 0.034941 0.8835 0.5368 K 0.1070 0.008994 0.1070 0.0515 Cl 0.5135 0.016219 0.5135 0.2726 Ca 30.1723 0.140673 30.1723 14.1679 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0342 0.020472 0.0342 0.0117 C 14.2339 14.2339 22.3033 O 52.0057 52.0057 61.1725 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 226 x= -14177.0 y= 2789.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 16.4 5.5 3.6 4.51 0.0164 5.5 0.0289 Mg 116.0 2.1 2.5 46.07 0.0635 2.1 0.0111 Sr 30.2 2.9 14.3 2.12 0.0023 2.9 0.0397 P 40.3 3.5 2.4 17.15 0.0487 3.5 0.0394 K 18.7 5.2 5.1 3.66 0.0125 5.2 0.0185 Cl 49.6 2.6 2.2 22.55 0.0104 2.6 0.0225 Ca 3602.8 0.4 17.7 204.12 0.7933 0.5 0.0333 Ba 11.0 4.8 10.8 1.02 0.0002 4.8 0.0748 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0557 Mn 4.3 10.8 2.7 1.57 0.0015 10.8 0.0627 Elt. k-ratio Correc. Na 0.0008 2.3284 Mg 0.0046 1.6964 Sr 0.0014 1.3750 P 0.0076 1.1951 K 0.0011 1.0229 Cl 0.0058 1.1147 Ca 0.2879 1.0925 Ba 0.0000 1.5390 Fe 0.0001 1.2527 Mn 0.0004 1.2757 iteration : 3 Analysis no. 226 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1902 0.014962 0.1902 0.1569 Mg 0.7796 0.016894 0.7796 0.6083 Sr 0.1935 0.012822 0.1935 0.0419 P 0.9126 0.035382 0.9126 0.5588 K 0.1131 0.009105 0.1131 0.0549 Cl 0.6474 0.017987 0.6474 0.3464 Ca 31.4514 0.144527 31.4514 14.8833 Ba 0.0065 0.019262 0.0065 0.0009 Fe 0.0159 0.014043 0.0159 0.0054 Mn 0.0560 0.021413 0.0560 0.0193 C 14.0239 14.0239 22.1450 O 51.6099 51.6099 61.1789 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 227 x= -14176.0 y= 2794.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 12.7 6.3 3.6 3.49 0.0116 6.3 0.0290 Mg 102.0 2.2 2.5 40.52 0.0557 2.2 0.0111 Sr 28.0 3.0 14.3 1.96 0.0020 3.0 0.0399 P 37.5 3.6 2.4 15.96 0.0451 3.7 0.0395 K 14.2 5.9 5.1 2.77 0.0083 6.0 0.0187 Cl 45.5 2.7 2.2 20.70 0.0095 2.7 0.0226 Ca 3220.3 0.4 17.7 182.44 0.7087 0.5 0.0335 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0559 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0629 Elt. k-ratio Correc. Na 0.0006 2.3328 Mg 0.0040 1.6988 Sr 0.0012 1.3787 P 0.0071 1.1991 K 0.0007 1.0344 Cl 0.0053 1.1214 Ca 0.2572 1.0974 Ba 0.0000 NaN Fe 0.0001 1.2572 Mn 0.0002 1.2793 iteration : 2 Analysis no. 227 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1352 0.013526 0.1352 0.1082 Mg 0.6847 0.015872 0.6847 0.5185 Sr 0.1672 0.012534 0.1672 0.0351 P 0.8482 0.034299 0.8482 0.5040 K 0.0764 0.008287 0.0764 0.0360 Cl 0.5955 0.017369 0.5955 0.3091 Ca 28.2250 0.134822 28.2250 12.9604 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0134 0.014020 0.0134 0.0044 Mn 0.0252 0.020122 0.0252 0.0084 C 15.4046 15.4046 23.6038 O 53.8246 53.8246 61.9120 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 228 x= -14176.0 y= 2798.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 26.3 4.4 3.6 7.25 0.0292 4.4 0.0289 Mg 124.7 2.0 2.5 49.52 0.0683 2.0 0.0111 Sr 32.0 2.8 14.3 2.24 0.0025 2.8 0.0398 P 41.7 3.5 2.4 17.75 0.0505 3.5 0.0394 K 16.1 5.6 5.1 3.15 0.0101 5.6 0.0186 Cl 44.2 2.7 2.2 20.08 0.0092 2.7 0.0225 Ca 3482.1 0.4 17.7 197.28 0.7665 0.5 0.0334 Ba 8.8 5.3 10.8 0.81 0.0000 5.3 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0557 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0627 Elt. k-ratio Correc. Na 0.0015 2.3255 Mg 0.0049 1.6980 Sr 0.0016 1.3772 P 0.0079 1.1974 K 0.0009 1.0269 Cl 0.0051 1.1176 Ca 0.2782 1.0939 Ba 0.0000 NaN Fe 0.0000 1.2538 Mn 0.0004 1.2765 iteration : 3 Analysis no. 228 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3386 0.018316 0.3386 0.2771 Mg 0.8401 0.017533 0.8401 0.6503 Sr 0.2151 0.013094 0.2151 0.0462 P 0.9480 0.036035 0.9480 0.5758 K 0.0918 0.008623 0.0918 0.0442 Cl 0.5746 0.017056 0.5746 0.3049 Ca 30.4304 0.141466 30.4304 14.2834 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0033 0.013677 0.0033 0.0011 Mn 0.0469 0.021037 0.0469 0.0161 C 14.3346 14.3346 22.4521 O 52.1765 52.1765 61.3489 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 229 x= -14175.0 y= 2803.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 19.5 5.1 3.6 5.38 0.0204 5.1 0.0289 Mg 100.0 2.2 2.5 39.71 0.0545 2.3 0.0111 Sr 29.1 2.9 14.3 2.03 0.0021 2.9 0.0398 P 43.2 3.4 2.4 18.39 0.0524 3.4 0.0395 K 12.9 6.2 5.1 2.53 0.0072 6.2 0.0188 Cl 46.9 2.7 2.2 21.33 0.0098 2.7 0.0226 Ca 3182.1 0.4 17.7 180.28 0.7001 0.5 0.0335 Ba 10.2 5.0 10.8 0.95 0.0000 5.0 0.0000 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0559 Mn 4.3 10.8 2.7 1.57 0.0015 10.8 0.0628 Elt. k-ratio Correc. Na 0.0010 2.3303 Mg 0.0039 1.6994 Sr 0.0013 1.3789 P 0.0082 1.1996 K 0.0006 1.0365 Cl 0.0055 1.1229 Ca 0.2541 1.0977 Ba 0.0000 NaN Fe 0.0001 1.2571 Mn 0.0004 1.2792 iteration : 3 Analysis no. 229 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2375 0.016117 0.2375 0.1900 Mg 0.6707 0.015714 0.6707 0.5074 Sr 0.1800 0.012688 0.1800 0.0378 P 0.9859 0.036719 0.9859 0.5853 K 0.0660 0.008027 0.0660 0.0310 Cl 0.6149 0.017635 0.6149 0.3189 Ca 27.8899 0.133783 27.8899 12.7962 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0126 0.013991 0.0126 0.0041 Mn 0.0561 0.021469 0.0561 0.0188 C 15.3997 15.3997 23.5773 O 53.8867 53.8867 61.9332 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 230 x= -14174.0 y= 2807.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 18.5 5.2 3.6 5.09 0.0191 5.2 0.0289 Mg 96.3 2.3 2.5 38.24 0.0524 2.3 0.0111 Sr 29.6 2.9 14.3 2.08 0.0022 2.9 0.0398 P 51.9 3.1 2.4 22.09 0.0636 3.1 0.0395 K 13.6 6.1 5.1 2.67 0.0078 6.1 0.0187 Cl 48.1 2.6 2.2 21.84 0.0101 2.6 0.0226 Ca 3285.7 0.4 17.7 186.15 0.7230 0.5 0.0334 Ba 10.2 4.9 10.8 0.95 0.0000 5.0 0.0000 Fe 3.8 8.1 3.3 1.15 0.0003 8.1 0.0558 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0628 Elt. k-ratio Correc. Na 0.0010 2.3283 Mg 0.0038 1.6976 Sr 0.0014 1.3768 P 0.0100 1.1978 K 0.0007 1.0340 Cl 0.0056 1.1217 Ca 0.2624 1.0965 Ba 0.0000 NaN Fe 0.0001 1.2558 Mn 0.0003 1.2781 iteration : 3 Analysis no. 230 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2216 0.015732 0.2216 0.1789 Mg 0.6446 0.015407 0.6446 0.4920 Sr 0.1867 0.012754 0.1867 0.0395 P 1.1942 0.040094 1.1942 0.7153 K 0.0717 0.008163 0.0717 0.0340 Cl 0.6299 0.017821 0.6299 0.3296 Ca 28.7733 0.136477 28.7733 13.3199 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0167 0.014102 0.0167 0.0056 Mn 0.0361 0.020586 0.0361 0.0122 C 14.9482 14.9482 23.0913 O 53.2770 53.2770 61.7817 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 231 x= -14173.0 y= 2811.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.3 4.0 3.6 8.63 0.0356 4.0 0.0287 Mg 162.0 1.8 2.5 64.33 0.0892 1.8 0.0110 Sr 38.3 2.6 14.3 2.68 0.0034 2.6 0.0398 P 55.8 3.0 2.4 23.75 0.0686 3.0 0.0395 K 15.4 5.7 5.1 3.01 0.0094 5.7 0.0187 Cl 64.9 2.3 2.2 29.48 0.0138 2.3 0.0226 Ca 3462.5 0.4 17.7 196.17 0.7625 0.5 0.0334 Ba 10.2 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 4.0 7.9 3.3 1.20 0.0004 8.0 0.0557 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0627 Elt. k-ratio Correc. Na 0.0018 2.3138 Mg 0.0065 1.6928 Sr 0.0021 1.3767 P 0.0108 1.1978 K 0.0008 1.0314 Cl 0.0077 1.1200 Ca 0.2767 1.0943 Ba 0.0000 NaN Fe 0.0002 1.2524 Mn 0.0001 1.2753 iteration : 3 Analysis no. 231 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4113 0.019710 0.4113 0.3387 Mg 1.0936 0.019954 1.0936 0.8516 Sr 0.2927 0.013977 0.2927 0.0632 P 1.2887 0.041564 1.2887 0.7875 K 0.0863 0.008520 0.0863 0.0418 Cl 0.8599 0.020585 0.8599 0.4591 Ca 30.2812 0.141045 30.2812 14.3000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0217 0.014218 0.0217 0.0074 Mn 0.0142 0.019563 0.0142 0.0049 C 13.9586 13.9586 21.9964 O 51.6916 51.6916 61.1494 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 232 x= -14173.0 y= 2816.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 15.0 5.8 3.6 4.14 0.0146 5.8 0.0290 Mg 73.2 2.6 2.5 29.08 0.0396 2.6 0.0111 Sr 29.7 2.9 14.3 2.08 0.0022 2.9 0.0399 P 42.7 3.4 2.4 18.15 0.0517 3.4 0.0395 K 13.8 6.0 5.1 2.71 0.0080 6.0 0.0188 Cl 44.2 2.7 2.2 20.08 0.0092 2.7 0.0227 Ca 3149.1 0.4 17.7 178.41 0.6933 0.5 0.0335 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.3 8.7 3.3 0.99 0.0000 8.7 0.0000 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0630 Elt. k-ratio Correc. Na 0.0007 2.3335 Mg 0.0029 1.7000 Sr 0.0014 1.3779 P 0.0081 1.1991 K 0.0007 1.0369 Cl 0.0051 1.1231 Ca 0.2516 1.0983 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2799 iteration : 2 Analysis no. 232 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1705 0.014485 0.1705 0.1358 Mg 0.4870 0.013487 0.4870 0.3669 Sr 0.1879 0.012783 0.1879 0.0393 P 0.9729 0.036505 0.9729 0.5751 K 0.0737 0.008235 0.0737 0.0345 Cl 0.5778 0.017149 0.5778 0.2984 Ca 27.6321 0.133036 27.6321 12.6237 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0106 0.019468 0.0106 0.0035 C 15.6373 15.6373 23.8385 O 54.2502 54.2502 62.0842 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 233 x= -14172.0 y= 2820.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 27.7 4.2 3.6 7.64 0.0310 4.3 0.0288 Mg 155.0 1.8 2.5 61.55 0.0854 1.8 0.0111 Sr 37.1 2.6 14.3 2.60 0.0033 2.6 0.0398 P 58.4 2.9 2.4 24.86 0.0720 2.9 0.0395 K 17.8 5.3 5.1 3.48 0.0116 5.3 0.0187 Cl 48.4 2.6 2.2 21.99 0.0102 2.6 0.0226 Ca 3468.7 0.4 17.7 196.52 0.7642 0.5 0.0334 Ba 10.2 5.0 10.8 0.95 0.0000 5.0 0.0000 Fe 3.6 8.3 3.3 1.09 0.0002 8.3 0.0557 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0628 Elt. k-ratio Correc. Na 0.0015 2.3170 Mg 0.0062 1.6935 Sr 0.0020 1.3767 P 0.0113 1.1978 K 0.0010 1.0300 Cl 0.0057 1.1201 Ca 0.2774 1.0941 Ba 0.0000 NaN Fe 0.0001 1.2527 Mn 0.0002 1.2755 iteration : 3 Analysis no. 233 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3585 0.018691 0.3585 0.2948 Mg 1.0465 0.019530 1.0465 0.8141 Sr 0.2776 0.013815 0.2776 0.0599 P 1.3521 0.042528 1.3521 0.8253 K 0.1064 0.008999 0.1064 0.0515 Cl 0.6341 0.017872 0.6341 0.3382 Ca 30.3455 0.141258 30.3455 14.3149 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0100 0.013880 0.0100 0.0034 Mn 0.0306 0.020321 0.0306 0.0105 C 13.9795 13.9795 22.0057 O 51.8592 51.8592 61.2816 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 234 x= -14171.0 y= 2825.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 15.6 5.7 3.6 4.29 0.0153 5.7 0.0290 Mg 55.1 3.0 2.5 21.87 0.0294 3.0 0.0111 Sr 24.2 3.2 14.3 1.70 0.0014 3.2 0.0400 P 45.6 3.3 2.4 19.39 0.0555 3.3 0.0397 K 12.5 6.3 5.1 2.45 0.0068 6.3 0.0192 Cl 57.5 2.4 2.2 26.15 0.0122 2.4 0.0229 Ca 2596.2 0.4 17.7 147.08 0.5710 0.5 0.0338 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0632 Elt. k-ratio Correc. Na 0.0008 2.3348 Mg 0.0021 1.7023 Sr 0.0009 1.3824 P 0.0087 1.2040 K 0.0006 1.0571 Cl 0.0068 1.1335 Ca 0.2072 1.1056 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2845 iteration : 2 Analysis no. 234 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1789 0.014710 0.1789 0.1372 Mg 0.3625 0.011759 0.3625 0.2628 Sr 0.1216 0.011998 0.1216 0.0245 P 1.0474 0.037847 1.0474 0.5960 K 0.0639 0.008102 0.0639 0.0288 Cl 0.7687 0.019661 0.7687 0.3821 Ca 22.9099 0.118356 22.9099 10.0744 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0015 0.019110 0.0015 0.0005 C 17.4347 17.4347 25.5833 O 57.1110 57.1110 62.9105 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 235 x= -14170.0 y= 2829.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 37.2 3.7 3.6 10.24 0.0432 3.7 0.0288 Mg 159.0 1.8 2.5 63.14 0.0876 1.8 0.0111 Sr 35.5 2.7 14.3 2.48 0.0030 2.7 0.0399 P 48.2 3.2 2.4 20.51 0.0589 3.2 0.0396 K 16.8 5.4 5.1 3.29 0.0108 5.5 0.0188 Cl 56.0 2.4 2.2 25.47 0.0119 2.4 0.0227 Ca 3328.4 0.4 17.7 188.57 0.7332 0.5 0.0335 Ba 8.8 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 4.1 7.8 3.3 1.24 0.0005 7.8 0.0558 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0628 Elt. k-ratio Correc. Na 0.0022 2.3166 Mg 0.0063 1.6965 Sr 0.0019 1.3795 P 0.0092 1.1999 K 0.0010 1.0342 Cl 0.0066 1.1217 Ca 0.2661 1.0958 Ba 0.0000 NaN Fe 0.0002 1.2542 Mn 0.0003 1.2767 iteration : 3 Analysis no. 235 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4992 0.021354 0.4992 0.4062 Mg 1.0760 0.019820 1.0760 0.8282 Sr 0.2584 0.013621 0.2584 0.0552 P 1.1080 0.038777 1.1080 0.6692 K 0.0989 0.008846 0.0989 0.0473 Cl 0.7402 0.019211 0.7402 0.3906 Ca 29.1577 0.137679 29.1577 13.6098 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0268 0.014392 0.0268 0.0090 Mn 0.0324 0.020422 0.0324 0.0110 C 14.5003 14.5003 22.5853 O 52.5022 52.5022 61.3883 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 236 x= -14170.0 y= 2834.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 43.9 3.4 3.6 12.09 0.0518 3.4 0.0289 Mg 90.2 2.4 2.5 35.81 0.0491 2.4 0.0111 Sr 31.0 2.8 14.3 2.17 0.0024 2.9 0.0399 P 36.8 3.7 2.4 15.64 0.0442 3.7 0.0396 K 17.6 5.3 5.1 3.45 0.0115 5.3 0.0188 Cl 42.3 2.8 2.2 19.22 0.0088 2.8 0.0226 Ca 3223.9 0.4 17.7 182.65 0.7100 0.5 0.0335 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0559 Mn 2.8 13.3 2.7 1.03 0.0001 13.4 0.0629 Elt. k-ratio Correc. Na 0.0026 2.3263 Mg 0.0036 1.7042 Sr 0.0015 1.3799 P 0.0069 1.2002 K 0.0010 1.0345 Cl 0.0049 1.1217 Ca 0.2577 1.0971 Ba 0.0000 NaN Fe 0.0000 1.2567 Mn 0.0000 1.2789 iteration : 3 Analysis no. 236 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6014 0.023160 0.6014 0.4824 Mg 0.6054 0.014986 0.6054 0.4594 Sr 0.2044 0.012997 0.2044 0.0430 P 0.8314 0.034021 0.8314 0.4950 K 0.1056 0.009008 0.1056 0.0498 Cl 0.5511 0.016776 0.5511 0.2867 Ca 28.2683 0.134976 28.2683 13.0073 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0034 0.013720 0.0034 0.0011 Mn 0.0033 0.019113 0.0033 0.0011 C 15.2619 15.2619 23.4339 O 53.5637 53.5637 61.7401 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 237 x= -14169.0 y= 2838.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 54.4 3.0 3.6 14.99 0.0653 3.1 0.0288 Mg 143.8 1.9 2.5 57.10 0.0791 1.9 0.0111 Sr 36.2 2.6 14.3 2.54 0.0031 2.6 0.0400 P 37.5 3.6 2.4 15.96 0.0451 3.7 0.0397 K 19.0 5.1 5.1 3.72 0.0128 5.1 0.0188 Cl 48.5 2.6 2.2 22.04 0.0102 2.6 0.0227 Ca 3166.3 0.4 17.7 179.39 0.6973 0.5 0.0335 Ba 10.4 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 4.0 7.9 3.3 1.20 0.0004 7.9 0.0559 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0629 Elt. k-ratio Correc. Na 0.0033 2.3177 Mg 0.0057 1.7027 Sr 0.0019 1.3827 P 0.0071 1.2029 K 0.0011 1.0381 Cl 0.0057 1.1239 Ca 0.2531 1.0976 Ba 0.0000 NaN Fe 0.0002 1.2561 Mn 0.0003 1.2782 iteration : 3 Analysis no. 237 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7557 0.025542 0.7557 0.6067 Mg 0.9748 0.018904 0.9748 0.7402 Sr 0.2684 0.013759 0.2684 0.0565 P 0.8514 0.034429 0.8514 0.5074 K 0.1174 0.009306 0.1174 0.0554 Cl 0.6377 0.017950 0.6377 0.3320 Ca 27.7748 0.133464 27.7748 12.7905 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0226 0.014291 0.0226 0.0075 Mn 0.0397 0.020767 0.0397 0.0133 C 15.1515 15.1515 23.2829 O 53.4059 53.4059 61.6075 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 238 x= -14168.0 y= 2843.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 24.6 4.5 3.6 6.77 0.0269 4.5 0.0290 Mg 113.1 2.1 2.5 44.91 0.0619 2.1 0.0111 Sr 28.2 3.0 14.3 1.98 0.0020 3.0 0.0400 P 36.0 3.7 2.4 15.30 0.0432 3.7 0.0396 K 15.9 5.6 5.1 3.12 0.0099 5.6 0.0188 Cl 49.0 2.6 2.2 22.25 0.0103 2.6 0.0227 Ca 3199.5 0.4 17.7 181.26 0.7048 0.5 0.0335 Ba 8.8 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 4.0 7.9 3.3 1.22 0.0004 7.9 0.0560 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0630 Elt. k-ratio Correc. Na 0.0013 2.3288 Mg 0.0045 1.7001 Sr 0.0012 1.3800 P 0.0068 1.2000 K 0.0009 1.0355 Cl 0.0057 1.1219 Ca 0.2558 1.0975 Ba 0.0000 NaN Fe 0.0002 1.2571 Mn 0.0001 1.2792 iteration : 3 Analysis no. 238 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3133 0.017814 0.3133 0.2508 Mg 0.7622 0.016737 0.7622 0.5772 Sr 0.1703 0.012592 0.1703 0.0358 P 0.8122 0.033671 0.8122 0.4827 K 0.0914 0.008675 0.0914 0.0430 Cl 0.6431 0.018006 0.6431 0.3339 Ca 28.0731 0.134403 28.0731 12.8936 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0243 0.014355 0.0243 0.0080 Mn 0.0124 0.019553 0.0124 0.0042 C 15.3692 15.3692 23.5550 O 53.7285 53.7285 61.8156 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 239 x= -14167.0 y= 2847.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 49.0 3.2 3.6 13.50 0.0584 3.2 0.0288 Mg 160.2 1.8 2.5 63.62 0.0883 1.8 0.0111 Sr 35.2 2.7 14.3 2.47 0.0030 2.7 0.0401 P 33.9 3.8 2.4 14.41 0.0405 3.9 0.0397 K 17.7 5.3 5.1 3.47 0.0116 5.3 0.0188 Cl 58.1 2.4 2.2 26.41 0.0123 2.4 0.0227 Ca 3203.5 0.4 17.7 181.49 0.7060 0.5 0.0335 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0559 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0630 Elt. k-ratio Correc. Na 0.0029 2.3166 Mg 0.0064 1.7004 Sr 0.0019 1.3826 P 0.0063 1.2024 K 0.0010 1.0372 Cl 0.0069 1.1228 Ca 0.2562 1.0973 Ba 0.0000 NaN Fe 0.0001 1.2558 Mn 0.0002 1.2780 iteration : 3 Analysis no. 239 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6754 0.024308 0.6754 0.5438 Mg 1.0874 0.019955 1.0874 0.8282 Sr 0.2564 0.013629 0.2564 0.0542 P 0.7632 0.032798 0.7632 0.4561 K 0.1068 0.009059 0.1068 0.0506 Cl 0.7698 0.019582 0.7698 0.4019 Ca 28.1132 0.134536 28.1132 12.9838 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0117 0.013974 0.0117 0.0039 Mn 0.0270 0.020210 0.0270 0.0091 C 15.0437 15.0437 23.1843 O 53.1452 53.1452 61.4842 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 240 x= -14167.0 y= 2852.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 28.5 4.2 3.6 7.86 0.0320 4.2 0.0290 Mg 104.0 2.2 2.5 41.32 0.0569 2.2 0.0111 Sr 27.9 3.0 14.3 1.95 0.0020 3.0 0.0400 P 32.4 3.9 2.4 13.77 0.0385 3.9 0.0396 K 16.0 5.6 5.1 3.14 0.0100 5.6 0.0188 Cl 54.2 2.5 2.2 24.65 0.0115 2.5 0.0227 Ca 3191.4 0.4 17.7 180.80 0.7031 0.5 0.0335 Ba 8.7 5.4 10.8 0.81 0.0000 5.4 0.0000 Fe 2.7 9.7 3.3 0.80 0.0000 9.7 0.0000 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0630 Elt. k-ratio Correc. Na 0.0016 2.3286 Mg 0.0041 1.7012 Sr 0.0012 1.3799 P 0.0060 1.1999 K 0.0009 1.0358 Cl 0.0064 1.1215 Ca 0.2552 1.0977 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2793 iteration : 3 Analysis no. 240 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3724 0.019034 0.3724 0.2979 Mg 0.7002 0.016067 0.7002 0.5298 Sr 0.1663 0.012544 0.1663 0.0349 P 0.7252 0.032025 0.7252 0.4306 K 0.0923 0.008698 0.0923 0.0434 Cl 0.7155 0.018913 0.7155 0.3711 Ca 28.0095 0.134219 28.0095 12.8513 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0143 0.019643 0.0143 0.0048 C 15.4477 15.4477 23.6513 O 53.7565 53.7565 61.7849 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 241 x= -14166.0 y= 2856.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.9 5.3 3.6 4.92 0.0183 5.3 0.0290 Mg 102.1 2.2 2.5 40.56 0.0558 2.2 0.0111 Sr 29.3 2.9 14.3 2.05 0.0022 2.9 0.0400 P 23.9 4.6 2.4 10.17 0.0277 4.6 0.0396 K 13.8 6.0 5.1 2.71 0.0080 6.0 0.0188 Cl 59.7 2.4 2.2 27.13 0.0127 2.4 0.0226 Ca 3215.2 0.4 17.7 182.15 0.7085 0.5 0.0335 Ba 10.5 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0560 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0630 Elt. k-ratio Correc. Na 0.0009 2.3325 Mg 0.0040 1.7002 Sr 0.0013 1.3795 P 0.0043 1.1995 K 0.0007 1.0344 Cl 0.0071 1.1200 Ca 0.2571 1.0974 Ba 0.0000 NaN Fe 0.0001 1.2573 Mn 0.0002 1.2794 iteration : 3 Analysis no. 241 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2134 0.015567 0.2134 0.1707 Mg 0.6869 0.015914 0.6869 0.5197 Sr 0.1837 0.012754 0.1837 0.0386 P 0.5209 0.027800 0.5209 0.3093 K 0.0736 0.008222 0.0736 0.0346 Cl 0.7899 0.019792 0.7899 0.4097 Ca 28.2167 0.134858 28.2167 12.9468 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0134 0.014040 0.0134 0.0044 Mn 0.0234 0.020066 0.0234 0.0078 C 15.5379 15.5379 23.7901 O 53.7404 53.7404 61.7684 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 242 x= -14165.0 y= 2861.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.7 3.5 3.6 11.22 0.0478 3.5 0.0289 Mg 123.2 2.0 2.5 48.93 0.0676 2.0 0.0111 Sr 28.9 2.9 14.3 2.02 0.0021 3.0 0.0401 P 27.8 4.2 2.4 11.83 0.0327 4.3 0.0398 K 14.7 5.8 5.1 2.88 0.0088 5.8 0.0190 Cl 65.7 2.2 2.2 29.88 0.0140 2.3 0.0228 Ca 2880.6 0.4 17.7 163.20 0.6343 0.5 0.0337 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0631 Elt. k-ratio Correc. Na 0.0024 2.3242 Mg 0.0049 1.7032 Sr 0.0013 1.3846 P 0.0051 1.2043 K 0.0008 1.0473 Cl 0.0078 1.1274 Ca 0.2302 1.1016 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2814 iteration : 3 Analysis no. 242 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5541 0.022360 0.5541 0.4346 Mg 0.8335 0.017506 0.8335 0.6183 Sr 0.1786 0.012730 0.1786 0.0367 P 0.6175 0.029936 0.6175 0.3595 K 0.0822 0.008520 0.0822 0.0379 Cl 0.8785 0.020878 0.8785 0.4468 Ca 25.3598 0.126067 25.3598 11.4074 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0307 0.020426 0.0307 0.0101 C 16.3588 16.3588 24.5550 O 55.1062 55.1062 62.0939 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 243 x= -14164.0 y= 2865.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 24.9 4.5 3.6 6.87 0.0274 4.5 0.0290 Mg 91.8 2.3 2.5 36.47 0.0500 2.4 0.0111 Sr 27.1 3.0 14.3 1.90 0.0018 3.1 0.0401 P 25.6 4.4 2.4 10.89 0.0299 4.4 0.0398 K 13.7 6.0 5.1 2.69 0.0079 6.0 0.0190 Cl 58.0 2.4 2.2 26.38 0.0123 2.4 0.0228 Ca 2803.3 0.4 17.7 158.82 0.6173 0.5 0.0337 Ba 9.6 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0632 Elt. k-ratio Correc. Na 0.0014 2.3327 Mg 0.0036 1.7035 Sr 0.0011 1.3838 P 0.0047 1.2041 K 0.0007 1.0485 Cl 0.0068 1.1281 Ca 0.2240 1.1027 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2829 iteration : 2 Analysis no. 243 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3192 0.017962 0.3192 0.2480 Mg 0.6171 0.015126 0.6171 0.4535 Sr 0.1567 0.012459 0.1567 0.0320 P 0.5641 0.028807 0.5641 0.3253 K 0.0737 0.008312 0.0737 0.0337 Cl 0.7725 0.019664 0.7725 0.3892 Ca 24.7025 0.124028 24.7025 11.0093 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0161 0.019787 0.0161 0.0052 C 16.8650 16.8650 25.0814 O 55.9131 55.9131 62.4224 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 244 x= -14164.0 y= 2870.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 48.7 3.2 3.6 13.43 0.0581 3.2 0.0289 Mg 127.2 2.0 2.5 50.52 0.0698 2.0 0.0111 Sr 32.4 2.8 14.3 2.27 0.0026 2.8 0.0402 P 27.6 4.3 2.4 11.75 0.0324 4.3 0.0398 K 16.2 5.6 5.1 3.17 0.0102 5.6 0.0191 Cl 64.9 2.3 2.2 29.51 0.0138 2.3 0.0228 Ca 2742.5 0.4 17.7 155.38 0.6037 0.5 0.0337 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.3 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0631 Elt. k-ratio Correc. Na 0.0029 2.3217 Mg 0.0051 1.7045 Sr 0.0016 1.3865 P 0.0051 1.2067 K 0.0009 1.0524 Cl 0.0077 1.1305 Ca 0.2191 1.1032 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2822 iteration : 3 Analysis no. 244 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6730 0.024297 0.6730 0.5233 Mg 0.8618 0.017802 0.8618 0.6339 Sr 0.2224 0.013265 0.2224 0.0454 P 0.6138 0.029891 0.6138 0.3543 K 0.0950 0.008870 0.0950 0.0435 Cl 0.8698 0.020808 0.8698 0.4385 Ca 24.1717 0.122347 24.1717 10.7808 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0307 0.020437 0.0307 0.0100 C 16.7418 16.7418 24.9169 O 55.7200 55.7200 62.2535 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 245 x= -14163.0 y= 2874.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 16.2 5.6 3.6 4.45 0.0161 5.6 0.0292 Mg 44.0 3.4 2.5 17.46 0.0232 3.4 0.0112 Sr 14.5 4.2 14.3 1.01 0.0000 4.2 0.0403 P 22.7 4.7 2.4 9.64 0.0261 4.7 0.0400 K 12.3 6.4 5.1 2.41 0.0066 6.4 0.0196 Cl 59.4 2.4 2.2 27.01 0.0126 2.4 0.0231 Ca 1913.2 0.5 17.7 108.39 0.4200 0.6 0.0341 Ba 5.9 6.5 10.8 0.54 0.0000 6.5 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0636 Elt. k-ratio Correc. Na 0.0008 2.3444 Mg 0.0017 1.7099 Sr 0.0000 1.3920 P 0.0041 1.2122 K 0.0006 1.0806 Cl 0.0070 1.1449 Ca 0.1524 1.1147 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2916 iteration : 2 Analysis no. 245 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1888 0.015010 0.1888 0.1375 Mg 0.2873 0.010607 0.2873 0.1979 Sr 0.0021 0.010438 0.0021 0.0004 P 0.4958 0.027407 0.4958 0.2680 K 0.0636 0.008240 0.0636 0.0272 Cl 0.8036 0.020185 0.8036 0.3794 Ca 16.9903 0.098925 16.9903 7.0964 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0199 0.020088 0.0199 0.0061 C 20.0952 20.0952 28.0079 O 61.0534 61.0534 63.8792 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 246 x= -14162.0 y= 2878.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 21.2 4.9 3.6 5.83 0.0226 4.9 0.0291 Mg 67.7 2.7 2.5 26.87 0.0365 2.7 0.0111 Sr 26.5 3.1 14.3 1.86 0.0018 3.1 0.0402 P 22.5 4.7 2.4 9.55 0.0258 4.7 0.0399 K 13.8 6.0 5.1 2.71 0.0080 6.0 0.0192 Cl 65.0 2.3 2.2 29.53 0.0138 2.3 0.0229 Ca 2491.4 0.4 17.7 141.15 0.5482 0.5 0.0338 Ba 9.8 5.0 10.8 0.91 0.0000 5.1 0.0000 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0563 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0633 Elt. k-ratio Correc. Na 0.0011 2.3368 Mg 0.0026 1.7055 Sr 0.0011 1.3859 P 0.0041 1.2068 K 0.0007 1.0596 Cl 0.0077 1.1335 Ca 0.1989 1.1067 Ba 0.0000 NaN Fe 0.0000 1.2651 Mn 0.0003 1.2856 iteration : 2 Analysis no. 246 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2634 0.016760 0.2634 0.2001 Mg 0.4506 0.013032 0.4506 0.3238 Sr 0.1499 0.012390 0.1499 0.0299 P 0.4888 0.027177 0.4888 0.2756 K 0.0754 0.008423 0.0754 0.0337 Cl 0.8727 0.020874 0.8727 0.4300 Ca 22.0178 0.115532 22.0178 9.5947 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0008 0.013744 0.0008 0.0003 Mn 0.0382 0.020820 0.0382 0.0121 C 18.0056 18.0056 26.1827 O 57.6369 57.6369 62.9172 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 247 x= -14161.0 y= 2883.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 33.4 3.9 3.6 9.21 0.0383 3.9 0.0290 Mg 107.4 2.2 2.5 42.67 0.0588 2.2 0.0111 Sr 28.8 2.9 14.3 2.01 0.0021 3.0 0.0401 P 24.3 4.5 2.4 10.32 0.0281 4.6 0.0398 K 16.3 5.5 5.1 3.20 0.0103 5.5 0.0191 Cl 67.0 2.2 2.2 30.47 0.0143 2.2 0.0228 Ca 2755.6 0.4 17.7 156.12 0.6066 0.5 0.0337 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0562 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0632 Elt. k-ratio Correc. Na 0.0019 2.3283 Mg 0.0043 1.7037 Sr 0.0013 1.3850 P 0.0044 1.2052 K 0.0009 1.0512 Cl 0.0080 1.1292 Ca 0.2201 1.1032 Ba 0.0000 NaN Fe 0.0001 1.2615 Mn 0.0003 1.2827 iteration : 2 Analysis no. 247 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4457 0.020447 0.4457 0.3460 Mg 0.7248 0.016351 0.7248 0.5322 Sr 0.1774 0.012718 0.1774 0.0361 P 0.5317 0.028112 0.5317 0.3063 K 0.0962 0.008890 0.0962 0.0439 Cl 0.8978 0.021108 0.8978 0.4519 Ca 24.2854 0.122707 24.2854 10.8130 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0084 0.013933 0.0084 0.0027 Mn 0.0326 0.020525 0.0326 0.0106 C 16.8999 16.8999 25.1093 O 55.9001 55.9001 62.3480 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 248 x= -14161.0 y= 2887.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.1 4.0 3.6 8.58 0.0354 4.0 0.0290 Mg 90.1 2.4 2.5 35.77 0.0490 2.4 0.0111 Sr 26.8 3.0 14.3 1.88 0.0018 3.1 0.0400 P 24.6 4.5 2.4 10.47 0.0286 4.5 0.0397 K 17.3 5.4 5.1 3.38 0.0112 5.4 0.0189 Cl 59.6 2.4 2.2 27.10 0.0127 2.4 0.0227 Ca 2957.3 0.4 17.7 167.54 0.6513 0.5 0.0336 Ba 9.2 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.6 8.4 3.3 1.08 0.0002 8.4 0.0561 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0631 Elt. k-ratio Correc. Na 0.0018 2.3313 Mg 0.0036 1.7041 Sr 0.0011 1.3825 P 0.0045 1.2024 K 0.0010 1.0432 Cl 0.0070 1.1250 Ca 0.2364 1.1007 Ba 0.0000 NaN Fe 0.0001 1.2599 Mn 0.0002 1.2814 iteration : 3 Analysis no. 248 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4119 0.019821 0.4119 0.3237 Mg 0.6050 0.014985 0.6050 0.4498 Sr 0.1535 0.012406 0.1535 0.0317 P 0.5390 0.028235 0.5390 0.3144 K 0.1036 0.009018 0.1036 0.0479 Cl 0.7923 0.019866 0.7923 0.4038 Ca 26.0151 0.128099 26.0151 11.7270 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0092 0.013941 0.0092 0.0030 Mn 0.0216 0.020012 0.0216 0.0071 C 16.3327 16.3327 24.5678 O 55.0160 55.0160 62.1240 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 249 x= -14160.0 y= 2892.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 32.7 3.9 3.6 9.02 0.0374 3.9 0.0243 Mg 86.1 2.4 2.5 34.18 0.0468 2.4 0.0096 Sr 3036.4 0.3 14.3 212.67 0.4326 57.7 0.0359 P 25.9 4.4 2.4 11.02 0.0303 4.4 0.0462 K 17.3 5.4 5.1 3.39 0.0112 5.4 0.0197 Cl 66.4 2.2 2.2 30.17 0.0141 2.2 0.0246 Ca 2823.2 0.4 17.7 159.95 0.6215 0.5 0.0324 Ba 8.4 5.4 10.8 0.78 0.0000 5.5 0.0000 Fe 3.3 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0570 Elt. k-ratio Correc. Na 0.0019 1.9575 Mg 0.0034 1.4753 Sr 0.2673 1.2416 P 0.0047 1.3988 K 0.0010 1.0849 Cl 0.0079 1.2199 Ca 0.2255 1.0604 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.1577 iteration : 3 Analysis no. 249 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3659 0.017022 0.3659 0.4284 Mg 0.4998 0.012682 0.4998 0.5535 Sr 33.1916 0.129789 33.1916 10.1974 P 0.6635 0.033634 0.6635 0.5767 K 0.1081 0.009387 0.1081 0.0745 Cl 0.9598 0.022690 0.9598 0.7288 Ca 23.9165 0.119770 23.9165 16.0633 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0080 0.017542 0.0080 0.0039 C 6.4290 6.4290 14.4088 O 33.8577 33.8577 56.9646 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 250 x= -14159.0 y= 2896.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 27.9 4.2 3.6 7.69 0.0313 4.2 0.0290 Mg 74.3 2.6 2.5 29.51 0.0402 2.6 0.0111 Sr 31.5 2.8 14.3 2.21 0.0025 2.8 0.0400 P 26.3 4.4 2.4 11.19 0.0308 4.4 0.0397 K 19.2 5.1 5.1 3.76 0.0130 5.1 0.0189 Cl 65.8 2.2 2.2 29.91 0.0140 2.3 0.0227 Ca 3023.9 0.4 17.7 171.32 0.6661 0.5 0.0336 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0561 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0631 Elt. k-ratio Correc. Na 0.0016 2.3316 Mg 0.0029 1.7030 Sr 0.0015 1.3802 P 0.0048 1.2011 K 0.0012 1.0416 Cl 0.0078 1.1237 Ca 0.2417 1.0998 Ba 0.0000 NaN Fe 0.0000 1.2588 Mn 0.0004 1.2805 iteration : 3 Analysis no. 250 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3640 0.018880 0.3640 0.2877 Mg 0.4959 0.013622 0.4959 0.3707 Sr 0.2104 0.013077 0.2104 0.0436 P 0.5796 0.029093 0.5796 0.3400 K 0.1200 0.009391 0.1200 0.0558 Cl 0.8765 0.020818 0.8765 0.4492 Ca 26.5851 0.129859 26.5851 12.0526 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013777 0.0042 0.0014 Mn 0.0508 0.021290 0.0508 0.0168 C 16.1066 16.1066 24.3667 O 54.6070 54.6070 62.0155 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 251 x= -14158.0 y= 2901.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.1 4.0 3.6 8.56 0.0353 4.0 0.0290 Mg 103.8 2.2 2.5 41.24 0.0568 2.2 0.0111 Sr 28.3 3.0 14.3 1.98 0.0020 3.0 0.0400 P 24.5 4.5 2.4 10.43 0.0285 4.5 0.0397 K 16.4 5.5 5.1 3.22 0.0104 5.5 0.0189 Cl 70.8 2.2 2.2 32.18 0.0151 2.2 0.0227 Ca 2984.3 0.4 17.7 169.07 0.6574 0.5 0.0336 Ba 11.0 4.8 10.8 1.02 0.0001 4.8 0.0748 Fe 3.3 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0631 Elt. k-ratio Correc. Na 0.0018 2.3281 Mg 0.0041 1.7022 Sr 0.0012 1.3821 P 0.0045 1.2021 K 0.0009 1.0434 Cl 0.0084 1.1245 Ca 0.2386 1.1003 Ba 0.0000 1.5366 Fe 0.0000 NaN Mn 0.0002 1.2809 iteration : 3 Analysis no. 251 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4106 0.019782 0.4106 0.3239 Mg 0.6994 0.016064 0.6994 0.5218 Sr 0.1715 0.012627 0.1715 0.0355 P 0.5365 0.028180 0.5365 0.3141 K 0.0964 0.008847 0.0964 0.0447 Cl 0.9463 0.021595 0.9463 0.4840 Ca 26.2507 0.128835 26.2507 11.8766 Ba 0.0059 0.019249 0.0059 0.0008 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0252 0.020172 0.0252 0.0083 C 16.1662 16.1662 24.4066 O 54.6913 54.6912 61.9837 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 252 x= -14158.0 y= 2905.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 21.8 4.8 3.6 6.00 0.0233 4.8 0.0291 Mg 54.7 3.0 2.5 21.71 0.0292 3.0 0.0111 Sr 23.6 3.3 14.3 1.65 0.0013 3.3 0.0401 P 21.3 4.8 2.4 9.06 0.0244 4.9 0.0398 K 18.6 5.2 5.1 3.64 0.0124 5.2 0.0191 Cl 55.3 2.5 2.2 25.15 0.0117 2.5 0.0228 Ca 2645.6 0.4 17.7 149.89 0.5823 0.5 0.0338 Ba 9.5 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0633 Elt. k-ratio Correc. Na 0.0012 2.3394 Mg 0.0021 1.7067 Sr 0.0008 1.3844 P 0.0038 1.2047 K 0.0011 1.0529 Cl 0.0065 1.1301 Ca 0.2113 1.1048 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2847 iteration : 2 Analysis no. 252 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2726 0.016980 0.2726 0.2090 Mg 0.3609 0.011755 0.3609 0.2616 Sr 0.1142 0.011924 0.1142 0.0230 P 0.4600 0.026485 0.4600 0.2617 K 0.1157 0.009364 0.1157 0.0522 Cl 0.7363 0.019245 0.7363 0.3660 Ca 23.3459 0.119758 23.3459 10.2639 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0271 0.020314 0.0271 0.0087 C 17.5849 17.5849 25.7983 O 56.9823 56.9823 62.7557 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 253 x= -14157.0 y= 2910.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 28.7 4.2 3.6 7.91 0.0323 4.2 0.0291 Mg 76.8 2.5 2.5 30.51 0.0416 2.6 0.0112 Sr 26.6 3.1 14.3 1.86 0.0018 3.1 0.0401 P 17.4 5.4 2.4 7.38 0.0193 5.4 0.0398 K 17.0 5.4 5.1 3.33 0.0110 5.4 0.0191 Cl 59.9 2.4 2.2 27.22 0.0127 2.4 0.0228 Ca 2752.3 0.4 17.7 155.93 0.6061 0.5 0.0337 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0562 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0632 Elt. k-ratio Correc. Na 0.0016 2.3357 Mg 0.0030 1.7064 Sr 0.0011 1.3846 P 0.0030 1.2046 K 0.0010 1.0494 Cl 0.0071 1.1280 Ca 0.2200 1.1032 Ba 0.0000 NaN Fe 0.0001 1.2623 Mn 0.0004 1.2834 iteration : 2 Analysis no. 253 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3767 0.019161 0.3767 0.2914 Mg 0.5143 0.013878 0.5143 0.3763 Sr 0.1514 0.012400 0.1514 0.0307 P 0.3642 0.024158 0.3642 0.2091 K 0.1021 0.009025 0.1021 0.0464 Cl 0.7985 0.019971 0.7985 0.4005 Ca 24.2669 0.122667 24.2669 10.7660 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0152 0.014150 0.0152 0.0048 Mn 0.0509 0.021345 0.0509 0.0165 C 17.1510 17.1510 25.3909 O 56.2088 56.2088 62.4674 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 254 x= -14156.0 y= 2914.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 22.6 4.7 3.6 6.22 0.0244 4.7 0.0291 Mg 69.8 2.7 2.5 27.71 0.0377 2.7 0.0111 Sr 28.3 3.0 14.3 1.98 0.0020 3.0 0.0400 P 21.5 4.8 2.4 9.13 0.0245 4.8 0.0397 K 17.8 5.3 5.1 3.49 0.0117 5.3 0.0189 Cl 58.9 2.4 2.2 26.75 0.0125 2.4 0.0227 Ca 3046.7 0.4 17.7 172.61 0.6712 0.5 0.0336 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 2.8 9.4 3.3 0.86 0.0000 9.4 0.0000 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0631 Elt. k-ratio Correc. Na 0.0012 2.3353 Mg 0.0027 1.7035 Sr 0.0012 1.3803 P 0.0038 1.2007 K 0.0010 1.0394 Cl 0.0070 1.1226 Ca 0.2436 1.0996 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2811 iteration : 2 Analysis no. 254 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2842 0.017220 0.2842 0.2243 Mg 0.4646 0.013213 0.4646 0.3469 Sr 0.1716 0.012615 0.1716 0.0355 P 0.4621 0.026485 0.4621 0.2707 K 0.1079 0.009098 0.1079 0.0501 Cl 0.7802 0.019703 0.7802 0.3993 Ca 26.7859 0.130488 26.7859 12.1267 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0125 0.019590 0.0125 0.0041 C 16.1987 16.1987 24.4716 O 54.7322 54.7322 62.0708 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 255 x= -14155.0 y= 2919.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 29.9 4.1 3.6 8.24 0.0339 4.1 0.0290 Mg 94.6 2.3 2.5 37.58 0.0516 2.3 0.0111 Sr 25.5 3.1 14.3 1.78 0.0016 3.1 0.0401 P 24.4 4.5 2.4 10.36 0.0283 4.5 0.0398 K 21.5 4.8 5.1 4.22 0.0151 4.8 0.0190 Cl 61.9 2.3 2.2 28.15 0.0132 2.3 0.0228 Ca 2805.3 0.4 17.7 158.93 0.6178 0.5 0.0337 Ba 9.2 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0562 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0632 Elt. k-ratio Correc. Na 0.0017 2.3312 Mg 0.0037 1.7041 Sr 0.0010 1.3841 P 0.0044 1.2039 K 0.0013 1.0487 Cl 0.0073 1.1278 Ca 0.2242 1.1027 Ba 0.0000 NaN Fe 0.0000 1.2614 Mn 0.0002 1.2827 iteration : 2 Analysis no. 255 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3940 0.019478 0.3940 0.3065 Mg 0.6367 0.015360 0.6367 0.4685 Sr 0.1372 0.012218 0.1372 0.0280 P 0.5338 0.028149 0.5338 0.3082 K 0.1406 0.009897 0.1406 0.0643 Cl 0.8264 0.020292 0.8264 0.4169 Ca 24.7248 0.124108 24.7248 11.0325 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013732 0.0017 0.0005 Mn 0.0253 0.020204 0.0253 0.0082 C 16.8081 16.8081 25.0270 O 55.7714 55.7714 62.3393 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 256 x= -14155.0 y= 2923.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 34.2 3.8 3.6 9.43 0.0394 3.8 0.0290 Mg 113.9 2.1 2.5 45.23 0.0624 2.1 0.0111 Sr 27.2 3.0 14.3 1.91 0.0019 3.0 0.0401 P 24.2 4.5 2.4 10.30 0.0281 4.6 0.0397 K 17.3 5.4 5.1 3.38 0.0112 5.4 0.0189 Cl 48.1 2.6 2.2 21.86 0.0101 2.6 0.0227 Ca 3077.9 0.4 17.7 174.38 0.6782 0.5 0.0336 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0561 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0631 Elt. k-ratio Correc. Na 0.0020 2.3299 Mg 0.0045 1.7040 Sr 0.0011 1.3829 P 0.0044 1.2023 K 0.0010 1.0384 Cl 0.0056 1.1231 Ca 0.2461 1.0989 Ba 0.0000 NaN Fe 0.0001 1.2585 Mn 0.0004 1.2804 iteration : 3 Analysis no. 256 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4582 0.020692 0.4582 0.3633 Mg 0.7698 0.016844 0.7698 0.5773 Sr 0.1585 0.012475 0.1585 0.0330 P 0.5294 0.028030 0.5294 0.3115 K 0.1032 0.008980 0.1032 0.0481 Cl 0.6322 0.017881 0.6322 0.3250 Ca 27.0488 0.131290 27.0488 12.3005 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0126 0.014032 0.0126 0.0041 Mn 0.0453 0.021057 0.0453 0.0150 C 15.8751 15.8751 24.0901 O 54.3668 54.3668 61.9321 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 257 x= -14154.0 y= 2928.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.8 3.5 3.6 11.25 0.0479 3.5 0.0289 Mg 140.7 1.9 2.5 55.86 0.0774 1.9 0.0111 Sr 38.6 2.5 14.3 2.70 0.0035 2.6 0.0401 P 20.2 5.0 2.4 8.60 0.0229 5.0 0.0398 K 17.9 5.3 5.1 3.50 0.0117 5.3 0.0189 Cl 80.8 2.0 2.2 36.72 0.0173 2.0 0.0227 Ca 3009.8 0.4 17.7 170.52 0.6631 0.5 0.0336 Ba 10.6 4.9 10.8 0.99 0.0000 4.9 0.0000 Fe 3.7 8.2 3.3 1.13 0.0002 8.2 0.0560 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0630 Elt. k-ratio Correc. Na 0.0024 2.3203 Mg 0.0056 1.7007 Sr 0.0022 1.3833 P 0.0036 1.2038 K 0.0010 1.0440 Cl 0.0096 1.1246 Ca 0.2406 1.0998 Ba 0.0000 NaN Fe 0.0001 1.2579 Mn 0.0003 1.2796 iteration : 3 Analysis no. 257 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5548 0.022352 0.5548 0.4401 Mg 0.9529 0.018688 0.9529 0.7149 Sr 0.2978 0.014097 0.2978 0.0620 P 0.4330 0.025839 0.4330 0.2549 K 0.1088 0.009147 0.1088 0.0507 Cl 1.0841 0.023039 1.0841 0.5576 Ca 26.4662 0.129495 26.4662 12.0415 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0143 0.014073 0.0143 0.0047 Mn 0.0325 0.020482 0.0325 0.0108 C 15.9012 15.9012 24.1417 O 54.1545 54.1545 61.7211 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 258 x= -14153.0 y= 2932.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.6 3.5 3.6 11.20 0.0476 3.5 0.0289 Mg 123.7 2.0 2.5 49.11 0.0679 2.0 0.0111 Sr 36.7 2.6 14.3 2.57 0.0032 2.6 0.0400 P 21.7 4.8 2.4 9.21 0.0248 4.8 0.0396 K 21.5 4.8 5.1 4.22 0.0151 4.8 0.0188 Cl 73.3 2.1 2.2 33.32 0.0157 2.1 0.0226 Ca 3311.0 0.4 17.7 187.58 0.7300 0.5 0.0335 Ba 10.8 4.8 10.8 1.00 0.0000 4.8 NaN Fe 3.6 8.4 3.3 1.08 0.0002 8.4 0.0559 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0630 Elt. k-ratio Correc. Na 0.0024 2.3220 Mg 0.0049 1.7006 Sr 0.0020 1.3796 P 0.0039 1.1999 K 0.0013 1.0332 Cl 0.0087 1.1187 Ca 0.2649 1.0961 Ba 0.0000 NaN Fe 0.0001 1.2551 Mn 0.0001 1.2775 iteration : 3 Analysis no. 258 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5523 0.022323 0.5523 0.4470 Mg 0.8357 0.017519 0.8357 0.6398 Sr 0.2736 0.013802 0.2736 0.0581 P 0.4668 0.026585 0.4668 0.2804 K 0.1385 0.009751 0.1385 0.0659 Cl 0.9761 0.021858 0.9761 0.5123 Ca 29.0384 0.137366 29.0384 13.4804 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0092 0.013895 0.0092 0.0031 Mn 0.0143 0.019626 0.0143 0.0048 C 14.9808 14.9808 23.2069 O 52.7143 52.7143 61.3013 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 259 x= -14152.0 y= 2936.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.3 4.0 3.6 8.62 0.0356 4.0 0.0290 Mg 105.8 2.2 2.5 42.01 0.0579 2.2 0.0111 Sr 31.2 2.8 14.3 2.18 0.0024 2.8 0.0400 P 21.3 4.8 2.4 9.04 0.0243 4.9 0.0397 K 21.3 4.8 5.1 4.17 0.0149 4.9 0.0188 Cl 64.4 2.3 2.2 29.29 0.0137 2.3 0.0227 Ca 3119.9 0.4 17.7 176.76 0.6876 0.5 0.0336 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.1 9.0 3.3 0.92 0.0000 9.1 0.0000 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0631 Elt. k-ratio Correc. Na 0.0018 2.3285 Mg 0.0042 1.7021 Sr 0.0015 1.3811 P 0.0038 1.2012 K 0.0013 1.0382 Cl 0.0076 1.1218 Ca 0.2495 1.0986 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2798 iteration : 3 Analysis no. 259 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4138 0.019847 0.4138 0.3293 Mg 0.7130 0.016217 0.7130 0.5368 Sr 0.2066 0.013042 0.2066 0.0431 P 0.4575 0.026385 0.4575 0.2703 K 0.1371 0.009751 0.1371 0.0642 Cl 0.8565 0.020577 0.8565 0.4421 Ca 27.4122 0.132413 27.4122 12.5155 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0270 0.020242 0.0270 0.0090 C 15.7602 15.7602 24.0113 O 54.0161 54.0161 61.7784 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 260 x= -14152.0 y= 2941.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.9 4.0 3.6 8.78 0.0364 4.0 0.0291 Mg 78.6 2.5 2.5 31.20 0.0426 2.5 0.0112 Sr 29.9 2.9 14.3 2.09 0.0022 2.9 0.0401 P 18.2 5.2 2.4 7.75 0.0204 5.2 0.0397 K 20.5 4.9 5.1 4.01 0.0142 5.0 0.0189 Cl 51.0 2.6 2.2 23.18 0.0108 2.6 0.0227 Ca 2991.2 0.4 17.7 169.46 0.6592 0.5 0.0336 Ba 9.1 5.3 10.8 0.84 0.0000 5.3 0.0000 Fe 3.9 8.0 3.3 1.18 0.0003 8.0 0.0561 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0632 Elt. k-ratio Correc. Na 0.0018 2.3344 Mg 0.0031 1.7060 Sr 0.0014 1.3824 P 0.0032 1.2026 K 0.0013 1.0407 Cl 0.0060 1.1237 Ca 0.2392 1.1000 Ba 0.0000 NaN Fe 0.0002 1.2597 Mn 0.0002 1.2813 iteration : 3 Analysis no. 260 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4239 0.020074 0.4239 0.3334 Mg 0.5264 0.014031 0.5264 0.3916 Sr 0.1906 0.012864 0.1906 0.0393 P 0.3842 0.024639 0.3842 0.2243 K 0.1306 0.009627 0.1306 0.0604 Cl 0.6727 0.018406 0.6727 0.3431 Ca 26.3150 0.129043 26.3150 11.8720 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0202 0.014273 0.0202 0.0065 Mn 0.0307 0.020434 0.0307 0.0101 C 16.3435 16.3435 24.6045 O 54.9621 54.9621 62.1147 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 261 x= -14151.0 y= 2945.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 29.4 4.1 3.6 8.11 0.0332 4.1 0.0290 Mg 83.5 2.4 2.5 33.17 0.0454 2.5 0.0111 Sr 30.5 2.9 14.3 2.13 0.0023 2.9 0.0399 P 20.7 4.9 2.4 8.81 0.0236 4.9 0.0396 K 21.5 4.8 5.1 4.22 0.0151 4.8 0.0187 Cl 61.7 2.3 2.2 28.06 0.0131 2.3 0.0226 Ca 3339.4 0.4 17.7 189.19 0.7364 0.5 0.0335 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0560 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0630 Elt. k-ratio Correc. Na 0.0017 2.3314 Mg 0.0033 1.7025 Sr 0.0014 1.3780 P 0.0037 1.1980 K 0.0013 1.0301 Cl 0.0073 1.1171 Ca 0.2673 1.0957 Ba 0.0000 NaN Fe 0.0000 1.2558 Mn 0.0003 1.2782 iteration : 3 Analysis no. 261 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3866 0.019339 0.3866 0.3122 Mg 0.5596 0.014432 0.5596 0.4274 Sr 0.1973 0.012912 0.1973 0.0418 P 0.4432 0.026014 0.4432 0.2656 K 0.1382 0.009725 0.1382 0.0656 Cl 0.8162 0.020076 0.8162 0.4273 Ca 29.2858 0.138125 29.2858 13.5641 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0034 0.013727 0.0034 0.0011 Mn 0.0380 0.020711 0.0380 0.0128 C 15.1393 15.1392 23.3985 O 52.9925 52.9925 61.4835 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 262 x= -14150.0 y= 2950.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 45.3 3.3 3.6 12.48 0.0537 3.3 0.0289 Mg 134.9 1.9 2.5 53.58 0.0742 2.0 0.0111 Sr 39.0 2.5 14.3 2.73 0.0035 2.5 0.0401 P 22.5 4.7 2.4 9.55 0.0259 4.7 0.0397 K 24.8 4.5 5.1 4.86 0.0182 4.5 0.0188 Cl 64.1 2.3 2.2 29.14 0.0137 2.3 0.0227 Ca 3238.1 0.4 17.7 183.45 0.7141 0.5 0.0336 Ba 12.3 4.5 10.8 1.14 0.0009 4.5 0.0749 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0560 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0630 Elt. k-ratio Correc. Na 0.0027 2.3207 Mg 0.0054 1.7017 Sr 0.0022 1.3814 P 0.0041 1.2017 K 0.0016 1.0353 Cl 0.0076 1.1205 Ca 0.2592 1.0967 Ba 0.0003 1.5367 Fe 0.0000 1.2555 Mn 0.0003 1.2778 iteration : 3 Analysis no. 262 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6217 0.023479 0.6217 0.5012 Mg 0.9143 0.018321 0.9143 0.6972 Sr 0.3028 0.014144 0.3028 0.0640 P 0.4870 0.027080 0.4870 0.2914 K 0.1668 0.010366 0.1668 0.0791 Cl 0.8513 0.020512 0.8513 0.4450 Ca 28.4206 0.135494 28.4206 13.1414 Ba 0.0399 0.019832 0.0399 0.0054 Fe 0.0034 0.013725 0.0034 0.0011 Mn 0.0398 0.020786 0.0398 0.0134 C 15.1315 15.1315 23.3474 O 53.0209 53.0209 61.4134 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 263 x= -14149.0 y= 2954.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 21.2 4.9 3.6 5.83 0.0226 4.9 0.0291 Mg 70.4 2.7 2.5 27.94 0.0380 2.7 0.0112 Sr 23.1 3.3 14.3 1.61 0.0013 3.3 0.0401 P 21.7 4.8 2.4 9.21 0.0248 4.8 0.0398 K 17.3 5.4 5.1 3.38 0.0112 5.4 0.0191 Cl 56.6 2.4 2.2 25.74 0.0120 2.4 0.0228 Ca 2721.9 0.4 17.7 154.21 0.5997 0.5 0.0338 Ba 9.3 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 2.9 13.2 2.7 1.05 0.0001 13.2 0.0633 Elt. k-ratio Correc. Na 0.0011 2.3374 Mg 0.0028 1.7052 Sr 0.0008 1.3841 P 0.0039 1.2041 K 0.0010 1.0504 Cl 0.0067 1.1287 Ca 0.2176 1.1038 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2841 iteration : 2 Analysis no. 263 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2636 0.016776 0.2636 0.2032 Mg 0.4696 0.013291 0.4696 0.3424 Sr 0.1075 0.011844 0.1075 0.0218 P 0.4686 0.026691 0.4686 0.2682 K 0.1044 0.009088 0.1044 0.0473 Cl 0.7541 0.019456 0.7541 0.3770 Ca 24.0226 0.121933 24.0226 10.6231 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0052 0.019305 0.0052 0.0017 C 17.2851 17.2851 25.5064 O 56.5193 56.5193 62.6090 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 264 x= -14149.0 y= 2959.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 23.6 4.6 3.6 6.51 0.0257 4.6 0.0290 Mg 109.1 2.1 2.5 43.32 0.0597 2.2 0.0111 Sr 34.5 2.7 14.3 2.41 0.0029 2.7 0.0400 P 19.9 5.0 2.4 8.45 0.0225 5.0 0.0397 K 20.5 4.9 5.1 4.02 0.0142 4.9 0.0188 Cl 72.2 2.1 2.2 32.84 0.0154 2.1 0.0227 Ca 3178.0 0.4 17.7 180.04 0.7007 0.5 0.0336 Ba 10.5 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 3.1 9.0 3.3 0.94 0.0000 9.0 0.0000 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0631 Elt. k-ratio Correc. Na 0.0013 2.3285 Mg 0.0043 1.6997 Sr 0.0018 1.3798 P 0.0035 1.2003 K 0.0013 1.0367 Cl 0.0086 1.1205 Ca 0.2543 1.0979 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2792 iteration : 3 Analysis no. 264 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2993 0.017522 0.2993 0.2393 Mg 0.7350 0.016449 0.7350 0.5560 Sr 0.2468 0.013503 0.2468 0.0518 P 0.4235 0.025574 0.4235 0.2514 K 0.1306 0.009601 0.1306 0.0614 Cl 0.9631 0.021741 0.9631 0.4994 Ca 27.9168 0.133973 27.9168 12.8051 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0270 0.020239 0.0270 0.0090 C 15.5876 15.5876 23.8586 O 53.6703 53.6703 61.6680 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 265 x= -14148.0 y= 2963.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 39.0 3.6 3.6 10.74 0.0456 3.6 0.0289 Mg 130.7 2.0 2.5 51.89 0.0719 2.0 0.0111 Sr 40.2 2.5 14.3 2.81 0.0037 2.5 0.0400 P 21.1 4.9 2.4 8.98 0.0241 4.9 0.0396 K 24.6 4.5 5.1 4.81 0.0179 4.5 0.0187 Cl 79.7 2.0 2.2 36.22 0.0171 2.0 0.0226 Ca 3433.3 0.4 17.7 194.51 0.7576 0.5 0.0335 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0559 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0630 Elt. k-ratio Correc. Na 0.0023 2.3203 Mg 0.0052 1.6988 Sr 0.0023 1.3780 P 0.0038 1.1986 K 0.0016 1.0298 Cl 0.0095 1.1164 Ca 0.2750 1.0945 Ba 0.0000 NaN Fe 0.0000 1.2534 Mn 0.0004 1.2761 iteration : 3 Analysis no. 265 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5277 0.021896 0.5277 0.4316 Mg 0.8838 0.018004 0.8838 0.6837 Sr 0.3159 0.014264 0.3159 0.0678 P 0.4533 0.026265 0.4533 0.2752 K 0.1639 0.010272 0.1639 0.0788 Cl 1.0621 0.022739 1.0621 0.5633 Ca 30.0932 0.140579 30.0932 14.1188 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013733 0.0042 0.0014 Mn 0.0488 0.021162 0.0488 0.0167 C 14.5232 14.5232 22.7375 O 51.9240 51.9240 61.0250 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 266 x= -14147.0 y= 2968.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 25.8 4.4 3.6 7.10 0.0285 4.4 0.0290 Mg 95.7 2.3 2.5 38.02 0.0523 2.3 0.0111 Sr 35.9 2.6 14.3 2.51 0.0031 2.7 0.0399 P 25.0 4.5 2.4 10.62 0.0291 4.5 0.0396 K 23.8 4.6 5.1 4.66 0.0172 4.6 0.0187 Cl 65.7 2.3 2.2 29.85 0.0140 2.3 0.0226 Ca 3358.1 0.4 17.7 190.25 0.7408 0.5 0.0335 Ba 10.8 4.8 10.8 1.00 0.0000 4.8 0.0750 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0560 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0630 Elt. k-ratio Correc. Na 0.0014 2.3287 Mg 0.0038 1.6999 Sr 0.0019 1.3772 P 0.0046 1.1981 K 0.0015 1.0307 Cl 0.0078 1.1175 Ca 0.2688 1.0955 Ba 0.0000 1.5379 Fe 0.0002 1.2550 Mn 0.0003 1.2775 iteration : 3 Analysis no. 266 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3316 0.018212 0.3316 0.2688 Mg 0.6431 0.015419 0.6431 0.4931 Sr 0.2632 0.013671 0.2632 0.0560 P 0.5460 0.028344 0.5460 0.3285 K 0.1572 0.010137 0.1572 0.0749 Cl 0.8706 0.020700 0.8706 0.4576 Ca 29.4503 0.138631 29.4503 13.6926 Ba 0.0013 0.019202 0.0013 0.0002 Fe 0.0210 0.014249 0.0210 0.0070 Mn 0.0343 0.020542 0.0343 0.0116 C 14.9503 14.9503 23.1950 O 52.7311 52.7311 61.4147 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 267 x= -14146.0 y= 2972.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 34.7 3.8 3.6 9.57 0.0401 3.8 0.0290 Mg 103.6 2.2 2.5 41.16 0.0567 2.2 0.0111 Sr 31.3 2.8 14.3 2.19 0.0024 2.8 0.0400 P 23.3 4.6 2.4 9.92 0.0270 4.6 0.0397 K 26.7 4.3 5.1 5.24 0.0199 4.3 0.0188 Cl 72.9 2.1 2.2 33.16 0.0156 2.1 0.0227 Ca 3231.7 0.4 17.7 183.09 0.7130 0.5 0.0336 Ba 9.5 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 4.2 7.8 3.3 1.26 0.0005 7.8 0.0560 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0631 Elt. k-ratio Correc. Na 0.0020 2.3265 Mg 0.0041 1.7016 Sr 0.0015 1.3794 P 0.0042 1.1994 K 0.0018 1.0353 Cl 0.0087 1.1195 Ca 0.2588 1.0971 Ba 0.0000 NaN Fe 0.0002 1.2561 Mn 0.0003 1.2784 iteration : 3 Analysis no. 267 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4655 0.020818 0.4655 0.3743 Mg 0.6986 0.016061 0.6986 0.5314 Sr 0.2074 0.013049 0.2074 0.0438 P 0.5069 0.027504 0.5069 0.3026 K 0.1830 0.010697 0.1830 0.0865 Cl 0.9725 0.021838 0.9725 0.5072 Ca 28.3881 0.135432 28.3881 13.0958 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0285 0.014487 0.0285 0.0094 Mn 0.0416 0.020885 0.0416 0.0140 C 15.2892 15.2892 23.5357 O 53.2187 53.2187 61.4992 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 268 x= -14146.0 y= 2977.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 26.0 4.4 3.6 7.16 0.0288 4.4 0.0291 Mg 72.0 2.6 2.5 28.58 0.0389 2.7 0.0112 Sr 26.0 3.1 14.3 1.82 0.0017 3.1 0.0402 P 24.8 4.5 2.4 10.53 0.0288 4.5 0.0399 K 22.3 4.7 5.1 4.37 0.0159 4.7 0.0191 Cl 60.5 2.3 2.2 27.48 0.0129 2.3 0.0229 Ca 2664.3 0.4 17.7 150.95 0.5871 0.5 0.0338 Ba 8.0 5.6 10.8 0.74 0.0000 5.6 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0563 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0634 Elt. k-ratio Correc. Na 0.0014 2.3346 Mg 0.0028 1.7052 Sr 0.0010 1.3844 P 0.0045 1.2049 K 0.0014 1.0533 Cl 0.0072 1.1302 Ca 0.2131 1.1045 Ba 0.0000 NaN Fe 0.0000 1.2631 Mn 0.0002 1.2840 iteration : 2 Analysis no. 268 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3355 0.018327 0.3355 0.2583 Mg 0.4808 0.013442 0.4808 0.3500 Sr 0.1432 0.012305 0.1432 0.0289 P 0.5444 0.028408 0.5444 0.3110 K 0.1482 0.010098 0.1482 0.0671 Cl 0.8086 0.020119 0.8086 0.4036 Ca 23.5342 0.120407 23.5342 10.3899 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013840 0.0042 0.0013 Mn 0.0253 0.020244 0.0253 0.0082 C 17.3466 17.3466 25.5550 O 56.6289 56.6289 62.6267 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 269 x= -14145.0 y= 2981.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.6 3.5 3.6 11.20 0.0477 3.5 0.0290 Mg 116.7 2.1 2.5 46.32 0.0640 2.1 0.0111 Sr 35.2 2.7 14.3 2.46 0.0030 2.7 0.0401 P 22.7 4.7 2.4 9.66 0.0262 4.7 0.0398 K 23.9 4.6 5.1 4.69 0.0173 4.6 0.0189 Cl 82.3 2.0 2.2 37.42 0.0177 2.0 0.0227 Ca 3078.1 0.4 17.7 174.39 0.6789 0.5 0.0336 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.6 8.3 3.3 1.09 0.0002 8.3 0.0561 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0631 Elt. k-ratio Correc. Na 0.0024 2.3221 Mg 0.0046 1.7013 Sr 0.0018 1.3813 P 0.0041 1.2017 K 0.0015 1.0415 Cl 0.0098 1.1228 Ca 0.2464 1.0991 Ba 0.0000 NaN Fe 0.0001 1.2573 Mn 0.0003 1.2792 iteration : 3 Analysis no. 269 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5528 0.022341 0.5528 0.4406 Mg 0.7883 0.017034 0.7883 0.5943 Sr 0.2555 0.013619 0.2555 0.0534 P 0.4933 0.027230 0.4933 0.2918 K 0.1602 0.010274 0.1602 0.0751 Cl 1.1047 0.023240 1.1047 0.5709 Ca 27.0791 0.131434 27.0791 12.3789 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0101 0.013954 0.0101 0.0033 Mn 0.0362 0.020658 0.0362 0.0121 C 15.6972 15.6972 23.9453 O 53.8227 53.8227 61.6344 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 270 x= -14144.0 y= 2986.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 26.9 4.3 3.6 7.40 0.0300 4.3 0.0290 Mg 95.4 2.3 2.5 37.90 0.0521 2.3 0.0111 Sr 31.2 2.8 14.3 2.19 0.0024 2.8 0.0401 P 26.3 4.4 2.4 11.17 0.0308 4.4 0.0397 K 23.1 4.7 5.1 4.52 0.0166 4.7 0.0190 Cl 75.3 2.1 2.2 34.22 0.0161 2.1 0.0228 Ca 3037.6 0.4 17.7 172.09 0.6701 0.5 0.0337 Ba 9.3 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.6 8.3 3.3 1.09 0.0002 8.3 0.0562 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0632 Elt. k-ratio Correc. Na 0.0015 2.3279 Mg 0.0038 1.7006 Sr 0.0015 1.3803 P 0.0048 1.2009 K 0.0015 1.0420 Cl 0.0090 1.1234 Ca 0.2432 1.0998 Ba 0.0000 NaN Fe 0.0001 1.2583 Mn 0.0001 1.2802 iteration : 2 Analysis no. 270 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3482 0.018558 0.3482 0.2760 Mg 0.6417 0.015411 0.6417 0.4811 Sr 0.2070 0.013053 0.2070 0.0431 P 0.5791 0.029106 0.5791 0.3407 K 0.1531 0.010129 0.1531 0.0714 Cl 1.0083 0.022260 1.0083 0.5183 Ca 26.7449 0.130428 26.7449 12.1604 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0101 0.013970 0.0101 0.0033 Mn 0.0125 0.019602 0.0125 0.0041 C 15.9595 15.9595 24.2144 O 54.3356 54.3356 61.8872 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 271 x= -14143.0 y= 2990.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 42.4 3.4 3.6 11.68 0.0500 3.5 0.0289 Mg 132.6 1.9 2.5 52.66 0.0730 2.0 0.0111 Sr 40.6 2.5 14.3 2.84 0.0038 2.5 0.0401 P 27.9 4.2 2.4 11.87 0.0329 4.2 0.0398 K 25.7 4.4 5.1 5.04 0.0190 4.4 0.0189 Cl 83.0 2.0 2.2 37.71 0.0178 2.0 0.0227 Ca 3129.4 0.4 17.7 177.29 0.6905 0.5 0.0336 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0561 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0631 Elt. k-ratio Correc. Na 0.0025 2.3179 Mg 0.0053 1.6992 Sr 0.0023 1.3807 P 0.0052 1.2018 K 0.0017 1.0408 Cl 0.0099 1.1228 Ca 0.2506 1.0983 Ba 0.0000 NaN Fe 0.0001 1.2561 Mn 0.0004 1.2782 iteration : 3 Analysis no. 271 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5781 0.022750 0.5781 0.4637 Mg 0.8978 0.018150 0.8978 0.6811 Sr 0.3221 0.014356 0.3221 0.0678 P 0.6196 0.029966 0.6196 0.3688 K 0.1755 0.010586 0.1755 0.0828 Cl 1.1137 0.023334 1.1137 0.5793 Ca 27.5222 0.132802 27.5222 12.6624 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0076 0.013869 0.0076 0.0025 Mn 0.0453 0.021046 0.0453 0.0152 C 15.3594 15.3594 23.5806 O 53.3588 53.3588 61.4959 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 272 x= -14143.0 y= 2995.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.3 5.4 3.6 4.76 0.0176 5.4 0.0291 Mg 77.5 2.5 2.5 30.79 0.0421 2.6 0.0111 Sr 27.5 3.0 14.3 1.93 0.0019 3.0 0.0401 P 23.9 4.6 2.4 10.17 0.0277 4.6 0.0398 K 20.4 5.0 5.1 3.99 0.0141 5.0 0.0191 Cl 68.5 2.2 2.2 31.12 0.0146 2.2 0.0229 Ca 2759.5 0.4 17.7 156.34 0.6084 0.5 0.0338 Ba 7.8 5.7 10.8 0.72 0.0000 5.7 0.0000 Fe 3.0 9.2 3.3 0.89 0.0000 9.2 0.0000 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0634 Elt. k-ratio Correc. Na 0.0009 2.3346 Mg 0.0030 1.7024 Sr 0.0012 1.3827 P 0.0043 1.2034 K 0.0012 1.0504 Cl 0.0081 1.1282 Ca 0.2208 1.1034 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2832 iteration : 2 Analysis no. 272 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2048 0.015383 0.2048 0.1587 Mg 0.5186 0.013923 0.5186 0.3801 Sr 0.1620 0.012530 0.1620 0.0329 P 0.5233 0.027930 0.5233 0.3010 K 0.1311 0.009707 0.1311 0.0598 Cl 0.9184 0.021344 0.9184 0.4615 Ca 24.3636 0.123038 24.3636 10.8300 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0198 0.019987 0.0198 0.0064 C 17.0538 17.0538 25.2963 O 56.1044 56.1044 62.4732 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 273 x= -14142.0 y= 2999.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 39.5 3.6 3.6 10.88 0.0462 3.6 0.0289 Mg 144.3 1.9 2.5 57.30 0.0795 1.9 0.0111 Sr 40.0 2.5 14.3 2.80 0.0037 2.5 0.0401 P 30.5 4.0 2.4 12.98 0.0362 4.1 0.0398 K 25.9 4.4 5.1 5.08 0.0192 4.4 0.0189 Cl 78.1 2.1 2.2 35.51 0.0168 2.1 0.0227 Ca 3169.8 0.4 17.7 179.58 0.6993 0.5 0.0336 Ba 11.0 4.8 10.8 1.02 0.0002 4.8 0.0749 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0560 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0631 Elt. k-ratio Correc. Na 0.0023 2.3173 Mg 0.0058 1.6980 Sr 0.0023 1.3806 P 0.0057 1.2015 K 0.0017 1.0395 Cl 0.0093 1.1225 Ca 0.2538 1.0979 Ba 0.0000 1.5364 Fe 0.0001 1.2557 Mn 0.0002 1.2779 iteration : 3 Analysis no. 273 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5346 0.022002 0.5346 0.4300 Mg 0.9774 0.018921 0.9774 0.7437 Sr 0.3144 0.014271 0.3144 0.0664 P 0.6824 0.031235 0.6824 0.4075 K 0.1770 0.010605 0.1770 0.0837 Cl 1.0465 0.022646 1.0465 0.5459 Ca 27.8641 0.133841 27.8641 12.8575 Ba 0.0065 0.019281 0.0065 0.0009 Fe 0.0117 0.013989 0.0117 0.0039 Mn 0.0216 0.019985 0.0216 0.0073 C 15.1907 15.1907 23.3904 O 53.1732 53.1732 61.4629 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 274 x= -14141.0 y= 3003.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 36.6 3.7 3.6 10.08 0.0425 3.7 0.0289 Mg 131.6 1.9 2.5 52.25 0.0724 2.0 0.0111 Sr 43.7 2.4 14.3 3.06 0.0042 2.4 0.0400 P 30.5 4.0 2.4 12.98 0.0362 4.1 0.0397 K 23.1 4.7 5.1 4.52 0.0166 4.7 0.0188 Cl 102.4 1.8 2.2 46.52 0.0221 1.8 0.0227 Ca 3359.2 0.4 17.7 190.31 0.7415 0.5 0.0336 Ba 10.8 4.8 10.8 1.01 0.0000 4.8 0.0750 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0559 Mn 4.2 10.9 2.7 1.55 0.0015 10.9 0.0630 Elt. k-ratio Correc. Na 0.0021 2.3153 Mg 0.0052 1.6953 Sr 0.0026 1.3766 P 0.0057 1.1982 K 0.0015 1.0350 Cl 0.0123 1.1185 Ca 0.2691 1.0956 Ba 0.0000 1.5369 Fe 0.0000 1.2532 Mn 0.0004 1.2758 iteration : 3 Analysis no. 274 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4910 0.021225 0.4910 0.4012 Mg 0.8885 0.018036 0.8885 0.6868 Sr 0.3584 0.014712 0.3584 0.0769 P 0.6807 0.031156 0.6807 0.4129 K 0.1521 0.010061 0.1521 0.0731 Cl 1.3760 0.025786 1.3760 0.7292 Ca 29.4819 0.138765 29.4819 13.8204 Ba 0.0020 0.019214 0.0020 0.0003 Fe 0.0008 0.013634 0.0008 0.0003 Mn 0.0543 0.021400 0.0543 0.0186 C 14.5483 14.5483 22.7575 O 51.9661 51.9661 61.0229 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 275 x= -14140.0 y= 3008.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 36.4 3.7 3.6 10.04 0.0423 3.7 0.0290 Mg 97.7 2.3 2.5 38.81 0.0534 2.3 0.0111 Sr 30.6 2.9 14.3 2.15 0.0023 2.9 0.0401 P 35.0 3.8 2.4 14.87 0.0420 3.8 0.0397 K 27.3 4.3 5.1 5.34 0.0204 4.3 0.0190 Cl 81.1 2.0 2.2 36.87 0.0174 2.0 0.0228 Ca 3067.1 0.4 17.7 173.76 0.6767 0.5 0.0337 Ba 9.8 5.0 10.8 0.91 0.0000 5.1 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0561 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0632 Elt. k-ratio Correc. Na 0.0021 2.3231 Mg 0.0039 1.7005 Sr 0.0014 1.3796 P 0.0066 1.2002 K 0.0018 1.0425 Cl 0.0097 1.1236 Ca 0.2456 1.0994 Ba 0.0000 NaN Fe 0.0001 1.2573 Mn 0.0003 1.2792 iteration : 3 Analysis no. 275 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4904 0.021256 0.4904 0.3909 Mg 0.6576 0.015595 0.6576 0.4958 Sr 0.1999 0.012964 0.1999 0.0418 P 0.7895 0.033286 0.7895 0.4671 K 0.1890 0.010868 0.1890 0.0886 Cl 1.0892 0.023098 1.0892 0.5630 Ca 26.9986 0.131212 26.9986 12.3447 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0109 0.013985 0.0109 0.0036 Mn 0.0398 0.020826 0.0398 0.0133 C 15.6349 15.6349 23.8553 O 53.9000 53.9000 61.7358 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 276 x= -14140.0 y= 3012.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 46.1 3.3 3.6 12.71 0.0548 3.3 0.0289 Mg 131.3 1.9 2.5 52.13 0.0722 2.0 0.0111 Sr 38.0 2.6 14.3 2.66 0.0034 2.6 0.0401 P 34.7 3.8 2.4 14.77 0.0416 3.8 0.0397 K 27.4 4.3 5.1 5.36 0.0205 4.3 0.0188 Cl 68.3 2.2 2.2 31.03 0.0146 2.2 0.0227 Ca 3251.1 0.4 17.7 184.19 0.7176 0.5 0.0336 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0560 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0631 Elt. k-ratio Correc. Na 0.0027 2.3174 Mg 0.0052 1.6997 Sr 0.0021 1.3798 P 0.0065 1.2005 K 0.0018 1.0363 Cl 0.0081 1.1213 Ca 0.2604 1.0968 Ba 0.0000 NaN Fe 0.0000 1.2550 Mn 0.0002 1.2774 iteration : 3 Analysis no. 276 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6340 0.023672 0.6340 0.5128 Mg 0.8888 0.018064 0.8888 0.6800 Sr 0.2898 0.013997 0.2898 0.0615 P 0.7837 0.033182 0.7837 0.4705 K 0.1888 0.010821 0.1888 0.0898 Cl 0.9101 0.021184 0.9101 0.4773 Ca 28.5626 0.135980 28.5626 13.2512 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0050 0.013783 0.0050 0.0017 Mn 0.0216 0.019982 0.0216 0.0073 C 14.9013 14.9013 23.0691 O 52.8142 52.8142 61.3788 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 277 x= -14139.0 y= 3017.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 23.6 4.6 3.6 6.49 0.0257 4.6 0.0290 Mg 128.0 2.0 2.5 50.82 0.0704 2.0 0.0111 Sr 38.1 2.6 14.3 2.67 0.0034 2.6 0.0400 P 32.6 3.9 2.4 13.87 0.0389 3.9 0.0397 K 23.1 4.7 5.1 4.52 0.0166 4.7 0.0189 Cl 80.6 2.0 2.2 36.63 0.0173 2.0 0.0227 Ca 3152.9 0.4 17.7 178.62 0.6958 0.5 0.0336 Ba 11.4 4.7 10.8 1.06 0.0004 4.7 0.0750 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0561 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0631 Elt. k-ratio Correc. Na 0.0013 2.3222 Mg 0.0051 1.6962 Sr 0.0021 1.3791 P 0.0061 1.2004 K 0.0015 1.0398 Cl 0.0096 1.1224 Ca 0.2525 1.0982 Ba 0.0001 1.5366 Fe 0.0001 1.2562 Mn 0.0001 1.2784 iteration : 3 Analysis no. 277 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2980 0.017475 0.2980 0.2391 Mg 0.8642 0.017797 0.8642 0.6559 Sr 0.2909 0.014004 0.2909 0.0612 P 0.7328 0.032211 0.7328 0.4364 K 0.1528 0.010110 0.1528 0.0721 Cl 1.0808 0.023000 1.0808 0.5623 Ca 27.7298 0.133449 27.7298 12.7622 Ba 0.0177 0.019477 0.0177 0.0024 Fe 0.0151 0.014099 0.0151 0.0050 Mn 0.0179 0.019830 0.0179 0.0060 C 15.3537 15.3537 23.5797 O 53.4463 53.4463 61.6176 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 278 x= -14138.0 y= 3021.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 44.4 3.4 3.6 12.24 0.0526 3.4 0.0289 Mg 148.7 1.8 2.5 59.07 0.0820 1.9 0.0111 Sr 40.2 2.5 14.3 2.81 0.0037 2.5 0.0401 P 32.4 3.9 2.4 13.79 0.0387 3.9 0.0398 K 29.2 4.1 5.1 5.72 0.0222 4.2 0.0190 Cl 84.5 2.0 2.2 38.42 0.0182 2.0 0.0228 Ca 3065.1 0.4 17.7 173.65 0.6764 0.5 0.0337 Ba 10.6 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0561 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0631 Elt. k-ratio Correc. Na 0.0026 2.3144 Mg 0.0059 1.6980 Sr 0.0023 1.3816 P 0.0061 1.2026 K 0.0020 1.0438 Cl 0.0101 1.1246 Ca 0.2455 1.0993 Ba 0.0000 NaN Fe 0.0000 1.2565 Mn 0.0002 1.2784 iteration : 3 Analysis no. 278 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6079 0.023230 0.6079 0.4863 Mg 1.0086 0.019222 1.0086 0.7631 Sr 0.3172 0.014313 0.3172 0.0666 P 0.7294 0.032181 0.7294 0.4330 K 0.2055 0.011201 0.2055 0.0967 Cl 1.1375 0.023595 1.1375 0.5900 Ca 26.9845 0.131173 26.9845 12.3807 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0050 0.013801 0.0050 0.0017 Mn 0.0198 0.019918 0.0198 0.0066 C 15.4315 15.4315 23.6259 O 53.5530 53.5530 61.5495 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 279 x= -14137.0 y= 3026.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 22.1 4.8 3.6 6.08 0.0238 4.8 0.0290 Mg 92.7 2.3 2.5 36.83 0.0506 2.3 0.0111 Sr 31.4 2.8 14.3 2.20 0.0025 2.8 0.0401 P 31.7 4.0 2.4 13.49 0.0378 4.0 0.0398 K 22.1 4.8 5.1 4.33 0.0157 4.8 0.0190 Cl 84.4 2.0 2.2 38.34 0.0181 2.0 0.0228 Ca 2938.9 0.4 17.7 166.50 0.6484 0.5 0.0337 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0562 Mn 2.5 14.3 2.7 0.90 0.0000 14.3 0.0000 Elt. k-ratio Correc. Na 0.0012 2.3267 Mg 0.0037 1.6988 Sr 0.0015 1.3800 P 0.0059 1.2012 K 0.0014 1.0465 Cl 0.0101 1.1256 Ca 0.2353 1.1012 Ba 0.0000 NaN Fe 0.0000 1.2591 Mn 0.0000 NaN iteration : 2 Analysis no. 279 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2761 0.017018 0.2761 0.2177 Mg 0.6225 0.015181 0.6225 0.4641 Sr 0.2092 0.013079 0.2092 0.0433 P 0.7115 0.031812 0.7115 0.4163 K 0.1457 0.010002 0.1457 0.0675 Cl 1.1362 0.023593 1.1362 0.5807 Ca 25.9123 0.127879 25.9123 11.7157 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0025 0.013753 0.0025 0.0008 Mn 0.0000 0.000000 0.0000 0.0000 C 16.2116 16.2116 24.4590 O 54.7724 54.7724 62.0349 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 280 x= -14137.0 y= 3030.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 47.3 3.2 3.6 13.03 0.0563 3.3 0.0289 Mg 109.3 2.1 2.5 43.42 0.0599 2.2 0.0111 Sr 34.6 2.7 14.3 2.43 0.0029 2.7 0.0400 P 42.0 3.4 2.4 17.87 0.0510 3.5 0.0397 K 29.7 4.1 5.1 5.82 0.0227 4.1 0.0190 Cl 97.4 1.8 2.2 44.28 0.0210 1.9 0.0228 Ca 3119.2 0.4 17.7 176.71 0.6884 0.5 0.0337 Ba 9.2 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 2.8 13.3 2.7 1.03 0.0001 13.4 0.0631 Elt. k-ratio Correc. Na 0.0028 2.3142 Mg 0.0043 1.6984 Sr 0.0018 1.3784 P 0.0080 1.1995 K 0.0020 1.0431 Cl 0.0117 1.1236 Ca 0.2498 1.0989 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2780 iteration : 3 Analysis no. 280 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6504 0.023920 0.6504 0.5228 Mg 0.7371 0.016475 0.7371 0.5604 Sr 0.2487 0.013526 0.2487 0.0524 P 0.9600 0.036342 0.9600 0.5727 K 0.2101 0.011284 0.2101 0.0993 Cl 1.3144 0.025283 1.3144 0.6850 Ca 27.4556 0.132634 27.4556 12.6577 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0033 0.019145 0.0033 0.0011 C 15.2054 15.2054 23.3922 O 53.2150 53.2150 61.4564 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 281 x= -14136.0 y= 3035.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.7 5.3 3.6 4.88 0.0182 5.3 0.0291 Mg 84.5 2.4 2.5 33.55 0.0460 2.5 0.0111 Sr 32.9 2.8 14.3 2.31 0.0027 2.8 0.0400 P 33.1 3.9 2.4 14.09 0.0396 3.9 0.0397 K 23.4 4.6 5.1 4.58 0.0168 4.6 0.0190 Cl 73.9 2.1 2.2 33.58 0.0158 2.1 0.0228 Ca 3061.3 0.4 17.7 173.43 0.6755 0.5 0.0337 Ba 10.0 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0562 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0632 Elt. k-ratio Correc. Na 0.0009 2.3293 Mg 0.0033 1.6986 Sr 0.0017 1.3784 P 0.0062 1.1998 K 0.0015 1.0416 Cl 0.0088 1.1234 Ca 0.2452 1.0995 Ba 0.0000 NaN Fe 0.0000 1.2580 Mn 0.0001 1.2799 iteration : 2 Analysis no. 281 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2112 0.015517 0.2112 0.1677 Mg 0.5655 0.014495 0.5655 0.4249 Sr 0.2279 0.013286 0.2279 0.0475 P 0.7447 0.032433 0.7447 0.4390 K 0.1556 0.010182 0.1556 0.0727 Cl 0.9893 0.022062 0.9893 0.5096 Ca 26.9562 0.131094 26.9562 12.2815 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013715 0.0017 0.0005 Mn 0.0180 0.019857 0.0180 0.0060 C 15.8577 15.8577 24.1091 O 54.2724 54.2724 61.9415 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 282 x= -14135.0 y= 3039.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 21.0 4.9 3.6 5.79 0.0224 4.9 0.0291 Mg 77.5 2.5 2.5 30.77 0.0421 2.6 0.0111 Sr 29.5 2.9 14.3 2.07 0.0022 2.9 0.0401 P 32.0 3.9 2.4 13.62 0.0382 4.0 0.0398 K 27.6 4.3 5.1 5.40 0.0207 4.3 0.0190 Cl 74.7 2.1 2.2 33.96 0.0160 2.1 0.0228 Ca 2940.4 0.4 17.7 166.59 0.6488 0.5 0.0337 Ba 8.8 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0562 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0633 Elt. k-ratio Correc. Na 0.0011 2.3306 Mg 0.0030 1.7006 Sr 0.0013 1.3798 P 0.0060 1.2008 K 0.0018 1.0455 Cl 0.0089 1.1253 Ca 0.2355 1.1010 Ba 0.0000 NaN Fe 0.0002 1.2593 Mn 0.0003 1.2809 iteration : 2 Analysis no. 282 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2609 0.016693 0.2609 0.2054 Mg 0.5178 0.013909 0.5178 0.3858 Sr 0.1862 0.012806 0.1862 0.0385 P 0.7187 0.031950 0.7187 0.4202 K 0.1922 0.010954 0.1922 0.0890 Cl 1.0026 0.022225 1.0026 0.5121 Ca 25.9255 0.127922 25.9255 11.7121 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0210 0.014312 0.0210 0.0068 Mn 0.0326 0.020537 0.0326 0.0107 C 16.2574 16.2574 24.5079 O 54.8850 54.8850 62.1114 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 283 x= -14134.0 y= 3044.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 14.9 5.8 3.6 4.09 0.0145 5.8 0.0291 Mg 69.9 2.7 2.5 27.77 0.0378 2.7 0.0111 Sr 26.4 3.1 14.3 1.85 0.0017 3.1 0.0401 P 31.5 4.0 2.4 13.38 0.0375 4.0 0.0398 K 20.3 5.0 5.1 3.97 0.0140 5.0 0.0191 Cl 77.2 2.1 2.2 35.08 0.0166 2.1 0.0229 Ca 2745.1 0.4 17.7 155.52 0.6054 0.5 0.0338 Ba 9.1 5.2 10.8 0.85 0.0000 5.2 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0564 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0634 Elt. k-ratio Correc. Na 0.0007 2.3331 Mg 0.0027 1.7007 Sr 0.0011 1.3814 P 0.0059 1.2025 K 0.0012 1.0521 Cl 0.0092 1.1289 Ca 0.2197 1.1037 Ba 0.0000 NaN Fe 0.0000 1.2619 Mn 0.0000 1.2830 iteration : 2 Analysis no. 283 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1687 0.014462 0.1687 0.1308 Mg 0.4657 0.013227 0.4657 0.3416 Sr 0.1485 0.012355 0.1485 0.0302 P 0.7063 0.031732 0.7063 0.4065 K 0.1305 0.009707 0.1305 0.0595 Cl 1.0401 0.022653 1.0401 0.5230 Ca 24.2518 0.122711 24.2518 10.7869 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013836 0.0042 0.0013 Mn 0.0015 0.019135 0.0015 0.0005 C 17.0031 17.0031 25.2364 O 56.0795 56.0795 62.4833 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 284 x= -14134.0 y= 3048.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 46.7 3.3 3.6 12.88 0.0556 3.3 0.0288 Mg 160.8 1.8 2.5 63.84 0.0888 1.8 0.0111 Sr 38.4 2.6 14.3 2.69 0.0035 2.6 0.0401 P 40.3 3.5 2.4 17.13 0.0488 3.5 0.0398 K 31.1 4.0 5.1 6.10 0.0240 4.0 0.0191 Cl 107.1 1.8 2.2 48.69 0.0232 1.8 0.0228 Ca 2946.2 0.4 17.7 166.91 0.6500 0.5 0.0337 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0561 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0631 Elt. k-ratio Correc. Na 0.0028 2.3085 Mg 0.0064 1.6956 Sr 0.0021 1.3818 P 0.0076 1.2029 K 0.0021 1.0502 Cl 0.0129 1.1274 Ca 0.2359 1.1010 Ba 0.0000 NaN Fe 0.0001 1.2568 Mn 0.0002 1.2786 iteration : 3 Analysis no. 284 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6406 0.023729 0.6406 0.5104 Mg 1.0899 0.019965 1.0899 0.8213 Sr 0.2949 0.014071 0.2949 0.0616 P 0.9202 0.035701 0.9202 0.5441 K 0.2236 0.011588 0.2236 0.1047 Cl 1.4533 0.026590 1.4533 0.7508 Ca 25.9728 0.128064 25.9728 11.8687 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0084 0.013907 0.0084 0.0028 Mn 0.0307 0.020416 0.0307 0.0102 C 15.5792 15.5792 23.7561 O 53.7864 53.7864 61.5693 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 285 x= -14133.0 y= 3053.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.5 4.0 3.6 8.69 0.0360 4.0 0.0290 Mg 115.0 2.1 2.5 45.67 0.0631 2.1 0.0111 Sr 37.2 2.6 14.3 2.60 0.0033 2.6 0.0401 P 36.3 3.7 2.4 15.45 0.0437 3.7 0.0398 K 25.2 4.4 5.1 4.94 0.0186 4.5 0.0191 Cl 87.6 1.9 2.2 39.80 0.0188 2.0 0.0228 Ca 2952.3 0.4 17.7 167.26 0.6514 0.5 0.0337 Ba 10.2 4.9 10.8 0.95 0.0000 4.9 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0562 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0632 Elt. k-ratio Correc. Na 0.0018 2.3200 Mg 0.0046 1.6977 Sr 0.0020 1.3804 P 0.0069 1.2020 K 0.0016 1.0474 Cl 0.0105 1.1264 Ca 0.2364 1.1009 Ba 0.0000 NaN Fe 0.0000 1.2580 Mn 0.0001 1.2798 iteration : 2 Analysis no. 285 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4166 0.019877 0.4166 0.3300 Mg 0.7758 0.016888 0.7758 0.5812 Sr 0.2802 0.013898 0.2802 0.0582 P 0.8237 0.033953 0.8237 0.4842 K 0.1724 0.010569 0.1724 0.0803 Cl 1.1814 0.024048 1.1814 0.6068 Ca 26.0257 0.128228 26.0257 11.8236 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013793 0.0042 0.0014 Mn 0.0161 0.019772 0.0161 0.0053 C 15.9295 15.9295 24.1490 O 54.3743 54.3743 61.8800 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 286 x= -14132.0 y= 3057.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 35.2 3.8 3.6 9.69 0.0407 3.8 0.0289 Mg 138.4 1.9 2.5 54.97 0.0763 1.9 0.0111 Sr 41.6 2.5 14.3 2.91 0.0039 2.5 0.0401 P 39.7 3.5 2.4 16.90 0.0481 3.6 0.0398 K 27.4 4.3 5.1 5.36 0.0205 4.3 0.0190 Cl 95.4 1.9 2.2 43.35 0.0206 1.9 0.0228 Ca 3073.8 0.4 17.7 174.15 0.6783 0.5 0.0337 Ba 10.9 4.8 10.8 1.02 0.0001 4.8 0.0750 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0631 Elt. k-ratio Correc. Na 0.0020 2.3141 Mg 0.0055 1.6951 Sr 0.0024 1.3794 P 0.0075 1.2012 K 0.0018 1.0448 Cl 0.0114 1.1248 Ca 0.2462 1.0993 Ba 0.0000 1.5358 Fe 0.0000 NaN Mn 0.0002 1.2781 iteration : 3 Analysis no. 286 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4699 0.020841 0.4699 0.3767 Mg 0.9358 0.018505 0.9358 0.7095 Sr 0.3335 0.014471 0.3335 0.0701 P 0.9056 0.035417 0.9056 0.5388 K 0.1903 0.010911 0.1903 0.0897 Cl 1.2876 0.025047 1.2876 0.6693 Ca 27.0629 0.131420 27.0629 12.4429 Ba 0.0046 0.019248 0.0046 0.0006 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0216 0.019996 0.0216 0.0072 C 15.3429 15.3429 23.5398 O 53.4453 53.4453 61.5554 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 287 x= -14131.0 y= 3061.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 34.2 3.8 3.6 9.43 0.0395 3.8 0.0289 Mg 98.7 2.2 2.5 39.21 0.0540 2.3 0.0111 Sr 31.1 2.8 14.3 2.18 0.0024 2.8 0.0402 P 40.7 3.5 2.4 17.30 0.0493 3.5 0.0399 K 24.3 4.5 5.1 4.76 0.0177 4.5 0.0196 Cl 143.8 1.5 2.2 65.35 0.0313 1.5 0.0231 Ca 2290.5 0.5 17.7 129.77 0.5045 0.5 0.0340 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 2.9 9.3 3.3 0.87 0.0000 9.3 0.0000 Mn 2.3 14.9 2.7 0.83 0.0000 14.9 0.0000 Elt. k-ratio Correc. Na 0.0020 2.3143 Mg 0.0039 1.6969 Sr 0.0015 1.3841 P 0.0077 1.2063 K 0.0016 1.0745 Cl 0.0174 1.1385 Ca 0.1831 1.1102 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 287 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4559 0.020586 0.4559 0.3465 Mg 0.6633 0.015646 0.6633 0.4769 Sr 0.2068 0.013084 0.2068 0.0412 P 0.9327 0.035979 0.9327 0.5261 K 0.1689 0.010680 0.1689 0.0755 Cl 1.9804 0.031095 1.9804 0.9760 Ca 20.3280 0.110171 20.3280 8.8618 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.9367 17.9367 26.0926 O 57.3273 57.3273 62.6034 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 288 x= -14131.0 y= 3066.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 3.7 11.7 3.6 1.01 0.0000 11.7 0.0294 Mg 4.8 10.2 2.5 1.91 0.0013 10.2 0.0113 Sr 9.4 5.2 14.3 0.66 0.0000 5.2 0.0000 P 1.3 20.0 2.4 0.53 0.0000 20.0 0.0000 K 2.7 13.6 5.1 0.53 0.0000 13.6 0.0000 Cl 105.6 1.8 2.2 48.01 0.0228 1.8 0.0240 Ca 24.8 4.5 17.7 1.41 0.0016 4.5 0.0350 Ba 6.6 6.1 10.8 0.62 0.0000 6.1 0.0000 Fe 1.7 12.2 3.3 0.51 0.0000 12.2 0.0000 Mn 1.6 17.7 2.7 0.59 0.0000 17.7 0.0000 Elt. k-ratio Correc. Na 0.0000 2.3569 Mg 0.0001 1.7187 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0127 1.1861 Ca 0.0006 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 288 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0003 0.009159 0.0003 0.0002 Mg 0.0159 0.004224 0.0159 0.0097 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.5074 0.027785 1.5074 0.6295 Ca 0.0658 0.013404 0.0658 0.0243 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9400 26.9400 33.2056 O 71.4706 71.4706 66.1307 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 289 x= -14130.0 y= 3070.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 7.4 8.2 3.6 2.03 0.0048 8.3 0.0295 Mg 9.1 7.4 2.5 3.61 0.0037 7.4 0.0113 Sr 11.9 4.6 14.3 0.83 0.0000 4.6 0.0000 P 1.4 19.2 2.4 0.57 0.0000 19.2 0.0000 K 5.3 9.7 5.1 1.04 0.0002 9.7 0.0212 Cl 60.4 2.3 2.2 27.44 0.0128 2.4 0.0241 Ca 28.2 4.2 17.7 1.59 0.0023 4.2 0.0350 Ba 5.7 6.6 10.8 0.53 0.0000 6.6 0.0000 Fe 1.4 13.3 3.3 0.42 0.0000 13.4 0.0000 Mn 1.6 17.7 2.7 0.59 0.0000 17.7 0.0000 Elt. k-ratio Correc. Na 0.0002 2.3627 Mg 0.0003 1.7233 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1673 Cl 0.0071 1.1875 Ca 0.0008 1.1415 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 289 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0567 0.011279 0.0567 0.0364 Mg 0.0461 0.005338 0.0461 0.0280 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0019 0.006892 0.0019 0.0007 Cl 0.8487 0.021136 0.8487 0.3533 Ca 0.0966 0.013919 0.0966 0.0356 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0324 27.0324 33.2136 O 71.9177 71.9177 66.3326 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 290 x= -14129.0 y= 3075.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 4.8 10.2 3.6 1.31 0.0014 10.3 0.0294 Mg 7.4 8.2 2.5 2.92 0.0027 8.3 0.0113 Sr 11.8 4.6 14.3 0.82 0.0000 4.6 0.0000 P 0.9 23.5 2.4 0.38 0.0000 23.6 0.0000 K 3.9 11.4 5.1 0.75 0.0000 11.4 0.0000 Cl 106.0 1.8 2.2 48.16 0.0229 1.8 0.0240 Ca 18.7 5.2 17.7 1.06 0.0002 5.2 0.0350 Ba 6.5 6.2 10.8 0.60 0.0000 6.2 0.0000 Fe 1.8 11.9 3.3 0.53 0.0000 12.0 0.0000 Mn 1.9 16.4 2.7 0.68 0.0000 16.4 0.0000 Elt. k-ratio Correc. Na 0.0001 2.3564 Mg 0.0002 1.7187 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0127 1.1863 Ca 0.0001 1.1420 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 290 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0170 0.009825 0.0170 0.0110 Mg 0.0337 0.004906 0.0337 0.0205 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.5125 0.027833 1.5125 0.6315 Ca 0.0092 0.012395 0.0092 0.0034 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9463 26.9463 33.2066 O 71.4812 71.4812 66.1270 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 291 x= -14128.0 y= 3079.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 4.9 10.1 3.6 1.34 0.0016 10.2 0.0295 Mg 5.9 9.2 2.5 2.34 0.0019 9.2 0.0113 Sr 12.1 4.5 14.3 0.85 0.0000 4.6 0.0000 P 1.1 21.8 2.4 0.45 0.0000 21.8 0.0000 K 2.6 13.9 5.1 0.51 0.0000 13.9 0.0000 Cl 63.7 2.3 2.2 28.95 0.0136 2.3 0.0241 Ca 10.7 6.8 17.7 0.60 0.0000 6.9 0.0000 Ba 6.9 6.0 10.8 0.64 0.0000 6.0 0.0000 Fe 1.6 12.4 3.3 0.49 0.0000 12.4 0.0000 Mn 1.4 19.2 2.7 0.50 0.0000 19.2 0.0000 Elt. k-ratio Correc. Na 0.0001 2.3632 Mg 0.0001 1.7228 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0076 1.1876 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 291 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0186 0.009913 0.0186 0.0119 Mg 0.0237 0.004542 0.0237 0.0144 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.8975 0.021700 0.8975 0.3734 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0837 27.0837 33.2556 O 71.9764 71.9764 66.3448 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 292 x= -14128.0 y= 3084.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 5.8 9.3 3.6 1.60 0.0028 9.3 0.0294 Mg 8.5 7.7 2.5 3.38 0.0034 7.7 0.0113 Sr 12.4 4.5 14.3 0.87 0.0000 4.5 0.0000 P 1.1 21.8 2.4 0.45 0.0000 21.8 0.0000 K 3.7 11.6 5.1 0.73 0.0000 11.6 0.0000 Cl 99.6 1.8 2.2 45.26 0.0215 1.8 0.0240 Ca 20.2 5.0 17.7 1.14 0.0006 5.0 0.0350 Ba 6.1 6.4 10.8 0.57 0.0000 6.4 0.0000 Fe 1.6 12.5 3.3 0.48 0.0000 12.5 0.0000 Mn 1.6 17.7 2.7 0.59 0.0000 17.7 0.0000 Elt. k-ratio Correc. Na 0.0001 2.3570 Mg 0.0002 1.7194 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0120 1.1865 Ca 0.0002 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 292 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0330 0.010426 0.0330 0.0212 Mg 0.0418 0.005187 0.0418 0.0254 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.4198 0.026996 1.4198 0.5926 Ca 0.0230 0.012649 0.0230 0.0085 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9511 26.9511 33.2013 O 71.5313 71.5313 66.1509 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 293 x= -14127.0 y= 3088.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 4.6 10.5 3.6 1.25 0.0012 10.5 0.0295 Mg 8.0 7.9 2.5 3.16 0.0030 7.9 0.0113 Sr 12.3 4.5 14.3 0.86 0.0000 4.5 0.0000 P 1.1 21.8 2.4 0.45 0.0000 21.8 0.0000 K 3.7 11.7 5.1 0.72 0.0000 11.7 0.0000 Cl 62.9 2.3 2.2 28.59 0.0134 2.3 0.0241 Ca 16.2 5.5 17.7 0.92 0.0000 5.6 0.0000 Ba 6.7 6.1 10.8 0.62 0.0000 6.1 0.0000 Fe 2.2 10.7 3.3 0.66 0.0000 10.7 0.0000 Mn 2.0 16.0 2.7 0.72 0.0000 16.0 0.0000 Elt. k-ratio Correc. Na 0.0001 2.3632 Mg 0.0002 1.7227 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0075 1.1877 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 293 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0141 0.009736 0.0141 0.0090 Mg 0.0380 0.005065 0.0380 0.0231 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.8859 0.021567 0.8859 0.3685 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0814 27.0814 33.2520 O 71.9807 71.9807 66.3474 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 294 x= -14126.0 y= 3093.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 11.0 6.7 3.6 3.03 0.0095 6.8 0.0294 Mg 13.7 6.0 2.5 5.44 0.0063 6.0 0.0113 Sr 10.5 4.9 14.3 0.74 0.0000 4.9 0.0000 P 1.1 21.3 2.4 0.47 0.0000 21.3 0.0000 K 5.4 9.6 5.1 1.06 0.0003 9.6 0.0213 Cl 102.0 1.8 2.2 46.39 0.0220 1.8 0.0240 Ca 26.9 4.3 17.7 1.52 0.0020 4.3 0.0350 Ba 6.6 6.2 10.8 0.61 0.0000 6.2 0.0000 Fe 1.9 11.4 3.3 0.58 0.0000 11.4 0.0000 Mn 1.4 18.9 2.7 0.52 0.0000 18.9 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3547 Mg 0.0005 1.7198 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1683 Cl 0.0123 1.1864 Ca 0.0007 1.1418 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 294 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1118 0.012980 0.1118 0.0721 Mg 0.0781 0.006296 0.0781 0.0476 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0029 0.006931 0.0029 0.0011 Cl 1.4556 0.027320 1.4556 0.6082 Ca 0.0846 0.013724 0.0846 0.0313 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8736 26.8736 33.1428 O 71.3933 71.3933 66.0970 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 295 x= -14125.0 y= 3097.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 12.2 6.4 3.6 3.36 0.0111 6.4 0.0294 Mg 9.8 7.2 2.5 3.87 0.0041 7.2 0.0113 Sr 9.1 5.2 14.3 0.64 0.0000 5.2 0.0000 P 1.5 18.2 2.4 0.64 0.0000 18.3 0.0000 K 4.4 10.6 5.1 0.86 0.0000 10.7 0.0000 Cl 81.4 2.0 2.2 36.98 0.0175 2.0 0.0241 Ca 21.1 4.9 17.7 1.20 0.0008 4.9 0.0350 Ba 6.0 6.5 10.8 0.55 0.0000 6.5 0.0000 Fe 2.2 10.6 3.3 0.67 0.0000 10.6 0.0000 Mn 1.1 21.3 2.7 0.41 0.0000 21.3 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3581 Mg 0.0003 1.7222 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0097 1.1871 Ca 0.0003 1.1417 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 295 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1303 0.013525 0.1303 0.0837 Mg 0.0506 0.005482 0.0506 0.0308 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.1547 0.024447 1.1547 0.4814 Ca 0.0317 0.012804 0.0317 0.0117 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9640 26.9640 33.1829 O 71.6687 71.6687 66.2095 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 296 x= -14125.0 y= 3102.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 11.6 6.6 3.6 3.18 0.0102 6.6 0.0294 Mg 14.3 5.9 2.5 5.66 0.0066 5.9 0.0113 Sr 10.1 5.0 14.3 0.71 0.0000 5.0 0.0000 P 1.7 17.4 2.4 0.70 0.0000 17.4 0.0000 K 5.2 9.8 5.1 1.01 0.0000 9.9 0.0213 Cl 96.5 1.9 2.2 43.88 0.0208 1.9 0.0241 Ca 20.2 5.0 17.7 1.14 0.0006 5.0 0.0350 Ba 6.4 6.3 10.8 0.59 0.0000 6.3 0.0000 Fe 1.6 12.7 3.3 0.47 0.0000 12.7 0.0000 Mn 1.5 18.6 2.7 0.54 0.0000 18.6 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3554 Mg 0.0005 1.7204 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1685 Cl 0.0116 1.1867 Ca 0.0002 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 296 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1202 0.013228 0.1202 0.0774 Mg 0.0820 0.006405 0.0820 0.0499 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0005 0.006850 0.0005 0.0002 Cl 1.3758 0.026590 1.3758 0.5743 Ca 0.0235 0.012656 0.0235 0.0087 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9098 26.9098 33.1597 O 71.4883 71.4883 66.1297 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 297 x= -14124.0 y= 3106.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 10.5 6.9 3.6 2.88 0.0088 6.9 0.0294 Mg 11.1 6.7 2.5 4.39 0.0048 6.7 0.0113 Sr 10.9 4.8 14.3 0.76 0.0000 4.8 0.0000 P 1.7 17.4 2.4 0.70 0.0000 17.4 0.0000 K 4.6 10.5 5.1 0.89 0.0000 10.5 0.0000 Cl 99.2 1.8 2.2 45.10 0.0214 1.8 0.0241 Ca 14.9 5.8 17.7 0.84 0.0000 5.8 0.0000 Ba 6.7 6.1 10.8 0.63 0.0000 6.1 0.0000 Fe 1.8 11.9 3.3 0.54 0.0000 11.9 0.0000 Mn 1.7 17.1 2.7 0.63 0.0000 17.2 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3556 Mg 0.0003 1.7202 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0119 1.1867 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 297 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1036 0.012739 0.1036 0.0667 Mg 0.0596 0.005760 0.0596 0.0363 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.4147 0.026950 1.4147 0.5905 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9269 26.9269 33.1774 O 71.4952 71.4952 66.1291 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 298 x= -14123.0 y= 3111.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 13.8 6.0 3.6 3.80 0.0131 6.0 0.0295 Mg 15.9 5.6 2.5 6.29 0.0075 5.6 0.0113 Sr 12.3 4.5 14.3 0.86 0.0000 4.5 0.0000 P 1.4 18.9 2.4 0.60 0.0000 18.9 0.0000 K 4.4 10.7 5.1 0.85 0.0000 10.7 0.0000 Cl 49.2 2.6 2.2 22.36 0.0104 2.6 0.0241 Ca 18.0 5.3 17.7 1.02 0.0001 5.3 0.0350 Ba 6.8 6.1 10.8 0.63 0.0000 6.1 0.0000 Fe 1.9 11.6 3.3 0.56 0.0000 11.6 0.0000 Mn 1.3 19.6 2.7 0.48 0.0000 19.6 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3622 Mg 0.0005 1.7252 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0058 1.1882 Ca 0.0000 1.1415 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 298 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1548 0.014220 0.1548 0.0993 Mg 0.0935 0.006723 0.0935 0.0567 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.6861 0.019156 0.6861 0.2853 Ca 0.0028 0.012270 0.0028 0.0010 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0457 27.0457 33.1977 O 72.0172 72.0172 66.3600 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 299 x= -14122.0 y= 3115.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 7.6 8.1 3.6 2.10 0.0051 8.1 0.0294 Mg 12.0 6.4 2.5 4.77 0.0053 6.5 0.0112 Sr 11.7 4.6 14.3 0.82 0.0000 4.6 0.0000 P 1.4 18.9 2.4 0.60 0.0000 18.9 0.0000 K 3.5 11.9 5.1 0.69 0.0000 12.0 0.0000 Cl 129.1 1.6 2.2 58.70 0.0280 1.6 0.0240 Ca 13.7 6.0 17.7 0.78 0.0000 6.0 0.0000 Ba 6.9 6.0 10.8 0.64 0.0000 6.0 0.0000 Fe 2.0 11.2 3.3 0.60 0.0000 11.3 0.0000 Mn 2.0 16.0 2.7 0.72 0.0000 16.0 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3515 Mg 0.0004 1.7169 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0156 1.1857 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 299 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0602 0.011353 0.0602 0.0388 Mg 0.0661 0.005947 0.0661 0.0404 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.8496 0.030696 1.8496 0.7739 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8480 26.8480 33.1580 O 71.1761 71.1761 65.9889 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 300 x= -14122.0 y= 3120.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 10.5 6.9 3.6 2.88 0.0088 6.9 0.0294 Mg 8.7 7.6 2.5 3.44 0.0034 7.6 0.0113 Sr 10.5 4.9 14.3 0.74 0.0000 4.9 0.0000 P 1.5 18.6 2.4 0.62 0.0000 18.6 0.0000 K 5.1 9.9 5.1 1.00 0.0000 9.9 NaN Cl 78.9 2.1 2.2 35.87 0.0169 2.1 0.0241 Ca 14.5 5.9 17.7 0.82 0.0000 5.9 0.0000 Ba 6.1 6.4 10.8 0.57 0.0000 6.4 0.0000 Fe 1.9 11.5 3.3 0.58 0.0000 11.5 0.0000 Mn 1.3 19.6 2.7 0.48 0.0000 19.6 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3591 Mg 0.0002 1.7222 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0094 1.1872 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 300 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1037 0.012758 0.1037 0.0666 Mg 0.0429 0.005230 0.0429 0.0261 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.1193 0.024088 1.1193 0.4664 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9969 26.9969 33.2049 O 71.7373 71.7373 66.2360 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 301 x= -14121.0 y= 3124.0 z= -278. carb2 trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 13.9 6.0 3.6 3.83 0.0133 6.0 0.0293 Mg 7.2 8.4 2.5 2.84 0.0026 8.4 0.0112 Sr 10.1 5.0 14.3 0.71 0.0000 5.0 0.0000 P 2.0 16.0 2.4 0.83 0.0000 16.0 0.0000 K 4.3 10.8 5.1 0.83 0.0000 10.9 0.0000 Cl 155.3 1.5 2.2 70.59 0.0338 1.5 0.0240 Ca 13.5 6.1 17.7 0.76 0.0000 6.1 0.0000 Ba 6.2 6.4 10.8 0.57 0.0000 6.4 0.0000 Fe 2.1 11.0 3.3 0.63 0.0000 11.0 0.0000 Mn 2.2 15.1 2.7 0.81 0.0000 15.1 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3463 Mg 0.0002 1.7159 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0188 1.1850 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 301 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1553 0.014165 0.1553 0.1004 Mg 0.0323 0.004848 0.0323 0.0198 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 2.2293 0.033641 2.2293 0.9350 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7481 26.7481 33.1141 O 70.8350 70.8350 65.8307 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 302 x= -15727.0 y= 2656.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 26.8 4.3 3.6 7.39 0.0299 4.3 0.0292 Mg 62.8 2.8 2.5 24.94 0.0338 2.8 0.0112 Sr 14.9 4.1 14.3 1.04 0.0001 4.1 0.0410 P 21.2 4.9 2.4 9.00 0.0242 4.9 0.0408 K 13.5 6.1 5.1 2.65 0.0078 6.1 0.0210 Cl 111.8 1.7 2.2 50.82 0.0242 1.7 0.0239 Ca 295.4 1.3 17.7 16.73 0.0617 1.3 0.0349 Ba 7.4 5.8 10.8 0.69 0.0000 5.8 0.0000 Fe 10.0 5.0 3.3 3.02 0.0038 5.0 0.0576 Mn 1.9 16.2 2.7 0.70 0.0000 16.2 0.0000 Elt. k-ratio Correc. Na 0.0015 2.3413 Mg 0.0024 1.7163 Sr 0.0001 1.4106 P 0.0038 1.2321 K 0.0007 1.1548 Cl 0.0135 1.1809 Ca 0.0224 1.1372 Ba 0.0000 NaN Fe 0.0018 1.2886 Mn 0.0000 NaN iteration : 2 Analysis no. 302 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3496 0.018659 0.3496 0.2311 Mg 0.4205 0.012670 0.4205 0.2629 Sr 0.0075 0.010676 0.0075 0.0013 P 0.4676 0.027051 0.4676 0.2294 K 0.0794 0.009123 0.0794 0.0309 Cl 1.5905 0.028456 1.5905 0.6817 Ca 2.5445 0.036869 2.5445 0.9647 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.2292 0.019853 0.2292 0.0624 Mn 0.0000 0.000000 0.0000 0.0000 C 25.2629 25.2629 31.9603 O 69.0483 69.0483 65.5755 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 303 x= -15727.0 y= 2661.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 34.2 3.8 3.6 9.43 0.0395 3.8 0.0290 Mg 171.5 1.7 2.5 68.09 0.0948 1.7 0.0111 Sr 40.0 2.5 14.3 2.80 0.0037 2.5 0.0398 P 18.6 5.2 2.4 7.89 0.0209 5.2 0.0394 K 8.5 7.7 5.1 1.66 0.0031 7.7 0.0180 Cl 9.7 5.8 2.2 4.42 0.0017 5.9 0.0222 Ca 4572.4 0.3 17.7 259.04 1.0111 0.4 0.0331 Ba 11.4 4.7 10.8 1.06 0.0004 4.7 0.0753 Fe 4.7 7.3 3.3 1.42 0.0008 7.3 0.0555 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0627 Elt. k-ratio Correc. Na 0.0020 2.3250 Mg 0.0069 1.6974 Sr 0.0023 1.3715 P 0.0033 1.1900 K 0.0003 0.9886 Cl 0.0009 1.0970 Ca 0.3670 1.0797 Ba 0.0001 1.5429 Fe 0.0004 1.2434 Mn 0.0003 1.2684 iteration : 3 Analysis no. 303 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4580 0.020682 0.4580 0.4048 Mg 1.1652 0.020656 1.1652 0.9741 Sr 0.3131 0.014191 0.3131 0.0726 P 0.3891 0.024625 0.3891 0.2553 K 0.0271 0.006664 0.0271 0.0141 Cl 0.1016 0.008505 0.1016 0.0582 Ca 39.6189 0.168533 39.6189 20.0849 Ba 0.0158 0.019530 0.0158 0.0023 Fe 0.0466 0.014872 0.0466 0.0169 Mn 0.0341 0.020419 0.0341 0.0126 C 11.0585 11.0585 18.7074 O 46.7720 46.7720 59.3968 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 304 x= -15726.0 y= 2666.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 36.7 3.7 3.6 10.12 0.0427 3.7 0.0289 Mg 245.2 1.4 2.5 97.37 0.1362 1.5 0.0111 Sr 43.5 2.4 14.3 3.05 0.0042 2.4 0.0399 P 27.9 4.2 2.4 11.85 0.0328 4.2 0.0395 K 8.0 7.9 5.1 1.56 0.0026 7.9 0.0181 Cl 17.3 4.4 2.2 7.86 0.0033 4.4 0.0223 Ca 4403.4 0.3 17.7 249.47 0.9736 0.4 0.0331 Ba 13.3 4.3 10.8 1.24 0.0016 4.3 0.0752 Fe 4.1 7.8 3.3 1.23 0.0004 7.8 0.0555 Mn 4.9 10.1 2.7 1.79 0.0021 10.2 0.0627 Elt. k-ratio Correc. Na 0.0021 2.3146 Mg 0.0099 1.6931 Sr 0.0026 1.3752 P 0.0051 1.1935 K 0.0002 0.9968 Cl 0.0019 1.1022 Ca 0.3533 1.0814 Ba 0.0004 1.5410 Fe 0.0002 1.2436 Mn 0.0006 1.2684 iteration : 3 Analysis no. 304 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4933 0.021268 0.4933 0.4336 Mg 1.6693 0.024750 1.6693 1.3879 Sr 0.3564 0.014683 0.3564 0.0822 P 0.6144 0.029750 0.6144 0.4008 K 0.0233 0.006594 0.0233 0.0120 Cl 0.2045 0.010928 0.2045 0.1166 Ca 38.2120 0.164467 38.2120 19.2653 Ba 0.0669 0.020349 0.0669 0.0098 Fe 0.0258 0.014282 0.0258 0.0093 Mn 0.0775 0.022263 0.0775 0.0285 C 11.1557 11.1557 18.7681 O 47.1009 47.1009 59.4858 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 305 x= -15726.0 y= 2671.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 38.7 3.6 3.6 10.67 0.0453 3.6 0.0288 Mg 285.6 1.3 2.5 113.42 0.1589 1.4 0.0111 Sr 43.2 2.4 14.3 3.03 0.0042 2.4 0.0400 P 38.2 3.6 2.4 16.26 0.0462 3.6 0.0396 K 9.6 7.2 5.1 1.88 0.0042 7.2 0.0182 Cl 16.7 4.5 2.2 7.61 0.0032 4.5 0.0224 Ca 4359.7 0.3 17.7 247.00 0.9639 0.4 0.0332 Ba 12.9 4.4 10.8 1.20 0.0013 4.4 0.0752 Fe 4.2 7.8 3.3 1.26 0.0005 7.8 0.0555 Mn 4.4 10.6 2.7 1.62 0.0017 10.7 0.0627 Elt. k-ratio Correc. Na 0.0023 2.3082 Mg 0.0115 1.6901 Sr 0.0026 1.3765 P 0.0072 1.1946 K 0.0004 0.9998 Cl 0.0018 1.1046 Ca 0.3498 1.0821 Ba 0.0004 1.5406 Fe 0.0002 1.2435 Mn 0.0005 1.2682 iteration : 3 Analysis no. 305 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5216 0.021735 0.5216 0.4587 Mg 1.9440 0.026745 1.9440 1.6171 Sr 0.3533 0.014662 0.3533 0.0815 P 0.8646 0.034584 0.8646 0.5643 K 0.0368 0.007020 0.0368 0.0191 Cl 0.1973 0.010791 0.1973 0.1125 Ca 37.8543 0.163439 37.8543 19.0947 Ba 0.0564 0.020173 0.0564 0.0083 Fe 0.0283 0.014352 0.0283 0.0102 Mn 0.0612 0.021587 0.0612 0.0225 C 11.0072 11.0072 18.5277 O 47.0748 47.0748 59.4833 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 306 x= -15726.0 y= 2676.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 39.1 3.6 3.6 10.78 0.0458 3.6 0.0288 Mg 297.9 1.3 2.5 118.30 0.1658 1.3 0.0111 Sr 41.4 2.5 14.3 2.90 0.0039 2.5 0.0400 P 34.6 3.8 2.4 14.70 0.0415 3.8 0.0396 K 8.9 7.5 5.1 1.75 0.0035 7.5 0.0182 Cl 19.7 4.1 2.2 8.96 0.0039 4.1 0.0224 Ca 4394.5 0.3 17.7 248.97 0.9717 0.4 0.0332 Ba 13.6 4.3 10.8 1.26 0.0017 4.3 0.0752 Fe 4.7 7.3 3.3 1.41 0.0008 7.3 0.0555 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0626 Elt. k-ratio Correc. Na 0.0023 2.3077 Mg 0.0120 1.6900 Sr 0.0024 1.3770 P 0.0065 1.1945 K 0.0003 0.9987 Cl 0.0022 1.1037 Ca 0.3526 1.0816 Ba 0.0005 1.5407 Fe 0.0004 1.2432 Mn 0.0004 1.2679 iteration : 3 Analysis no. 306 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5275 0.021834 0.5275 0.4651 Mg 2.0282 0.027337 2.0282 1.6916 Sr 0.3306 0.014423 0.3306 0.0765 P 0.7765 0.032961 0.7765 0.5082 K 0.0311 0.006843 0.0311 0.0161 Cl 0.2374 0.011598 0.2374 0.1357 Ca 38.1408 0.164265 38.1408 19.2905 Ba 0.0741 0.020461 0.0741 0.0109 Fe 0.0449 0.014823 0.0449 0.0163 Mn 0.0468 0.020966 0.0468 0.0173 C 10.9073 10.9073 18.4085 O 46.8549 46.8549 59.3633 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 307 x= -15725.0 y= 2681.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 40.5 3.5 3.6 11.15 0.0475 3.5 0.0288 Mg 298.9 1.3 2.5 118.68 0.1663 1.3 0.0111 Sr 41.6 2.4 14.3 2.91 0.0039 2.5 0.0401 P 34.9 3.8 2.4 14.85 0.0419 3.8 0.0396 K 9.6 7.2 5.1 1.88 0.0042 7.2 0.0183 Cl 19.3 4.1 2.2 8.79 0.0038 4.2 0.0224 Ca 4207.0 0.3 17.7 238.35 0.9300 0.4 0.0332 Ba 12.5 4.5 10.8 1.16 0.0011 4.5 0.0752 Fe 4.0 7.9 3.3 1.20 0.0004 8.0 0.0556 Mn 3.9 11.3 2.7 1.44 0.0012 11.3 0.0627 Elt. k-ratio Correc. Na 0.0024 2.3073 Mg 0.0120 1.6906 Sr 0.0024 1.3789 P 0.0066 1.1967 K 0.0004 1.0044 Cl 0.0021 1.1071 Ca 0.3375 1.0840 Ba 0.0003 1.5401 Fe 0.0002 1.2452 Mn 0.0003 1.2695 iteration : 3 Analysis no. 307 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5475 0.022177 0.5475 0.4758 Mg 2.0354 0.027392 2.0354 1.6731 Sr 0.3341 0.014476 0.3341 0.0762 P 0.7863 0.033179 0.7863 0.5072 K 0.0370 0.007052 0.0370 0.0189 Cl 0.2331 0.011536 0.2331 0.1314 Ca 36.5893 0.159774 36.5893 18.2386 Ba 0.0452 0.019985 0.0452 0.0066 Fe 0.0216 0.014177 0.0216 0.0077 Mn 0.0432 0.020835 0.0432 0.0157 C 11.4990 11.4990 19.1271 O 47.8282 47.8282 59.7217 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 308 x= -15725.0 y= 2686.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 31.2 4.0 3.6 8.59 0.0355 4.0 0.0288 Mg 238.5 1.4 2.5 94.70 0.1324 1.5 0.0111 Sr 46.5 2.3 14.3 3.25 0.0046 2.3 0.0399 P 59.8 2.9 2.4 25.45 0.0740 2.9 0.0395 K 12.1 6.4 5.1 2.37 0.0065 6.4 0.0183 Cl 35.2 3.1 2.2 16.00 0.0073 3.1 0.0224 Ca 4290.4 0.3 17.7 243.07 0.9485 0.4 0.0332 Ba 13.9 4.2 10.8 1.29 0.0019 4.3 0.0752 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0555 Mn 4.8 10.2 2.7 1.77 0.0021 10.2 0.0626 Elt. k-ratio Correc. Na 0.0018 2.3067 Mg 0.0096 1.6871 Sr 0.0029 1.3721 P 0.0116 1.1923 K 0.0006 1.0052 Cl 0.0041 1.1071 Ca 0.3442 1.0831 Ba 0.0005 1.5398 Fe 0.0001 1.2432 Mn 0.0006 1.2678 iteration : 3 Analysis no. 308 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4091 0.019666 0.4091 0.3596 Mg 1.6174 0.024311 1.6174 1.3448 Sr 0.3914 0.015024 0.3914 0.0903 P 1.3829 0.042937 1.3829 0.9023 K 0.0576 0.007635 0.0576 0.0298 Cl 0.4491 0.015217 0.4491 0.2560 Ca 37.2851 0.161799 37.2851 18.7997 Ba 0.0820 0.020575 0.0820 0.0121 Fe 0.0150 0.013958 0.0150 0.0054 Mn 0.0757 0.022180 0.0757 0.0278 C 11.0091 11.0091 18.5232 O 47.2256 47.2256 59.6490 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 309 x= -15725.0 y= 2690.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 45.5 3.3 3.6 12.53 0.0540 3.3 0.0288 Mg 240.4 1.4 2.5 95.46 0.1335 1.5 0.0111 Sr 44.6 2.4 14.3 3.13 0.0044 2.4 0.0399 P 46.1 3.3 2.4 19.62 0.0563 3.3 0.0395 K 14.0 6.0 5.1 2.75 0.0082 6.0 0.0183 Cl 31.3 3.3 2.2 14.22 0.0064 3.3 0.0224 Ca 4246.0 0.3 17.7 240.55 0.9387 0.4 0.0332 Ba 12.8 4.4 10.8 1.19 0.0012 4.4 0.0752 Fe 4.1 7.8 3.3 1.25 0.0005 7.8 0.0556 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0627 Elt. k-ratio Correc. Na 0.0027 2.3071 Mg 0.0097 1.6915 Sr 0.0027 1.3747 P 0.0088 1.1940 K 0.0007 1.0049 Cl 0.0036 1.1067 Ca 0.3407 1.0836 Ba 0.0003 1.5399 Fe 0.0002 1.2441 Mn 0.0004 1.2686 iteration : 3 Analysis no. 309 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6218 0.023418 0.6218 0.5433 Mg 1.6346 0.024474 1.6346 1.3510 Sr 0.3699 0.014822 0.3699 0.0848 P 1.0546 0.037848 1.0546 0.6839 K 0.0732 0.008045 0.0732 0.0376 Cl 0.3954 0.014386 0.3954 0.2240 Ca 36.9163 0.160729 36.9163 18.5019 Ba 0.0531 0.020112 0.0531 0.0078 Fe 0.0275 0.014336 0.0275 0.0099 Mn 0.0486 0.021055 0.0486 0.0178 C 11.2963 11.2963 18.8923 O 47.5087 47.5087 59.6458 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 310 x= -15724.0 y= 2695.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 25.3 4.4 3.6 6.98 0.0280 4.5 0.0290 Mg 150.6 1.8 2.5 59.80 0.0831 1.8 0.0111 Sr 39.6 2.5 14.3 2.77 0.0036 2.5 0.0398 P 48.4 3.2 2.4 20.58 0.0592 3.2 0.0395 K 17.0 5.4 5.1 3.33 0.0110 5.4 0.0184 Cl 38.1 3.0 2.2 17.31 0.0079 3.0 0.0225 Ca 4071.0 0.4 17.7 230.64 0.8998 0.4 0.0333 Ba 11.3 4.7 10.8 1.05 0.0003 4.7 0.0752 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0557 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0628 Elt. k-ratio Correc. Na 0.0014 2.3196 Mg 0.0060 1.6928 Sr 0.0022 1.3713 P 0.0093 1.1919 K 0.0010 1.0091 Cl 0.0044 1.1081 Ca 0.3266 1.0863 Ba 0.0001 1.5403 Fe 0.0001 1.2470 Mn 0.0003 1.2711 iteration : 3 Analysis no. 310 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3239 0.018020 0.3239 0.2779 Mg 1.0184 0.019287 1.0184 0.8263 Sr 0.3073 0.014127 0.3073 0.0692 P 1.1069 0.038668 1.1069 0.7047 K 0.0983 0.008691 0.0983 0.0496 Cl 0.4885 0.015806 0.4885 0.2717 Ca 35.4755 0.156557 35.4755 17.4545 Ba 0.0131 0.019454 0.0131 0.0019 Fe 0.0125 0.013926 0.0125 0.0044 Mn 0.0396 0.020702 0.0396 0.0142 C 12.2151 12.2151 20.0552 O 48.9007 48.9007 60.2704 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 311 x= -15724.0 y= 2700.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 29.5 4.1 3.6 8.13 0.0334 4.1 0.0290 Mg 144.4 1.9 2.5 57.34 0.0796 1.9 0.0111 Sr 32.6 2.8 14.3 2.28 0.0026 2.8 0.0399 P 49.2 3.2 2.4 20.92 0.0603 3.2 0.0396 K 15.9 5.6 5.1 3.12 0.0100 5.6 0.0185 Cl 32.3 3.2 2.2 14.70 0.0067 3.2 0.0225 Ca 3820.2 0.4 17.7 216.43 0.8442 0.5 0.0334 Ba 10.5 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0558 Mn 4.4 10.6 2.7 1.62 0.0017 10.7 0.0629 Elt. k-ratio Correc. Na 0.0017 2.3220 Mg 0.0058 1.6960 Sr 0.0016 1.3745 P 0.0094 1.1943 K 0.0009 1.0159 Cl 0.0037 1.1124 Ca 0.3064 1.0894 Ba 0.0000 NaN Fe 0.0001 1.2499 Mn 0.0005 1.2734 iteration : 3 Analysis no. 311 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3871 0.019316 0.3871 0.3255 Mg 0.9775 0.018916 0.9775 0.7775 Sr 0.2233 0.013205 0.2233 0.0493 P 1.1284 0.039059 1.1284 0.7042 K 0.0899 0.008529 0.0899 0.0444 Cl 0.4120 0.014690 0.4120 0.2247 Ca 33.3754 0.150388 33.3754 16.0971 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0109 0.013909 0.0109 0.0038 Mn 0.0615 0.021676 0.0615 0.0216 C 13.0418 13.0418 20.9898 O 50.2922 50.2922 60.7621 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 312 x= -15724.0 y= 2705.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 14.2 5.9 3.6 3.92 0.0136 5.9 0.0290 Mg 152.5 1.8 2.5 60.58 0.0842 1.8 0.0111 Sr 32.0 2.8 14.3 2.24 0.0025 2.8 0.0400 P 47.2 3.3 2.4 20.09 0.0578 3.3 0.0396 K 12.7 6.3 5.1 2.49 0.0070 6.3 0.0186 Cl 40.7 2.9 2.2 18.51 0.0085 2.9 0.0226 Ca 3658.0 0.4 17.7 207.24 0.8082 0.5 0.0335 Ba 11.3 4.7 10.8 1.05 0.0003 4.7 0.0751 Fe 4.3 7.6 3.3 1.30 0.0006 7.7 0.0559 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0630 Elt. k-ratio Correc. Na 0.0007 2.3245 Mg 0.0061 1.6935 Sr 0.0016 1.3755 P 0.0091 1.1956 K 0.0006 1.0213 Cl 0.0047 1.1150 Ca 0.2933 1.0916 Ba 0.0001 1.5391 Fe 0.0003 1.2517 Mn 0.0001 1.2749 iteration : 3 Analysis no. 312 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1583 0.014153 0.1583 0.1315 Mg 1.0323 0.019421 1.0323 0.8107 Sr 0.2159 0.013126 0.2159 0.0470 P 1.0826 0.038337 1.0826 0.6672 K 0.0636 0.007892 0.0636 0.0310 Cl 0.5277 0.016419 0.5277 0.2841 Ca 32.0146 0.146362 32.0146 15.2474 Ba 0.0144 0.019459 0.0144 0.0020 Fe 0.0326 0.014568 0.0326 0.0112 Mn 0.0179 0.019784 0.0179 0.0062 C 13.6394 13.6394 21.6767 O 51.2008 51.2008 61.0850 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 313 x= -15723.0 y= 2710.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 16.0 5.6 3.6 4.41 0.0160 5.6 0.0290 Mg 166.3 1.7 2.5 66.04 0.0919 1.8 0.0111 Sr 35.4 2.7 14.3 2.48 0.0030 2.7 0.0399 P 58.2 2.9 2.4 24.75 0.0719 2.9 0.0395 K 15.9 5.6 5.1 3.12 0.0100 5.6 0.0185 Cl 34.6 3.1 2.2 15.72 0.0071 3.1 0.0226 Ca 3844.8 0.4 17.7 217.83 0.8496 0.4 0.0334 Ba 10.2 5.0 10.8 0.95 0.0000 5.0 0.0000 Fe 3.6 8.3 3.3 1.09 0.0002 8.3 0.0558 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0629 Elt. k-ratio Correc. Na 0.0008 2.3198 Mg 0.0067 1.6908 Sr 0.0019 1.3733 P 0.0113 1.1938 K 0.0009 1.0166 Cl 0.0040 1.1131 Ca 0.3083 1.0893 Ba 0.0000 NaN Fe 0.0001 1.2493 Mn 0.0003 1.2730 iteration : 3 Analysis no. 313 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1849 0.014824 0.1849 0.1561 Mg 1.1252 0.020258 1.1252 0.8984 Sr 0.2569 0.013582 0.2569 0.0569 P 1.3449 0.042402 1.3449 0.8426 K 0.0899 0.008535 0.0899 0.0446 Cl 0.4429 0.015169 0.4429 0.2424 Ca 33.5875 0.151022 33.5875 16.2624 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0100 0.013877 0.0100 0.0035 Mn 0.0379 0.020653 0.0379 0.0134 C 12.8242 12.8242 20.7198 O 50.0957 50.0957 60.7599 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 314 x= -15723.0 y= 2715.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 12.5 6.3 3.6 3.43 0.0114 6.3 0.0291 Mg 99.0 2.2 2.5 39.33 0.0542 2.3 0.0111 Sr 23.5 3.3 14.3 1.65 0.0013 3.3 0.0401 P 55.6 3.0 2.4 23.66 0.0686 3.0 0.0397 K 12.3 6.4 5.1 2.40 0.0066 6.4 0.0189 Cl 35.1 3.1 2.2 15.96 0.0073 3.1 0.0228 Ca 3091.5 0.4 17.7 175.14 0.6824 0.5 0.0337 Ba 5.7 6.6 10.8 0.53 0.0000 6.6 0.0000 Fe 3.1 9.0 3.3 0.93 0.0000 9.0 0.0000 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0633 Elt. k-ratio Correc. Na 0.0006 2.3311 Mg 0.0039 1.6980 Sr 0.0008 1.3790 P 0.0108 1.1996 K 0.0006 1.0392 Cl 0.0040 1.1255 Ca 0.2477 1.0990 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2802 iteration : 2 Analysis no. 314 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1325 0.013477 0.1325 0.1054 Mg 0.6659 0.015682 0.6659 0.5008 Sr 0.1128 0.011886 0.1128 0.0235 P 1.2897 0.041679 1.2897 0.7610 K 0.0608 0.007929 0.0608 0.0284 Cl 0.4552 0.015450 0.4552 0.2347 Ca 27.2180 0.131904 27.2180 12.4112 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0125 0.019614 0.0125 0.0042 C 15.5840 15.5840 23.7130 O 54.4685 54.4685 62.2178 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 315 x= -15723.0 y= 2720.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 29.8 4.1 3.6 8.20 0.0337 4.1 0.0289 Mg 188.1 1.6 2.5 74.71 0.1042 1.7 0.0111 Sr 40.1 2.5 14.3 2.81 0.0037 2.5 0.0399 P 69.9 2.7 2.4 29.75 0.0870 2.7 0.0396 K 15.9 5.6 5.1 3.12 0.0100 5.6 0.0186 Cl 36.0 3.0 2.2 16.38 0.0075 3.0 0.0226 Ca 3829.0 0.4 17.7 216.93 0.8462 0.4 0.0334 Ba 12.4 4.5 10.8 1.15 0.0010 4.5 0.0751 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0558 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0628 Elt. k-ratio Correc. Na 0.0017 2.3111 Mg 0.0075 1.6901 Sr 0.0023 1.3739 P 0.0136 1.1949 K 0.0009 1.0192 Cl 0.0042 1.1153 Ca 0.3071 1.0892 Ba 0.0003 1.5385 Fe 0.0001 1.2483 Mn 0.0003 1.2719 iteration : 3 Analysis no. 315 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3890 0.019300 0.3890 0.3298 Mg 1.2747 0.021564 1.2747 1.0223 Sr 0.3146 0.014228 0.3146 0.0700 P 1.6297 0.046502 1.6297 1.0256 K 0.0901 0.008557 0.0901 0.0449 Cl 0.4639 0.015501 0.4639 0.2550 Ca 33.4485 0.150603 33.4485 16.2670 Ba 0.0419 0.019912 0.0419 0.0060 Fe 0.0125 0.013941 0.0125 0.0044 Mn 0.0360 0.020557 0.0360 0.0128 C 12.5203 12.5203 20.3187 O 49.7787 49.7787 60.6436 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 316 x= -15722.0 y= 2725.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.8 5.8 3.6 4.07 0.0144 5.8 0.0290 Mg 114.8 2.1 2.5 45.59 0.0630 2.1 0.0111 Sr 35.2 2.7 14.3 2.46 0.0030 2.7 0.0399 P 69.9 2.7 2.4 29.73 0.0869 2.7 0.0395 K 16.0 5.6 5.1 3.14 0.0101 5.6 0.0186 Cl 44.8 2.7 2.2 20.39 0.0094 2.7 0.0227 Ca 3640.7 0.4 17.7 206.26 0.8045 0.5 0.0335 Ba 10.3 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0559 Mn 4.5 10.5 2.7 1.66 0.0018 10.5 0.0630 Elt. k-ratio Correc. Na 0.0007 2.3218 Mg 0.0046 1.6918 Sr 0.0019 1.3718 P 0.0136 1.1936 K 0.0009 1.0242 Cl 0.0052 1.1171 Ca 0.2920 1.0919 Ba 0.0000 NaN Fe 0.0000 1.2510 Mn 0.0005 1.2743 iteration : 3 Analysis no. 316 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1664 0.014357 0.1664 0.1386 Mg 0.7720 0.016821 0.7720 0.6081 Sr 0.2539 0.013539 0.2539 0.0555 P 1.6271 0.046444 1.6271 1.0057 K 0.0914 0.008621 0.0914 0.0448 Cl 0.5856 0.017232 0.5856 0.3162 Ca 31.8792 0.145976 31.8792 15.2272 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0025 0.013670 0.0025 0.0009 Mn 0.0652 0.021847 0.0652 0.0227 C 13.4300 13.4300 21.4061 O 51.1266 51.1266 61.1743 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 317 x= -15722.0 y= 2730.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.3 4.6 3.6 6.42 0.0254 4.6 0.0289 Mg 140.7 1.9 2.5 55.88 0.0776 1.9 0.0111 Sr 36.3 2.6 14.3 2.54 0.0032 2.6 0.0399 P 74.3 2.6 2.4 31.60 0.0926 2.6 0.0396 K 17.1 5.4 5.1 3.35 0.0111 5.4 0.0187 Cl 42.3 2.8 2.2 19.25 0.0089 2.8 0.0227 Ca 3553.0 0.4 17.7 201.29 0.7850 0.5 0.0335 Ba 10.3 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0559 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0630 Elt. k-ratio Correc. Na 0.0013 2.3163 Mg 0.0056 1.6915 Sr 0.0020 1.3739 P 0.0145 1.1956 K 0.0010 1.0278 Cl 0.0049 1.1198 Ca 0.2849 1.0930 Ba 0.0000 NaN Fe 0.0001 1.2516 Mn 0.0001 1.2746 iteration : 3 Analysis no. 317 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2937 0.017360 0.2937 0.2435 Mg 0.9501 0.018628 0.9501 0.7452 Sr 0.2680 0.013714 0.2680 0.0583 P 1.7360 0.047963 1.7360 1.0685 K 0.1010 0.008875 0.1010 0.0493 Cl 0.5526 0.016806 0.5526 0.2971 Ca 31.1397 0.143772 31.1397 14.8116 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0151 0.014055 0.0151 0.0051 Mn 0.0161 0.019699 0.0161 0.0056 C 13.5291 13.5291 21.4736 O 51.3988 51.3988 61.2421 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 318 x= -15722.0 y= 2735.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 12.5 6.3 3.6 3.45 0.0115 6.3 0.0289 Mg 129.3 2.0 2.5 51.33 0.0711 2.0 0.0111 Sr 39.5 2.5 14.3 2.77 0.0036 2.5 0.0399 P 77.6 2.5 2.4 33.01 0.0969 2.6 0.0396 K 13.2 6.1 5.1 2.59 0.0075 6.2 0.0188 Cl 48.4 2.6 2.2 21.99 0.0102 2.6 0.0227 Ca 3454.6 0.4 17.7 195.72 0.7632 0.5 0.0335 Ba 11.2 4.7 10.8 1.04 0.0002 4.7 0.0751 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0560 Mn 4.2 11.0 2.7 1.53 0.0014 11.0 0.0630 Elt. k-ratio Correc. Na 0.0006 2.3184 Mg 0.0052 1.6898 Sr 0.0022 1.3732 P 0.0152 1.1959 K 0.0007 1.0315 Cl 0.0057 1.1217 Ca 0.2770 1.0942 Ba 0.0001 1.5373 Fe 0.0000 1.2523 Mn 0.0004 1.2752 iteration : 3 Analysis no. 318 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1326 0.013426 0.1326 0.1092 Mg 0.8704 0.017830 0.8704 0.6782 Sr 0.3075 0.014146 0.3075 0.0665 P 1.8162 0.049035 1.8162 1.1104 K 0.0684 0.008085 0.0684 0.0331 Cl 0.6368 0.017945 0.6368 0.3401 Ca 30.3058 0.141271 30.3058 14.3191 Ba 0.0105 0.019375 0.0105 0.0014 Fe 0.0042 0.013736 0.0042 0.0014 Mn 0.0525 0.021325 0.0525 0.0181 C 13.8606 13.8606 21.8535 O 51.9346 51.9346 61.4689 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 319 x= -15721.0 y= 2740.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.0 5.0 3.6 5.50 0.0211 5.0 0.0289 Mg 125.6 2.0 2.5 49.88 0.0691 2.0 0.0111 Sr 39.4 2.5 14.3 2.76 0.0036 2.5 0.0399 P 86.7 2.4 2.4 36.88 0.1086 2.4 0.0396 K 15.7 5.6 5.1 3.07 0.0097 5.7 0.0188 Cl 47.9 2.6 2.2 21.75 0.0101 2.6 0.0227 Ca 3501.0 0.4 17.7 198.35 0.7735 0.5 0.0335 Ba 12.6 4.4 10.8 1.17 0.0011 4.5 0.0751 Fe 3.8 8.1 3.3 1.15 0.0003 8.1 0.0559 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0630 Elt. k-ratio Correc. Na 0.0011 2.3150 Mg 0.0050 1.6900 Sr 0.0022 1.3723 P 0.0170 1.1952 K 0.0009 1.0310 Cl 0.0056 1.1217 Ca 0.2807 1.0935 Ba 0.0003 1.5371 Fe 0.0001 1.2513 Mn 0.0003 1.2743 iteration : 3 Analysis no. 319 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2435 0.016228 0.2435 0.2018 Mg 0.8455 0.017579 0.8455 0.6628 Sr 0.3058 0.014121 0.3058 0.0665 P 2.0348 0.051825 2.0348 1.2517 K 0.0891 0.008606 0.0891 0.0434 Cl 0.6295 0.017851 0.6295 0.3383 Ca 30.6973 0.142443 30.6973 14.5929 Ba 0.0491 0.020016 0.0491 0.0068 Fe 0.0167 0.014103 0.0167 0.0057 Mn 0.0361 0.020599 0.0361 0.0125 C 13.5298 13.5298 21.4625 O 51.5228 51.5228 61.3550 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 320 x= -15721.0 y= 2745.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.5 4.9 3.6 5.64 0.0217 5.0 0.0289 Mg 99.3 2.2 2.5 39.45 0.0544 2.3 0.0111 Sr 36.3 2.6 14.3 2.54 0.0032 2.6 0.0399 P 94.2 2.3 2.4 40.10 0.1183 2.3 0.0396 K 14.9 5.8 5.1 2.91 0.0090 5.8 0.0189 Cl 50.9 2.6 2.2 23.12 0.0107 2.6 0.0228 Ca 3341.7 0.4 17.7 189.32 0.7381 0.5 0.0336 Ba 11.3 4.7 10.8 1.05 0.0003 4.7 0.0751 Fe 4.2 7.7 3.3 1.28 0.0005 7.7 0.0560 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0631 Elt. k-ratio Correc. Na 0.0011 2.3162 Mg 0.0039 1.6910 Sr 0.0020 1.3722 P 0.0186 1.1955 K 0.0008 1.0365 Cl 0.0060 1.1249 Ca 0.2679 1.0958 Ba 0.0001 1.5367 Fe 0.0002 1.2531 Mn 0.0001 1.2757 iteration : 3 Analysis no. 320 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2511 0.016409 0.2511 0.2057 Mg 0.6654 0.015644 0.6654 0.5155 Sr 0.2683 0.013706 0.2683 0.0577 P 2.2178 0.054084 2.2178 1.3484 K 0.0828 0.008484 0.0828 0.0399 Cl 0.6728 0.018435 0.6728 0.3574 Ca 29.3537 0.138412 29.3537 13.7920 Ba 0.0131 0.019413 0.0131 0.0018 Fe 0.0310 0.014539 0.0310 0.0105 Mn 0.0179 0.019801 0.0179 0.0061 C 14.0245 14.0245 21.9888 O 52.4016 52.4016 61.6763 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 321 x= -15721.0 y= 2749.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 28.3 4.2 3.6 7.79 0.0318 4.2 0.0288 Mg 178.4 1.7 2.5 70.85 0.0987 1.7 0.0110 Sr 36.9 2.6 14.3 2.58 0.0032 2.6 0.0399 P 99.9 2.2 2.4 42.52 0.1257 2.3 0.0396 K 17.0 5.4 5.1 3.32 0.0109 5.4 0.0189 Cl 67.8 2.2 2.2 30.82 0.0145 2.2 0.0228 Ca 3363.6 0.4 17.7 190.56 0.7429 0.5 0.0336 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0559 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0630 Elt. k-ratio Correc. Na 0.0016 2.3028 Mg 0.0071 1.6857 Sr 0.0020 1.3743 P 0.0197 1.1967 K 0.0010 1.0388 Cl 0.0081 1.1260 Ca 0.2696 1.0957 Ba 0.0000 NaN Fe 0.0001 1.2517 Mn 0.0001 1.2745 iteration : 3 Analysis no. 321 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3654 0.018791 0.3654 0.3017 Mg 1.2049 0.020936 1.2049 0.9412 Sr 0.2754 0.013799 0.2754 0.0597 P 2.3575 0.055775 2.3575 1.4449 K 0.1008 0.008938 0.1008 0.0490 Cl 0.9079 0.021213 0.9079 0.4862 Ca 29.5415 0.138983 29.5415 13.9927 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0117 0.013955 0.0117 0.0040 Mn 0.0179 0.019779 0.0179 0.0062 C 13.5321 13.5321 21.3887 O 51.6849 51.6849 61.3258 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 322 x= -15720.0 y= 2754.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 13.9 6.0 3.6 3.82 0.0132 6.0 0.0291 Mg 78.9 2.5 2.5 31.32 0.0429 2.5 0.0111 Sr 23.5 3.3 14.3 1.65 0.0013 3.3 0.0401 P 80.0 2.5 2.4 34.05 0.1000 2.5 0.0398 K 13.2 6.1 5.1 2.59 0.0075 6.2 0.0192 Cl 43.7 2.8 2.2 19.87 0.0092 2.8 0.0230 Ca 2677.8 0.4 17.7 151.71 0.5908 0.5 0.0339 Ba 8.9 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0564 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0634 Elt. k-ratio Correc. Na 0.0007 2.3271 Mg 0.0031 1.6971 Sr 0.0008 1.3802 P 0.0157 1.2023 K 0.0007 1.0563 Cl 0.0051 1.1356 Ca 0.2144 1.1045 Ba 0.0000 NaN Fe 0.0001 1.2616 Mn 0.0002 1.2827 iteration : 2 Analysis no. 322 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1533 0.014035 0.1533 0.1190 Mg 0.5267 0.014010 0.5267 0.3867 Sr 0.1129 0.011900 0.1129 0.0230 P 1.8858 0.050084 1.8858 1.0864 K 0.0701 0.008280 0.0701 0.0320 Cl 0.5796 0.017307 0.5796 0.2917 Ca 23.6807 0.120929 23.6807 10.5425 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0076 0.013943 0.0076 0.0024 Mn 0.0217 0.020080 0.0217 0.0070 C 16.5821 16.5821 24.6340 O 56.3796 56.3796 62.8753 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 323 x= -15720.0 y= 2759.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 13.8 6.0 3.6 3.79 0.0131 6.0 0.0290 Mg 71.4 2.6 2.5 28.34 0.0387 2.7 0.0111 Sr 27.6 3.0 14.3 1.93 0.0019 3.0 0.0400 P 79.6 2.5 2.4 33.88 0.0995 2.5 0.0398 K 13.8 6.0 5.1 2.70 0.0080 6.0 0.0191 Cl 50.6 2.6 2.2 22.98 0.0107 2.6 0.0230 Ca 2858.6 0.4 17.7 161.95 0.6309 0.5 0.0338 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.0 9.1 3.3 0.92 0.0000 9.1 0.0000 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0633 Elt. k-ratio Correc. Na 0.0007 2.3258 Mg 0.0028 1.6958 Sr 0.0012 1.3774 P 0.0156 1.2000 K 0.0007 1.0505 Cl 0.0059 1.1319 Ca 0.2290 1.1021 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2809 iteration : 2 Analysis no. 323 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1517 0.013985 0.1517 0.1194 Mg 0.4745 0.013328 0.4745 0.3531 Sr 0.1625 0.012503 0.1625 0.0335 P 1.8724 0.049860 1.8724 1.0932 K 0.0744 0.008357 0.0744 0.0344 Cl 0.6728 0.018498 0.6728 0.3432 Ca 25.2349 0.125799 25.2349 11.3864 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0235 0.020135 0.0235 0.0077 C 15.9861 15.9861 24.0700 O 55.3472 55.3472 62.5590 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 324 x= -15720.0 y= 2764.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.5 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.5 15.0 Na 17.5 5.3 3.6 4.81 0.0178 5.4 0.0290 Mg 92.3 2.3 2.5 36.67 0.0504 2.3 0.0111 Sr 33.8 2.7 14.3 2.37 0.0028 2.7 0.0400 P 84.9 2.4 2.4 36.14 0.1063 2.4 0.0397 K 16.1 5.6 5.1 3.15 0.0101 5.6 0.0190 Cl 46.3 2.7 2.2 21.02 0.0097 2.7 0.0229 Ca 3048.9 0.4 17.7 172.73 0.6730 0.5 0.0337 Ba 10.3 4.9 10.8 0.95 0.0000 4.9 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0562 Mn 2.6 13.9 2.7 0.96 0.0000 13.9 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3205 Mg 0.0036 1.6934 Sr 0.0017 1.3758 P 0.0167 1.1989 K 0.0009 1.0448 Cl 0.0054 1.1295 Ca 0.2443 1.0997 Ba 0.0000 NaN Fe 0.0000 1.2569 Mn 0.0000 NaN iteration : 2 Analysis no. 324 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2067 0.015372 0.2067 0.1652 Mg 0.6180 0.015106 0.6180 0.4672 Sr 0.2385 0.013393 0.2385 0.0500 P 1.9986 0.051449 1.9986 1.1856 K 0.0937 0.008805 0.0937 0.0440 Cl 0.6115 0.017680 0.6115 0.3169 Ca 26.8596 0.130813 26.8596 12.3134 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0034 0.013759 0.0034 0.0011 Mn 0.0000 0.000000 0.0000 0.0000 C 15.1907 15.1907 23.2382 O 54.1792 54.1792 62.2183 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 325 x= -15719.0 y= 2769.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 22.7 4.7 3.6 6.25 0.0246 4.7 0.0289 Mg 126.9 2.0 2.5 50.38 0.0698 2.0 0.0111 Sr 32.9 2.8 14.3 2.30 0.0027 2.8 0.0400 P 87.4 2.4 2.4 37.18 0.1095 2.4 0.0397 K 15.0 5.8 5.1 2.94 0.0091 5.8 0.0191 Cl 65.2 2.3 2.2 29.65 0.0139 2.3 0.0229 Ca 3044.7 0.4 17.7 172.50 0.6723 0.5 0.0337 Ba 9.8 5.0 10.8 0.91 0.0000 5.0 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0561 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0632 Elt. k-ratio Correc. Na 0.0012 2.3134 Mg 0.0051 1.6909 Sr 0.0016 1.3766 P 0.0172 1.1991 K 0.0008 1.0469 Cl 0.0077 1.1299 Ca 0.2440 1.0998 Ba 0.0000 NaN Fe 0.0000 1.2561 Mn 0.0002 1.2781 iteration : 2 Analysis no. 325 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2837 0.017129 0.2837 0.2276 Mg 0.8546 0.017679 0.8546 0.6486 Sr 0.2271 0.013270 0.2271 0.0478 P 2.0589 0.052218 2.0589 1.2261 K 0.0849 0.008602 0.0849 0.0401 Cl 0.8756 0.020895 0.8756 0.4556 Ca 26.8322 0.130744 26.8322 12.3488 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0059 0.013831 0.0059 0.0019 Mn 0.0234 0.020091 0.0234 0.0079 C 14.9698 14.9698 22.9897 O 53.7840 53.7840 62.0059 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 326 x= -15719.0 y= 2774.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 33.1 3.9 3.6 9.11 0.0380 3.9 0.0289 Mg 132.2 1.9 2.5 52.49 0.0728 2.0 0.0111 Sr 33.4 2.7 14.3 2.34 0.0027 2.7 0.0402 P 73.2 2.6 2.4 31.13 0.0912 2.6 0.0399 K 17.0 5.4 5.1 3.32 0.0109 5.4 0.0193 Cl 49.1 2.6 2.2 22.31 0.0104 2.6 0.0230 Ca 2678.7 0.4 17.7 151.76 0.5909 0.5 0.0339 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0634 Elt. k-ratio Correc. Na 0.0019 2.3162 Mg 0.0053 1.6968 Sr 0.0017 1.3832 P 0.0143 1.2053 K 0.0010 1.0574 Cl 0.0058 1.1362 Ca 0.2145 1.1042 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2817 iteration : 2 Analysis no. 326 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4393 0.020292 0.4393 0.3423 Mg 0.8941 0.018108 0.8941 0.6591 Sr 0.2343 0.013404 0.2343 0.0479 P 1.7236 0.048000 1.7236 0.9969 K 0.1026 0.009100 0.1026 0.0470 Cl 0.6549 0.018306 0.6549 0.3309 Ca 23.6820 0.120921 23.6820 10.5858 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0162 0.019811 0.0162 0.0053 C 16.3504 16.3504 24.3883 O 55.9027 55.9027 62.5963 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 327 x= -15719.0 y= 2779.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 48.5 3.2 3.6 13.36 0.0579 3.2 0.0288 Mg 193.9 1.6 2.5 76.98 0.1074 1.6 0.0111 Sr 43.0 2.4 14.3 3.01 0.0041 2.4 0.0400 P 75.5 2.6 2.4 32.11 0.0942 2.6 0.0397 K 17.2 5.4 5.1 3.36 0.0111 5.4 0.0187 Cl 38.2 3.0 2.2 17.37 0.0080 3.0 0.0227 Ca 3543.1 0.4 17.7 200.73 0.7829 0.5 0.0335 Ba 11.2 4.7 10.8 1.04 0.0003 4.7 0.0751 Fe 3.6 8.4 3.3 1.08 0.0002 8.4 0.0559 Mn 4.3 10.8 2.7 1.57 0.0015 10.8 0.0630 Elt. k-ratio Correc. Na 0.0029 2.3051 Mg 0.0078 1.6926 Sr 0.0025 1.3774 P 0.0148 1.1987 K 0.0010 1.0293 Cl 0.0044 1.1215 Ca 0.2841 1.0927 Ba 0.0001 1.5368 Fe 0.0001 1.2504 Mn 0.0004 1.2735 iteration : 3 Analysis no. 327 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6660 0.024122 0.6660 0.5548 Mg 1.3162 0.021935 1.3162 1.0371 Sr 0.3506 0.014644 0.3506 0.0766 P 1.7698 0.048483 1.7698 1.0942 K 0.1016 0.008899 0.1016 0.0498 Cl 0.4965 0.016030 0.4965 0.2682 Ca 31.0475 0.143482 31.0475 14.8345 Ba 0.0124 0.019404 0.0124 0.0017 Fe 0.0092 0.013869 0.0092 0.0032 Mn 0.0561 0.021454 0.0561 0.0195 C 13.2096 13.2096 21.0613 O 50.9644 50.9644 60.9990 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 328 x= -15718.0 y= 2784.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 11.3 6.7 3.6 3.10 0.0098 6.7 0.0291 Mg 59.6 2.9 2.5 23.65 0.0320 2.9 0.0111 Sr 27.9 3.0 14.3 1.95 0.0020 3.0 0.0401 P 62.0 2.8 2.4 26.37 0.0768 2.9 0.0398 K 13.7 6.0 5.1 2.69 0.0079 6.0 0.0191 Cl 46.0 2.7 2.2 20.92 0.0097 2.7 0.0229 Ca 2858.9 0.4 17.7 161.97 0.6310 0.5 0.0338 Ba 10.5 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.0 9.1 3.3 0.92 0.0000 9.1 0.0000 Mn 2.5 14.3 2.7 0.90 0.0000 14.3 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3318 Mg 0.0023 1.6985 Sr 0.0012 1.3784 P 0.0120 1.2007 K 0.0007 1.0484 Cl 0.0054 1.1301 Ca 0.2290 1.1021 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 328 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1146 0.012971 0.1146 0.0897 Mg 0.3938 0.012224 0.3938 0.2917 Sr 0.1666 0.012562 0.1666 0.0342 P 1.4454 0.044021 1.4454 0.8401 K 0.0739 0.008330 0.0739 0.0340 Cl 0.6088 0.017653 0.6088 0.3091 Ca 25.2381 0.125810 25.2381 11.3361 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.3227 16.3227 24.4651 O 55.6362 55.6362 62.5999 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 329 x= -15718.0 y= 2789.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 26.6 4.3 3.6 7.33 0.0297 4.3 0.0289 Mg 154.7 1.8 2.5 61.45 0.0855 1.8 0.0111 Sr 38.9 2.5 14.3 2.72 0.0035 2.6 0.0400 P 71.9 2.6 2.4 30.60 0.0896 2.7 0.0397 K 18.2 5.2 5.1 3.56 0.0121 5.3 0.0188 Cl 69.2 2.2 2.2 31.47 0.0148 2.2 0.0228 Ca 3438.1 0.4 17.7 194.78 0.7599 0.5 0.0336 Ba 11.3 4.7 10.8 1.05 0.0004 4.7 0.0751 Fe 4.0 7.9 3.3 1.20 0.0004 7.9 0.0560 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0631 Elt. k-ratio Correc. Na 0.0015 2.3113 Mg 0.0062 1.6900 Sr 0.0022 1.3747 P 0.0141 1.1966 K 0.0011 1.0336 Cl 0.0082 1.1215 Ca 0.2758 1.0945 Ba 0.0001 1.5369 Fe 0.0002 1.2518 Mn 0.0002 1.2747 iteration : 3 Analysis no. 329 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3424 0.018372 0.3424 0.2827 Mg 1.0460 0.019536 1.0460 0.8169 Sr 0.2998 0.014079 0.2998 0.0649 P 1.6816 0.047264 1.6816 1.0305 K 0.1105 0.009139 0.1105 0.0537 Cl 0.9246 0.021359 0.9246 0.4951 Ca 30.1847 0.140938 30.1847 14.2952 Ba 0.0151 0.019458 0.0151 0.0021 Fe 0.0226 0.014288 0.0226 0.0077 Mn 0.0306 0.020373 0.0306 0.0106 C 13.7621 13.7621 21.7488 O 51.5800 51.5800 61.1919 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 330 x= -15718.0 y= 2794.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 15.1 5.7 3.6 4.16 0.0148 5.8 0.0291 Mg 78.9 2.5 2.5 31.32 0.0429 2.5 0.0111 Sr 25.8 3.1 14.3 1.81 0.0017 3.1 0.0402 P 56.8 3.0 2.4 24.17 0.0701 3.0 0.0399 K 14.9 5.8 5.1 2.91 0.0090 5.8 0.0192 Cl 45.5 2.7 2.2 20.69 0.0096 2.7 0.0230 Ca 2691.8 0.4 17.7 152.50 0.5939 0.5 0.0339 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0564 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0634 Elt. k-ratio Correc. Na 0.0007 2.3312 Mg 0.0031 1.6999 Sr 0.0010 1.3818 P 0.0110 1.2034 K 0.0008 1.0539 Cl 0.0053 1.1331 Ca 0.2155 1.1042 Ba 0.0000 NaN Fe 0.0000 1.2622 Mn 0.0002 1.2832 iteration : 2 Analysis no. 330 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1724 0.014555 0.1724 0.1334 Mg 0.5275 0.014032 0.5275 0.3862 Sr 0.1409 0.012269 0.1409 0.0286 P 1.3234 0.042266 1.3234 0.7602 K 0.0842 0.008627 0.0842 0.0383 Cl 0.6034 0.017606 0.6034 0.3028 Ca 23.7976 0.121291 23.7976 10.5649 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0008 0.013742 0.0008 0.0003 Mn 0.0198 0.020003 0.0198 0.0064 C 16.8660 16.8660 24.9858 O 56.4639 56.4639 62.7930 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 331 x= -15717.0 y= 2799.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 19.8 5.0 3.6 5.45 0.0208 5.0 0.0291 Mg 88.2 2.4 2.5 35.04 0.0481 2.4 0.0111 Sr 26.5 3.1 14.3 1.85 0.0017 3.1 0.0401 P 63.4 2.8 2.4 26.96 0.0786 2.8 0.0398 K 15.9 5.6 5.1 3.12 0.0100 5.6 0.0191 Cl 51.1 2.6 2.2 23.22 0.0108 2.6 0.0229 Ca 2822.8 0.4 17.7 159.92 0.6230 0.5 0.0338 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0634 Elt. k-ratio Correc. Na 0.0010 2.3265 Mg 0.0035 1.6982 Sr 0.0011 1.3802 P 0.0123 1.2018 K 0.0009 1.0505 Cl 0.0060 1.1313 Ca 0.2261 1.1025 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2816 iteration : 2 Analysis no. 331 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2418 0.016241 0.2418 0.1893 Mg 0.5916 0.014816 0.5916 0.4382 Sr 0.1490 0.012358 0.1490 0.0306 P 1.4807 0.044552 1.4807 0.8607 K 0.0930 0.008823 0.0930 0.0428 Cl 0.6799 0.018582 0.6799 0.3453 Ca 24.9276 0.124841 24.9276 11.1972 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0162 0.019811 0.0162 0.0053 C 16.2616 16.2616 24.3747 O 55.5587 55.5587 62.5159 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 332 x= -15717.0 y= 2804.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.7 5.8 3.6 4.04 0.0142 5.9 0.0291 Mg 89.4 2.4 2.5 35.49 0.0488 2.4 0.0111 Sr 29.6 2.9 14.3 2.07 0.0022 2.9 0.0401 P 62.6 2.8 2.4 26.62 0.0776 2.8 0.0399 K 14.1 5.9 5.1 2.76 0.0083 6.0 0.0192 Cl 55.8 2.4 2.2 25.34 0.0118 2.4 0.0230 Ca 2764.8 0.4 17.7 156.64 0.6102 0.5 0.0338 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0564 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0634 Elt. k-ratio Correc. Na 0.0007 2.3272 Mg 0.0035 1.6972 Sr 0.0014 1.3803 P 0.0122 1.2025 K 0.0007 1.0529 Cl 0.0066 1.1323 Ca 0.2215 1.1032 Ba 0.0000 NaN Fe 0.0000 1.2606 Mn 0.0004 1.2819 iteration : 2 Analysis no. 332 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1654 0.014356 0.1654 0.1291 Mg 0.5993 0.014905 0.5993 0.4424 Sr 0.1876 0.012833 0.1876 0.0384 P 1.4623 0.044302 1.4623 0.8470 K 0.0776 0.008456 0.0776 0.0356 Cl 0.7457 0.019405 0.7457 0.3774 Ca 24.4305 0.123288 24.4305 10.9362 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0025 0.013779 0.0025 0.0008 Mn 0.0510 0.021365 0.0510 0.0166 C 16.4531 16.4531 24.5769 O 55.8251 55.8251 62.5995 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 333 x= -15717.0 y= 2808.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 37.3 3.7 3.6 10.27 0.0434 3.7 0.0289 Mg 154.6 1.8 2.5 61.39 0.0854 1.8 0.0111 Sr 38.3 2.6 14.3 2.68 0.0035 2.6 0.0401 P 72.2 2.6 2.4 30.71 0.0899 2.6 0.0399 K 18.1 5.3 5.1 3.54 0.0120 5.3 0.0191 Cl 74.4 2.1 2.2 33.84 0.0160 2.1 0.0229 Ca 2939.7 0.4 17.7 166.55 0.6491 0.5 0.0338 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0562 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0632 Elt. k-ratio Correc. Na 0.0022 2.3090 Mg 0.0062 1.6931 Sr 0.0021 1.3802 P 0.0141 1.2024 K 0.0011 1.0506 Cl 0.0089 1.1311 Ca 0.2356 1.1009 Ba 0.0000 NaN Fe 0.0001 1.2568 Mn 0.0002 1.2785 iteration : 3 Analysis no. 333 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5006 0.021376 0.5006 0.3991 Mg 1.0468 0.019560 1.0468 0.7895 Sr 0.2945 0.014063 0.2945 0.0616 P 1.6956 0.047569 1.6956 1.0035 K 0.1115 0.009268 0.1115 0.0523 Cl 1.0048 0.022316 1.0048 0.5195 Ca 25.9341 0.127975 25.9341 11.8611 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0185 0.014219 0.0185 0.0061 Mn 0.0253 0.020185 0.0253 0.0084 C 15.3102 15.3102 23.3659 O 54.0582 54.0582 61.9331 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 334 x= -15716.0 y= 2813.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 16.3 5.5 3.6 4.48 0.0163 5.6 0.0291 Mg 66.9 2.7 2.5 26.57 0.0362 2.8 0.0111 Sr 23.2 3.3 14.3 1.63 0.0013 3.3 0.0401 P 77.5 2.5 2.4 32.96 0.0967 2.6 0.0399 K 15.9 5.6 5.1 3.11 0.0099 5.6 0.0193 Cl 50.8 2.6 2.2 23.10 0.0107 2.6 0.0231 Ca 2565.8 0.4 17.7 145.36 0.5659 0.5 0.0339 Ba 7.8 5.7 10.8 0.73 0.0000 5.7 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0564 Mn 2.6 13.9 2.7 0.96 0.0000 13.9 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3272 Mg 0.0026 1.6981 Sr 0.0008 1.3808 P 0.0152 1.2032 K 0.0009 1.0605 Cl 0.0060 1.1373 Ca 0.2054 1.1061 Ba 0.0000 NaN Fe 0.0000 1.2628 Mn 0.0000 NaN iteration : 2 Analysis no. 334 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1893 0.014972 0.1893 0.1458 Mg 0.4445 0.012933 0.4445 0.3237 Sr 0.1096 0.011861 0.1096 0.0221 P 1.8250 0.049305 1.8250 1.0430 K 0.0934 0.008896 0.0934 0.0423 Cl 0.6797 0.018632 0.6797 0.3394 Ca 22.7151 0.117870 22.7151 10.0327 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0051 0.013878 0.0051 0.0016 Mn 0.0000 0.000000 0.0000 0.0000 C 16.9935 16.9935 25.0458 O 56.9448 56.9448 63.0036 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 335 x= -15716.0 y= 2818.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 26.1 4.4 3.6 7.18 0.0290 4.4 0.0289 Mg 138.1 1.9 2.5 54.83 0.0761 1.9 0.0111 Sr 37.3 2.6 14.3 2.61 0.0033 2.6 0.0401 P 92.5 2.3 2.4 39.37 0.1162 2.3 0.0398 K 17.3 5.4 5.1 3.38 0.0112 5.4 0.0192 Cl 64.6 2.3 2.2 29.35 0.0138 2.3 0.0230 Ca 2898.1 0.4 17.7 164.19 0.6400 0.5 0.0338 Ba 10.7 4.8 10.8 0.99 0.0000 4.8 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0633 Elt. k-ratio Correc. Na 0.0014 2.3098 Mg 0.0055 1.6903 Sr 0.0020 1.3780 P 0.0182 1.2013 K 0.0010 1.0527 Cl 0.0077 1.1336 Ca 0.2323 1.1016 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2788 iteration : 2 Analysis no. 335 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3340 0.018192 0.3340 0.2658 Mg 0.9317 0.018448 0.9317 0.7014 Sr 0.2809 0.013898 0.2809 0.0587 P 2.1885 0.053877 2.1885 1.2928 K 0.1048 0.009126 0.1048 0.0491 Cl 0.8695 0.020867 0.8695 0.4487 Ca 25.5860 0.126912 25.5860 11.6801 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0180 0.019860 0.0180 0.0060 C 15.2925 15.2925 23.2954 O 54.3940 54.3940 62.2020 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 336 x= -15716.0 y= 2823.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 19.4 5.1 3.6 5.35 0.0204 5.1 0.0291 Mg 68.8 2.7 2.5 27.33 0.0372 2.7 0.0111 Sr 20.7 3.5 14.3 1.45 0.0009 3.5 0.0402 P 78.3 2.5 2.4 33.31 0.0978 2.5 0.0400 K 14.3 5.9 5.1 2.79 0.0085 5.9 0.0195 Cl 60.7 2.3 2.2 27.57 0.0129 2.3 0.0232 Ca 2298.5 0.5 17.7 130.22 0.5068 0.5 0.0341 Ba 7.5 5.8 10.8 0.69 0.0000 5.8 0.0000 Fe 3.1 8.9 3.3 0.95 0.0000 9.0 0.0000 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0636 Elt. k-ratio Correc. Na 0.0010 2.3258 Mg 0.0027 1.6990 Sr 0.0006 1.3836 P 0.0153 1.2058 K 0.0007 1.0708 Cl 0.0072 1.1426 Ca 0.1839 1.1096 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2858 iteration : 2 Analysis no. 336 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2366 0.016121 0.2366 0.1790 Mg 0.4581 0.013125 0.4581 0.3279 Sr 0.0786 0.011478 0.0786 0.0156 P 1.8495 0.049699 1.8495 1.0389 K 0.0803 0.008637 0.0803 0.0357 Cl 0.8216 0.020405 0.8216 0.4032 Ca 20.4097 0.110463 20.4096 8.8598 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0125 0.019715 0.0125 0.0040 C 17.8167 17.8167 25.8085 O 58.2365 58.2365 63.3274 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 337 x= -15715.0 y= 2828.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 26.9 4.3 3.6 7.42 0.0301 4.3 0.0290 Mg 122.3 2.0 2.5 48.55 0.0673 2.0 0.0111 Sr 32.5 2.8 14.3 2.27 0.0026 2.8 0.0404 P 78.7 2.5 2.4 33.48 0.0983 2.5 0.0402 K 12.7 6.3 5.1 2.49 0.0070 6.3 0.0198 Cl 66.8 2.2 2.2 30.38 0.0143 2.2 0.0233 Ca 1994.7 0.5 17.7 113.01 0.4393 0.6 0.0342 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 2.9 9.3 3.3 0.87 0.0000 9.3 0.0000 Mn 2.9 13.2 2.7 1.05 0.0001 13.2 0.0637 Elt. k-ratio Correc. Na 0.0015 2.3162 Mg 0.0049 1.6969 Sr 0.0016 1.3886 P 0.0154 1.2120 K 0.0006 1.0837 Cl 0.0079 1.1501 Ca 0.1594 1.1135 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2872 iteration : 2 Analysis no. 337 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3476 0.018504 0.3476 0.2588 Mg 0.8262 0.017422 0.8262 0.5819 Sr 0.2239 0.013330 0.2239 0.0437 P 1.8686 0.050076 1.8686 1.0326 K 0.0675 0.008382 0.0675 0.0296 Cl 0.9143 0.021531 0.9143 0.4414 Ca 17.7515 0.101625 17.7515 7.5809 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0052 0.019390 0.0052 0.0016 C 18.5526 18.5526 26.4388 O 59.4425 59.4425 63.5907 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 338 x= -15715.0 y= 2833.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.2 5.0 3.6 5.57 0.0214 5.0 0.0291 Mg 76.4 2.6 2.5 30.33 0.0415 2.6 0.0112 Sr 22.2 3.4 14.3 1.55 0.0011 3.4 0.0404 P 61.7 2.8 2.4 26.24 0.0764 2.9 0.0402 K 10.4 6.9 5.1 2.03 0.0049 7.0 0.0198 Cl 83.8 2.0 2.2 38.09 0.0180 2.0 0.0233 Ca 1917.4 0.5 17.7 108.63 0.4221 0.6 0.0342 Ba 7.6 5.7 10.8 0.70 0.0000 5.7 0.0000 Fe 2.9 9.3 3.3 0.88 0.0000 9.3 0.0000 Mn 2.7 13.6 2.7 1.00 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0011 2.3259 Mg 0.0030 1.7005 Sr 0.0007 1.3884 P 0.0120 1.2107 K 0.0004 1.0856 Cl 0.0100 1.1488 Ca 0.1532 1.1148 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 338 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2486 0.016400 0.2486 0.1832 Mg 0.5107 0.013823 0.5107 0.3560 Sr 0.0976 0.011767 0.0976 0.0189 P 1.4507 0.044300 1.4507 0.7935 K 0.0467 0.007821 0.0467 0.0202 Cl 1.1527 0.024023 1.1527 0.5508 Ca 17.0772 0.099344 17.0772 7.2184 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 19.2497 19.2497 27.1519 O 60.1661 60.1661 63.7071 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 339 x= -15715.0 y= 2838.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 18.6 5.2 3.6 5.11 0.0193 5.2 0.0291 Mg 89.3 2.4 2.5 35.45 0.0487 2.4 0.0112 Sr 25.4 3.1 14.3 1.78 0.0016 3.1 0.0406 P 47.4 3.2 2.4 20.15 0.0580 3.3 0.0405 K 8.3 7.8 5.1 1.63 0.0030 7.8 0.0202 Cl 83.8 2.0 2.2 38.07 0.0180 2.0 0.0236 Ca 1294.5 0.6 17.7 73.34 0.2837 0.7 0.0345 Ba 8.0 5.6 10.8 0.74 0.0000 5.6 0.0000 Fe 2.7 9.7 3.3 0.81 0.0000 9.7 0.0000 Mn 2.4 14.4 2.7 0.89 0.0000 14.4 0.0000 Elt. k-ratio Correc. Na 0.0010 2.3292 Mg 0.0035 1.7039 Sr 0.0010 1.3971 P 0.0091 1.2199 K 0.0003 1.1101 Cl 0.0100 1.1614 Ca 0.1030 1.1233 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 339 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2242 0.015843 0.2242 0.1582 Mg 0.6012 0.014961 0.6012 0.4013 Sr 0.1376 0.012349 0.1376 0.0255 P 1.1093 0.039214 1.1093 0.5810 K 0.0291 0.007448 0.0291 0.0121 Cl 1.1651 0.024285 1.1651 0.5331 Ca 11.5660 0.079524 11.5660 4.6817 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 21.5260 21.5260 29.0758 O 63.6416 63.6416 64.5313 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 340 x= -15714.0 y= 2843.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 19.7 5.0 3.6 5.42 0.0207 5.1 0.0291 Mg 59.1 2.9 2.5 23.45 0.0318 2.9 0.0112 Sr 19.0 3.6 14.3 1.33 0.0007 3.6 0.0405 P 50.2 3.2 2.4 21.36 0.0617 3.2 0.0403 K 7.9 8.0 5.1 1.54 0.0025 8.0 0.0200 Cl 90.8 1.9 2.2 41.26 0.0196 1.9 0.0234 Ca 1674.2 0.5 17.7 94.85 0.3681 0.6 0.0343 Ba 9.1 5.2 10.8 0.85 0.0000 5.2 0.0000 Fe 2.6 9.8 3.3 0.78 0.0000 9.9 0.0000 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0639 Elt. k-ratio Correc. Na 0.0010 2.3307 Mg 0.0023 1.7038 Sr 0.0004 1.3912 P 0.0097 1.2133 K 0.0002 1.0945 Cl 0.0109 1.1524 Ca 0.1336 1.1182 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2918 iteration : 2 Analysis no. 340 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2409 0.016245 0.2409 0.1742 Mg 0.3918 0.012219 0.3918 0.2680 Sr 0.0580 0.011259 0.0580 0.0110 P 1.1733 0.040133 1.1733 0.6298 K 0.0247 0.007220 0.0247 0.0105 Cl 1.2556 0.025074 1.2556 0.5888 Ca 14.9387 0.091918 14.9387 6.1966 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0015 0.019286 0.0015 0.0005 C 20.2942 20.2942 28.0907 O 61.6214 61.6214 64.0299 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 341 x= -15714.0 y= 2848.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 19.8 5.0 3.6 5.45 0.0208 5.0 0.0292 Mg 74.5 2.6 2.5 29.59 0.0405 2.6 0.0112 Sr 25.8 3.1 14.3 1.81 0.0017 3.1 0.0406 P 42.2 3.4 2.4 17.96 0.0514 3.5 0.0405 K 8.5 7.7 5.1 1.67 0.0031 7.7 0.0202 Cl 74.3 2.1 2.2 33.76 0.0159 2.1 0.0235 Ca 1373.5 0.6 17.7 77.81 0.3013 0.7 0.0345 Ba 9.2 5.2 10.8 0.85 0.0000 5.2 0.0000 Fe 3.1 9.0 3.3 0.92 0.0000 9.1 0.0000 Mn 2.6 14.0 2.7 0.94 0.0000 14.0 0.0000 Elt. k-ratio Correc. Na 0.0010 2.3327 Mg 0.0029 1.7060 Sr 0.0010 1.3965 P 0.0081 1.2192 K 0.0003 1.1058 Cl 0.0089 1.1592 Ca 0.1094 1.1220 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 341 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2426 0.016295 0.2426 0.1717 Mg 0.4996 0.013706 0.4996 0.3345 Sr 0.1428 0.012412 0.1428 0.0265 P 0.9820 0.037070 0.9820 0.5159 K 0.0308 0.007476 0.0308 0.0128 Cl 1.0279 0.022855 1.0279 0.4718 Ca 12.2702 0.082192 12.2702 4.9821 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 21.4027 21.4027 28.9984 O 63.4015 63.4015 64.4862 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 342 x= -15714.0 y= 2853.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.1 4.6 3.6 6.37 0.0252 4.7 0.0292 Mg 83.0 2.5 2.5 32.97 0.0452 2.5 0.0112 Sr 23.8 3.2 14.3 1.66 0.0014 3.3 0.0408 P 40.1 3.5 2.4 17.07 0.0487 3.5 0.0407 K 8.6 7.6 5.1 1.68 0.0032 7.7 0.0205 Cl 68.8 2.2 2.2 31.29 0.0147 2.2 0.0237 Ca 920.4 0.7 17.7 52.14 0.2006 0.8 0.0346 Ba 8.7 5.3 10.8 0.81 0.0000 5.4 0.0000 Fe 2.7 9.7 3.3 0.81 0.0000 9.7 0.0000 Mn 2.1 15.6 2.7 0.76 0.0000 15.6 0.0000 Elt. k-ratio Correc. Na 0.0013 2.3339 Mg 0.0033 1.7092 Sr 0.0008 1.4031 P 0.0076 1.2257 K 0.0003 1.1252 Cl 0.0082 1.1695 Ca 0.0728 1.1284 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 342 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2931 0.017441 0.2931 0.2014 Mg 0.5597 0.014480 0.5597 0.3636 Sr 0.1180 0.012145 0.1180 0.0213 P 0.9351 0.036358 0.9351 0.4768 K 0.0318 0.007621 0.0318 0.0129 Cl 0.9587 0.022216 0.9587 0.4271 Ca 8.2152 0.066022 8.2152 3.2370 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 22.9569 22.9569 30.1843 O 65.9314 65.9314 65.0758 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 343 x= -15713.0 y= 2858.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 24.7 4.5 3.6 6.81 0.0272 4.5 0.0291 Mg 85.7 2.4 2.5 34.04 0.0467 2.4 0.0112 Sr 24.2 3.2 14.3 1.70 0.0014 3.2 0.0403 P 64.5 2.8 2.4 27.45 0.0801 2.8 0.0400 K 12.2 6.4 5.1 2.39 0.0066 6.4 0.0195 Cl 76.9 2.1 2.2 34.95 0.0165 2.1 0.0231 Ca 2397.5 0.5 17.7 135.83 0.5289 0.5 0.0340 Ba 8.3 5.5 10.8 0.77 0.0000 5.5 0.0000 Fe 4.1 7.8 3.3 1.23 0.0004 7.9 0.0566 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0636 Elt. k-ratio Correc. Na 0.0014 2.3235 Mg 0.0034 1.6991 Sr 0.0009 1.3838 P 0.0126 1.2057 K 0.0006 1.0675 Cl 0.0092 1.1394 Ca 0.1919 1.1082 Ba 0.0000 NaN Fe 0.0002 1.2641 Mn 0.0001 1.2846 iteration : 2 Analysis no. 343 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3158 0.017879 0.3158 0.2408 Mg 0.5750 0.014624 0.5750 0.4147 Sr 0.1222 0.012053 0.1222 0.0244 P 1.5144 0.045124 1.5144 0.8570 K 0.0621 0.008141 0.0621 0.0279 Cl 1.0467 0.022846 1.0467 0.5175 Ca 21.2708 0.113263 21.2708 9.3018 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0254 0.014507 0.0254 0.0080 Mn 0.0125 0.019700 0.0125 0.0040 C 17.5508 17.5508 25.6111 O 57.5042 57.5042 62.9930 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 344 x= -15713.0 y= 2863.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 25.1 4.5 3.6 6.91 0.0277 4.5 0.0291 Mg 84.8 2.4 2.5 33.69 0.0462 2.4 0.0112 Sr 31.1 2.8 14.3 2.18 0.0024 2.8 0.0401 P 38.6 3.6 2.4 16.43 0.0467 3.6 0.0398 K 17.2 5.4 5.1 3.37 0.0112 5.4 0.0190 Cl 57.5 2.4 2.2 26.13 0.0122 2.4 0.0228 Ca 3007.8 0.4 17.7 170.40 0.6645 0.5 0.0338 Ba 9.4 5.1 10.8 0.88 0.0000 5.2 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0634 Elt. k-ratio Correc. Na 0.0014 2.3289 Mg 0.0033 1.7007 Sr 0.0015 1.3799 P 0.0073 1.2010 K 0.0010 1.0425 Cl 0.0068 1.1253 Ca 0.2412 1.1000 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2805 iteration : 2 Analysis no. 344 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3218 0.018032 0.3218 0.2545 Mg 0.5693 0.014562 0.5693 0.4259 Sr 0.2057 0.013051 0.2057 0.0427 P 0.8798 0.034980 0.8798 0.5165 K 0.1034 0.009029 0.1034 0.0481 Cl 0.7654 0.019583 0.7654 0.3925 Ca 26.5274 0.129826 26.5274 12.0340 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0015 0.019119 0.0015 0.0005 C 15.9724 15.9724 24.1787 O 54.6531 54.6531 62.1066 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 345 x= -15713.0 y= 2868.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.6 5.3 3.6 4.84 0.0180 5.3 0.0292 Mg 63.3 2.8 2.5 25.12 0.0341 2.8 0.0112 Sr 26.8 3.1 14.3 1.88 0.0018 3.1 0.0401 P 26.6 4.3 2.4 11.30 0.0312 4.3 0.0397 K 20.9 4.9 5.1 4.10 0.0146 4.9 0.0188 Cl 50.0 2.6 2.2 22.72 0.0106 2.6 0.0227 Ca 3347.8 0.4 17.7 189.67 0.7401 0.5 0.0336 Ba 8.4 5.4 10.8 0.78 0.0000 5.5 0.0000 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0562 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0633 Elt. k-ratio Correc. Na 0.0009 2.3369 Mg 0.0025 1.7021 Sr 0.0011 1.3766 P 0.0049 1.1968 K 0.0013 1.0285 Cl 0.0059 1.1169 Ca 0.2686 1.0956 Ba 0.0000 NaN Fe 0.0001 1.2562 Mn 0.0002 1.2786 iteration : 3 Analysis no. 345 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2099 0.015532 0.2099 0.1693 Mg 0.4205 0.012622 0.4205 0.3209 Sr 0.1530 0.012387 0.1530 0.0324 P 0.5853 0.029204 0.5853 0.3504 K 0.1332 0.009622 0.1332 0.0632 Cl 0.6566 0.018166 0.6566 0.3435 Ca 29.4259 0.138664 29.4259 13.6155 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0177 0.014193 0.0177 0.0059 Mn 0.0253 0.020195 0.0253 0.0085 C 15.1740 15.1740 23.4289 O 53.1987 53.1987 61.6616 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 346 x= -15712.0 y= 2872.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 36.5 3.7 3.6 10.06 0.0425 3.7 0.0290 Mg 126.9 2.0 2.5 50.38 0.0699 2.0 0.0112 Sr 36.1 2.6 14.3 2.53 0.0031 2.6 0.0401 P 31.0 4.0 2.4 13.17 0.0369 4.0 0.0398 K 20.0 5.0 5.1 3.92 0.0138 5.0 0.0188 Cl 74.8 2.1 2.2 33.99 0.0160 2.1 0.0227 Ca 3402.8 0.4 17.7 192.78 0.7525 0.5 0.0336 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0561 Mn 5.1 9.9 2.7 1.88 0.0024 9.9 0.0632 Elt. k-ratio Correc. Na 0.0021 2.3210 Mg 0.0051 1.6985 Sr 0.0019 1.3777 P 0.0058 1.1981 K 0.0012 1.0308 Cl 0.0089 1.1176 Ca 0.2731 1.0947 Ba 0.0000 NaN Fe 0.0001 1.2535 Mn 0.0007 1.2762 iteration : 3 Analysis no. 346 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4923 0.021301 0.4923 0.4023 Mg 0.8592 0.017774 0.8592 0.6641 Sr 0.2673 0.013747 0.2673 0.0573 P 0.6927 0.031423 0.6927 0.4201 K 0.1259 0.009476 0.1259 0.0605 Cl 0.9981 0.022113 0.9981 0.5289 Ca 29.8945 0.140081 29.8945 14.0124 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0109 0.013967 0.0109 0.0037 Mn 0.0873 0.022799 0.0873 0.0298 C 14.4993 14.4993 22.6787 O 52.0725 52.0725 61.1421 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 347 x= -15712.0 y= 2877.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 16.4 5.5 3.6 4.51 0.0164 5.5 0.0292 Mg 67.9 2.7 2.5 26.95 0.0367 2.7 0.0112 Sr 24.1 3.2 14.3 1.69 0.0014 3.2 0.0403 P 25.9 4.4 2.4 11.00 0.0303 4.4 0.0400 K 16.1 5.6 5.1 3.15 0.0101 5.6 0.0194 Cl 75.4 2.1 2.2 34.28 0.0162 2.1 0.0230 Ca 2461.3 0.5 17.7 139.45 0.5432 0.5 0.0340 Ba 9.3 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0566 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0637 Elt. k-ratio Correc. Na 0.0008 2.3357 Mg 0.0027 1.7035 Sr 0.0009 1.3852 P 0.0048 1.2060 K 0.0009 1.0614 Cl 0.0090 1.1339 Ca 0.1971 1.1073 Ba 0.0000 NaN Fe 0.0000 1.2652 Mn 0.0001 1.2857 iteration : 2 Analysis no. 347 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1917 0.015079 0.1917 0.1456 Mg 0.4529 0.013076 0.4529 0.3253 Sr 0.1208 0.012049 0.1208 0.0241 P 0.5729 0.029074 0.5729 0.3229 K 0.0953 0.008954 0.0953 0.0426 Cl 1.0215 0.022529 1.0215 0.5030 Ca 21.8292 0.115073 21.8292 9.5078 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013814 0.0017 0.0005 Mn 0.0181 0.019977 0.0181 0.0057 C 18.0285 18.0285 26.2031 O 57.6674 57.6674 62.9194 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 348 x= -15712.0 y= 2882.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 32.1 3.9 3.6 8.84 0.0367 4.0 0.0291 Mg 98.8 2.2 2.5 39.23 0.0541 2.3 0.0112 Sr 31.5 2.8 14.3 2.20 0.0025 2.8 0.0402 P 28.5 4.2 2.4 12.11 0.0337 4.2 0.0399 K 18.6 5.2 5.1 3.64 0.0124 5.2 0.0191 Cl 83.1 2.0 2.2 37.78 0.0179 2.0 0.0229 Ca 2952.5 0.4 17.7 167.27 0.6524 0.5 0.0338 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0563 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0634 Elt. k-ratio Correc. Na 0.0018 2.3253 Mg 0.0039 1.7009 Sr 0.0015 1.3811 P 0.0053 1.2018 K 0.0011 1.0456 Cl 0.0100 1.1252 Ca 0.2368 1.1007 Ba 0.0000 NaN Fe 0.0001 1.2588 Mn 0.0002 1.2805 iteration : 3 Analysis no. 348 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4265 0.020110 0.4265 0.3367 Mg 0.6662 0.015710 0.6662 0.4975 Sr 0.2109 0.013125 0.2109 0.0437 P 0.6341 0.030298 0.6341 0.3716 K 0.1153 0.009331 0.1153 0.0535 Cl 1.1205 0.023452 1.1205 0.5737 Ca 26.0625 0.128407 26.0625 11.8028 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0126 0.014077 0.0126 0.0041 Mn 0.0271 0.020314 0.0271 0.0090 C 16.1272 16.1272 24.3711 O 54.5970 54.5970 61.9364 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 349 x= -15711.0 y= 2887.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 21.6 4.8 3.6 5.94 0.0232 4.8 0.0291 Mg 93.2 2.3 2.5 37.00 0.0510 2.3 0.0112 Sr 24.7 3.2 14.3 1.73 0.0015 3.2 0.0403 P 23.9 4.6 2.4 10.15 0.0277 4.6 0.0400 K 14.2 5.9 5.1 2.78 0.0084 5.9 0.0194 Cl 103.6 1.8 2.2 47.08 0.0224 1.8 0.0230 Ca 2490.4 0.4 17.7 141.09 0.5497 0.5 0.0340 Ba 9.0 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0566 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0636 Elt. k-ratio Correc. Na 0.0012 2.3289 Mg 0.0037 1.7011 Sr 0.0009 1.3850 P 0.0043 1.2055 K 0.0007 1.0625 Cl 0.0125 1.1331 Ca 0.1995 1.1070 Ba 0.0000 NaN Fe 0.0000 1.2640 Mn 0.0004 1.2846 iteration : 2 Analysis no. 349 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2693 0.016894 0.2693 0.2057 Mg 0.6275 0.015264 0.6275 0.4534 Sr 0.1276 0.012136 0.1276 0.0256 P 0.5240 0.028004 0.5240 0.2971 K 0.0793 0.008563 0.0793 0.0356 Cl 1.4138 0.026328 1.4138 0.7002 Ca 22.0851 0.115903 22.0851 9.6759 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0034 0.013855 0.0034 0.0011 Mn 0.0493 0.021352 0.0493 0.0157 C 17.7623 17.7623 25.9682 O 57.0584 57.0584 62.6214 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 350 x= -15711.0 y= 2892.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 39.7 3.5 3.6 10.95 0.0466 3.6 0.0291 Mg 112.0 2.1 2.5 44.48 0.0615 2.1 0.0112 Sr 29.9 2.9 14.3 2.09 0.0022 2.9 0.0403 P 28.5 4.2 2.4 12.13 0.0337 4.2 0.0400 K 18.0 5.3 5.1 3.53 0.0119 5.3 0.0192 Cl 74.0 2.1 2.2 33.64 0.0159 2.1 0.0230 Ca 2682.7 0.4 17.7 151.98 0.5925 0.5 0.0339 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.5 8.4 3.3 1.06 0.0001 8.5 0.0565 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0635 Elt. k-ratio Correc. Na 0.0023 2.3240 Mg 0.0045 1.7033 Sr 0.0014 1.3855 P 0.0053 1.2058 K 0.0011 1.0546 Cl 0.0088 1.1309 Ca 0.2150 1.1042 Ba 0.0000 NaN Fe 0.0001 1.2618 Mn 0.0001 1.2828 iteration : 2 Analysis no. 350 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5409 0.022175 0.5409 0.4190 Mg 0.7587 0.016747 0.7587 0.5558 Sr 0.1922 0.012936 0.1922 0.0391 P 0.6374 0.030425 0.6374 0.3664 K 0.1116 0.009300 0.1116 0.0508 Cl 0.9994 0.022265 0.9994 0.5019 Ca 23.7405 0.121153 23.7405 10.5471 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0068 0.013932 0.0068 0.0022 Mn 0.0107 0.019593 0.0107 0.0035 C 16.9685 16.9685 25.1555 O 56.0333 56.0333 62.3587 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 351 x= -15711.0 y= 2897.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.6 4.9 3.6 5.68 0.0219 4.9 0.0292 Mg 60.4 2.9 2.5 23.97 0.0325 2.9 0.0112 Sr 20.4 3.5 14.3 1.43 0.0009 3.5 0.0404 P 28.4 4.2 2.4 12.06 0.0335 4.2 0.0401 K 16.1 5.6 5.1 3.15 0.0101 5.6 0.0195 Cl 75.6 2.1 2.2 34.38 0.0162 2.1 0.0231 Ca 2257.2 0.5 17.7 127.88 0.4979 0.5 0.0341 Ba 7.9 5.6 10.8 0.73 0.0000 5.6 0.0000 Fe 2.7 9.6 3.3 0.82 0.0000 9.6 0.0000 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0638 Elt. k-ratio Correc. Na 0.0011 2.3360 Mg 0.0024 1.7055 Sr 0.0005 1.3873 P 0.0053 1.2080 K 0.0009 1.0691 Cl 0.0090 1.1382 Ca 0.1807 1.1100 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2875 iteration : 2 Analysis no. 351 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2558 0.016619 0.2558 0.1916 Mg 0.4014 0.012366 0.4014 0.2843 Sr 0.0754 0.011469 0.0754 0.0148 P 0.6349 0.030403 0.6349 0.3529 K 0.0960 0.009020 0.0960 0.0423 Cl 1.0287 0.022649 1.0287 0.4995 Ca 20.0563 0.109322 20.0563 8.6154 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0236 0.020259 0.0236 0.0074 C 18.6780 18.6780 26.7734 O 58.7499 58.7499 63.2183 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 352 x= -15710.0 y= 2902.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 31.7 4.0 3.6 8.73 0.0362 4.0 0.0291 Mg 90.0 2.4 2.5 35.75 0.0492 2.4 0.0112 Sr 28.8 2.9 14.3 2.01 0.0021 3.0 0.0403 P 28.3 4.2 2.4 12.02 0.0334 4.2 0.0400 K 18.0 5.3 5.1 3.52 0.0119 5.3 0.0192 Cl 88.9 1.9 2.2 40.41 0.0192 1.9 0.0229 Ca 2698.3 0.4 17.7 152.87 0.5958 0.5 0.0339 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.3 8.7 3.3 0.99 0.0000 8.7 0.0000 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0635 Elt. k-ratio Correc. Na 0.0018 2.3262 Mg 0.0036 1.7020 Sr 0.0013 1.3833 P 0.0052 1.2040 K 0.0011 1.0547 Cl 0.0107 1.1299 Ca 0.2162 1.1041 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2827 iteration : 2 Analysis no. 352 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4206 0.020001 0.4206 0.3260 Mg 0.6059 0.015011 0.6059 0.4443 Sr 0.1777 0.012744 0.1777 0.0362 P 0.6303 0.030250 0.6303 0.3627 K 0.1111 0.009290 0.1111 0.0507 Cl 1.2052 0.024337 1.2052 0.6059 Ca 23.8763 0.121582 23.8763 10.6176 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0235 0.020181 0.0235 0.0076 C 16.9937 16.9937 25.2170 O 55.9556 55.9556 62.3319 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 353 x= -15710.0 y= 2907.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.8 4.6 3.6 6.55 0.0260 4.6 0.0292 Mg 67.9 2.7 2.5 26.95 0.0367 2.7 0.0112 Sr 24.4 3.2 14.3 1.71 0.0015 3.2 0.0403 P 26.3 4.4 2.4 11.17 0.0308 4.4 0.0399 K 22.4 4.7 5.1 4.39 0.0160 4.7 0.0192 Cl 65.1 2.3 2.2 29.58 0.0139 2.3 0.0229 Ca 2716.5 0.4 17.7 153.90 0.5999 0.5 0.0339 Ba 9.8 5.0 10.8 0.91 0.0000 5.1 0.0000 Fe 2.9 9.2 3.3 0.89 0.0000 9.3 0.0000 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0635 Elt. k-ratio Correc. Na 0.0013 2.3345 Mg 0.0027 1.7043 Sr 0.0009 1.3832 P 0.0048 1.2036 K 0.0014 1.0516 Cl 0.0077 1.1290 Ca 0.2177 1.1039 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2835 iteration : 2 Analysis no. 353 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3031 0.017661 0.3031 0.2342 Mg 0.4531 0.013081 0.4531 0.3312 Sr 0.1246 0.012082 0.1246 0.0253 P 0.5814 0.029221 0.5814 0.3336 K 0.1492 0.010120 0.1492 0.0678 Cl 0.8733 0.020869 0.8733 0.4377 Ca 24.0323 0.122072 24.0323 10.6545 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0235 0.020194 0.0235 0.0076 C 17.1519 17.1519 25.3745 O 56.3076 56.3076 62.5336 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 354 x= -15710.0 y= 2912.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 42.9 3.4 3.6 11.82 0.0507 3.4 0.0290 Mg 136.5 1.9 2.5 54.20 0.0753 1.9 0.0112 Sr 34.4 2.7 14.3 2.41 0.0029 2.7 0.0404 P 30.1 4.1 2.4 12.81 0.0358 4.1 0.0401 K 19.7 5.0 5.1 3.86 0.0135 5.0 0.0192 Cl 68.9 2.2 2.2 31.33 0.0148 2.2 0.0230 Ca 2759.6 0.4 17.7 156.34 0.6097 0.5 0.0339 Ba 11.1 4.7 10.8 1.03 0.0002 4.8 0.0751 Fe 3.5 8.4 3.3 1.06 0.0001 8.5 0.0564 Mn 3.9 11.3 2.7 1.44 0.0012 11.3 0.0635 Elt. k-ratio Correc. Na 0.0025 2.3206 Mg 0.0055 1.7022 Sr 0.0018 1.3857 P 0.0056 1.2062 K 0.0012 1.0522 Cl 0.0082 1.1302 Ca 0.2213 1.1029 Ba 0.0001 1.5349 Fe 0.0001 1.2604 Mn 0.0003 1.2816 iteration : 3 Analysis no. 354 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5875 0.022951 0.5875 0.4584 Mg 0.9280 0.018485 0.9280 0.6849 Sr 0.2477 0.013591 0.2477 0.0507 P 0.6768 0.031233 0.6768 0.3920 K 0.1260 0.009618 0.1260 0.0578 Cl 0.9284 0.021497 0.9284 0.4698 Ca 24.4044 0.123243 24.4044 10.9231 Ba 0.0092 0.019350 0.0092 0.0012 Fe 0.0068 0.013921 0.0068 0.0022 Mn 0.0437 0.021069 0.0437 0.0143 C 16.5746 16.5746 24.7553 O 55.4671 55.4671 62.1903 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 355 x= -15709.0 y= 2917.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 19.0 5.1 3.6 5.22 0.0198 5.1 0.0292 Mg 74.7 2.6 2.5 29.65 0.0406 2.6 0.0112 Sr 21.6 3.4 14.3 1.51 0.0010 3.4 0.0403 P 27.2 4.3 2.4 11.58 0.0320 4.3 0.0400 K 15.8 5.6 5.1 3.09 0.0098 5.6 0.0194 Cl 99.4 1.8 2.2 45.20 0.0215 1.8 0.0230 Ca 2496.7 0.4 17.7 141.45 0.5512 0.5 0.0340 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0636 Elt. k-ratio Correc. Na 0.0010 2.3310 Mg 0.0029 1.7015 Sr 0.0006 1.3840 P 0.0050 1.2046 K 0.0009 1.0619 Cl 0.0120 1.1329 Ca 0.2000 1.1071 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2850 iteration : 2 Analysis no. 355 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2305 0.016009 0.2305 0.1759 Mg 0.4996 0.013690 0.4996 0.3606 Sr 0.0894 0.011634 0.0894 0.0179 P 0.6052 0.029743 0.6052 0.3428 K 0.0928 0.008897 0.0928 0.0416 Cl 1.3560 0.025801 1.3560 0.6711 Ca 22.1471 0.116116 22.1471 9.6950 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0089 0.019544 0.0089 0.0028 C 17.7956 17.7956 25.9952 O 57.1750 57.1750 62.6970 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 356 x= -15709.0 y= 2922.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 34.1 3.8 3.6 9.39 0.0393 3.8 0.0291 Mg 93.1 2.3 2.5 36.98 0.0509 2.3 0.0112 Sr 30.8 2.8 14.3 2.15 0.0024 2.9 0.0402 P 27.6 4.3 2.4 11.72 0.0325 4.3 0.0399 K 21.7 4.8 5.1 4.26 0.0154 4.8 0.0191 Cl 71.9 2.2 2.2 32.70 0.0154 2.2 0.0229 Ca 2968.6 0.4 17.7 168.18 0.6562 0.5 0.0338 Ba 10.3 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0564 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0634 Elt. k-ratio Correc. Na 0.0020 2.3272 Mg 0.0037 1.7025 Sr 0.0015 1.3814 P 0.0051 1.2019 K 0.0014 1.0441 Cl 0.0086 1.1248 Ca 0.2381 1.1004 Ba 0.0000 NaN Fe 0.0001 1.2589 Mn 0.0003 1.2805 iteration : 3 Analysis no. 356 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4570 0.020695 0.4570 0.3608 Mg 0.6278 0.015276 0.6278 0.4689 Sr 0.2021 0.013026 0.2021 0.0419 P 0.6124 0.029857 0.6124 0.3589 K 0.1422 0.009923 0.1422 0.0660 Cl 0.9656 0.021846 0.9656 0.4944 Ca 26.2057 0.128859 26.2057 11.8682 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0076 0.013930 0.0076 0.0025 Mn 0.0400 0.020891 0.0400 0.0132 C 16.1162 16.1162 24.3557 O 54.6234 54.6234 61.9695 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 357 x= -15709.0 y= 2927.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.1 3.8 3.6 9.66 0.0406 3.8 0.0291 Mg 124.9 2.0 2.5 49.58 0.0688 2.0 0.0112 Sr 32.9 2.8 14.3 2.30 0.0027 2.8 0.0403 P 27.6 4.3 2.4 11.72 0.0325 4.3 0.0400 K 21.6 4.8 5.1 4.23 0.0152 4.8 0.0191 Cl 73.0 2.1 2.2 33.19 0.0157 2.1 0.0229 Ca 2931.3 0.4 17.7 166.07 0.6479 0.5 0.0338 Ba 10.1 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.4 8.6 3.3 1.03 0.0001 8.6 0.0564 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0634 Elt. k-ratio Correc. Na 0.0020 2.3232 Mg 0.0050 1.7008 Sr 0.0017 1.3830 P 0.0051 1.2034 K 0.0013 1.0460 Cl 0.0087 1.1261 Ca 0.2351 1.1009 Ba 0.0000 NaN Fe 0.0000 1.2590 Mn 0.0002 1.2806 iteration : 3 Analysis no. 357 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4712 0.020935 0.4712 0.3716 Mg 0.8468 0.017662 0.8468 0.6317 Sr 0.2287 0.013352 0.2287 0.0473 P 0.6132 0.029894 0.6132 0.3590 K 0.1411 0.009913 0.1411 0.0655 Cl 0.9815 0.022030 0.9815 0.5020 Ca 25.8859 0.127870 25.8859 11.7103 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0034 0.013803 0.0034 0.0011 Mn 0.0272 0.020321 0.0272 0.0090 C 16.1279 16.1279 24.3461 O 54.6731 54.6731 61.9565 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 358 x= -15708.0 y= 2931.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 39.4 3.6 3.6 10.86 0.0462 3.6 0.0291 Mg 103.1 2.2 2.5 40.94 0.0565 2.2 0.0112 Sr 25.2 3.1 14.3 1.76 0.0016 3.2 0.0404 P 27.6 4.3 2.4 11.75 0.0326 4.3 0.0400 K 22.1 4.8 5.1 4.32 0.0157 4.8 0.0192 Cl 70.0 2.2 2.2 31.82 0.0150 2.2 0.0230 Ca 2669.6 0.4 17.7 151.24 0.5897 0.5 0.0339 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.5 8.4 3.3 1.06 0.0001 8.5 0.0565 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0636 Elt. k-ratio Correc. Na 0.0023 2.3265 Mg 0.0041 1.7047 Sr 0.0010 1.3857 P 0.0051 1.2055 K 0.0014 1.0544 Cl 0.0083 1.1307 Ca 0.2140 1.1044 Ba 0.0000 NaN Fe 0.0001 1.2622 Mn 0.0002 1.2832 iteration : 2 Analysis no. 358 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5372 0.022127 0.5372 0.4152 Mg 0.6977 0.016087 0.6977 0.5102 Sr 0.1338 0.012222 0.1338 0.0271 P 0.6155 0.029971 0.6155 0.3531 K 0.1466 0.010087 0.1466 0.0666 Cl 0.9437 0.021670 0.9437 0.4731 Ca 23.6348 0.120833 23.6348 10.4794 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0068 0.013941 0.0068 0.0022 Mn 0.0235 0.020197 0.0235 0.0076 C 17.0662 17.0662 25.2506 O 56.1943 56.1943 62.4149 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 359 x= -15708.0 y= 2936.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 18.4 5.2 3.6 5.07 0.0191 5.2 0.0292 Mg 70.7 2.7 2.5 28.06 0.0383 2.7 0.0112 Sr 28.1 3.0 14.3 1.97 0.0020 3.0 0.0402 P 23.8 4.6 2.4 10.11 0.0276 4.6 0.0399 K 17.6 5.3 5.1 3.45 0.0116 5.3 0.0191 Cl 63.8 2.3 2.2 29.00 0.0136 2.3 0.0229 Ca 2923.3 0.4 17.7 165.62 0.6461 0.5 0.0338 Ba 9.1 5.3 10.8 0.84 0.0000 5.3 0.0000 Fe 3.1 9.0 3.3 0.94 0.0000 9.0 0.0000 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0635 Elt. k-ratio Correc. Na 0.0010 2.3353 Mg 0.0028 1.7026 Sr 0.0012 1.3809 P 0.0043 1.2016 K 0.0010 1.0439 Cl 0.0076 1.1249 Ca 0.2345 1.1011 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2819 iteration : 2 Analysis no. 359 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2226 0.015841 0.2226 0.1745 Mg 0.4722 0.013335 0.4722 0.3500 Sr 0.1692 0.012626 0.1692 0.0348 P 0.5200 0.027865 0.5200 0.3024 K 0.1070 0.009129 0.1070 0.0493 Cl 0.8529 0.020603 0.8529 0.4334 Ca 25.8189 0.127666 25.8189 11.6051 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0217 0.020092 0.0217 0.0071 C 16.5334 16.5334 24.7984 O 55.2820 55.2820 62.2450 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 360 x= -15708.0 y= 2941.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 42.0 3.4 3.6 11.57 0.0495 3.5 0.0290 Mg 156.0 1.8 2.5 61.97 0.0863 1.8 0.0112 Sr 37.1 2.6 14.3 2.60 0.0033 2.6 0.0403 P 32.2 3.9 2.4 13.70 0.0385 4.0 0.0400 K 24.6 4.5 5.1 4.82 0.0180 4.5 0.0191 Cl 81.3 2.0 2.2 36.95 0.0175 2.0 0.0229 Ca 2944.7 0.4 17.7 166.83 0.6509 0.5 0.0338 Ba 11.3 4.7 10.8 1.05 0.0003 4.7 0.0752 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0563 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0634 Elt. k-ratio Correc. Na 0.0025 2.3156 Mg 0.0062 1.6985 Sr 0.0020 1.3835 P 0.0060 1.2041 K 0.0016 1.0473 Cl 0.0097 1.1269 Ca 0.2362 1.1007 Ba 0.0001 1.5354 Fe 0.0000 1.2578 Mn 0.0002 1.2796 iteration : 3 Analysis no. 360 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5728 0.022675 0.5728 0.4541 Mg 1.0612 0.019736 1.0612 0.7958 Sr 0.2804 0.013944 0.2804 0.0583 P 0.7268 0.032186 0.7268 0.4277 K 0.1675 0.010481 0.1675 0.0781 Cl 1.0970 0.023236 1.0970 0.5640 Ca 25.9995 0.128219 25.9995 11.8236 Ba 0.0138 0.019435 0.0138 0.0018 Fe 0.0059 0.013867 0.0059 0.0019 Mn 0.0253 0.020223 0.0253 0.0084 C 15.8249 15.8249 24.0144 O 54.2249 54.2249 61.7719 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 361 x= -15707.0 y= 2946.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.8 5.3 3.6 4.89 0.0183 5.3 0.0293 Mg 60.4 2.9 2.5 23.99 0.0325 2.9 0.0112 Sr 22.1 3.4 14.3 1.54 0.0011 3.4 0.0403 P 25.4 4.4 2.4 10.79 0.0297 4.5 0.0400 K 22.6 4.7 5.1 4.42 0.0161 4.7 0.0193 Cl 65.6 2.3 2.2 29.80 0.0140 2.3 0.0230 Ca 2569.8 0.4 17.7 145.59 0.5675 0.5 0.0340 Ba 7.8 5.6 10.8 0.73 0.0000 5.7 0.0000 Fe 3.0 9.1 3.3 0.91 0.0000 9.1 0.0000 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0637 Elt. k-ratio Correc. Na 0.0009 2.3373 Mg 0.0024 1.7045 Sr 0.0007 1.3842 P 0.0047 1.2047 K 0.0014 1.0565 Cl 0.0078 1.1315 Ca 0.2060 1.1059 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2851 iteration : 2 Analysis no. 361 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2130 0.015618 0.2130 0.1628 Mg 0.4016 0.012367 0.4016 0.2903 Sr 0.0956 0.011717 0.0956 0.0192 P 0.5603 0.028791 0.5603 0.3178 K 0.1512 0.010200 0.1512 0.0680 Cl 0.8826 0.021003 0.8826 0.4374 Ca 22.7768 0.118122 22.7768 9.9844 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0089 0.019547 0.0089 0.0028 C 17.7128 17.7128 25.9098 O 57.1971 57.1971 62.8075 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 362 x= -15707.0 y= 2951.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.9 3.7 3.6 9.90 0.0417 3.7 0.0291 Mg 105.2 2.2 2.5 41.77 0.0577 2.2 0.0112 Sr 31.5 2.8 14.3 2.20 0.0025 2.8 0.0402 P 29.2 4.1 2.4 12.43 0.0346 4.1 0.0398 K 24.5 4.5 5.1 4.80 0.0179 4.5 0.0189 Cl 71.6 2.2 2.2 32.53 0.0153 2.2 0.0228 Ca 3196.3 0.4 17.7 181.08 0.7068 0.5 0.0337 Ba 10.7 4.8 10.8 0.99 0.0000 4.8 0.0000 Fe 3.6 8.3 3.3 1.09 0.0002 8.3 0.0563 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0633 Elt. k-ratio Correc. Na 0.0021 2.3244 Mg 0.0042 1.7008 Sr 0.0015 1.3794 P 0.0054 1.1996 K 0.0016 1.0367 Cl 0.0085 1.1208 Ca 0.2565 1.0976 Ba 0.0000 NaN Fe 0.0001 1.2563 Mn 0.0002 1.2785 iteration : 3 Analysis no. 362 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4842 0.021177 0.4842 0.3889 Mg 0.7107 0.016212 0.7107 0.5400 Sr 0.2107 0.013112 0.2107 0.0444 P 0.6513 0.030623 0.6513 0.3883 K 0.1650 0.010358 0.1650 0.0779 Cl 0.9571 0.021714 0.9571 0.4985 Ca 28.1545 0.134840 28.1545 12.9720 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0101 0.013978 0.0101 0.0033 Mn 0.0216 0.020040 0.0216 0.0073 C 15.2973 15.2973 23.5191 O 53.3375 53.3375 61.5602 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 363 x= -15707.0 y= 2956.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 12.1 6.4 3.6 3.32 0.0109 6.5 0.0292 Mg 64.1 2.8 2.5 25.46 0.0346 2.8 0.0112 Sr 33.6 2.7 14.3 2.35 0.0028 2.7 0.0401 P 24.9 4.5 2.4 10.58 0.0290 4.5 0.0398 K 21.8 4.8 5.1 4.27 0.0154 4.8 0.0189 Cl 73.4 2.1 2.2 33.37 0.0157 2.1 0.0228 Ca 3132.2 0.4 17.7 177.45 0.6925 0.5 0.0338 Ba 10.8 4.8 10.8 1.00 0.0000 4.8 NaN Fe 3.1 8.9 3.3 0.95 0.0000 9.0 0.0000 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0634 Elt. k-ratio Correc. Na 0.0005 2.3345 Mg 0.0025 1.6996 Sr 0.0017 1.3771 P 0.0045 1.1987 K 0.0014 1.0378 Cl 0.0088 1.1208 Ca 0.2513 1.0984 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2797 iteration : 2 Analysis no. 363 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1269 0.013347 0.1269 0.1011 Mg 0.4260 0.012692 0.4260 0.3210 Sr 0.2363 0.013393 0.2363 0.0494 P 0.5453 0.028382 0.5453 0.3224 K 0.1422 0.009881 0.1422 0.0666 Cl 0.9823 0.021982 0.9823 0.5074 Ca 27.6069 0.133168 27.6069 12.6130 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0418 0.020955 0.0418 0.0139 C 15.8233 15.8233 24.1239 O 54.0690 54.0690 61.8813 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 364 x= -15706.0 y= 2961.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 27.7 4.2 3.6 7.64 0.0311 4.3 0.0290 Mg 147.4 1.8 2.5 58.55 0.0815 1.9 0.0111 Sr 38.9 2.5 14.3 2.72 0.0035 2.6 0.0402 P 30.9 4.0 2.4 13.15 0.0368 4.0 0.0398 K 29.2 4.1 5.1 5.73 0.0223 4.1 0.0189 Cl 86.7 2.0 2.2 39.41 0.0187 2.0 0.0228 Ca 3257.1 0.4 17.7 184.53 0.7204 0.5 0.0337 Ba 11.0 4.8 10.8 1.02 0.0001 4.8 0.0752 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0562 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0633 Elt. k-ratio Correc. Na 0.0016 2.3184 Mg 0.0059 1.6949 Sr 0.0022 1.3787 P 0.0058 1.1996 K 0.0020 1.0369 Cl 0.0104 1.1203 Ca 0.2614 1.0968 Ba 0.0000 1.5369 Fe 0.0001 1.2547 Mn 0.0003 1.2771 iteration : 3 Analysis no. 364 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3602 0.018781 0.3602 0.2919 Mg 0.9996 0.019137 0.9996 0.7662 Sr 0.3009 0.014132 0.3009 0.0640 P 0.6926 0.031449 0.6926 0.4165 K 0.2050 0.011156 0.2050 0.0977 Cl 1.1652 0.023845 1.1652 0.6123 Ca 28.6744 0.136423 28.6744 13.3277 Ba 0.0059 0.019320 0.0059 0.0008 Fe 0.0134 0.014060 0.0134 0.0045 Mn 0.0344 0.020593 0.0344 0.0117 C 14.8941 14.8941 23.1007 O 52.6543 52.6543 61.3062 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 365 x= -15706.0 y= 2966.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 16.9 5.4 3.6 4.65 0.0171 5.5 0.0292 Mg 72.4 2.6 2.5 28.76 0.0393 2.6 0.0112 Sr 23.9 3.2 14.3 1.67 0.0014 3.2 0.0403 P 28.4 4.2 2.4 12.09 0.0336 4.2 0.0400 K 22.6 4.7 5.1 4.43 0.0162 4.7 0.0193 Cl 76.6 2.1 2.2 34.81 0.0164 2.1 0.0230 Ca 2586.2 0.4 17.7 146.52 0.5712 0.5 0.0340 Ba 8.8 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 4.1 7.8 3.3 1.23 0.0004 7.9 0.0566 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0636 Elt. k-ratio Correc. Na 0.0009 2.3343 Mg 0.0028 1.7024 Sr 0.0009 1.3837 P 0.0053 1.2044 K 0.0014 1.0572 Cl 0.0092 1.1316 Ca 0.2073 1.1057 Ba 0.0000 NaN Fe 0.0002 1.2636 Mn 0.0001 1.2844 iteration : 2 Analysis no. 365 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1992 0.015263 0.1992 0.1528 Mg 0.4843 0.013494 0.4843 0.3514 Sr 0.1176 0.012001 0.1176 0.0237 P 0.6344 0.030346 0.6344 0.3612 K 0.1518 0.010216 0.1518 0.0684 Cl 1.0360 0.022660 1.0360 0.5153 Ca 22.9194 0.118576 22.9194 10.0834 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0254 0.014510 0.0254 0.0080 Mn 0.0125 0.019708 0.0125 0.0040 C 17.5298 17.5298 25.7352 O 56.8896 56.8896 62.6967 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 366 x= -15706.0 y= 2971.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 30.0 4.1 3.6 8.26 0.0340 4.1 0.0290 Mg 127.9 2.0 2.5 50.80 0.0705 2.0 0.0112 Sr 37.1 2.6 14.3 2.60 0.0033 2.6 0.0402 P 31.8 4.0 2.4 13.51 0.0379 4.0 0.0399 K 26.0 4.4 5.1 5.09 0.0193 4.4 0.0191 Cl 85.0 2.0 2.2 38.63 0.0183 2.0 0.0229 Ca 2970.4 0.4 17.7 168.28 0.6566 0.5 0.0338 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0563 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0634 Elt. k-ratio Correc. Na 0.0017 2.3204 Mg 0.0051 1.6975 Sr 0.0020 1.3811 P 0.0059 1.2024 K 0.0017 1.0462 Cl 0.0102 1.1257 Ca 0.2383 1.1006 Ba 0.0000 NaN Fe 0.0000 1.2580 Mn 0.0001 1.2797 iteration : 2 Analysis no. 366 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3942 0.019467 0.3942 0.3125 Mg 0.8663 0.017843 0.8663 0.6496 Sr 0.2803 0.013923 0.2803 0.0583 P 0.7148 0.031927 0.7148 0.4206 K 0.1789 0.010706 0.1789 0.0834 Cl 1.1472 0.023726 1.1472 0.5898 Ca 26.2253 0.128927 26.2253 11.9263 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0059 0.013868 0.0059 0.0019 Mn 0.0143 0.019722 0.0143 0.0048 C 15.8938 15.8938 24.1191 O 54.2790 54.2790 61.8337 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 367 x= -15705.0 y= 2976.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 28.7 4.2 3.6 7.91 0.0324 4.2 0.0291 Mg 115.0 2.1 2.5 45.67 0.0632 2.1 0.0112 Sr 34.9 2.7 14.3 2.45 0.0030 2.7 0.0402 P 33.1 3.9 2.4 14.07 0.0396 3.9 0.0399 K 24.3 4.5 5.1 4.76 0.0177 4.6 0.0191 Cl 92.3 1.9 2.2 41.95 0.0199 1.9 0.0229 Ca 2934.1 0.4 17.7 166.23 0.6485 0.5 0.0338 Ba 10.3 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.5 8.4 3.3 1.06 0.0001 8.5 0.0563 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0634 Elt. k-ratio Correc. Na 0.0016 2.3214 Mg 0.0046 1.6977 Sr 0.0018 1.3806 P 0.0062 1.2019 K 0.0016 1.0477 Cl 0.0111 1.1261 Ca 0.2354 1.1011 Ba 0.0000 NaN Fe 0.0001 1.2583 Mn 0.0003 1.2800 iteration : 2 Analysis no. 367 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3757 0.019106 0.3757 0.2971 Mg 0.7772 0.016919 0.7772 0.5814 Sr 0.2532 0.013614 0.2532 0.0525 P 0.7461 0.032526 0.7461 0.4380 K 0.1646 0.010423 0.1646 0.0765 Cl 1.2489 0.024720 1.2489 0.6405 Ca 25.9150 0.127969 25.9150 11.7567 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0067 0.013898 0.0067 0.0022 Mn 0.0326 0.020558 0.0326 0.0108 C 16.0251 16.0251 24.2596 O 54.4549 54.4549 61.8845 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 368 x= -15705.0 y= 2981.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 40.8 3.5 3.6 11.24 0.0480 3.5 0.0290 Mg 120.5 2.0 2.5 47.83 0.0663 2.1 0.0112 Sr 33.4 2.7 14.3 2.34 0.0027 2.7 0.0403 P 33.8 3.8 2.4 14.38 0.0406 3.9 0.0400 K 30.0 4.1 5.1 5.88 0.0230 4.1 0.0191 Cl 81.7 2.0 2.2 37.11 0.0176 2.0 0.0229 Ca 2906.6 0.4 17.7 164.67 0.6424 0.5 0.0338 Ba 9.0 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.9 8.0 3.3 1.18 0.0003 8.0 0.0564 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0634 Elt. k-ratio Correc. Na 0.0024 2.3198 Mg 0.0048 1.7004 Sr 0.0017 1.3823 P 0.0064 1.2030 K 0.0020 1.0482 Cl 0.0098 1.1270 Ca 0.2331 1.1013 Ba 0.0000 NaN Fe 0.0002 1.2585 Mn 0.0003 1.2801 iteration : 3 Analysis no. 368 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5558 0.022411 0.5558 0.4390 Mg 0.8162 0.017343 0.8162 0.6097 Sr 0.2345 0.013413 0.2345 0.0486 P 0.7651 0.032905 0.7651 0.4485 K 0.2141 0.011409 0.2141 0.0994 Cl 1.1022 0.023290 1.1022 0.5645 Ca 25.6763 0.127224 25.6763 11.6317 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0202 0.014304 0.0202 0.0066 Mn 0.0326 0.020561 0.0326 0.0108 C 16.0365 16.0365 24.2419 O 54.5465 54.5465 61.8994 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 369 x= -15705.0 y= 2986.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 22.2 4.7 3.6 6.11 0.0239 4.8 0.0290 Mg 147.8 1.8 2.5 58.69 0.0817 1.9 0.0111 Sr 42.4 2.4 14.3 2.97 0.0040 2.4 0.0401 P 31.8 4.0 2.4 13.53 0.0380 4.0 0.0398 K 25.0 4.5 5.1 4.90 0.0184 4.5 0.0189 Cl 95.8 1.9 2.2 43.53 0.0207 1.9 0.0228 Ca 3288.4 0.4 17.7 186.30 0.7273 0.5 0.0337 Ba 11.5 4.7 10.8 1.07 0.0005 4.7 0.0752 Fe 4.0 7.9 3.3 1.21 0.0004 7.9 0.0562 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0632 Elt. k-ratio Correc. Na 0.0012 2.3178 Mg 0.0059 1.6929 Sr 0.0025 1.3775 P 0.0060 1.1990 K 0.0016 1.0367 Cl 0.0115 1.1198 Ca 0.2640 1.0964 Ba 0.0001 1.5368 Fe 0.0002 1.2540 Mn 0.0002 1.2765 iteration : 3 Analysis no. 369 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2771 0.017018 0.2771 0.2253 Mg 1.0008 0.019138 1.0008 0.7696 Sr 0.3435 0.014583 0.3435 0.0733 P 0.7140 0.031862 0.7140 0.4309 K 0.1692 0.010445 0.1692 0.0809 Cl 1.2898 0.025035 1.2898 0.6800 Ca 28.9399 0.137227 28.9399 13.4953 Ba 0.0203 0.019562 0.0203 0.0028 Fe 0.0235 0.014351 0.0235 0.0079 Mn 0.0271 0.020257 0.0271 0.0092 C 14.7757 14.7757 22.9922 O 52.4190 52.4190 61.2327 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 370 x= -15704.0 y= 2991.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 39.7 3.5 3.6 10.95 0.0466 3.6 0.0290 Mg 113.0 2.1 2.5 44.87 0.0621 2.1 0.0112 Sr 34.8 2.7 14.3 2.44 0.0029 2.7 0.0402 P 32.0 4.0 2.4 13.60 0.0382 4.0 0.0399 K 29.8 4.1 5.1 5.83 0.0228 4.1 0.0192 Cl 99.7 1.8 2.2 45.34 0.0216 1.8 0.0229 Ca 2881.4 0.4 17.7 163.24 0.6368 0.5 0.0339 Ba 10.5 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0564 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0634 Elt. k-ratio Correc. Na 0.0023 2.3182 Mg 0.0045 1.6992 Sr 0.0018 1.3813 P 0.0060 1.2024 K 0.0020 1.0502 Cl 0.0120 1.1269 Ca 0.2311 1.1018 Ba 0.0000 NaN Fe 0.0000 1.2585 Mn 0.0002 1.2801 iteration : 2 Analysis no. 370 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5397 0.022126 0.5397 0.4260 Mg 0.7640 0.016786 0.7640 0.5703 Sr 0.2515 0.013600 0.2515 0.0521 P 0.7197 0.032024 0.7197 0.4216 K 0.2124 0.011390 0.2124 0.0985 Cl 1.3531 0.025704 1.3531 0.6925 Ca 25.4637 0.126571 25.4637 11.5270 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0059 0.013875 0.0059 0.0019 Mn 0.0290 0.020396 0.0290 0.0096 C 16.1239 16.1239 24.3565 O 54.5371 54.5371 61.8440 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 371 x= -15704.0 y= 2995.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 21.5 4.8 3.6 5.93 0.0231 4.8 0.0292 Mg 70.5 2.7 2.5 28.00 0.0382 2.7 0.0112 Sr 23.9 3.2 14.3 1.68 0.0014 3.2 0.0403 P 32.0 3.9 2.4 13.62 0.0382 4.0 0.0400 K 25.1 4.5 5.1 4.91 0.0184 4.5 0.0194 Cl 68.9 2.2 2.2 31.30 0.0147 2.2 0.0231 Ca 2471.2 0.4 17.7 140.00 0.5456 0.5 0.0340 Ba 7.6 5.7 10.8 0.71 0.0000 5.7 0.0000 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0637 Elt. k-ratio Correc. Na 0.0012 2.3336 Mg 0.0028 1.7038 Sr 0.0009 1.3851 P 0.0060 1.2059 K 0.0016 1.0613 Cl 0.0082 1.1344 Ca 0.1980 1.1072 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2853 iteration : 2 Analysis no. 371 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2692 0.016914 0.2692 0.2049 Mg 0.4715 0.013330 0.4715 0.3395 Sr 0.1187 0.012025 0.1187 0.0237 P 0.7230 0.032141 0.7230 0.4085 K 0.1737 0.010701 0.1737 0.0777 Cl 0.9309 0.021566 0.9309 0.4595 Ca 21.9219 0.115386 21.9219 9.5715 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0346 0.020725 0.0346 0.0110 C 17.8511 17.8511 26.0084 O 57.5054 57.5054 62.8953 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 372 x= -15704.0 y= 3000.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.7 3.7 3.6 9.83 0.0414 3.8 0.0290 Mg 108.9 2.1 2.5 43.24 0.0598 2.2 0.0112 Sr 35.5 2.7 14.3 2.49 0.0031 2.7 0.0402 P 34.8 3.8 2.4 14.79 0.0418 3.8 0.0399 K 27.7 4.2 5.1 5.43 0.0209 4.3 0.0191 Cl 94.7 1.9 2.2 43.06 0.0205 1.9 0.0229 Ca 2929.4 0.4 17.7 165.96 0.6475 0.5 0.0338 Ba 10.1 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0563 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0634 Elt. k-ratio Correc. Na 0.0021 2.3192 Mg 0.0043 1.6985 Sr 0.0019 1.3804 P 0.0066 1.2018 K 0.0019 1.0483 Cl 0.0114 1.1263 Ca 0.2350 1.1012 Ba 0.0000 NaN Fe 0.0000 1.2581 Mn 0.0001 1.2798 iteration : 2 Analysis no. 372 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4793 0.021063 0.4793 0.3794 Mg 0.7353 0.016472 0.7353 0.5505 Sr 0.2602 0.013692 0.2602 0.0540 P 0.7874 0.033308 0.7874 0.4625 K 0.1944 0.011028 0.1944 0.0904 Cl 1.2829 0.025045 1.2829 0.6584 Ca 25.8763 0.127852 25.8763 11.7469 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013819 0.0042 0.0014 Mn 0.0180 0.019893 0.0180 0.0060 C 15.9817 15.9817 24.2099 O 54.3803 54.3803 61.8406 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 373 x= -15703.0 y= 3005.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.3 5.4 3.6 4.76 0.0176 5.4 0.0292 Mg 75.3 2.6 2.5 29.91 0.0409 2.6 0.0112 Sr 31.8 2.8 14.3 2.23 0.0025 2.8 0.0402 P 31.9 4.0 2.4 13.55 0.0380 4.0 0.0399 K 25.2 4.5 5.1 4.93 0.0185 4.5 0.0191 Cl 75.3 2.1 2.2 34.22 0.0162 2.1 0.0229 Ca 2969.2 0.4 17.7 168.22 0.6563 0.5 0.0338 Ba 9.8 5.0 10.8 0.91 0.0000 5.0 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0564 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0634 Elt. k-ratio Correc. Na 0.0009 2.3308 Mg 0.0030 1.6995 Sr 0.0016 1.3790 P 0.0060 1.2004 K 0.0016 1.0444 Cl 0.0090 1.1247 Ca 0.2382 1.1007 Ba 0.0000 NaN Fe 0.0001 1.2590 Mn 0.0002 1.2807 iteration : 2 Analysis no. 373 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2049 0.015390 0.2049 0.1617 Mg 0.5035 0.013733 0.5035 0.3759 Sr 0.2149 0.013159 0.2149 0.0445 P 0.7161 0.031924 0.7161 0.4194 K 0.1718 0.010549 0.1718 0.0797 Cl 1.0117 0.022334 1.0117 0.5177 Ca 26.2164 0.128903 26.2164 11.8672 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0084 0.013957 0.0084 0.0027 Mn 0.0198 0.019990 0.0198 0.0065 C 16.1794 16.1794 24.4391 O 54.7529 54.7529 62.0855 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 374 x= -15703.0 y= 3010.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 42.9 3.4 3.6 11.83 0.0508 3.4 0.0289 Mg 141.7 1.9 2.5 56.28 0.0783 1.9 0.0111 Sr 41.1 2.5 14.3 2.88 0.0038 2.5 0.0401 P 38.1 3.6 2.4 16.21 0.0461 3.6 0.0398 K 32.2 3.9 5.1 6.30 0.0250 4.0 0.0190 Cl 105.2 1.8 2.2 47.81 0.0228 1.8 0.0228 Ca 3216.1 0.4 17.7 182.20 0.7112 0.5 0.0337 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0632 Elt. k-ratio Correc. Na 0.0025 2.3109 Mg 0.0057 1.6950 Sr 0.0024 1.3780 P 0.0072 1.1995 K 0.0022 1.0406 Cl 0.0127 1.1217 Ca 0.2581 1.0975 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2765 iteration : 3 Analysis no. 374 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5858 0.022868 0.5858 0.4754 Mg 0.9603 0.018761 0.9603 0.7372 Sr 0.3277 0.014418 0.3277 0.0698 P 0.8671 0.034738 0.8671 0.5223 K 0.2309 0.011670 0.2309 0.1102 Cl 1.4220 0.026268 1.4220 0.7484 Ca 28.3279 0.135376 28.3279 13.1876 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0417 0.020905 0.0417 0.0142 C 14.7846 14.7846 22.9672 O 52.4520 52.4520 61.1677 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 375 x= -15703.0 y= 3015.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.8 5.3 3.6 4.91 0.0183 5.3 0.0291 Mg 77.1 2.5 2.5 30.63 0.0419 2.6 0.0112 Sr 29.0 2.9 14.3 2.03 0.0021 2.9 0.0402 P 34.2 3.8 2.4 14.55 0.0411 3.8 0.0399 K 28.9 4.2 5.1 5.67 0.0220 4.2 0.0192 Cl 95.5 1.9 2.2 43.41 0.0206 1.9 0.0229 Ca 2788.8 0.4 17.7 158.00 0.6162 0.5 0.0339 Ba 8.3 5.5 10.8 0.77 0.0000 5.5 0.0000 Fe 2.9 9.3 3.3 0.88 0.0000 9.3 0.0000 Mn 2.5 14.1 2.7 0.92 0.0000 14.1 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3275 Mg 0.0030 1.6983 Sr 0.0013 1.3799 P 0.0064 1.2013 K 0.0020 1.0523 Cl 0.0115 1.1280 Ca 0.2236 1.1033 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 375 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2129 0.015571 0.2129 0.1663 Mg 0.5156 0.013883 0.5156 0.3809 Sr 0.1807 0.012758 0.1807 0.0370 P 0.7737 0.033044 0.7737 0.4485 K 0.2055 0.011272 0.2055 0.0943 Cl 1.2955 0.025182 1.2955 0.6561 Ca 24.6741 0.124122 24.6741 11.0526 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 16.6739 16.6739 24.9234 O 55.4681 55.4681 62.2409 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 376 x= -15702.0 y= 3020.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 21.0 4.9 3.6 5.78 0.0224 4.9 0.0291 Mg 86.8 2.4 2.5 34.46 0.0474 2.4 0.0112 Sr 28.9 2.9 14.3 2.03 0.0021 3.0 0.0402 P 42.8 3.4 2.4 18.19 0.0521 3.4 0.0399 K 30.2 4.1 5.1 5.92 0.0232 4.1 0.0192 Cl 76.9 2.1 2.2 34.95 0.0165 2.1 0.0229 Ca 2788.9 0.4 17.7 158.01 0.6162 0.5 0.0339 Ba 10.1 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0564 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0635 Elt. k-ratio Correc. Na 0.0011 2.3268 Mg 0.0034 1.6988 Sr 0.0013 1.3806 P 0.0082 1.2021 K 0.0021 1.0519 Cl 0.0092 1.1293 Ca 0.2236 1.1031 Ba 0.0000 NaN Fe 0.0000 1.2604 Mn 0.0002 1.2817 iteration : 2 Analysis no. 376 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2601 0.016678 0.2601 0.2033 Mg 0.5825 0.014718 0.5825 0.4306 Sr 0.1796 0.012751 0.1796 0.0368 P 0.9820 0.036798 0.9820 0.5696 K 0.2166 0.011482 0.2166 0.0995 Cl 1.0381 0.022657 1.0381 0.5261 Ca 24.6711 0.124104 24.6711 11.0591 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0059 0.013895 0.0059 0.0019 Mn 0.0198 0.020007 0.0198 0.0065 C 16.5391 16.5391 24.7397 O 55.5050 55.5050 62.3268 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 377 x= -15702.0 y= 3025.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.9 4.9 3.6 5.76 0.0223 4.9 0.0291 Mg 81.5 2.5 2.5 32.37 0.0444 2.5 0.0112 Sr 26.3 3.1 14.3 1.84 0.0017 3.1 0.0402 P 44.3 3.4 2.4 18.83 0.0540 3.4 0.0399 K 28.0 4.2 5.1 5.48 0.0211 4.2 0.0193 Cl 85.7 2.0 2.2 38.94 0.0185 2.0 0.0230 Ca 2696.1 0.4 17.7 152.74 0.5956 0.5 0.0339 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0635 Elt. k-ratio Correc. Na 0.0011 2.3264 Mg 0.0032 1.6988 Sr 0.0011 1.3810 P 0.0085 1.2024 K 0.0019 1.0557 Cl 0.0103 1.1309 Ca 0.2162 1.1044 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2825 iteration : 2 Analysis no. 377 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2593 0.016659 0.2593 0.2015 Mg 0.5462 0.014272 0.5462 0.4013 Sr 0.1475 0.012358 0.1475 0.0301 P 1.0188 0.037427 1.0188 0.5874 K 0.1979 0.011149 0.1979 0.0904 Cl 1.1618 0.023929 1.1618 0.5852 Ca 23.8727 0.121601 23.8727 10.6367 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0254 0.020269 0.0254 0.0082 C 16.8283 16.8283 25.0204 O 55.9422 55.9422 62.4388 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 378 x= -15702.0 y= 3030.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 47.7 3.2 3.6 13.15 0.0570 3.3 0.0289 Mg 145.4 1.9 2.5 57.75 0.0803 1.9 0.0111 Sr 38.6 2.5 14.3 2.70 0.0035 2.6 0.0402 P 50.4 3.1 2.4 21.45 0.0620 3.2 0.0399 K 29.7 4.1 5.1 5.82 0.0227 4.1 0.0192 Cl 99.3 1.8 2.2 45.13 0.0215 1.8 0.0229 Ca 2902.5 0.4 17.7 164.44 0.6415 0.5 0.0339 Ba 9.2 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0633 Elt. k-ratio Correc. Na 0.0028 2.3084 Mg 0.0058 1.6959 Sr 0.0022 1.3812 P 0.0097 1.2028 K 0.0020 1.0517 Cl 0.0119 1.1291 Ca 0.2328 1.1015 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2788 iteration : 3 Analysis no. 378 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6567 0.024011 0.6567 0.5220 Mg 0.9864 0.019017 0.9864 0.7417 Sr 0.2981 0.014121 0.2981 0.0622 P 1.1687 0.039889 1.1687 0.6896 K 0.2122 0.011398 0.2122 0.0992 Cl 1.3492 0.025694 1.3492 0.6955 Ca 25.6441 0.127131 25.6441 11.6935 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0326 0.020540 0.0326 0.0108 C 15.6172 15.6172 23.7634 O 54.0348 54.0348 61.7220 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 379 x= -15701.0 y= 3035.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 27.3 4.3 3.6 7.51 0.0305 4.3 0.0292 Mg 65.5 2.8 2.5 26.02 0.0354 2.8 0.0112 Sr 20.5 3.5 14.3 1.44 0.0009 3.5 0.0403 P 49.8 3.2 2.4 21.17 0.0611 3.2 0.0401 K 30.4 4.1 5.1 5.96 0.0234 4.1 0.0195 Cl 70.7 2.2 2.2 32.15 0.0152 2.2 0.0231 Ca 2359.5 0.5 17.7 133.68 0.5208 0.5 0.0341 Ba 7.8 5.7 10.8 0.72 0.0000 5.7 0.0000 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0567 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0637 Elt. k-ratio Correc. Na 0.0015 2.3291 Mg 0.0026 1.7032 Sr 0.0006 1.3849 P 0.0096 1.2060 K 0.0021 1.0670 Cl 0.0084 1.1381 Ca 0.1890 1.1088 Ba 0.0000 NaN Fe 0.0001 1.2653 Mn 0.0001 1.2856 iteration : 2 Analysis no. 379 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3551 0.018730 0.3551 0.2692 Mg 0.4367 0.012855 0.4367 0.3131 Sr 0.0768 0.011473 0.0768 0.0153 P 1.1560 0.039742 1.1560 0.6505 K 0.2214 0.011680 0.2214 0.0987 Cl 0.9602 0.021922 0.9602 0.4720 Ca 20.9560 0.112276 20.9560 9.1126 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0178 0.014305 0.0178 0.0056 Mn 0.0144 0.019813 0.0144 0.0046 C 17.9258 17.9258 26.0111 O 57.8798 57.8798 63.0474 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 380 x= -15701.0 y= 3040.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 36.7 3.7 3.6 10.11 0.0427 3.7 0.0290 Mg 108.1 2.1 2.5 42.93 0.0593 2.2 0.0111 Sr 36.5 2.6 14.3 2.55 0.0032 2.6 0.0402 P 57.4 2.9 2.4 24.43 0.0710 3.0 0.0399 K 26.8 4.3 5.1 5.26 0.0201 4.3 0.0191 Cl 77.9 2.1 2.2 35.42 0.0167 2.1 0.0229 Ca 2987.0 0.4 17.7 169.23 0.6603 0.5 0.0338 Ba 10.2 4.9 10.8 0.95 0.0000 4.9 0.0000 Fe 3.0 9.2 3.3 0.89 0.0000 9.2 0.0000 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0634 Elt. k-ratio Correc. Na 0.0021 2.3160 Mg 0.0043 1.6967 Sr 0.0020 1.3787 P 0.0111 1.2008 K 0.0018 1.0473 Cl 0.0093 1.1278 Ca 0.2396 1.1004 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2789 iteration : 3 Analysis no. 380 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4936 0.021303 0.4936 0.3934 Mg 0.7290 0.016394 0.7290 0.5495 Sr 0.2715 0.013806 0.2715 0.0568 P 1.3368 0.042449 1.3368 0.7907 K 0.1864 0.010864 0.1864 0.0874 Cl 1.0511 0.022776 1.0511 0.5431 Ca 26.3691 0.129374 26.3691 12.0532 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0216 0.020046 0.0216 0.0072 C 15.4956 15.4956 23.6355 O 54.0451 54.0451 61.8832 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 381 x= -15701.0 y= 3045.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.5 3.8 3.6 9.77 0.0411 3.8 0.0290 Mg 97.7 2.3 2.5 38.81 0.0535 2.3 0.0111 Sr 33.5 2.7 14.3 2.35 0.0028 2.7 0.0402 P 67.8 2.7 2.4 28.86 0.0844 2.7 0.0400 K 31.9 4.0 5.1 6.26 0.0248 4.0 0.0193 Cl 76.1 2.1 2.2 34.61 0.0164 2.1 0.0231 Ca 2687.0 0.4 17.7 152.23 0.5936 0.5 0.0339 Ba 9.6 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.1 9.0 3.3 0.94 0.0000 9.0 0.0000 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0635 Elt. k-ratio Correc. Na 0.0021 2.3159 Mg 0.0039 1.6971 Sr 0.0017 1.3806 P 0.0132 1.2032 K 0.0022 1.0582 Cl 0.0091 1.1343 Ca 0.2154 1.1045 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2812 iteration : 2 Analysis no. 381 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4757 0.020978 0.4757 0.3716 Mg 0.6576 0.015596 0.6576 0.4859 Sr 0.2357 0.013414 0.2357 0.0483 P 1.5926 0.046192 1.5926 0.9234 K 0.2326 0.011827 0.2326 0.1069 Cl 1.0324 0.022651 1.0324 0.5230 Ca 23.7926 0.121345 23.7926 10.6606 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0125 0.019660 0.0125 0.0041 C 16.3620 16.3620 24.4638 O 55.6062 55.6062 62.4126 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 382 x= -15700.0 y= 3050.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 48.1 3.2 3.6 13.25 0.0574 3.2 0.0289 Mg 130.1 2.0 2.5 51.65 0.0717 2.0 0.0111 Sr 35.4 2.7 14.3 2.48 0.0030 2.7 0.0403 P 68.4 2.7 2.4 29.09 0.0852 2.7 0.0400 K 31.9 4.0 5.1 6.25 0.0247 4.0 0.0194 Cl 90.0 1.9 2.2 40.92 0.0194 1.9 0.0231 Ca 2643.9 0.4 17.7 149.79 0.5841 0.5 0.0340 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 4.1 7.8 3.3 1.23 0.0004 7.8 0.0564 Mn 2.3 14.9 2.7 0.83 0.0000 14.9 0.0000 Elt. k-ratio Correc. Na 0.0029 2.3079 Mg 0.0052 1.6964 Sr 0.0019 1.3823 P 0.0134 1.2046 K 0.0022 1.0612 Cl 0.0108 1.1356 Ca 0.2120 1.1050 Ba 0.0000 NaN Fe 0.0002 1.2596 Mn 0.0000 NaN iteration : 2 Analysis no. 382 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6619 0.024093 0.6619 0.5175 Mg 0.8808 0.017985 0.8808 0.6514 Sr 0.2597 0.013704 0.2597 0.0533 P 1.6082 0.046442 1.6082 0.9333 K 0.2329 0.011856 0.2329 0.1071 Cl 1.2280 0.024629 1.2280 0.6226 Ca 23.4237 0.120188 23.4237 10.5055 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0262 0.014492 0.0262 0.0084 Mn 0.0000 0.000000 0.0000 0.0000 C 16.2697 16.2697 24.3493 O 55.4090 55.4090 62.2515 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 383 x= -15700.0 y= 3054.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 46.4 3.3 3.6 12.78 0.0552 3.3 0.0289 Mg 123.3 2.0 2.5 48.95 0.0679 2.0 0.0111 Sr 36.3 2.6 14.3 2.54 0.0032 2.6 0.0402 P 71.3 2.6 2.4 30.35 0.0889 2.7 0.0400 K 34.5 3.8 5.1 6.76 0.0271 3.8 0.0194 Cl 86.2 2.0 2.2 39.16 0.0186 2.0 0.0231 Ca 2648.7 0.4 17.7 150.06 0.5851 0.5 0.0340 Ba 10.7 4.8 10.8 0.99 0.0000 4.8 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0564 Mn 2.9 13.1 2.7 1.07 0.0002 13.1 0.0635 Elt. k-ratio Correc. Na 0.0028 2.3084 Mg 0.0049 1.6961 Sr 0.0020 1.3817 P 0.0139 1.2043 K 0.0024 1.0610 Cl 0.0103 1.1358 Ca 0.2123 1.1050 Ba 0.0000 NaN Fe 0.0001 1.2595 Mn 0.0001 1.2807 iteration : 2 Analysis no. 383 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6366 0.023689 0.6366 0.4979 Mg 0.8335 0.017501 0.8335 0.6166 Sr 0.2697 0.013810 0.2697 0.0553 P 1.6794 0.047414 1.6794 0.9750 K 0.2555 0.012265 0.2555 0.1175 Cl 1.1738 0.024101 1.1738 0.5953 Ca 23.4630 0.120307 23.4630 10.5262 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0084 0.013964 0.0084 0.0027 Mn 0.0070 0.019396 0.0070 0.0023 C 16.2453 16.2453 24.3202 O 55.4277 55.4277 62.2909 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 384 x= -15700.0 y= 3059.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 47.7 3.2 3.6 13.14 0.0569 3.3 0.0289 Mg 121.8 2.0 2.5 48.35 0.0670 2.1 0.0111 Sr 34.3 2.7 14.3 2.40 0.0029 2.7 0.0403 P 69.4 2.7 2.4 29.52 0.0864 2.7 0.0400 K 32.5 3.9 5.1 6.37 0.0253 3.9 0.0194 Cl 89.6 1.9 2.2 40.71 0.0193 1.9 0.0231 Ca 2614.2 0.4 17.7 148.10 0.5774 0.5 0.0340 Ba 11.0 4.8 10.8 1.02 0.0002 4.8 0.0751 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0564 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0635 Elt. k-ratio Correc. Na 0.0028 2.3087 Mg 0.0049 1.6969 Sr 0.0018 1.3823 P 0.0136 1.2046 K 0.0022 1.0622 Cl 0.0108 1.1361 Ca 0.2096 1.1054 Ba 0.0000 1.5334 Fe 0.0000 1.2600 Mn 0.0002 1.2811 iteration : 2 Analysis no. 384 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6561 0.024003 0.6561 0.5118 Mg 0.8235 0.017402 0.8235 0.6076 Sr 0.2455 0.013540 0.2455 0.0503 P 1.6323 0.046772 1.6323 0.9450 K 0.2388 0.011969 0.2388 0.1095 Cl 1.2218 0.024573 1.2218 0.6180 Ca 23.1642 0.119359 23.1642 10.3645 Ba 0.0065 0.019289 0.0065 0.0009 Fe 0.0042 0.013840 0.0042 0.0014 Mn 0.0198 0.019998 0.0198 0.0065 C 16.3844 16.3844 24.4631 O 55.6029 55.6029 62.3215 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 385 x= -15699.0 y= 3064.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 30.9 4.0 3.6 8.52 0.0353 4.0 0.0291 Mg 73.6 2.6 2.5 29.24 0.0400 2.6 0.0112 Sr 20.0 3.5 14.3 1.40 0.0008 3.5 0.0408 P 33.9 3.8 2.4 14.41 0.0406 3.9 0.0406 K 14.5 5.9 5.1 2.84 0.0087 5.9 0.0206 Cl 124.1 1.6 2.2 56.39 0.0269 1.6 0.0237 Ca 912.8 0.7 17.7 51.71 0.1991 0.8 0.0347 Ba 8.1 5.6 10.8 0.75 0.0000 5.6 0.0000 Fe 2.0 11.2 3.3 0.60 0.0000 11.3 0.0000 Mn 1.7 17.1 2.7 0.63 0.0000 17.2 0.0000 Elt. k-ratio Correc. Na 0.0018 2.3269 Mg 0.0029 1.7075 Sr 0.0005 1.4009 P 0.0064 1.2231 K 0.0008 1.1275 Cl 0.0150 1.1674 Ca 0.0722 1.1290 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 385 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4096 0.019799 0.4096 0.2823 Mg 0.4941 0.013644 0.4941 0.3222 Sr 0.0709 0.011514 0.0709 0.0128 P 0.7791 0.033478 0.7791 0.3986 K 0.0869 0.009160 0.0869 0.0352 Cl 1.7511 0.029674 1.7511 0.7827 Ca 8.1559 0.065802 8.1559 3.2248 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 22.8936 22.8936 30.2059 O 65.3588 65.3588 64.7354 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 386 x= -15699.0 y= 3069.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 10.4 6.9 3.6 2.85 0.0087 7.0 0.0295 Mg 8.8 7.5 2.5 3.49 0.0035 7.5 0.0113 Sr 9.8 5.1 14.3 0.68 0.0000 5.1 0.0000 P 2.6 14.0 2.4 1.09 0.0003 14.0 0.0411 K 5.4 9.7 5.1 1.05 0.0002 9.7 0.0213 Cl 86.8 2.0 2.2 39.44 0.0187 2.0 0.0241 Ca 39.0 3.6 17.7 2.21 0.0047 3.6 0.0351 Ba 6.7 6.1 10.8 0.62 0.0000 6.1 0.0000 Fe 2.1 11.0 3.3 0.63 0.0000 11.0 0.0000 Mn 1.6 17.7 2.7 0.59 0.0000 17.7 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3576 Mg 0.0003 1.7213 Sr 0.0000 NaN P 0.0000 1.2358 K 0.0000 1.1673 Cl 0.0104 1.1864 Ca 0.0017 1.1415 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 386 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1023 0.012728 0.1023 0.0659 Mg 0.0440 0.005272 0.0440 0.0268 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0050 0.012370 0.0050 0.0024 K 0.0024 0.006922 0.0024 0.0009 Cl 1.2352 0.025267 1.2352 0.5157 Ca 0.1963 0.015510 0.1963 0.0725 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8935 26.8935 33.1450 O 71.5213 71.5213 66.1708 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 387 x= -15699.0 y= 3074.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 15.9 5.6 3.6 4.37 0.0158 5.6 0.0294 Mg 14.0 6.0 2.5 5.56 0.0065 6.0 0.0113 Sr 10.8 4.8 14.3 0.76 0.0000 4.8 0.0000 P 2.3 14.9 2.4 0.96 0.0000 14.9 0.0000 K 5.9 9.2 5.1 1.16 0.0007 9.2 0.0213 Cl 125.5 1.6 2.2 57.04 0.0273 1.6 0.0241 Ca 30.0 4.1 17.7 1.70 0.0027 4.1 0.0351 Ba 6.4 6.2 10.8 0.60 0.0000 6.3 0.0000 Fe 2.1 11.0 3.3 0.63 0.0000 11.0 0.0000 Mn 1.2 20.8 2.7 0.42 0.0000 20.9 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3497 Mg 0.0005 1.7185 Sr 0.0000 NaN P 0.0000 NaN K 0.0001 1.1686 Cl 0.0152 1.1856 Ca 0.0010 1.1420 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 387 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1853 0.014982 0.1853 0.1197 Mg 0.0803 0.006361 0.0803 0.0491 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0077 0.007109 0.0077 0.0029 Cl 1.7993 0.030308 1.7993 0.7537 Ca 0.1134 0.014221 0.1134 0.0420 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7604 26.7604 33.0857 O 71.0536 71.0536 65.9470 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 388 x= -15698.0 y= 3079.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 9.5 7.3 3.6 2.61 0.0075 7.3 0.0294 Mg 12.8 6.2 2.5 5.08 0.0058 6.3 0.0113 Sr 11.4 4.7 14.3 0.79 0.0000 4.7 0.0000 P 1.3 20.0 2.4 0.53 0.0000 20.0 0.0000 K 5.4 9.6 5.1 1.06 0.0003 9.6 0.0213 Cl 157.1 1.5 2.2 71.41 0.0343 1.5 0.0241 Ca 26.3 4.4 17.7 1.49 0.0019 4.4 0.0351 Ba 6.1 6.4 10.8 0.57 0.0000 6.4 0.0000 Fe 2.2 10.8 3.3 0.65 0.0000 10.8 0.0000 Mn 2.0 16.0 2.7 0.72 0.0000 16.0 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3465 Mg 0.0004 1.7145 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1695 Cl 0.0191 1.1847 Ca 0.0007 1.1423 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 388 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0882 0.012251 0.0882 0.0571 Mg 0.0718 0.006111 0.0718 0.0439 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0029 0.006952 0.0029 0.0011 Cl 2.2591 0.033890 2.2591 0.9481 Ca 0.0798 0.013670 0.0798 0.0296 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7173 26.7173 33.0972 O 70.7811 70.7811 65.8230 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 389 x= -15698.0 y= 3084.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 9.4 7.3 3.6 2.59 0.0075 7.3 0.0295 Mg 11.2 6.7 2.5 4.43 0.0049 6.7 0.0113 Sr 10.8 4.8 14.3 0.76 0.0000 4.8 0.0000 P 1.6 17.9 2.4 0.66 0.0000 18.0 0.0000 K 4.9 10.1 5.1 0.95 0.0000 10.2 0.0000 Cl 107.6 1.8 2.2 48.92 0.0233 1.8 0.0241 Ca 23.9 4.6 17.7 1.35 0.0014 4.6 0.0351 Ba 7.1 5.9 10.8 0.66 0.0000 5.9 0.0000 Fe 1.8 11.8 3.3 0.55 0.0000 11.8 0.0000 Mn 1.8 16.9 2.7 0.65 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3545 Mg 0.0004 1.7192 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0130 1.1862 Ca 0.0005 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 389 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0877 0.012268 0.0877 0.0565 Mg 0.0604 0.005787 0.0604 0.0368 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.5394 0.028095 1.5394 0.6432 Ca 0.0571 0.013276 0.0571 0.0211 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8842 26.8842 33.1592 O 71.3711 71.3711 66.0831 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 390 x= -15698.0 y= 3089.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 12.4 6.4 3.6 3.41 0.0113 6.4 0.0296 Mg 13.0 6.2 2.5 5.14 0.0059 6.2 0.0113 Sr 11.8 4.6 14.3 0.83 0.0000 4.6 0.0000 P 1.0 22.3 2.4 0.43 0.0000 22.4 0.0000 K 6.3 8.9 5.1 1.23 0.0011 8.9 0.0213 Cl 47.7 2.6 2.2 21.69 0.0101 2.6 0.0241 Ca 17.8 5.3 17.7 1.01 0.0000 5.3 0.0351 Ba 5.8 6.5 10.8 0.54 0.0000 6.6 0.0000 Fe 2.1 10.9 3.3 0.64 0.0000 10.9 0.0000 Mn 1.6 17.9 2.7 0.57 0.0000 18.0 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3631 Mg 0.0004 1.7252 Sr 0.0000 NaN P 0.0000 NaN K 0.0001 1.1676 Cl 0.0056 1.1882 Ca 0.0000 1.1415 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 390 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1330 0.013640 0.1330 0.0853 Mg 0.0732 0.006179 0.0732 0.0444 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0110 0.007215 0.0110 0.0042 Cl 0.6657 0.018910 0.6657 0.2768 Ca 0.0009 0.012256 0.0009 0.0003 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0642 27.0642 33.2126 O 72.0518 72.0518 66.3764 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 391 x= -15697.0 y= 3094.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 9.5 7.2 3.6 2.62 0.0076 7.3 0.0295 Mg 9.1 7.4 2.5 3.61 0.0037 7.4 0.0113 Sr 10.4 4.9 14.3 0.73 0.0000 4.9 0.0000 P 1.5 18.2 2.4 0.64 0.0000 18.3 0.0000 K 5.0 10.0 5.1 0.97 0.0000 10.1 0.0000 Cl 99.9 1.8 2.2 45.41 0.0216 1.8 0.0241 Ca 17.5 5.3 17.7 0.99 0.0000 5.4 0.0000 Ba 6.3 6.3 10.8 0.59 0.0000 6.3 0.0000 Fe 2.0 11.3 3.3 0.59 0.0000 11.3 0.0000 Mn 1.4 19.2 2.7 0.50 0.0000 19.2 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3559 Mg 0.0003 1.7201 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0120 1.1866 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 391 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0893 0.012324 0.0893 0.0575 Mg 0.0461 0.005338 0.0461 0.0281 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.4274 0.027092 1.4274 0.5958 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9356 26.9356 33.1866 O 71.5016 71.5016 66.1321 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 392 x= -15697.0 y= 3099.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 11.6 6.6 3.6 3.18 0.0102 6.6 0.0296 Mg 13.5 6.1 2.5 5.34 0.0061 6.1 0.0113 Sr 12.2 4.5 14.3 0.85 0.0000 4.5 0.0000 P 1.7 17.4 2.4 0.70 0.0000 17.4 0.0000 K 4.5 10.6 5.1 0.87 0.0000 10.6 0.0000 Cl 48.2 2.6 2.2 21.92 0.0102 2.6 0.0241 Ca 17.3 5.4 17.7 0.98 0.0000 5.4 0.0000 Ba 6.5 6.2 10.8 0.61 0.0000 6.2 0.0000 Fe 1.4 13.2 3.3 0.43 0.0000 13.3 0.0000 Mn 1.6 17.7 2.7 0.59 0.0000 17.7 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3632 Mg 0.0004 1.7250 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0057 1.1882 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 392 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1208 0.013294 0.1208 0.0775 Mg 0.0767 0.006277 0.0767 0.0465 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.6731 0.019005 0.6731 0.2798 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0696 27.0696 33.2169 O 72.0598 72.0598 66.3792 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 393 x= -15697.0 y= 3104.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 10.6 6.9 3.6 2.92 0.0090 6.9 0.0295 Mg 12.1 6.4 2.5 4.81 0.0054 6.4 0.0113 Sr 11.1 4.7 14.3 0.78 0.0000 4.7 0.0000 P 2.0 15.8 2.4 0.85 0.0000 15.8 0.0000 K 5.1 9.9 5.1 0.99 0.0000 10.0 0.0000 Cl 106.0 1.8 2.2 48.18 0.0230 1.8 0.0241 Ca 12.7 6.3 17.7 0.72 0.0000 6.3 0.0000 Ba 6.0 6.5 10.8 0.56 0.0000 6.5 0.0000 Fe 2.0 11.2 3.3 0.61 0.0000 11.2 0.0000 Mn 1.8 16.9 2.7 0.65 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3544 Mg 0.0004 1.7195 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0128 1.1865 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 393 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1060 0.012824 0.1060 0.0683 Mg 0.0671 0.005988 0.0671 0.0409 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.5161 0.027894 1.5161 0.6332 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9013 26.9013 33.1664 O 71.4096 71.4096 66.0912 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 394 x= -15696.0 y= 3109.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 9.9 7.1 3.6 2.72 0.0080 7.1 0.0296 Mg 12.4 6.3 2.5 4.92 0.0056 6.4 0.0113 Sr 10.0 5.0 14.3 0.70 0.0000 5.0 0.0000 P 1.7 17.4 2.4 0.70 0.0000 17.4 0.0000 K 5.0 10.0 5.1 0.98 0.0000 10.0 0.0000 Cl 61.3 2.3 2.2 27.86 0.0131 2.3 0.0242 Ca 19.9 5.0 17.7 1.12 0.0005 5.0 0.0351 Ba 5.8 6.6 10.8 0.54 0.0000 6.6 0.0000 Fe 1.6 12.5 3.3 0.48 0.0000 12.5 0.0000 Mn 1.4 18.9 2.7 0.52 0.0000 18.9 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3616 Mg 0.0004 1.7235 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0073 1.1877 Ca 0.0002 1.1416 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 394 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0949 0.012521 0.0949 0.0609 Mg 0.0693 0.006064 0.0693 0.0421 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.8643 0.021343 0.8643 0.3597 Ca 0.0203 0.012620 0.0203 0.0075 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0343 27.0343 33.2099 O 71.9169 71.9169 66.3200 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 395 x= -15696.0 y= 3113.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 11.4 6.6 3.6 3.13 0.0100 6.6 0.0296 Mg 13.4 6.1 2.5 5.32 0.0061 6.1 0.0113 Sr 11.5 4.7 14.3 0.80 0.0000 4.7 0.0000 P 1.6 17.9 2.4 0.66 0.0000 18.0 0.0000 K 4.7 10.4 5.1 0.91 0.0000 10.4 0.0000 Cl 62.9 2.3 2.2 28.60 0.0134 2.3 0.0242 Ca 16.3 5.5 17.7 0.92 0.0000 5.6 0.0000 Ba 7.1 5.9 10.8 0.66 0.0000 5.9 0.0000 Fe 2.3 10.4 3.3 0.70 0.0000 10.4 0.0000 Mn 1.4 18.9 2.7 0.52 0.0000 18.9 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3609 Mg 0.0004 1.7236 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0075 1.1878 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 395 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1177 0.013199 0.1177 0.0756 Mg 0.0764 0.006265 0.0764 0.0464 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.8884 0.021621 0.8884 0.3698 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0254 27.0254 33.2030 O 71.8922 71.8922 66.3053 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 396 x= -15696.0 y= 3118.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 13.5 6.1 3.6 3.71 0.0127 6.1 0.0294 Mg 15.4 5.7 2.5 6.12 0.0072 5.7 0.0113 Sr 11.0 4.8 14.3 0.77 0.0000 4.8 0.0000 P 2.4 14.6 2.4 1.00 0.0000 14.6 0.0000 K 4.7 10.4 5.1 0.91 0.0000 10.4 0.0000 Cl 118.8 1.7 2.2 53.99 0.0258 1.7 0.0241 Ca 17.3 5.4 17.7 0.98 0.0000 5.4 0.0000 Ba 6.7 6.1 10.8 0.62 0.0000 6.1 0.0000 Fe 1.9 11.6 3.3 0.56 0.0000 11.6 0.0000 Mn 1.7 17.4 2.7 0.61 0.0000 17.4 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3513 Mg 0.0005 1.7187 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0143 1.1861 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 396 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1491 0.014034 0.1491 0.0961 Mg 0.0901 0.006626 0.0901 0.0550 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.7021 0.029503 1.7021 0.7119 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8357 26.8357 33.1300 O 71.2231 71.2231 66.0070 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 397 x= -15695.0 y= 3123.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 10.0 7.1 3.6 2.74 0.0082 7.1 0.0296 Mg 9.4 7.3 2.5 3.71 0.0038 7.3 0.0113 Sr 11.1 4.7 14.3 0.78 0.0000 4.8 0.0000 P 2.0 16.0 2.4 0.83 0.0000 16.0 0.0000 K 3.8 11.5 5.1 0.75 0.0000 11.5 0.0000 Cl 65.0 2.3 2.2 29.55 0.0139 2.3 0.0242 Ca 12.9 6.2 17.7 0.73 0.0000 6.2 0.0000 Ba 6.7 6.1 10.8 0.62 0.0000 6.1 0.0000 Fe 1.9 11.5 3.3 0.57 0.0000 11.6 0.0000 Mn 1.0 22.3 2.7 0.37 0.0000 22.4 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3613 Mg 0.0003 1.7234 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0077 1.1877 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 397 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0964 0.012573 0.0964 0.0619 Mg 0.0480 0.005410 0.0480 0.0291 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.9189 0.021971 0.9189 0.3825 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0396 27.0396 33.2192 O 71.8971 71.8971 66.3073 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 398 x= -15695.0 y= 3128.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.6 5.8 3.6 4.03 0.0142 5.9 0.0294 Mg 13.3 6.1 2.5 5.28 0.0061 6.1 0.0113 Sr 11.3 4.7 14.3 0.79 0.0000 4.7 0.0000 P 2.7 13.6 2.4 1.15 0.0005 13.6 0.0410 K 5.5 9.6 5.1 1.07 0.0003 9.6 0.0214 Cl 145.3 1.5 2.2 66.05 0.0317 1.5 0.0241 Ca 16.2 5.6 17.7 0.92 0.0000 5.6 0.0000 Ba 7.0 6.0 10.8 0.65 0.0000 6.0 0.0000 Fe 2.2 10.6 3.3 0.67 0.0000 10.7 0.0000 Mn 1.7 17.1 2.7 0.63 0.0000 17.2 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3469 Mg 0.0004 1.7165 Sr 0.0000 NaN P 0.0001 1.2334 K 0.0000 1.1697 Cl 0.0176 1.1853 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 398 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1664 0.014489 0.1664 0.1076 Mg 0.0754 0.006223 0.0754 0.0461 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0087 0.012544 0.0087 0.0042 K 0.0034 0.006976 0.0034 0.0013 Cl 2.0901 0.032637 2.0901 0.8762 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7474 26.7474 33.0973 O 70.9087 70.9087 65.8674 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 399 x= -15695.0 y= 3133.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 16.5 5.5 3.6 4.55 0.0166 5.5 0.0294 Mg 11.7 6.5 2.5 4.65 0.0052 6.5 0.0113 Sr 10.1 5.0 14.3 0.71 0.0000 5.0 0.0000 P 2.4 14.4 2.4 1.02 0.0001 14.4 0.0410 K 4.9 10.1 5.1 0.96 0.0000 10.1 0.0000 Cl 123.0 1.6 2.2 55.89 0.0267 1.6 0.0241 Ca 15.3 5.7 17.7 0.87 0.0000 5.7 0.0000 Ba 5.9 6.5 10.8 0.55 0.0000 6.5 0.0000 Fe 1.6 12.6 3.3 0.48 0.0000 12.6 0.0000 Mn 1.8 16.9 2.7 0.65 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3502 Mg 0.0004 1.7190 Sr 0.0000 NaN P 0.0000 1.2346 K 0.0000 NaN Cl 0.0149 1.1860 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 399 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1953 0.015239 0.1953 0.1260 Mg 0.0643 0.005904 0.0643 0.0392 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0012 0.012168 0.0012 0.0006 K 0.0000 0.000000 0.0000 0.0000 Cl 1.7633 0.030020 1.7633 0.7378 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8166 26.8166 33.1205 O 71.1592 71.1592 65.9758 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 400 x= -15694.0 y= 3138.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 22.9 4.7 3.6 6.31 0.0249 4.7 0.0294 Mg 10.8 6.8 2.5 4.29 0.0047 6.8 0.0113 Sr 10.3 4.9 14.3 0.72 0.0000 4.9 0.0000 P 3.3 12.3 2.4 1.40 0.0012 12.3 0.0411 K 5.5 9.5 5.1 1.08 0.0004 9.5 0.0214 Cl 118.8 1.7 2.2 53.99 0.0258 1.7 0.0241 Ca 13.4 6.1 17.7 0.76 0.0000 6.1 0.0000 Ba 7.1 5.9 10.8 0.66 0.0000 5.9 0.0000 Fe 1.9 11.5 3.3 0.57 0.0000 11.6 0.0000 Mn 2.0 16.0 2.7 0.72 0.0000 16.0 0.0000 Elt. k-ratio Correc. Na 0.0012 2.3491 Mg 0.0003 1.7205 Sr 0.0000 NaN P 0.0002 1.2349 K 0.0000 1.1691 Cl 0.0144 1.1862 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 400 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2924 0.017511 0.2924 0.1887 Mg 0.0580 0.005720 0.0580 0.0354 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0237 0.013281 0.0237 0.0114 K 0.0038 0.006986 0.0038 0.0015 Cl 1.7034 0.029526 1.7034 0.7129 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7811 26.7811 33.0826 O 71.1375 71.1375 65.9676 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 401 x= -15694.0 y= 3143.0 z= -279. carb2 left trav 1 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 28.8 4.2 3.6 7.93 0.0325 4.2 0.0295 Mg 15.7 5.6 2.5 6.23 0.0074 5.7 0.0113 Sr 11.1 4.8 14.3 0.77 0.0000 4.8 0.0000 P 7.5 8.2 2.4 3.17 0.0066 8.2 0.0411 K 7.1 8.4 5.1 1.38 0.0018 8.4 0.0213 Cl 77.7 2.1 2.2 35.32 0.0167 2.1 0.0242 Ca 20.6 4.9 17.7 1.17 0.0007 4.9 0.0351 Ba 6.6 6.1 10.8 0.61 0.0000 6.2 0.0000 Fe 1.9 11.4 3.3 0.58 0.0000 11.4 0.0000 Mn 1.6 17.7 2.7 0.59 0.0000 17.7 0.0000 Elt. k-ratio Correc. Na 0.0016 2.3525 Mg 0.0005 1.7244 Sr 0.0000 NaN P 0.0010 1.2371 K 0.0002 1.1681 Cl 0.0093 1.1878 Ca 0.0002 1.1416 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 401 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3817 0.019392 0.3817 0.2459 Mg 0.0926 0.006709 0.0926 0.0564 Sr 0.0000 0.000000 0.0000 0.0000 P 0.1277 0.017533 0.1277 0.0610 K 0.0187 0.007474 0.0187 0.0071 Cl 1.1049 0.023976 1.1049 0.4615 Ca 0.0272 0.012751 0.0272 0.0100 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7788 26.7788 33.0144 O 71.4684 71.4684 66.1436 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 402 x= -16244.0 y= 2686.0 z= -284. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 13.8 6.0 3.6 3.79 0.0131 6.0 0.0295 Mg 36.1 3.7 2.5 14.32 0.0189 3.7 0.0113 Sr 20.6 3.5 14.3 1.44 0.0009 3.5 0.0409 P 4.5 10.6 2.4 1.89 0.0027 10.6 0.0408 K 5.9 9.2 5.1 1.15 0.0007 9.2 0.0205 Cl 77.1 2.1 2.2 35.05 0.0166 2.1 0.0237 Ca 1017.6 0.7 17.7 57.65 0.2227 0.8 0.0347 Ba 6.9 6.0 10.8 0.64 0.0000 6.0 0.0000 Fe 5.6 6.7 3.3 1.70 0.0013 6.7 0.0576 Mn 2.7 13.7 2.7 0.98 0.0000 13.7 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3502 Mg 0.0014 1.7152 Sr 0.0006 1.4025 P 0.0004 1.2241 K 0.0001 1.1185 Cl 0.0092 1.1630 Ca 0.0808 1.1267 Ba 0.0000 NaN Fe 0.0006 1.2823 Mn 0.0000 NaN iteration : 2 Analysis no. 402 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1538 0.014172 0.1538 0.1055 Mg 0.2344 0.009735 0.2344 0.1522 Sr 0.0789 0.011649 0.0789 0.0142 P 0.0521 0.014456 0.0521 0.0265 K 0.0069 0.006799 0.0069 0.0028 Cl 1.0741 0.023405 1.0741 0.4780 Ca 9.1066 0.069829 9.1066 3.5848 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0800 0.016254 0.0800 0.0226 Mn 0.0000 0.000000 0.0000 0.0000 C 23.3355 23.3355 30.6527 O 65.8777 65.8777 64.9607 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 403 x= -16244.0 y= 2691.0 z= -284. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 55.7 3.0 3.6 15.36 0.0674 3.0 0.0290 Mg 195.1 1.6 2.5 77.48 0.1083 1.6 0.0112 Sr 45.0 2.4 14.3 3.15 0.0044 2.4 0.0401 P 22.0 4.8 2.4 9.34 0.0253 4.8 0.0397 K 8.9 7.5 5.1 1.75 0.0035 7.5 0.0182 Cl 18.0 4.3 2.2 8.17 0.0035 4.3 0.0224 Ca 4299.4 0.3 17.7 243.58 0.9527 0.4 0.0333 Ba 13.6 4.3 10.8 1.27 0.0017 4.3 0.0755 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0558 Mn 4.3 10.8 2.7 1.59 0.0016 10.8 0.0629 Elt. k-ratio Correc. Na 0.0034 2.3158 Mg 0.0078 1.6994 Sr 0.0027 1.3755 P 0.0040 1.1942 K 0.0003 0.9987 Cl 0.0019 1.1029 Ca 0.3458 1.0825 Ba 0.0005 1.5407 Fe 0.0001 1.2447 Mn 0.0005 1.2693 iteration : 3 Analysis no. 403 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7789 0.025945 0.7789 0.6786 Mg 1.3327 0.022138 1.3327 1.0983 Sr 0.3759 0.014916 0.3759 0.0859 P 0.4736 0.026729 0.4736 0.3063 K 0.0311 0.006858 0.0311 0.0160 Cl 0.2142 0.011146 0.2142 0.1210 Ca 37.4272 0.162307 37.4272 18.7034 Ba 0.0750 0.020518 0.0750 0.0109 Fe 0.0108 0.013883 0.0108 0.0039 Mn 0.0578 0.021501 0.0578 0.0211 C 11.5895 11.5895 19.3263 O 47.6333 47.6333 59.6284 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 404 x= -16243.0 y= 2695.0 z= -284. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 59.0 2.9 3.6 16.27 0.0717 2.9 0.0290 Mg 222.4 1.5 2.5 88.32 0.1237 1.5 0.0112 Sr 46.5 2.3 14.3 3.26 0.0046 2.3 0.0402 P 21.4 4.8 2.4 9.09 0.0245 4.8 0.0398 K 9.0 7.5 5.1 1.75 0.0036 7.5 0.0183 Cl 12.5 5.2 2.2 5.68 0.0023 5.2 0.0225 Ca 4201.8 0.3 17.7 238.05 0.9313 0.4 0.0334 Ba 12.7 4.4 10.8 1.18 0.0012 4.4 0.0755 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0559 Mn 4.6 10.5 2.7 1.68 0.0018 10.5 0.0630 Elt. k-ratio Correc. Na 0.0036 2.3132 Mg 0.0090 1.6992 Sr 0.0029 1.3780 P 0.0038 1.1965 K 0.0003 1.0016 Cl 0.0013 1.1052 Ca 0.3380 1.0836 Ba 0.0003 1.5402 Fe 0.0000 1.2456 Mn 0.0005 1.2699 iteration : 3 Analysis no. 404 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.8276 0.026650 0.8276 0.7163 Mg 1.5219 0.023682 1.5219 1.2459 Sr 0.3945 0.015132 0.3945 0.0896 P 0.4601 0.026452 0.4601 0.2956 K 0.0317 0.006893 0.0317 0.0161 Cl 0.1403 0.009536 0.1403 0.0787 Ca 36.6252 0.159995 36.6252 18.1816 Ba 0.0506 0.020126 0.0506 0.0073 Fe 0.0008 0.013593 0.0008 0.0003 Mn 0.0669 0.021901 0.0669 0.0242 C 11.8178 11.8178 19.5766 O 48.0625 48.0625 59.7678 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 405 x= -16243.0 y= 2700.0 z= -284. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 40.7 3.5 3.6 11.22 0.0480 3.5 0.0289 Mg 288.0 1.3 2.5 114.36 0.1607 1.4 0.0111 Sr 44.9 2.4 14.3 3.14 0.0044 2.4 0.0401 P 34.4 3.8 2.4 14.64 0.0414 3.8 0.0397 K 9.1 7.4 5.1 1.77 0.0037 7.4 0.0181 Cl 13.8 4.9 2.2 6.26 0.0026 4.9 0.0224 Ca 4649.8 0.3 17.7 263.43 1.0314 0.4 0.0332 Ba 14.1 4.2 10.8 1.31 0.0021 4.2 0.0756 Fe 4.4 7.6 3.3 1.33 0.0006 7.6 0.0557 Mn 4.9 10.1 2.7 1.79 0.0021 10.2 0.0628 Elt. k-ratio Correc. Na 0.0024 2.3077 Mg 0.0116 1.6898 Sr 0.0027 1.3741 P 0.0065 1.1919 K 0.0003 0.9906 Cl 0.0014 1.0991 Ca 0.3743 1.0782 Ba 0.0006 1.5416 Fe 0.0003 1.2404 Mn 0.0006 1.2657 iteration : 3 Analysis no. 405 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5529 0.022311 0.5529 0.4977 Mg 1.9657 0.026935 1.9657 1.6737 Sr 0.3739 0.014892 0.3739 0.0883 P 0.7735 0.032919 0.7735 0.5168 K 0.0321 0.006844 0.0321 0.0170 Cl 0.1567 0.009888 0.1567 0.0915 Ca 40.3579 0.170790 40.3579 20.8381 Ba 0.0889 0.020765 0.0889 0.0134 Fe 0.0358 0.014575 0.0358 0.0133 Mn 0.0776 0.022283 0.0776 0.0292 C 10.0721 10.0721 17.3538 O 45.5130 45.5130 58.8672 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 406 x= -16242.0 y= 2705.0 z= -284. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 34.3 3.8 3.6 9.46 0.0397 3.8 0.0289 Mg 295.5 1.3 2.5 117.34 0.1648 1.3 0.0111 Sr 42.4 2.4 14.3 2.97 0.0040 2.4 0.0402 P 41.7 3.5 2.4 17.73 0.0507 3.5 0.0398 K 10.2 7.0 5.1 1.99 0.0047 7.0 0.0184 Cl 25.9 3.6 2.2 11.79 0.0053 3.6 0.0225 Ca 4172.8 0.3 17.7 236.41 0.9246 0.4 0.0334 Ba 12.7 4.4 10.8 1.18 0.0012 4.4 0.0754 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0558 Mn 4.4 10.7 2.7 1.61 0.0016 10.7 0.0630 Elt. k-ratio Correc. Na 0.0020 2.3065 Mg 0.0119 1.6884 Sr 0.0025 1.3778 P 0.0080 1.1961 K 0.0004 1.0063 Cl 0.0029 1.1080 Ca 0.3356 1.0844 Ba 0.0003 1.5398 Fe 0.0001 1.2450 Mn 0.0005 1.2694 iteration : 3 Analysis no. 406 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4569 0.020594 0.4569 0.3971 Mg 2.0145 0.027260 2.0145 1.6559 Sr 0.3447 0.014606 0.3447 0.0786 P 0.9512 0.036182 0.9512 0.6136 K 0.0417 0.007214 0.0417 0.0213 Cl 0.3240 0.013233 0.3240 0.1826 Ca 36.3883 0.159313 36.3883 18.1385 Ba 0.0519 0.020136 0.0519 0.0076 Fe 0.0117 0.013912 0.0117 0.0042 Mn 0.0596 0.021582 0.0596 0.0217 C 11.4869 11.4869 19.1069 O 47.8685 47.8685 59.7721 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 407 x= -16242.0 y= 2710.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.4 3.8 3.6 9.75 0.0411 3.8 0.0289 Mg 298.3 1.3 2.5 118.44 0.1664 1.3 0.0111 Sr 42.1 2.4 14.3 2.95 0.0040 2.5 0.0402 P 43.5 3.4 2.4 18.51 0.0531 3.4 0.0398 K 9.9 7.1 5.1 1.94 0.0044 7.1 0.0184 Cl 26.9 3.5 2.2 12.21 0.0055 3.5 0.0225 Ca 4220.6 0.3 17.7 239.12 0.9355 0.4 0.0334 Ba 13.7 4.3 10.8 1.27 0.0018 4.3 0.0755 Fe 4.5 7.4 3.3 1.37 0.0007 7.4 0.0558 Mn 4.3 10.8 2.7 1.59 0.0016 10.8 0.0629 Elt. k-ratio Correc. Na 0.0020 2.3058 Mg 0.0120 1.6883 Sr 0.0025 1.3774 P 0.0083 1.1956 K 0.0004 1.0052 Cl 0.0030 1.1074 Ca 0.3395 1.0837 Ba 0.0005 1.5397 Fe 0.0003 1.2443 Mn 0.0005 1.2687 iteration : 3 Analysis no. 407 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4726 0.020880 0.4726 0.4127 Mg 2.0339 0.027398 2.0339 1.6801 Sr 0.3407 0.014564 0.3407 0.0781 P 0.9958 0.036944 0.9958 0.6455 K 0.0396 0.007148 0.0396 0.0203 Cl 0.3366 0.013447 0.3366 0.1906 Ca 36.7922 0.160495 36.7922 18.4298 Ba 0.0769 0.020545 0.0769 0.0112 Fe 0.0409 0.014758 0.0409 0.0147 Mn 0.0578 0.021500 0.0578 0.0211 C 11.2723 11.2723 18.8420 O 47.5406 47.5406 59.6539 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 408 x= -16242.0 y= 2714.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 39.2 3.6 3.6 10.80 0.0460 3.6 0.0289 Mg 293.3 1.3 2.5 116.47 0.1637 1.3 0.0111 Sr 44.8 2.4 14.3 3.14 0.0044 2.4 0.0402 P 53.7 3.0 2.4 22.85 0.0663 3.1 0.0398 K 10.6 6.9 5.1 2.07 0.0050 6.9 0.0184 Cl 30.6 3.3 2.2 13.90 0.0063 3.3 0.0226 Ca 4205.1 0.3 17.7 238.24 0.9323 0.4 0.0334 Ba 12.6 4.5 10.8 1.17 0.0011 4.5 0.0755 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0558 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0630 Elt. k-ratio Correc. Na 0.0023 2.3018 Mg 0.0118 1.6869 Sr 0.0027 1.3762 P 0.0104 1.1952 K 0.0004 1.0072 Cl 0.0035 1.1087 Ca 0.3384 1.0841 Ba 0.0003 1.5396 Fe 0.0001 1.2440 Mn 0.0004 1.2685 iteration : 3 Analysis no. 408 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5284 0.021854 0.5284 0.4620 Mg 1.9986 0.027144 1.9986 1.6531 Sr 0.3736 0.014904 0.3736 0.0857 P 1.2427 0.040939 1.2427 0.8065 K 0.0451 0.007318 0.0451 0.0232 Cl 0.3877 0.014302 0.3877 0.2198 Ca 36.6801 0.160195 36.6801 18.3973 Ba 0.0473 0.020069 0.0473 0.0069 Fe 0.0175 0.014083 0.0175 0.0063 Mn 0.0451 0.020957 0.0451 0.0165 C 11.1547 11.1547 18.6693 O 47.4792 47.4792 59.6534 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 409 x= -16241.0 y= 2719.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.8 3.7 3.6 9.87 0.0417 3.8 0.0289 Mg 261.1 1.4 2.5 103.67 0.1455 1.4 0.0111 Sr 42.8 2.4 14.3 3.00 0.0041 2.4 0.0401 P 73.7 2.6 2.4 31.37 0.0922 2.6 0.0398 K 11.0 6.8 5.1 2.15 0.0054 6.8 0.0185 Cl 35.5 3.1 2.2 16.14 0.0074 3.1 0.0227 Ca 4043.1 0.4 17.7 229.06 0.8964 0.4 0.0335 Ba 13.0 4.4 10.8 1.21 0.0014 4.4 0.0755 Fe 3.7 8.2 3.3 1.13 0.0002 8.2 0.0559 Mn 4.4 10.7 2.7 1.61 0.0016 10.7 0.0630 Elt. k-ratio Correc. Na 0.0021 2.3014 Mg 0.0105 1.6860 Sr 0.0025 1.3746 P 0.0144 1.1947 K 0.0005 1.0138 Cl 0.0041 1.1129 Ca 0.3253 1.0862 Ba 0.0004 1.5387 Fe 0.0001 1.2451 Mn 0.0005 1.2693 iteration : 3 Analysis no. 409 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4786 0.020970 0.4786 0.4146 Mg 1.7765 0.025538 1.7765 1.4559 Sr 0.3487 0.014632 0.3487 0.0793 P 1.7263 0.047885 1.7263 1.1102 K 0.0487 0.007461 0.0487 0.0248 Cl 0.4569 0.015406 0.4569 0.2567 Ca 35.3338 0.156280 35.3338 17.5605 Ba 0.0598 0.020263 0.0598 0.0087 Fe 0.0142 0.013997 0.0142 0.0051 Mn 0.0597 0.021594 0.0597 0.0216 C 11.4697 11.4697 19.0216 O 48.2272 48.2272 60.0410 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 410 x= -16241.0 y= 2724.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.6 5.3 3.6 4.85 0.0181 5.3 0.0292 Mg 74.1 2.6 2.5 29.41 0.0403 2.6 0.0112 Sr 23.3 3.3 14.3 1.63 0.0013 3.3 0.0405 P 62.1 2.8 2.4 26.43 0.0772 2.9 0.0403 K 11.1 6.7 5.1 2.17 0.0055 6.7 0.0198 Cl 75.8 2.1 2.2 34.47 0.0163 2.1 0.0234 Ca 1951.5 0.5 17.7 110.56 0.4307 0.6 0.0343 Ba 9.8 5.0 10.8 0.91 0.0000 5.1 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 2.5 14.1 2.7 0.92 0.0000 14.1 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3274 Mg 0.0029 1.7005 Sr 0.0008 1.3880 P 0.0121 1.2105 K 0.0005 1.0837 Cl 0.0091 1.1481 Ca 0.1563 1.1143 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 410 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2102 0.015520 0.2102 0.1552 Mg 0.4959 0.013649 0.4959 0.3463 Sr 0.1117 0.011973 0.1117 0.0216 P 1.4649 0.044556 1.4649 0.8028 K 0.0530 0.008001 0.0530 0.0230 Cl 1.0424 0.022918 1.0424 0.4991 Ca 17.4156 0.100590 17.4156 7.3757 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 19.1491 19.1491 27.0620 O 60.0572 60.0572 63.7143 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 411 x= -16240.0 y= 2729.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.3 5.4 3.6 4.77 0.0177 5.4 0.0293 Mg 70.5 2.7 2.5 28.00 0.0383 2.7 0.0113 Sr 21.2 3.4 14.3 1.48 0.0010 3.4 0.0409 P 34.6 3.8 2.4 14.72 0.0417 3.8 0.0408 K 8.3 7.8 5.1 1.62 0.0029 7.8 0.0205 Cl 77.3 2.1 2.2 35.13 0.0166 2.1 0.0238 Ca 977.3 0.7 17.7 55.37 0.2138 0.8 0.0347 Ba 8.0 5.6 10.8 0.75 0.0000 5.6 0.0000 Fe 2.6 9.8 3.3 0.79 0.0000 9.8 0.0000 Mn 2.4 14.4 2.7 0.89 0.0000 14.4 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3370 Mg 0.0028 1.7089 Sr 0.0006 1.4017 P 0.0065 1.2240 K 0.0003 1.1225 Cl 0.0093 1.1672 Ca 0.0776 1.1277 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 411 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2066 0.015476 0.2066 0.1423 Mg 0.4738 0.013393 0.4738 0.3086 Sr 0.0860 0.011741 0.0860 0.0155 P 0.7996 0.033913 0.7996 0.4087 K 0.0291 0.007536 0.0291 0.0118 Cl 1.0805 0.023518 1.0805 0.4825 Ca 8.7479 0.068354 8.7479 3.4557 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 22.8944 22.8944 30.1791 O 65.6821 65.6821 64.9957 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 412 x= -16240.0 y= 2733.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.8 4.9 3.6 5.72 0.0222 4.9 0.0293 Mg 62.8 2.8 2.5 24.94 0.0339 2.8 0.0113 Sr 21.0 3.4 14.3 1.47 0.0010 3.5 0.0409 P 31.6 4.0 2.4 13.45 0.0378 4.0 0.0407 K 8.1 7.9 5.1 1.58 0.0027 7.9 0.0204 Cl 91.3 1.9 2.2 41.50 0.0197 1.9 0.0237 Ca 1094.1 0.7 17.7 61.99 0.2398 0.7 0.0347 Ba 8.3 5.5 10.8 0.77 0.0000 5.5 0.0000 Fe 2.3 10.4 3.3 0.70 0.0000 10.4 0.0000 Mn 1.9 16.4 2.7 0.68 0.0000 16.4 0.0000 Elt. k-ratio Correc. Na 0.0011 2.3353 Mg 0.0025 1.7086 Sr 0.0006 1.3997 P 0.0059 1.2219 K 0.0002 1.1177 Cl 0.0110 1.1638 Ca 0.0870 1.1261 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 412 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2585 0.016697 0.2585 0.1795 Mg 0.4199 0.012654 0.4199 0.2758 Sr 0.0840 0.011698 0.0840 0.0153 P 0.7239 0.032425 0.7239 0.3731 K 0.0271 0.007447 0.0271 0.0111 Cl 1.2784 0.025450 1.2784 0.5756 Ca 9.7983 0.072669 9.7983 3.9025 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 22.5054 22.5054 29.9111 O 64.9044 64.9044 64.7560 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 413 x= -16240.0 y= 2738.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 25.2 4.4 3.6 6.95 0.0279 4.5 0.0292 Mg 78.4 2.5 2.5 31.12 0.0427 2.5 0.0112 Sr 20.7 3.5 14.3 1.45 0.0009 3.5 0.0409 P 33.4 3.9 2.4 14.21 0.0401 3.9 0.0407 K 9.1 7.4 5.1 1.78 0.0037 7.4 0.0205 Cl 102.7 1.8 2.2 46.66 0.0223 1.8 0.0237 Ca 1068.8 0.7 17.7 60.55 0.2341 0.7 0.0347 Ba 7.6 5.7 10.8 0.70 0.0000 5.8 0.0000 Fe 2.1 11.0 3.3 0.63 0.0000 11.0 0.0000 Mn 2.1 15.4 2.7 0.78 0.0000 15.4 0.0000 Elt. k-ratio Correc. Na 0.0014 2.3306 Mg 0.0031 1.7075 Sr 0.0006 1.4002 P 0.0063 1.2222 K 0.0003 1.1196 Cl 0.0124 1.1645 Ca 0.0850 1.1265 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 413 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3250 0.018134 0.3250 0.2258 Mg 0.5280 0.014092 0.5280 0.3470 Sr 0.0794 0.011640 0.0794 0.0145 P 0.7686 0.033296 0.7686 0.3963 K 0.0368 0.007752 0.0368 0.0150 Cl 1.4422 0.026985 1.4422 0.6497 Ca 9.5724 0.071759 9.5724 3.8145 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 22.4540 22.4540 29.8583 O 64.7935 64.7935 64.6789 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 414 x= -16239.0 y= 2743.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.6 5.3 3.6 4.85 0.0181 5.3 0.0293 Mg 60.6 2.9 2.5 24.07 0.0327 2.9 0.0113 Sr 19.7 3.6 14.3 1.38 0.0008 3.6 0.0409 P 28.8 4.2 2.4 12.26 0.0342 4.2 0.0407 K 6.9 8.5 5.1 1.35 0.0017 8.5 0.0205 Cl 108.2 1.8 2.2 49.16 0.0235 1.8 0.0237 Ca 1017.4 0.7 17.7 57.64 0.2227 0.8 0.0347 Ba 7.6 5.7 10.8 0.71 0.0000 5.7 0.0000 Fe 2.6 9.8 3.3 0.78 0.0000 9.9 0.0000 Mn 2.4 14.4 2.7 0.89 0.0000 14.4 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3350 Mg 0.0024 1.7077 Sr 0.0005 1.3998 P 0.0054 1.2220 K 0.0001 1.1217 Cl 0.0131 1.1648 Ca 0.0808 1.1273 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 414 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2109 0.015574 0.2109 0.1458 Mg 0.4044 0.012431 0.4044 0.2645 Sr 0.0678 0.011482 0.0678 0.0123 P 0.6547 0.031047 0.6547 0.3359 K 0.0166 0.007140 0.0166 0.0067 Cl 1.5219 0.027704 1.5219 0.6822 Ca 9.1113 0.069873 9.1113 3.6128 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 22.7928 22.7928 30.1584 O 65.2195 65.2195 64.7813 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 415 x= -16239.0 y= 2747.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.8 4.6 3.6 6.55 0.0261 4.6 0.0294 Mg 75.1 2.6 2.5 29.81 0.0409 2.6 0.0113 Sr 20.8 3.5 14.3 1.46 0.0009 3.5 0.0410 P 32.2 3.9 2.4 13.70 0.0386 4.0 0.0409 K 10.8 6.8 5.1 2.12 0.0053 6.8 0.0206 Cl 59.0 2.4 2.2 26.83 0.0126 2.4 0.0238 Ca 874.4 0.8 17.7 49.54 0.1908 0.8 0.0348 Ba 8.0 5.6 10.8 0.74 0.0000 5.6 0.0000 Fe 2.9 9.3 3.3 0.87 0.0000 9.3 0.0000 Mn 2.1 15.4 2.7 0.78 0.0000 15.4 0.0000 Elt. k-ratio Correc. Na 0.0013 2.3385 Mg 0.0030 1.7122 Sr 0.0006 1.4047 P 0.0060 1.2267 K 0.0005 1.1262 Cl 0.0070 1.1699 Ca 0.0693 1.1289 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 415 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3042 0.017730 0.3042 0.2079 Mg 0.5064 0.013837 0.5064 0.3273 Sr 0.0818 0.011708 0.0818 0.0147 P 0.7417 0.032847 0.7417 0.3761 K 0.0527 0.008253 0.0527 0.0212 Cl 0.8197 0.020668 0.8197 0.3632 Ca 7.8191 0.064382 7.8191 3.0643 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 23.2833 23.2833 30.4486 O 66.3909 66.3909 65.1768 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 416 x= -16238.0 y= 2752.0 z= -283. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.0 4.7 3.6 6.34 0.0251 4.7 0.0293 Mg 56.4 3.0 2.5 22.38 0.0303 3.0 0.0112 Sr 19.4 3.6 14.3 1.36 0.0007 3.6 0.0408 P 36.1 3.7 2.4 15.36 0.0436 3.7 0.0406 K 9.4 7.3 5.1 1.83 0.0039 7.3 0.0203 Cl 101.4 1.8 2.2 46.11 0.0220 1.8 0.0236 Ca 1259.5 0.6 17.7 71.36 0.2766 0.7 0.0346 Ba 8.2 5.5 10.8 0.76 0.0000 5.5 0.0000 Fe 2.7 9.6 3.3 0.83 0.0000 9.6 0.0000 Mn 2.2 15.1 2.7 0.81 0.0000 15.1 0.0000 Elt. k-ratio Correc. Na 0.0013 2.3326 Mg 0.0022 1.7072 Sr 0.0005 1.3967 P 0.0068 1.2188 K 0.0003 1.1113 Cl 0.0122 1.1600 Ca 0.1004 1.1239 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 416 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2922 0.017439 0.2922 0.2054 Mg 0.3747 0.011998 0.3747 0.2492 Sr 0.0637 0.011402 0.0637 0.0117 P 0.8332 0.034458 0.8332 0.4347 K 0.0388 0.007762 0.0388 0.0160 Cl 1.4196 0.026728 1.4196 0.6471 Ca 11.2835 0.078530 11.2835 4.5497 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 21.8509 21.8509 29.4005 O 63.8434 63.8434 64.4856 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 417 x= -16238.0 y= 2757.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 24.2 4.5 3.6 6.67 0.0266 4.6 0.0292 Mg 85.8 2.4 2.5 34.06 0.0469 2.4 0.0112 Sr 22.0 3.4 14.3 1.54 0.0011 3.4 0.0408 P 40.2 3.5 2.4 17.11 0.0489 3.5 0.0405 K 9.5 7.2 5.1 1.86 0.0041 7.3 0.0202 Cl 97.8 1.8 2.2 44.46 0.0212 1.8 0.0236 Ca 1443.4 0.6 17.7 81.77 0.3176 0.6 0.0345 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 2.5 9.9 3.3 0.77 0.0000 10.0 0.0000 Mn 2.6 13.9 2.7 0.96 0.0000 13.9 0.0000 Elt. k-ratio Correc. Na 0.0013 2.3280 Mg 0.0034 1.7045 Sr 0.0007 1.3956 P 0.0077 1.2175 K 0.0004 1.1039 Cl 0.0118 1.1569 Ca 0.1153 1.1213 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 417 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3096 0.017795 0.3096 0.2207 Mg 0.5786 0.014709 0.5786 0.3901 Sr 0.0962 0.011830 0.0962 0.0180 P 0.9335 0.036243 0.9335 0.4939 K 0.0399 0.007751 0.0399 0.0167 Cl 1.3638 0.026178 1.3638 0.6304 Ca 12.9232 0.084715 12.9232 5.2838 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 21.0643 21.0643 28.7388 O 62.6909 62.6909 64.2077 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 418 x= -16238.0 y= 2762.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 28.7 4.2 3.6 7.91 0.0325 4.2 0.0292 Mg 102.6 2.2 2.5 40.76 0.0564 2.2 0.0112 Sr 25.6 3.1 14.3 1.79 0.0016 3.1 0.0408 P 38.1 3.6 2.4 16.21 0.0462 3.6 0.0406 K 10.7 6.8 5.1 2.10 0.0052 6.8 0.0202 Cl 69.6 2.2 2.2 31.64 0.0149 2.2 0.0236 Ca 1441.8 0.6 17.7 81.68 0.3172 0.6 0.0345 Ba 8.4 5.4 10.8 0.78 0.0000 5.5 0.0000 Fe 2.6 9.8 3.3 0.79 0.0000 9.8 0.0000 Mn 2.3 14.7 2.7 0.85 0.0000 14.7 0.0000 Elt. k-ratio Correc. Na 0.0016 2.3291 Mg 0.0041 1.7066 Sr 0.0010 1.3980 P 0.0072 1.2198 K 0.0005 1.1025 Cl 0.0083 1.1577 Ca 0.1151 1.1209 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 418 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3775 0.019201 0.3775 0.2687 Mg 0.6966 0.016097 0.6966 0.4689 Sr 0.1402 0.012414 0.1402 0.0262 P 0.8833 0.035386 0.8833 0.4665 K 0.0507 0.008053 0.0507 0.0212 Cl 0.9622 0.022162 0.9622 0.4440 Ca 12.9040 0.084630 12.9040 5.2672 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 21.0918 21.0918 28.7286 O 62.8937 62.8937 64.3088 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 419 x= -16237.0 y= 2766.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.4 4.6 3.6 6.45 0.0256 4.6 0.0293 Mg 70.5 2.7 2.5 28.00 0.0383 2.7 0.0112 Sr 19.3 3.6 14.3 1.35 0.0007 3.6 0.0407 P 41.9 3.5 2.4 17.81 0.0510 3.5 0.0404 K 10.4 6.9 5.1 2.04 0.0049 6.9 0.0199 Cl 73.8 2.1 2.2 33.56 0.0159 2.1 0.0234 Ca 1753.3 0.5 17.7 99.33 0.3866 0.6 0.0344 Ba 8.3 5.5 10.8 0.77 0.0000 5.5 0.0000 Fe 2.5 10.0 3.3 0.76 0.0000 10.0 0.0000 Mn 2.5 14.1 2.7 0.92 0.0000 14.1 0.0000 Elt. k-ratio Correc. Na 0.0013 2.3325 Mg 0.0028 1.7059 Sr 0.0004 1.3925 P 0.0080 1.2139 K 0.0004 1.0897 Cl 0.0088 1.1504 Ca 0.1403 1.1168 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 419 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2982 0.017569 0.2982 0.2164 Mg 0.4729 0.013369 0.4729 0.3246 Sr 0.0625 0.011354 0.0625 0.0119 P 0.9712 0.036841 0.9712 0.5231 K 0.0475 0.007883 0.0475 0.0202 Cl 1.0162 0.022667 1.0162 0.4781 Ca 15.6693 0.094571 15.6693 6.5218 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 20.1260 20.1260 27.9529 O 61.3363 61.3363 63.9510 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 420 x= -16237.0 y= 2771.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 40.0 3.5 3.6 11.03 0.0471 3.6 0.0291 Mg 120.1 2.0 2.5 47.70 0.0662 2.1 0.0112 Sr 27.9 3.0 14.3 1.95 0.0020 3.0 0.0407 P 42.9 3.4 2.4 18.24 0.0523 3.4 0.0405 K 12.2 6.4 5.1 2.39 0.0066 6.4 0.0199 Cl 76.7 2.1 2.2 34.88 0.0165 2.1 0.0234 Ca 1835.2 0.5 17.7 103.97 0.4049 0.6 0.0344 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 2.5 10.0 3.3 0.75 0.0000 10.1 0.0000 Mn 2.9 13.2 2.7 1.05 0.0001 13.2 0.0641 Elt. k-ratio Correc. Na 0.0024 2.3213 Mg 0.0048 1.7044 Sr 0.0012 1.3939 P 0.0082 1.2153 K 0.0006 1.0876 Cl 0.0092 1.1498 Ca 0.1469 1.1155 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2896 iteration : 2 Analysis no. 420 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5459 0.022271 0.5459 0.4001 Mg 0.8171 0.017389 0.8171 0.5664 Sr 0.1683 0.012734 0.1683 0.0324 P 0.9971 0.037311 0.9971 0.5424 K 0.0635 0.008314 0.0635 0.0273 Cl 1.0569 0.023090 1.0569 0.5023 Ca 16.3905 0.097072 16.3905 6.8907 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0052 0.019476 0.0052 0.0016 C 19.5377 19.5377 27.4090 O 60.4178 60.4178 63.6277 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 421 x= -16237.0 y= 2776.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 16.2 5.5 3.6 4.47 0.0163 5.6 0.0293 Mg 69.1 2.7 2.5 27.45 0.0375 2.7 0.0112 Sr 20.7 3.5 14.3 1.45 0.0009 3.5 0.0405 P 42.8 3.4 2.4 18.19 0.0522 3.4 0.0402 K 13.6 6.1 5.1 2.66 0.0078 6.1 0.0196 Cl 67.4 2.2 2.2 30.64 0.0144 2.2 0.0233 Ca 2194.6 0.5 17.7 124.33 0.4849 0.5 0.0342 Ba 8.9 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 2.6 9.8 3.3 0.79 0.0000 9.8 0.0000 Mn 2.6 14.0 2.7 0.94 0.0000 14.0 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3338 Mg 0.0027 1.7031 Sr 0.0006 1.3872 P 0.0082 1.2084 K 0.0007 1.0720 Cl 0.0080 1.1411 Ca 0.1760 1.1109 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 421 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1897 0.015041 0.1897 0.1417 Mg 0.4624 0.013217 0.4624 0.3268 Sr 0.0787 0.011533 0.0787 0.0154 P 0.9890 0.037057 0.9890 0.5484 K 0.0744 0.008509 0.0744 0.0327 Cl 0.9174 0.021504 0.9174 0.4444 Ca 19.5496 0.107742 19.5496 8.3777 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 18.6846 18.6846 26.7190 O 59.0542 59.0542 63.3938 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 422 x= -16236.0 y= 2781.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 30.7 4.0 3.6 8.46 0.0351 4.1 0.0291 Mg 117.1 2.1 2.5 46.48 0.0645 2.1 0.0112 Sr 29.8 2.9 14.3 2.08 0.0022 2.9 0.0405 P 46.5 3.3 2.4 19.79 0.0570 3.3 0.0402 K 15.3 5.7 5.1 3.00 0.0094 5.7 0.0194 Cl 70.4 2.2 2.2 32.00 0.0151 2.2 0.0231 Ca 2540.6 0.4 17.7 143.94 0.5620 0.5 0.0341 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0638 Elt. k-ratio Correc. Na 0.0018 2.3225 Mg 0.0047 1.7001 Sr 0.0014 1.3853 P 0.0089 1.2065 K 0.0008 1.0608 Cl 0.0084 1.1355 Ca 0.2040 1.1060 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2835 iteration : 2 Analysis no. 422 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4065 0.019737 0.4065 0.3127 Mg 0.7938 0.017123 0.7938 0.5776 Sr 0.1907 0.012939 0.1907 0.0385 P 1.0791 0.038538 1.0791 0.6161 K 0.0889 0.008807 0.0889 0.0402 Cl 0.9550 0.021859 0.9550 0.4763 Ca 22.5576 0.117490 22.5576 9.9525 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0383 0.020894 0.0383 0.0123 C 17.1876 17.1876 25.3048 O 56.7026 56.7026 62.6690 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 423 x= -16236.0 y= 2785.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 18.4 5.2 3.6 5.06 0.0191 5.2 0.0293 Mg 69.8 2.7 2.5 27.73 0.0379 2.7 0.0112 Sr 22.0 3.4 14.3 1.54 0.0011 3.4 0.0404 P 42.5 3.4 2.4 18.09 0.0519 3.4 0.0402 K 13.4 6.1 5.1 2.63 0.0077 6.1 0.0194 Cl 64.4 2.3 2.2 29.26 0.0138 2.3 0.0231 Ca 2465.0 0.4 17.7 139.65 0.5452 0.5 0.0341 Ba 8.2 5.5 10.8 0.76 0.0000 5.5 0.0000 Fe 2.3 10.5 3.3 0.69 0.0000 10.5 0.0000 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0639 Elt. k-ratio Correc. Na 0.0010 2.3331 Mg 0.0027 1.7026 Sr 0.0007 1.3845 P 0.0081 1.2055 K 0.0007 1.0617 Cl 0.0077 1.1356 Ca 0.1979 1.1072 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2854 iteration : 2 Analysis no. 423 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2221 0.015838 0.2221 0.1691 Mg 0.4672 0.013280 0.4672 0.3364 Sr 0.0945 0.011725 0.0945 0.0189 P 0.9806 0.036868 0.9806 0.5540 K 0.0724 0.008394 0.0724 0.0324 Cl 0.8706 0.020929 0.8706 0.4297 Ca 21.9080 0.115423 21.9080 9.5652 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0144 0.019846 0.0144 0.0046 C 17.7756 17.7756 25.8979 O 57.5946 57.5946 62.9918 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 424 x= -16235.0 y= 2790.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 31.0 4.0 3.6 8.53 0.0354 4.0 0.0291 Mg 118.3 2.1 2.5 46.96 0.0652 2.1 0.0112 Sr 30.7 2.9 14.3 2.15 0.0024 2.9 0.0403 P 45.1 3.3 2.4 19.17 0.0552 3.3 0.0400 K 16.6 5.5 5.1 3.25 0.0106 5.5 0.0191 Cl 81.3 2.0 2.2 36.93 0.0175 2.0 0.0229 Ca 3031.7 0.4 17.7 171.76 0.6714 0.5 0.0339 Ba 10.6 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 4.0 7.9 3.3 1.20 0.0004 7.9 0.0565 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0636 Elt. k-ratio Correc. Na 0.0018 2.3203 Mg 0.0047 1.6975 Sr 0.0015 1.3797 P 0.0087 1.2005 K 0.0009 1.0443 Cl 0.0097 1.1255 Ca 0.2437 1.0997 Ba 0.0000 NaN Fe 0.0002 1.2573 Mn 0.0002 1.2791 iteration : 3 Analysis no. 424 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4099 0.019793 0.4099 0.3268 Mg 0.8010 0.017185 0.8010 0.6040 Sr 0.2013 0.013023 0.2013 0.0421 P 1.0385 0.037763 1.0385 0.6145 K 0.0983 0.008933 0.0983 0.0461 Cl 1.0972 0.023245 1.0972 0.5672 Ca 26.7963 0.130769 26.7963 12.2528 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0228 0.014389 0.0228 0.0075 Mn 0.0290 0.020418 0.0290 0.0097 C 15.5486 15.5486 23.7248 O 53.9572 53.9572 61.8047 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 425 x= -16235.0 y= 2795.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.0 6.0 3.6 3.86 0.0134 6.0 0.0293 Mg 87.3 2.4 2.5 34.68 0.0478 2.4 0.0112 Sr 22.7 3.3 14.3 1.59 0.0012 3.3 0.0404 P 39.2 3.6 2.4 16.66 0.0476 3.6 0.0401 K 13.5 6.1 5.1 2.65 0.0078 6.1 0.0193 Cl 58.3 2.4 2.2 26.50 0.0124 2.4 0.0231 Ca 2686.1 0.4 17.7 152.18 0.5945 0.5 0.0340 Ba 8.9 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.0 9.1 3.3 0.92 0.0000 9.1 0.0000 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0638 Elt. k-ratio Correc. Na 0.0007 2.3335 Mg 0.0035 1.7009 Sr 0.0007 1.3832 P 0.0075 1.2037 K 0.0007 1.0531 Cl 0.0069 1.1311 Ca 0.2158 1.1042 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2836 iteration : 2 Analysis no. 425 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1565 0.014178 0.1565 0.1209 Mg 0.5882 0.014811 0.5882 0.4297 Sr 0.1037 0.011835 0.1037 0.0210 P 0.8974 0.035385 0.8974 0.5145 K 0.0727 0.008349 0.0727 0.0330 Cl 0.7824 0.019865 0.7824 0.3919 Ca 23.8231 0.121516 23.8231 10.5548 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0236 0.020242 0.0236 0.0076 C 17.0780 17.0780 25.2487 O 56.4744 56.4744 62.6778 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 426 x= -16235.0 y= 2799.0 z= -282. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 36.1 3.7 3.6 9.94 0.0420 3.7 0.0291 Mg 128.1 2.0 2.5 50.86 0.0707 2.0 0.0112 Sr 32.6 2.8 14.3 2.28 0.0026 2.8 0.0403 P 47.3 3.2 2.4 20.11 0.0580 3.3 0.0400 K 17.7 5.3 5.1 3.47 0.0117 5.3 0.0190 Cl 62.1 2.3 2.2 28.23 0.0133 2.3 0.0229 Ca 3122.6 0.4 17.7 176.91 0.6916 0.5 0.0338 Ba 9.8 5.0 10.8 0.91 0.0000 5.1 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0564 Mn 4.3 10.8 2.7 1.59 0.0016 10.8 0.0635 Elt. k-ratio Correc. Na 0.0021 2.3198 Mg 0.0051 1.6985 Sr 0.0016 1.3800 P 0.0091 1.2007 K 0.0010 1.0403 Cl 0.0074 1.1245 Ca 0.2510 1.0982 Ba 0.0000 NaN Fe 0.0000 1.2563 Mn 0.0005 1.2784 iteration : 3 Analysis no. 426 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4863 0.021213 0.4863 0.3901 Mg 0.8693 0.017895 0.8693 0.6596 Sr 0.2250 0.013304 0.2250 0.0473 P 1.0921 0.038653 1.0921 0.6502 K 0.1077 0.009133 0.1077 0.0508 Cl 0.8305 0.020363 0.8305 0.4320 Ca 27.5672 0.133121 27.5672 12.6835 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0059 0.013875 0.0059 0.0019 Mn 0.0583 0.021680 0.0583 0.0196 C 15.2029 15.2029 23.3411 O 53.5548 53.5548 61.7240 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 427 x= -16234.0 y= 2804.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.6 5.8 3.6 4.03 0.0142 5.9 0.0293 Mg 81.6 2.5 2.5 32.39 0.0445 2.5 0.0112 Sr 19.8 3.5 14.3 1.39 0.0008 3.6 0.0404 P 41.9 3.5 2.4 17.81 0.0510 3.5 0.0401 K 15.5 5.7 5.1 3.03 0.0096 5.7 0.0194 Cl 57.0 2.4 2.2 25.92 0.0121 2.4 0.0231 Ca 2531.0 0.4 17.7 143.39 0.5599 0.5 0.0341 Ba 9.3 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0568 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0638 Elt. k-ratio Correc. Na 0.0007 2.3345 Mg 0.0032 1.7021 Sr 0.0005 1.3846 P 0.0080 1.2051 K 0.0009 1.0587 Cl 0.0068 1.1343 Ca 0.2032 1.1062 Ba 0.0000 NaN Fe 0.0000 1.2643 Mn 0.0003 1.2850 iteration : 2 Analysis no. 427 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1656 0.014423 0.1656 0.1266 Mg 0.5486 0.014330 0.5486 0.3966 Sr 0.0680 0.011371 0.0680 0.0136 P 0.9643 0.036579 0.9643 0.5470 K 0.0900 0.008823 0.0900 0.0405 Cl 0.7668 0.019708 0.7668 0.3800 Ca 22.4785 0.117245 22.4785 9.8538 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013912 0.0042 0.0013 Mn 0.0383 0.020920 0.0383 0.0123 C 17.5666 17.5666 25.6965 O 57.3089 57.3089 62.9317 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 428 x= -16234.0 y= 2809.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 29.6 4.1 3.6 8.16 0.0336 4.1 0.0292 Mg 116.8 2.1 2.5 46.38 0.0644 2.1 0.0112 Sr 26.6 3.1 14.3 1.86 0.0018 3.1 0.0403 P 45.7 3.3 2.4 19.43 0.0559 3.3 0.0399 K 19.5 5.1 5.1 3.81 0.0133 5.1 0.0189 Cl 52.9 2.5 2.2 24.06 0.0112 2.5 0.0229 Ca 3246.3 0.4 17.7 183.91 0.7192 0.5 0.0338 Ba 9.1 5.3 10.8 0.84 0.0000 5.3 0.0000 Fe 3.1 8.9 3.3 0.95 0.0000 9.0 0.0000 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0635 Elt. k-ratio Correc. Na 0.0017 2.3243 Mg 0.0047 1.6988 Sr 0.0011 1.3787 P 0.0088 1.1987 K 0.0012 1.0348 Cl 0.0063 1.1216 Ca 0.2610 1.0968 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2782 iteration : 3 Analysis no. 428 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3903 0.019431 0.3903 0.3149 Mg 0.7915 0.017092 0.7915 0.6040 Sr 0.1505 0.012398 0.1505 0.0319 P 1.0514 0.037947 1.0514 0.6296 K 0.1220 0.009428 0.1220 0.0579 Cl 0.7015 0.018795 0.7015 0.3670 Ca 28.6275 0.136360 28.6275 13.2481 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0363 0.020727 0.0363 0.0123 C 14.9504 14.9504 23.0871 O 53.1785 53.1785 61.6473 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 429 x= -16233.0 y= 2814.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 18.9 5.1 3.6 5.20 0.0197 5.2 0.0293 Mg 95.0 2.3 2.5 37.74 0.0521 2.3 0.0112 Sr 25.5 3.1 14.3 1.78 0.0016 3.1 0.0403 P 37.3 3.7 2.4 15.87 0.0452 3.7 0.0400 K 16.1 5.6 5.1 3.15 0.0101 5.6 0.0190 Cl 52.3 2.5 2.2 23.77 0.0111 2.5 0.0229 Ca 3098.0 0.4 17.7 175.52 0.6861 0.5 0.0339 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0636 Elt. k-ratio Correc. Na 0.0010 2.3314 Mg 0.0038 1.7001 Sr 0.0010 1.3796 P 0.0071 1.1998 K 0.0009 1.0383 Cl 0.0062 1.1231 Ca 0.2490 1.0988 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2801 iteration : 2 Analysis no. 429 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2294 0.016003 0.2294 0.1825 Mg 0.6412 0.015433 0.6412 0.4823 Sr 0.1374 0.012239 0.1374 0.0287 P 0.8494 0.034454 0.8494 0.5014 K 0.0934 0.008778 0.0934 0.0437 Cl 0.6936 0.018711 0.6936 0.3577 Ca 27.3594 0.132490 27.3594 12.4802 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0254 0.020265 0.0254 0.0084 C 15.7073 15.7073 23.9093 O 54.2635 54.2635 62.0059 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 430 x= -16233.0 y= 2818.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 34.6 3.8 3.6 9.53 0.0400 3.8 0.0291 Mg 121.9 2.0 2.5 48.39 0.0672 2.0 0.0112 Sr 33.5 2.7 14.3 2.34 0.0028 2.7 0.0402 P 41.6 3.5 2.4 17.68 0.0506 3.5 0.0398 K 20.1 5.0 5.1 3.94 0.0139 5.0 0.0188 Cl 74.2 2.1 2.2 33.72 0.0159 2.1 0.0228 Ca 3464.5 0.4 17.7 196.28 0.7678 0.5 0.0337 Ba 11.0 4.8 10.8 1.02 0.0001 4.8 0.0755 Fe 4.2 7.8 3.3 1.26 0.0005 7.8 0.0562 Mn 5.0 10.0 2.7 1.83 0.0022 10.1 0.0634 Elt. k-ratio Correc. Na 0.0020 2.3201 Mg 0.0049 1.6972 Sr 0.0017 1.3760 P 0.0079 1.1964 K 0.0012 1.0293 Cl 0.0089 1.1171 Ca 0.2786 1.0939 Ba 0.0000 1.5376 Fe 0.0002 1.2526 Mn 0.0006 1.2754 iteration : 3 Analysis no. 430 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4639 0.020806 0.4639 0.3816 Mg 0.8257 0.017441 0.8257 0.6425 Sr 0.2347 0.013385 0.2347 0.0507 P 0.9501 0.036188 0.9501 0.5800 K 0.1269 0.009502 0.1269 0.0614 Cl 0.9915 0.022062 0.9915 0.5289 Ca 30.4803 0.141945 30.4803 14.3812 Ba 0.0059 0.019363 0.0059 0.0008 Fe 0.0286 0.014507 0.0286 0.0097 Mn 0.0819 0.022612 0.0819 0.0282 C 14.1458 14.1458 22.2717 O 51.6648 51.6648 61.0635 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 431 x= -16233.0 y= 2823.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 22.7 4.7 3.6 6.25 0.0246 4.7 0.0292 Mg 102.0 2.2 2.5 40.50 0.0560 2.2 0.0112 Sr 26.7 3.1 14.3 1.87 0.0018 3.1 0.0403 P 40.5 3.5 2.4 17.21 0.0492 3.5 0.0400 K 18.2 5.2 5.1 3.56 0.0121 5.3 0.0191 Cl 54.1 2.5 2.2 24.59 0.0115 2.5 0.0230 Ca 2943.2 0.4 17.7 166.75 0.6518 0.5 0.0339 Ba 8.1 5.6 10.8 0.75 0.0000 5.6 0.0000 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0566 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0636 Elt. k-ratio Correc. Na 0.0012 2.3293 Mg 0.0041 1.7005 Sr 0.0011 1.3814 P 0.0077 1.2018 K 0.0011 1.0443 Cl 0.0064 1.1266 Ca 0.2365 1.1007 Ba 0.0000 NaN Fe 0.0001 1.2593 Mn 0.0003 1.2809 iteration : 2 Analysis no. 431 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2865 0.017301 0.2865 0.2258 Mg 0.6897 0.015991 0.6897 0.5141 Sr 0.1527 0.012446 0.1527 0.0316 P 0.9277 0.035888 0.9277 0.5426 K 0.1120 0.009260 0.1120 0.0519 Cl 0.7209 0.019082 0.7209 0.3684 Ca 26.0350 0.128418 26.0350 11.7693 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0135 0.014139 0.0135 0.0044 Mn 0.0401 0.020936 0.0401 0.0132 C 16.0944 16.0944 24.2783 O 54.9275 54.9275 62.2004 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 432 x= -16232.0 y= 2828.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 40.5 3.5 3.6 11.15 0.0477 3.5 0.0291 Mg 147.9 1.8 2.5 58.73 0.0819 1.9 0.0112 Sr 32.5 2.8 14.3 2.28 0.0026 2.8 0.0403 P 39.9 3.5 2.4 16.98 0.0485 3.6 0.0399 K 19.8 5.0 5.1 3.88 0.0136 5.0 0.0189 Cl 74.5 2.1 2.2 33.88 0.0160 2.1 0.0228 Ca 3356.9 0.4 17.7 190.18 0.7439 0.5 0.0338 Ba 10.0 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0563 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0634 Elt. k-ratio Correc. Na 0.0024 2.3161 Mg 0.0059 1.6971 Sr 0.0016 1.3786 P 0.0076 1.1986 K 0.0012 1.0331 Cl 0.0089 1.1195 Ca 0.2700 1.0954 Ba 0.0000 NaN Fe 0.0001 1.2538 Mn 0.0002 1.2764 iteration : 3 Analysis no. 432 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5515 0.022341 0.5515 0.4503 Mg 1.0059 0.019227 1.0059 0.7768 Sr 0.2236 0.013277 0.2236 0.0479 P 0.9118 0.035557 0.9118 0.5526 K 0.1248 0.009481 0.1248 0.0599 Cl 0.9987 0.022165 0.9987 0.5288 Ca 29.5737 0.139230 29.5737 13.8504 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0151 0.014127 0.0151 0.0051 Mn 0.0271 0.020293 0.0271 0.0093 C 14.4307 14.4307 22.5524 O 52.1371 52.1371 61.1665 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 433 x= -16232.0 y= 2833.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 19.6 5.0 3.6 5.40 0.0207 5.1 0.0293 Mg 74.9 2.6 2.5 29.75 0.0408 2.6 0.0112 Sr 19.5 3.6 14.3 1.36 0.0007 3.6 0.0404 P 35.7 3.7 2.4 15.17 0.0430 3.8 0.0401 K 17.8 5.3 5.1 3.49 0.0118 5.3 0.0193 Cl 54.9 2.5 2.2 24.93 0.0117 2.5 0.0230 Ca 2676.9 0.4 17.7 151.66 0.5924 0.5 0.0340 Ba 9.1 5.2 10.8 0.85 0.0000 5.2 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0567 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0638 Elt. k-ratio Correc. Na 0.0010 2.3353 Mg 0.0030 1.7036 Sr 0.0005 1.3837 P 0.0067 1.2037 K 0.0010 1.0526 Cl 0.0065 1.1307 Ca 0.2150 1.1043 Ba 0.0000 NaN Fe 0.0001 1.2630 Mn 0.0002 1.2840 iteration : 2 Analysis no. 433 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2412 0.016299 0.2412 0.1860 Mg 0.5029 0.013755 0.5029 0.3668 Sr 0.0640 0.011309 0.0640 0.0129 P 0.8120 0.033830 0.8120 0.4647 K 0.1099 0.009262 0.1099 0.0498 Cl 0.7342 0.019280 0.7342 0.3671 Ca 23.7413 0.121254 23.7413 10.5003 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0085 0.014026 0.0085 0.0027 Mn 0.0254 0.020329 0.0254 0.0082 C 17.1773 17.1773 25.3515 O 56.5834 56.5834 62.6900 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 434 x= -16231.0 y= 2837.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.5 4.9 3.6 5.64 0.0218 5.0 0.0292 Mg 103.8 2.2 2.5 41.22 0.0570 2.2 0.0112 Sr 31.1 2.8 14.3 2.18 0.0024 2.8 0.0402 P 38.8 3.6 2.4 16.49 0.0470 3.6 0.0399 K 16.8 5.4 5.1 3.29 0.0108 5.5 0.0189 Cl 68.9 2.2 2.2 31.33 0.0148 2.2 0.0228 Ca 3255.3 0.4 17.7 184.43 0.7214 0.5 0.0338 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0755 Fe 4.0 7.9 3.3 1.20 0.0004 7.9 0.0564 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0635 Elt. k-ratio Correc. Na 0.0011 2.3265 Mg 0.0041 1.6973 Sr 0.0015 1.3772 P 0.0074 1.1980 K 0.0010 1.0349 Cl 0.0082 1.1204 Ca 0.2618 1.0967 Ba 0.0000 1.5376 Fe 0.0002 1.2557 Mn 0.0001 1.2780 iteration : 3 Analysis no. 434 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2531 0.016538 0.2531 0.2043 Mg 0.7010 0.016103 0.7010 0.5351 Sr 0.2065 0.013068 0.2065 0.0437 P 0.8836 0.035049 0.8836 0.5293 K 0.0995 0.008906 0.0995 0.0472 Cl 0.9223 0.021354 0.9223 0.4826 Ca 28.7140 0.136638 28.7140 13.2916 Ba 0.0026 0.019312 0.0026 0.0004 Fe 0.0228 0.014375 0.0228 0.0076 Mn 0.0180 0.019905 0.0180 0.0061 C 15.0541 15.0541 23.2534 O 53.1226 53.1226 61.5988 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 435 x= -16231.0 y= 2842.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 54.7 3.0 3.6 15.08 0.0662 3.0 0.0290 Mg 159.2 1.8 2.5 63.20 0.0882 1.8 0.0112 Sr 35.6 2.6 14.3 2.49 0.0031 2.7 0.0404 P 41.5 3.5 2.4 17.66 0.0506 3.5 0.0401 K 20.9 4.9 5.1 4.09 0.0146 4.9 0.0190 Cl 66.3 2.2 2.2 30.12 0.0142 2.2 0.0229 Ca 3138.8 0.4 17.7 177.83 0.6954 0.5 0.0338 Ba 10.3 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0564 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0635 Elt. k-ratio Correc. Na 0.0033 2.3125 Mg 0.0064 1.6998 Sr 0.0019 1.3823 P 0.0079 1.2024 K 0.0013 1.0404 Cl 0.0079 1.1244 Ca 0.2524 1.0979 Ba 0.0000 NaN Fe 0.0001 1.2556 Mn 0.0003 1.2778 iteration : 3 Analysis no. 435 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7639 0.025720 0.7639 0.6149 Mg 1.0857 0.019990 1.0857 0.8267 Sr 0.2623 0.013753 0.2623 0.0554 P 0.9538 0.036357 0.9538 0.5699 K 0.1347 0.009749 0.1347 0.0638 Cl 0.8885 0.021021 0.8885 0.4638 Ca 27.7107 0.133568 27.7107 12.7955 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0126 0.014074 0.0126 0.0042 Mn 0.0381 0.020807 0.0381 0.0128 C 15.0061 15.0061 23.1220 O 53.1436 53.1436 61.4709 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 436 x= -16231.0 y= 2847.0 z= -281. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 31.6 4.0 3.6 8.71 0.0362 4.0 0.0293 Mg 74.9 2.6 2.5 29.75 0.0408 2.6 0.0112 Sr 27.6 3.0 14.3 1.93 0.0019 3.0 0.0403 P 27.4 4.3 2.4 11.64 0.0323 4.3 0.0400 K 17.8 5.3 5.1 3.49 0.0118 5.3 0.0190 Cl 58.0 2.4 2.2 26.38 0.0124 2.4 0.0229 Ca 3122.6 0.4 17.7 176.91 0.6919 0.5 0.0339 Ba 10.7 4.8 10.8 1.00 0.0000 4.8 0.0000 Fe 3.1 9.0 3.3 0.94 0.0000 9.0 0.0000 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0636 Elt. k-ratio Correc. Na 0.0018 2.3316 Mg 0.0030 1.7038 Sr 0.0012 1.3797 P 0.0051 1.1998 K 0.0010 1.0370 Cl 0.0069 1.1215 Ca 0.2511 1.0983 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2799 iteration : 3 Analysis no. 436 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4218 0.020082 0.4218 0.3358 Mg 0.5031 0.013761 0.5031 0.3789 Sr 0.1633 0.012566 0.1633 0.0341 P 0.6078 0.029766 0.6078 0.3592 K 0.1083 0.009127 0.1083 0.0507 Cl 0.7723 0.019658 0.7723 0.3987 Ca 27.5773 0.133171 27.5773 12.5937 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0364 0.020762 0.0364 0.0121 C 15.7332 15.7332 23.9754 O 54.0766 54.0766 61.8614 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 437 x= -16230.0 y= 2851.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 37.7 3.6 3.6 10.38 0.0441 3.7 0.0292 Mg 101.2 2.2 2.5 40.20 0.0556 2.2 0.0112 Sr 29.2 2.9 14.3 2.04 0.0021 2.9 0.0402 P 35.3 3.8 2.4 15.02 0.0426 3.8 0.0399 K 21.9 4.8 5.1 4.29 0.0156 4.8 0.0189 Cl 74.0 2.1 2.2 33.66 0.0159 2.1 0.0228 Ca 3322.8 0.4 17.7 188.25 0.7364 0.5 0.0338 Ba 12.2 4.5 10.8 1.13 0.0009 4.5 0.0755 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0564 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0635 Elt. k-ratio Correc. Na 0.0022 2.3228 Mg 0.0040 1.7002 Sr 0.0013 1.3775 P 0.0067 1.1975 K 0.0014 1.0329 Cl 0.0089 1.1187 Ca 0.2673 1.0958 Ba 0.0002 1.5376 Fe 0.0001 1.2547 Mn 0.0001 1.2772 iteration : 3 Analysis no. 437 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5111 0.021674 0.5111 0.4150 Mg 0.6844 0.015931 0.6844 0.5257 Sr 0.1823 0.012780 0.1823 0.0388 P 0.7995 0.033505 0.7995 0.4819 K 0.1426 0.009873 0.1426 0.0681 Cl 0.9912 0.022079 0.9912 0.5220 Ca 29.2846 0.138358 29.2846 13.6402 Ba 0.0375 0.019895 0.0375 0.0051 Fe 0.0126 0.014062 0.0126 0.0042 Mn 0.0162 0.019806 0.0162 0.0055 C 14.7740 14.7741 22.9630 O 52.5640 52.5640 61.3306 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 438 x= -16230.0 y= 2856.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.9 4.9 3.6 5.76 0.0224 4.9 0.0293 Mg 81.9 2.5 2.5 32.53 0.0447 2.5 0.0112 Sr 22.8 3.3 14.3 1.60 0.0012 3.3 0.0404 P 33.6 3.9 2.4 14.28 0.0403 3.9 0.0401 K 18.7 5.2 5.1 3.66 0.0126 5.2 0.0191 Cl 54.9 2.5 2.2 24.95 0.0117 2.5 0.0230 Ca 2883.1 0.4 17.7 163.34 0.6385 0.5 0.0340 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0566 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0637 Elt. k-ratio Correc. Na 0.0011 2.3338 Mg 0.0032 1.7026 Sr 0.0008 1.3818 P 0.0063 1.2019 K 0.0011 1.0453 Cl 0.0065 1.1266 Ca 0.2317 1.1015 Ba 0.0000 NaN Fe 0.0002 1.2606 Mn 0.0001 1.2820 iteration : 2 Analysis no. 438 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2607 0.016747 0.2607 0.2041 Mg 0.5514 0.014370 0.5514 0.4082 Sr 0.1048 0.011843 0.1048 0.0215 P 0.7599 0.032829 0.7599 0.4415 K 0.1164 0.009371 0.1164 0.0536 Cl 0.7322 0.019223 0.7322 0.3716 Ca 25.5269 0.126859 25.5269 11.4604 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0212 0.014383 0.0212 0.0068 Mn 0.0181 0.019970 0.0181 0.0059 C 16.4821 16.4821 24.6923 O 55.4263 55.4263 62.3341 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 439 x= -16229.0 y= 2861.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 30.6 4.0 3.6 8.44 0.0349 4.1 0.0292 Mg 102.7 2.2 2.5 40.78 0.0564 2.2 0.0112 Sr 28.9 2.9 14.3 2.03 0.0021 3.0 0.0402 P 37.0 3.7 2.4 15.75 0.0448 3.7 0.0399 K 23.2 4.6 5.1 4.54 0.0167 4.7 0.0189 Cl 64.6 2.3 2.2 29.38 0.0138 2.3 0.0228 Ca 3380.0 0.4 17.7 191.49 0.7491 0.5 0.0338 Ba 10.8 4.8 10.8 1.00 0.0000 4.8 0.0755 Fe 4.6 7.4 3.3 1.39 0.0007 7.4 0.0563 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0635 Elt. k-ratio Correc. Na 0.0017 2.3256 Mg 0.0041 1.6994 Sr 0.0013 1.3769 P 0.0070 1.1969 K 0.0015 1.0304 Cl 0.0077 1.1178 Ca 0.2719 1.0951 Ba 0.0000 1.5380 Fe 0.0003 1.2543 Mn 0.0002 1.2770 iteration : 3 Analysis no. 439 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4056 0.019739 0.4056 0.3304 Mg 0.6942 0.016037 0.6942 0.5348 Sr 0.1795 0.012741 0.1795 0.0384 P 0.8403 0.034248 0.8403 0.5080 K 0.1529 0.010075 0.1529 0.0732 Cl 0.8607 0.020644 0.8607 0.4546 Ca 29.7722 0.139832 29.7722 13.9105 Ba 0.0007 0.019282 0.0007 0.0001 Fe 0.0429 0.014939 0.0429 0.0144 Mn 0.0290 0.020386 0.0290 0.0099 C 14.6179 14.6179 22.7910 O 52.4042 52.4042 61.3346 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 440 x= -16229.0 y= 2866.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.9 5.8 3.6 4.09 0.0145 5.8 0.0293 Mg 73.2 2.6 2.5 29.08 0.0398 2.6 0.0112 Sr 23.0 3.3 14.3 1.61 0.0013 3.3 0.0404 P 24.7 4.5 2.4 10.51 0.0289 4.5 0.0401 K 13.2 6.1 5.1 2.59 0.0075 6.2 0.0192 Cl 67.6 2.2 2.2 30.74 0.0145 2.2 0.0230 Ca 2715.6 0.4 17.7 153.85 0.6012 0.5 0.0340 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.1 9.0 3.3 0.93 0.0000 9.0 0.0000 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0638 Elt. k-ratio Correc. Na 0.0007 2.3367 Mg 0.0029 1.7029 Sr 0.0008 1.3831 P 0.0045 1.2033 K 0.0007 1.0511 Cl 0.0081 1.1287 Ca 0.2182 1.1038 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2837 iteration : 2 Analysis no. 440 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1696 0.014540 0.1696 0.1310 Mg 0.4910 0.013599 0.4910 0.3587 Sr 0.1071 0.011881 0.1071 0.0217 P 0.5450 0.028474 0.5450 0.3124 K 0.0700 0.008267 0.0700 0.0318 Cl 0.9110 0.021315 0.9110 0.4563 Ca 24.0819 0.122339 24.0819 10.6684 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0328 0.020661 0.0328 0.0106 C 17.2081 17.2081 25.4385 O 56.3835 56.3835 62.5706 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 441 x= -16229.0 y= 2870.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.1 4.6 3.6 6.37 0.0252 4.7 0.0292 Mg 109.5 2.1 2.5 43.50 0.0603 2.2 0.0112 Sr 30.1 2.9 14.3 2.11 0.0023 2.9 0.0404 P 27.9 4.2 2.4 11.85 0.0330 4.2 0.0400 K 15.2 5.7 5.1 2.97 0.0093 5.8 0.0192 Cl 82.9 2.0 2.2 37.69 0.0179 2.0 0.0229 Ca 2923.8 0.4 17.7 165.65 0.6475 0.5 0.0339 Ba 9.1 5.2 10.8 0.84 0.0000 5.3 0.0000 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0566 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0637 Elt. k-ratio Correc. Na 0.0013 2.3268 Mg 0.0044 1.6993 Sr 0.0014 1.3814 P 0.0052 1.2020 K 0.0008 1.0462 Cl 0.0100 1.1256 Ca 0.2350 1.1010 Ba 0.0000 NaN Fe 0.0001 1.2592 Mn 0.0002 1.2808 iteration : 2 Analysis no. 441 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2930 0.017433 0.2930 0.2308 Mg 0.7416 0.016561 0.7416 0.5526 Sr 0.1942 0.012954 0.1942 0.0401 P 0.6210 0.030071 0.6210 0.3631 K 0.0864 0.008657 0.0864 0.0400 Cl 1.1207 0.023486 1.1207 0.5725 Ca 25.8747 0.127933 25.8747 11.6914 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0161 0.014215 0.0161 0.0052 Mn 0.0272 0.020366 0.0272 0.0090 C 16.2357 16.2357 24.4800 O 54.7894 54.7894 62.0153 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 442 x= -16228.0 y= 2875.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.9 4.9 3.6 5.76 0.0224 4.9 0.0293 Mg 89.9 2.4 2.5 35.69 0.0492 2.4 0.0112 Sr 29.8 2.9 14.3 2.08 0.0022 2.9 0.0404 P 31.9 4.0 2.4 13.55 0.0381 4.0 0.0401 K 15.1 5.8 5.1 2.95 0.0092 5.8 0.0191 Cl 63.6 2.3 2.2 28.92 0.0136 2.3 0.0230 Ca 2912.3 0.4 17.7 165.00 0.6451 0.5 0.0340 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0755 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0637 Elt. k-ratio Correc. Na 0.0011 2.3307 Mg 0.0036 1.7008 Sr 0.0014 1.3812 P 0.0060 1.2021 K 0.0008 1.0452 Cl 0.0076 1.1262 Ca 0.2341 1.1011 Ba 0.0000 1.5365 Fe 0.0000 NaN Mn 0.0002 1.2814 iteration : 2 Analysis no. 442 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2604 0.016726 0.2604 0.2045 Mg 0.6061 0.015027 0.6061 0.4502 Sr 0.1902 0.012906 0.1902 0.0392 P 0.7186 0.032037 0.7186 0.4189 K 0.0855 0.008629 0.0855 0.0395 Cl 0.8535 0.020647 0.8535 0.4347 Ca 25.7793 0.127643 25.7793 11.6130 Ba 0.0026 0.019302 0.0026 0.0003 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0199 0.020046 0.0199 0.0065 C 16.3499 16.3499 24.5773 O 55.1340 55.1340 62.2159 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 443 x= -16228.0 y= 2880.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 29.9 4.1 3.6 8.23 0.0340 4.1 0.0293 Mg 78.0 2.5 2.5 30.98 0.0425 2.6 0.0112 Sr 23.0 3.3 14.3 1.61 0.0013 3.3 0.0404 P 31.6 4.0 2.4 13.43 0.0377 4.0 0.0401 K 18.6 5.2 5.1 3.64 0.0125 5.2 0.0191 Cl 53.7 2.5 2.2 24.39 0.0114 2.5 0.0230 Ca 2889.0 0.4 17.7 163.67 0.6398 0.5 0.0340 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.1 9.0 3.3 0.94 0.0000 9.0 0.0000 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0637 Elt. k-ratio Correc. Na 0.0017 2.3322 Mg 0.0031 1.7044 Sr 0.0008 1.3823 P 0.0059 1.2021 K 0.0011 1.0449 Cl 0.0063 1.1264 Ca 0.2322 1.1015 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2821 iteration : 2 Analysis no. 443 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3955 0.019576 0.3955 0.3096 Mg 0.5248 0.014041 0.5248 0.3886 Sr 0.1076 0.011881 0.1076 0.0221 P 0.7112 0.031890 0.7112 0.4132 K 0.1155 0.009346 0.1155 0.0532 Cl 0.7149 0.019007 0.7149 0.3629 Ca 25.5741 0.126999 25.5741 11.4830 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0089 0.019540 0.0089 0.0029 C 16.4707 16.4707 24.6783 O 55.3768 55.3768 62.2862 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 444 x= -16227.0 y= 2885.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.7 4.9 3.6 5.71 0.0221 4.9 0.0293 Mg 100.9 2.2 2.5 40.06 0.0554 2.2 0.0112 Sr 27.7 3.0 14.3 1.94 0.0019 3.0 0.0403 P 32.7 3.9 2.4 13.89 0.0392 3.9 0.0400 K 16.7 5.5 5.1 3.27 0.0108 5.5 0.0190 Cl 62.4 2.3 2.2 28.36 0.0133 2.3 0.0229 Ca 3131.9 0.4 17.7 177.43 0.6940 0.5 0.0339 Ba 9.2 5.2 10.8 0.86 0.0000 5.2 0.0000 Fe 2.9 9.3 3.3 0.88 0.0000 9.3 0.0000 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0636 Elt. k-ratio Correc. Na 0.0011 2.3294 Mg 0.0040 1.6995 Sr 0.0012 1.3794 P 0.0061 1.1996 K 0.0010 1.0377 Cl 0.0074 1.1221 Ca 0.2519 1.0983 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2796 iteration : 2 Analysis no. 444 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2572 0.016648 0.2572 0.2052 Mg 0.6819 0.015901 0.6819 0.5146 Sr 0.1645 0.012580 0.1645 0.0344 P 0.7366 0.032350 0.7366 0.4362 K 0.0990 0.008912 0.0990 0.0464 Cl 0.8333 0.020376 0.8333 0.4311 Ca 27.6648 0.133452 27.6648 12.6608 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0180 0.019934 0.0180 0.0060 C 15.5951 15.5951 23.8161 O 53.9496 53.9496 61.8490 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 445 x= -16227.0 y= 2889.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 39.3 3.6 3.6 10.84 0.0462 3.6 0.0291 Mg 164.6 1.7 2.5 65.35 0.0913 1.8 0.0112 Sr 38.1 2.6 14.3 2.67 0.0034 2.6 0.0403 P 37.4 3.7 2.4 15.90 0.0452 3.7 0.0400 K 18.6 5.2 5.1 3.64 0.0125 5.2 0.0189 Cl 69.2 2.2 2.2 31.46 0.0149 2.2 0.0228 Ca 3337.8 0.4 17.7 189.10 0.7400 0.5 0.0338 Ba 11.3 4.7 10.8 1.05 0.0003 4.7 0.0755 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0563 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0635 Elt. k-ratio Correc. Na 0.0023 2.3154 Mg 0.0066 1.6965 Sr 0.0021 1.3797 P 0.0071 1.2000 K 0.0011 1.0335 Cl 0.0083 1.1201 Ca 0.2686 1.0953 Ba 0.0001 1.5369 Fe 0.0001 1.2537 Mn 0.0004 1.2763 iteration : 3 Analysis no. 445 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5343 0.022046 0.5343 0.4359 Mg 1.1213 0.020298 1.1213 0.8653 Sr 0.2929 0.014077 0.2929 0.0627 P 0.8513 0.034504 0.8513 0.5155 K 0.1143 0.009246 0.1143 0.0548 Cl 0.9260 0.021395 0.9260 0.4899 Ca 29.4163 0.138763 29.4163 13.7662 Ba 0.0131 0.019487 0.0131 0.0018 Fe 0.0126 0.014056 0.0126 0.0042 Mn 0.0509 0.021344 0.0509 0.0174 C 14.4677 14.4677 22.5931 O 52.1993 52.1993 61.1931 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 446 x= -16227.0 y= 2894.0 z= -280. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.1 5.9 3.6 3.89 0.0136 6.0 0.0294 Mg 41.2 3.5 2.5 16.34 0.0218 3.5 0.0112 Sr 25.1 3.2 14.3 1.76 0.0016 3.2 0.0404 P 28.8 4.2 2.4 12.24 0.0341 4.2 0.0401 K 14.6 5.9 5.1 2.85 0.0088 5.9 0.0193 Cl 57.9 2.4 2.2 26.31 0.0123 2.4 0.0231 Ca 2595.7 0.4 17.7 147.05 0.5745 0.5 0.0341 Ba 7.9 5.6 10.8 0.73 0.0000 5.6 0.0000 Fe 3.0 9.1 3.3 0.91 0.0000 9.1 0.0000 Mn 2.5 14.1 2.7 0.92 0.0000 14.1 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3399 Mg 0.0016 1.7048 Sr 0.0010 1.3829 P 0.0053 1.2042 K 0.0008 1.0549 Cl 0.0069 1.1314 Ca 0.2085 1.1054 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 446 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1585 0.014260 0.1585 0.1212 Mg 0.2686 0.010307 0.2686 0.1943 Sr 0.1335 0.012219 0.1335 0.0268 P 0.6442 0.030580 0.6442 0.3657 K 0.0819 0.008598 0.0819 0.0369 Cl 0.7772 0.019808 0.7772 0.3855 Ca 23.0447 0.119061 23.0447 10.1105 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.6743 17.6743 25.8756 O 57.2171 57.2171 62.8835 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 447 x= -16226.0 y= 2899.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 19.2 5.1 3.6 5.28 0.0201 5.1 0.0293 Mg 89.0 2.4 2.5 35.36 0.0487 2.4 0.0112 Sr 26.3 3.1 14.3 1.84 0.0017 3.1 0.0403 P 28.2 4.2 2.4 11.98 0.0333 4.2 0.0399 K 17.7 5.3 5.1 3.46 0.0116 5.3 0.0189 Cl 61.7 2.3 2.2 28.03 0.0132 2.3 0.0228 Ca 3263.5 0.4 17.7 184.89 0.7232 0.5 0.0338 Ba 10.2 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0564 Mn 4.5 10.6 2.7 1.64 0.0017 10.6 0.0636 Elt. k-ratio Correc. Na 0.0010 2.3327 Mg 0.0035 1.7005 Sr 0.0011 1.3780 P 0.0052 1.1979 K 0.0010 1.0325 Cl 0.0073 1.1188 Ca 0.2625 1.0965 Ba 0.0000 NaN Fe 0.0001 1.2564 Mn 0.0005 1.2787 iteration : 3 Analysis no. 447 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2342 0.016125 0.2342 0.1884 Mg 0.5999 0.014951 0.5999 0.4565 Sr 0.1474 0.012356 0.1474 0.0311 P 0.6262 0.030119 0.6262 0.3739 K 0.1065 0.009056 0.1065 0.0504 Cl 0.8205 0.020195 0.8205 0.4280 Ca 28.7808 0.136836 28.7808 13.2800 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0084 0.013956 0.0084 0.0028 Mn 0.0638 0.021923 0.0638 0.0215 C 15.2702 15.2702 23.5119 O 53.3420 53.3420 61.6557 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 448 x= -16226.0 y= 2903.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 31.2 4.0 3.6 8.59 0.0357 4.0 0.0292 Mg 106.3 2.2 2.5 42.23 0.0585 2.2 0.0112 Sr 32.8 2.8 14.3 2.29 0.0027 2.8 0.0402 P 27.9 4.2 2.4 11.85 0.0330 4.2 0.0399 K 19.2 5.1 5.1 3.76 0.0130 5.1 0.0188 Cl 74.3 2.1 2.2 33.76 0.0160 2.1 0.0228 Ca 3415.8 0.4 17.7 193.52 0.7572 0.5 0.0337 Ba 11.0 4.8 10.8 1.02 0.0001 4.8 0.0755 Fe 3.0 9.2 3.3 0.89 0.0000 9.2 0.0000 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0635 Elt. k-ratio Correc. Na 0.0018 2.3245 Mg 0.0042 1.6990 Sr 0.0016 1.3767 P 0.0052 1.1970 K 0.0012 1.0292 Cl 0.0089 1.1164 Ca 0.2748 1.0946 Ba 0.0000 1.5382 Fe 0.0000 NaN Mn 0.0002 1.2768 iteration : 3 Analysis no. 448 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4138 0.019892 0.4138 0.3377 Mg 0.7194 0.016316 0.7194 0.5553 Sr 0.2264 0.013298 0.2264 0.0485 P 0.6185 0.029949 0.6185 0.3746 K 0.1189 0.009323 0.1189 0.0570 Cl 0.9926 0.022071 0.9926 0.5252 Ca 30.0815 0.140772 30.0815 14.0806 Ba 0.0059 0.019378 0.0059 0.0008 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0253 0.020220 0.0253 0.0086 C 14.6070 14.6070 22.8155 O 52.1908 52.1908 61.1961 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 449 x= -16225.0 y= 2908.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 36.3 3.7 3.6 10.00 0.0423 3.7 0.0292 Mg 102.4 2.2 2.5 40.68 0.0563 2.2 0.0112 Sr 25.9 3.1 14.3 1.81 0.0017 3.1 0.0404 P 32.2 3.9 2.4 13.68 0.0385 4.0 0.0401 K 18.5 5.2 5.1 3.62 0.0124 5.2 0.0192 Cl 70.2 2.2 2.2 31.91 0.0151 2.2 0.0230 Ca 2769.5 0.4 17.7 156.90 0.6131 0.5 0.0340 Ba 10.2 5.0 10.8 0.95 0.0000 5.0 0.0000 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0566 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0637 Elt. k-ratio Correc. Na 0.0021 2.3262 Mg 0.0041 1.7033 Sr 0.0010 1.3840 P 0.0060 1.2040 K 0.0011 1.0510 Cl 0.0084 1.1291 Ca 0.2225 1.1029 Ba 0.0000 NaN Fe 0.0001 1.2609 Mn 0.0003 1.2822 iteration : 2 Analysis no. 449 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4908 0.021330 0.4908 0.3824 Mg 0.6940 0.016054 0.6940 0.5115 Sr 0.1425 0.012340 0.1425 0.0291 P 0.7269 0.032223 0.7269 0.4204 K 0.1153 0.009380 0.1153 0.0528 Cl 0.9470 0.021711 0.9470 0.4785 Ca 24.5416 0.123771 24.5416 10.9691 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0127 0.014132 0.0127 0.0041 Mn 0.0364 0.020796 0.0364 0.0119 C 16.6691 16.6691 24.8616 O 55.6236 55.6236 62.2785 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 450 x= -16225.0 y= 2913.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 25.2 4.5 3.6 6.93 0.0279 4.5 0.0293 Mg 68.9 2.7 2.5 27.37 0.0374 2.7 0.0112 Sr 25.8 3.1 14.3 1.81 0.0017 3.1 0.0404 P 24.8 4.5 2.4 10.55 0.0290 4.5 0.0401 K 13.2 6.1 5.1 2.59 0.0075 6.2 0.0194 Cl 99.7 1.8 2.2 45.31 0.0216 1.8 0.0231 Ca 2543.7 0.4 17.7 144.11 0.5628 0.5 0.0341 Ba 9.5 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.0 9.2 3.3 0.90 0.0000 9.2 0.0000 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0638 Elt. k-ratio Correc. Na 0.0014 2.3301 Mg 0.0027 1.7027 Sr 0.0010 1.3836 P 0.0045 1.2045 K 0.0007 1.0600 Cl 0.0120 1.1319 Ca 0.2042 1.1062 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2843 iteration : 2 Analysis no. 450 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3243 0.018120 0.3243 0.2485 Mg 0.4610 0.013198 0.4610 0.3341 Sr 0.1422 0.012332 0.1422 0.0286 P 0.5479 0.028551 0.5479 0.3116 K 0.0706 0.008336 0.0706 0.0318 Cl 1.3608 0.025859 1.3608 0.6761 Ca 22.5935 0.117624 22.5935 9.9299 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0328 0.020667 0.0328 0.0105 C 17.6248 17.6248 25.8483 O 56.8422 56.8422 62.5807 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 451 x= -16225.0 y= 2918.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 25.7 4.4 3.6 7.09 0.0286 4.4 0.0292 Mg 83.3 2.4 2.5 33.09 0.0455 2.5 0.0112 Sr 27.9 3.0 14.3 1.95 0.0020 3.0 0.0405 P 30.6 4.0 2.4 13.02 0.0365 4.1 0.0402 K 17.6 5.3 5.1 3.45 0.0116 5.3 0.0195 Cl 88.3 1.9 2.2 40.15 0.0191 1.9 0.0232 Ca 2387.8 0.5 17.7 135.28 0.5283 0.5 0.0342 Ba 10.6 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0639 Elt. k-ratio Correc. Na 0.0014 2.3284 Mg 0.0033 1.7024 Sr 0.0012 1.3858 P 0.0057 1.2071 K 0.0010 1.0657 Cl 0.0106 1.1361 Ca 0.1917 1.1082 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2854 iteration : 2 Analysis no. 451 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3325 0.018286 0.3325 0.2523 Mg 0.5611 0.014490 0.5611 0.4028 Sr 0.1681 0.012674 0.1681 0.0335 P 0.6911 0.031571 0.6911 0.3893 K 0.1095 0.009340 0.1095 0.0489 Cl 1.2072 0.024459 1.2072 0.5940 Ca 21.2460 0.113307 21.2460 9.2477 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0199 0.020110 0.0199 0.0063 C 18.0173 18.0173 26.1695 O 57.6474 57.6474 62.8559 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 452 x= -16224.0 y= 2922.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 32.5 3.9 3.6 8.95 0.0374 3.9 0.0293 Mg 95.6 2.3 2.5 37.96 0.0525 2.3 0.0112 Sr 29.4 2.9 14.3 2.06 0.0022 2.9 0.0406 P 26.4 4.4 2.4 11.21 0.0310 4.4 0.0404 K 17.0 5.4 5.1 3.33 0.0110 5.4 0.0196 Cl 82.5 2.0 2.2 37.51 0.0178 2.0 0.0233 Ca 2210.6 0.5 17.7 125.24 0.4889 0.5 0.0343 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.1 9.0 3.3 0.94 0.0000 9.0 0.0000 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0640 Elt. k-ratio Correc. Na 0.0019 2.3276 Mg 0.0038 1.7046 Sr 0.0013 1.3892 P 0.0049 1.2104 K 0.0010 1.0718 Cl 0.0099 1.1397 Ca 0.1774 1.1104 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2869 iteration : 2 Analysis no. 452 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4341 0.020303 0.4341 0.3254 Mg 0.6473 0.015533 0.6473 0.4589 Sr 0.1865 0.012928 0.1865 0.0367 P 0.5889 0.029528 0.5889 0.3277 K 0.1049 0.009272 0.1049 0.0462 Cl 1.1298 0.023738 1.1298 0.5491 Ca 19.7022 0.108273 19.7022 8.4710 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0292 0.020558 0.0292 0.0092 C 18.6029 18.6029 26.6899 O 58.5741 58.5741 63.0859 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 453 x= -16224.0 y= 2927.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.0 4.7 3.6 6.34 0.0251 4.7 0.0294 Mg 46.8 3.3 2.5 18.59 0.0250 3.3 0.0113 Sr 20.0 3.5 14.3 1.40 0.0008 3.5 0.0406 P 22.3 4.7 2.4 9.47 0.0257 4.7 0.0403 K 13.7 6.0 5.1 2.68 0.0079 6.1 0.0195 Cl 72.1 2.1 2.2 32.76 0.0155 2.2 0.0232 Ca 2282.7 0.5 17.7 129.32 0.5049 0.5 0.0342 Ba 8.3 5.5 10.8 0.77 0.0000 5.5 0.0000 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0570 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0640 Elt. k-ratio Correc. Na 0.0013 2.3389 Mg 0.0018 1.7078 Sr 0.0005 1.3873 P 0.0040 1.2077 K 0.0007 1.0669 Cl 0.0086 1.1368 Ca 0.1832 1.1095 Ba 0.0000 NaN Fe 0.0000 1.2674 Mn 0.0003 1.2875 iteration : 2 Analysis no. 453 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2932 0.017499 0.2932 0.2196 Mg 0.3086 0.010983 0.3086 0.2187 Sr 0.0710 0.011439 0.0710 0.0140 P 0.4872 0.027250 0.4872 0.2709 K 0.0750 0.008497 0.0750 0.0330 Cl 0.9802 0.022155 0.9802 0.4762 Ca 20.3306 0.110333 20.3306 8.7363 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0009 0.013852 0.0009 0.0003 Mn 0.0384 0.020976 0.0384 0.0121 C 18.7069 18.7069 26.8241 O 58.7080 58.7080 63.1949 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 454 x= -16224.0 y= 2932.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 45.2 3.3 3.6 12.46 0.0539 3.3 0.0292 Mg 119.2 2.0 2.5 47.34 0.0658 2.1 0.0112 Sr 31.9 2.8 14.3 2.24 0.0025 2.8 0.0405 P 34.1 3.8 2.4 14.49 0.0410 3.8 0.0402 K 24.1 4.6 5.1 4.73 0.0176 4.6 0.0193 Cl 69.7 2.2 2.2 31.68 0.0150 2.2 0.0231 Ca 2719.2 0.4 17.7 154.05 0.6023 0.5 0.0341 Ba 11.1 4.7 10.8 1.03 0.0002 4.8 0.0754 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0567 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0638 Elt. k-ratio Correc. Na 0.0027 2.3206 Mg 0.0048 1.7029 Sr 0.0016 1.3851 P 0.0064 1.2057 K 0.0016 1.0536 Cl 0.0083 1.1309 Ca 0.2186 1.1035 Ba 0.0001 1.5349 Fe 0.0000 1.2608 Mn 0.0001 1.2820 iteration : 3 Analysis no. 454 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6243 0.023595 0.6243 0.4861 Mg 0.8108 0.017324 0.8108 0.5971 Sr 0.2177 0.013267 0.2177 0.0445 P 0.7749 0.033182 0.7749 0.4478 K 0.1646 0.010482 0.1646 0.0754 Cl 0.9421 0.021684 0.9421 0.4757 Ca 24.1218 0.122482 24.1218 10.7729 Ba 0.0085 0.019391 0.0085 0.0011 Fe 0.0051 0.013911 0.0051 0.0016 Mn 0.0162 0.019894 0.0162 0.0053 C 16.6651 16.6651 24.8358 O 55.6486 55.6486 62.2566 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 455 x= -16223.0 y= 2937.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 16.1 5.6 3.6 4.43 0.0161 5.6 0.0294 Mg 66.8 2.7 2.5 26.53 0.0362 2.8 0.0112 Sr 23.3 3.3 14.3 1.63 0.0013 3.3 0.0405 P 25.9 4.4 2.4 11.02 0.0305 4.4 0.0402 K 15.2 5.7 5.1 2.97 0.0093 5.8 0.0194 Cl 65.7 2.2 2.2 29.88 0.0141 2.3 0.0231 Ca 2564.8 0.4 17.7 145.31 0.5679 0.5 0.0341 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.1 9.0 3.3 0.93 0.0000 9.0 0.0000 Mn 2.7 13.6 2.7 1.00 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3368 Mg 0.0026 1.7038 Sr 0.0008 1.3844 P 0.0048 1.2050 K 0.0008 1.0566 Cl 0.0078 1.1318 Ca 0.2061 1.1058 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 455 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1879 0.015018 0.1879 0.1436 Mg 0.4470 0.013018 0.4470 0.3232 Sr 0.1109 0.011948 0.1109 0.0222 P 0.5754 0.029164 0.5754 0.3264 K 0.0873 0.008748 0.0873 0.0392 Cl 0.8876 0.021092 0.8876 0.4398 Ca 22.7927 0.118290 22.7927 9.9912 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.7041 17.7041 25.8968 O 57.2070 57.2070 62.8176 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 456 x= -16223.0 y= 2941.0 z= -279. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 45.0 3.3 3.6 12.39 0.0536 3.4 0.0291 Mg 129.4 2.0 2.5 51.37 0.0715 2.0 0.0112 Sr 34.4 2.7 14.3 2.41 0.0029 2.7 0.0404 P 31.0 4.0 2.4 13.19 0.0370 4.0 0.0401 K 21.7 4.8 5.1 4.26 0.0154 4.8 0.0193 Cl 94.4 1.9 2.2 42.91 0.0204 1.9 0.0230 Ca 2826.8 0.4 17.7 160.15 0.6262 0.5 0.0340 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0754 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0566 Mn 3.1 12.8 2.7 1.13 0.0003 12.8 0.0637 Elt. k-ratio Correc. Na 0.0027 2.3166 Mg 0.0052 1.7002 Sr 0.0018 1.3834 P 0.0058 1.2041 K 0.0014 1.0515 Cl 0.0114 1.1283 Ca 0.2273 1.1023 Ba 0.0000 1.5351 Fe 0.0001 1.2591 Mn 0.0001 1.2806 iteration : 3 Analysis no. 456 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6194 0.023488 0.6194 0.4870 Mg 0.8798 0.018016 0.8798 0.6544 Sr 0.2482 0.013604 0.2482 0.0512 P 0.6993 0.031690 0.6993 0.4081 K 0.1435 0.010018 0.1435 0.0664 Cl 1.2837 0.025106 1.2837 0.6546 Ca 25.0497 0.125386 25.0497 11.2981 Ba 0.0033 0.019300 0.0033 0.0004 Fe 0.0118 0.014094 0.0118 0.0038 Mn 0.0125 0.019698 0.0125 0.0041 C 16.2542 16.2542 24.4634 O 54.7946 54.7946 61.9085 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 457 x= -16222.0 y= 2946.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 27.2 4.3 3.6 7.50 0.0306 4.3 0.0293 Mg 74.4 2.6 2.5 29.55 0.0405 2.6 0.0112 Sr 29.2 2.9 14.3 2.05 0.0022 2.9 0.0404 P 28.8 4.2 2.4 12.26 0.0342 4.2 0.0401 K 20.7 4.9 5.1 4.06 0.0145 4.9 0.0193 Cl 86.4 2.0 2.2 39.28 0.0187 2.0 0.0230 Ca 2705.7 0.4 17.7 153.29 0.5993 0.5 0.0341 Ba 9.5 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.2 8.8 3.3 0.97 0.0000 8.8 0.0000 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0638 Elt. k-ratio Correc. Na 0.0015 2.3287 Mg 0.0029 1.7020 Sr 0.0013 1.3822 P 0.0054 1.2033 K 0.0013 1.0538 Cl 0.0104 1.1294 Ca 0.2175 1.1040 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2827 iteration : 2 Analysis no. 457 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3552 0.018760 0.3552 0.2755 Mg 0.4993 0.013707 0.4993 0.3663 Sr 0.1837 0.012839 0.1837 0.0374 P 0.6452 0.030597 0.6452 0.3714 K 0.1352 0.009852 0.1352 0.0617 Cl 1.1739 0.024062 1.1739 0.5904 Ca 24.0104 0.122140 24.0104 10.6810 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0254 0.020325 0.0254 0.0083 C 17.0016 17.0016 25.2378 O 55.9701 55.9701 62.3704 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 458 x= -16222.0 y= 2951.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 46.8 3.3 3.6 12.91 0.0560 3.3 0.0291 Mg 128.3 2.0 2.5 50.96 0.0709 2.0 0.0112 Sr 30.9 2.8 14.3 2.17 0.0024 2.9 0.0405 P 29.5 4.1 2.4 12.53 0.0350 4.1 0.0403 K 20.5 4.9 5.1 4.01 0.0142 5.0 0.0194 Cl 87.4 2.0 2.2 39.72 0.0189 2.0 0.0231 Ca 2580.5 0.4 17.7 146.19 0.5714 0.5 0.0341 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0568 Mn 2.8 13.3 2.7 1.03 0.0001 13.4 0.0638 Elt. k-ratio Correc. Na 0.0028 2.3184 Mg 0.0051 1.7026 Sr 0.0015 1.3867 P 0.0055 1.2071 K 0.0013 1.0594 Cl 0.0105 1.1330 Ca 0.2074 1.1055 Ba 0.0000 NaN Fe 0.0000 1.2621 Mn 0.0000 1.2830 iteration : 2 Analysis no. 458 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6477 0.023961 0.6477 0.4998 Mg 0.8739 0.017972 0.8739 0.6379 Sr 0.2056 0.013137 0.2056 0.0416 P 0.6632 0.031019 0.6632 0.3799 K 0.1338 0.009856 0.1338 0.0607 Cl 1.1913 0.024275 1.1913 0.5961 Ca 22.9246 0.118702 22.9246 10.1469 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0059 0.013951 0.0059 0.0019 Mn 0.0034 0.019306 0.0034 0.0011 C 17.1232 17.1232 25.2910 O 56.2274 56.2274 62.3432 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 459 x= -16222.0 y= 2955.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 22.4 4.7 3.6 6.18 0.0243 4.7 0.0292 Mg 116.4 2.1 2.5 46.21 0.0641 2.1 0.0112 Sr 32.7 2.8 14.3 2.29 0.0027 2.8 0.0404 P 26.9 4.3 2.4 11.43 0.0317 4.3 0.0401 K 19.2 5.1 5.1 3.76 0.0131 5.1 0.0192 Cl 81.7 2.0 2.2 37.13 0.0176 2.0 0.0230 Ca 2809.5 0.4 17.7 159.17 0.6223 0.5 0.0340 Ba 11.2 4.7 10.8 1.04 0.0003 4.7 0.0754 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0566 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0637 Elt. k-ratio Correc. Na 0.0012 2.3264 Mg 0.0046 1.6992 Sr 0.0016 1.3828 P 0.0050 1.2037 K 0.0012 1.0502 Cl 0.0098 1.1279 Ca 0.2259 1.1024 Ba 0.0001 1.5355 Fe 0.0001 1.2602 Mn 0.0003 1.2816 iteration : 2 Analysis no. 459 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2825 0.017205 0.2825 0.2210 Mg 0.7891 0.017074 0.7891 0.5837 Sr 0.2268 0.013354 0.2268 0.0465 P 0.5978 0.029618 0.5978 0.3470 K 0.1218 0.009526 0.1218 0.0560 Cl 1.1062 0.023370 1.1062 0.5610 Ca 24.8984 0.124911 24.8984 11.1686 Ba 0.0118 0.019450 0.0118 0.0015 Fe 0.0110 0.014080 0.0110 0.0035 Mn 0.0364 0.020796 0.0364 0.0119 C 16.5812 16.5812 24.8193 O 55.3369 55.3369 62.1799 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 460 x= -16221.0 y= 2960.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 44.4 3.4 3.6 12.24 0.0528 3.4 0.0291 Mg 125.3 2.0 2.5 49.76 0.0692 2.0 0.0112 Sr 31.6 2.8 14.3 2.22 0.0025 2.8 0.0405 P 29.3 4.1 2.4 12.47 0.0348 4.1 0.0402 K 21.4 4.8 5.1 4.19 0.0151 4.8 0.0193 Cl 88.3 1.9 2.2 40.13 0.0191 1.9 0.0231 Ca 2744.2 0.4 17.7 155.47 0.6078 0.5 0.0340 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.1 9.0 3.3 0.92 0.0000 9.1 0.0000 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0638 Elt. k-ratio Correc. Na 0.0026 2.3190 Mg 0.0050 1.7016 Sr 0.0015 1.3846 P 0.0055 1.2050 K 0.0013 1.0536 Cl 0.0106 1.1297 Ca 0.2206 1.1033 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2816 iteration : 3 Analysis no. 460 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6119 0.023380 0.6119 0.4776 Mg 0.8525 0.017748 0.8525 0.6295 Sr 0.2139 0.013218 0.2139 0.0438 P 0.6584 0.030889 0.6584 0.3815 K 0.1408 0.009974 0.1408 0.0646 Cl 1.2003 0.024324 1.2003 0.6076 Ca 24.3388 0.123166 24.3388 10.8982 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0328 0.020637 0.0328 0.0107 C 16.5939 16.5939 24.7944 O 55.3568 55.3568 62.0920 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 461 x= -16221.0 y= 2965.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.8 5.3 3.6 4.91 0.0184 5.3 0.0294 Mg 54.5 3.0 2.5 21.63 0.0293 3.0 0.0113 Sr 19.3 3.6 14.3 1.35 0.0007 3.6 0.0405 P 24.0 4.6 2.4 10.19 0.0279 4.6 0.0402 K 17.4 5.4 5.1 3.41 0.0114 5.4 0.0195 Cl 79.6 2.0 2.2 36.16 0.0172 2.0 0.0231 Ca 2404.9 0.5 17.7 136.25 0.5323 0.5 0.0342 Ba 7.2 5.9 10.8 0.67 0.0000 5.9 0.0000 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0569 Mn 3.9 11.4 2.7 1.42 0.0011 11.4 0.0640 Elt. k-ratio Correc. Na 0.0009 2.3379 Mg 0.0021 1.7053 Sr 0.0004 1.3855 P 0.0044 1.2058 K 0.0010 1.0630 Cl 0.0095 1.1342 Ca 0.1932 1.1080 Ba 0.0000 NaN Fe 0.0001 1.2659 Mn 0.0003 1.2862 iteration : 2 Analysis no. 461 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2144 0.015681 0.2144 0.1622 Mg 0.3614 0.011797 0.3614 0.2586 Sr 0.0623 0.011308 0.0623 0.0124 P 0.5280 0.028144 0.5280 0.2965 K 0.1075 0.009278 0.1075 0.0478 Cl 1.0828 0.023203 1.0828 0.5311 Ca 21.4018 0.113826 21.4018 9.2856 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0127 0.014198 0.0127 0.0040 Mn 0.0421 0.021120 0.0421 0.0133 C 18.2424 18.2424 26.4114 O 57.9446 57.9446 62.9772 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 462 x= -16220.0 y= 2970.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 34.3 3.8 3.6 9.46 0.0398 3.8 0.0292 Mg 126.6 2.0 2.5 50.26 0.0699 2.0 0.0112 Sr 34.3 2.7 14.3 2.40 0.0029 2.7 0.0405 P 27.7 4.2 2.4 11.79 0.0328 4.3 0.0402 K 21.0 4.9 5.1 4.12 0.0147 4.9 0.0194 Cl 95.0 1.9 2.2 43.17 0.0206 1.9 0.0231 Ca 2611.9 0.4 17.7 147.97 0.5785 0.5 0.0341 Ba 10.4 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0638 Elt. k-ratio Correc. Na 0.0020 2.3204 Mg 0.0051 1.6998 Sr 0.0018 1.3852 P 0.0051 1.2062 K 0.0013 1.0586 Cl 0.0115 1.1320 Ca 0.2099 1.1051 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2826 iteration : 2 Analysis no. 462 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4606 0.020761 0.4606 0.3563 Mg 0.8605 0.017822 0.8605 0.6295 Sr 0.2467 0.013606 0.2467 0.0501 P 0.6200 0.030124 0.6200 0.3560 K 0.1385 0.009956 0.1385 0.0630 Cl 1.2963 0.025272 1.2963 0.6502 Ca 23.2003 0.119585 23.2003 10.2929 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0328 0.020658 0.0328 0.0106 C 17.0745 17.0745 25.2780 O 56.0697 56.0697 62.3135 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 463 x= -16220.0 y= 2974.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 18.8 5.2 3.6 5.18 0.0197 5.2 0.0294 Mg 56.2 3.0 2.5 22.30 0.0302 3.0 0.0113 Sr 22.9 3.3 14.3 1.60 0.0012 3.3 0.0405 P 26.2 4.4 2.4 11.15 0.0308 4.4 0.0402 K 19.0 5.1 5.1 3.72 0.0128 5.1 0.0195 Cl 75.9 2.1 2.2 34.49 0.0163 2.1 0.0231 Ca 2444.0 0.5 17.7 138.47 0.5411 0.5 0.0342 Ba 8.4 5.4 10.8 0.78 0.0000 5.5 0.0000 Fe 2.8 9.5 3.3 0.83 0.0000 9.5 0.0000 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0640 Elt. k-ratio Correc. Na 0.0010 2.3362 Mg 0.0022 1.7045 Sr 0.0008 1.3849 P 0.0048 1.2057 K 0.0011 1.0617 Cl 0.0091 1.1339 Ca 0.1964 1.1075 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2858 iteration : 2 Analysis no. 463 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2294 0.016037 0.2294 0.1741 Mg 0.3732 0.011971 0.3732 0.2678 Sr 0.1057 0.011885 0.1057 0.0211 P 0.5831 0.029342 0.5831 0.3284 K 0.1210 0.009584 0.1210 0.0540 Cl 1.0313 0.022669 1.0313 0.5075 Ca 21.7472 0.114950 21.7472 9.4655 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0218 0.020212 0.0218 0.0069 C 18.0692 18.0692 26.2440 O 57.7180 57.7180 62.9307 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 464 x= -16220.0 y= 2979.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 24.3 4.5 3.6 6.69 0.0267 4.6 0.0293 Mg 71.5 2.6 2.5 28.40 0.0389 2.7 0.0112 Sr 26.1 3.1 14.3 1.83 0.0017 3.1 0.0404 P 27.0 4.3 2.4 11.47 0.0318 4.3 0.0401 K 20.7 4.9 5.1 4.05 0.0144 4.9 0.0192 Cl 80.4 2.0 2.2 36.52 0.0173 2.0 0.0230 Ca 2812.6 0.4 17.7 159.35 0.6232 0.5 0.0340 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.3 8.7 3.3 0.99 0.0000 8.7 0.0000 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0638 Elt. k-ratio Correc. Na 0.0013 2.3311 Mg 0.0028 1.7022 Sr 0.0011 1.3813 P 0.0050 1.2019 K 0.0013 1.0492 Cl 0.0096 1.1269 Ca 0.2262 1.1026 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2823 iteration : 2 Analysis no. 464 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3111 0.017854 0.3111 0.2427 Mg 0.4793 0.013447 0.4793 0.3537 Sr 0.1451 0.012361 0.1451 0.0297 P 0.5996 0.029635 0.5996 0.3471 K 0.1342 0.009801 0.1342 0.0616 Cl 1.0871 0.023170 1.0871 0.5499 Ca 24.9398 0.125067 24.9398 11.1584 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0107 0.019645 0.0107 0.0035 C 16.7368 16.7368 24.9878 O 55.5562 55.5562 62.2658 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 465 x= -16219.0 y= 2984.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 20.0 5.0 3.6 5.51 0.0212 5.0 0.0293 Mg 83.9 2.4 2.5 33.33 0.0459 2.5 0.0112 Sr 31.0 2.8 14.3 2.17 0.0024 2.9 0.0405 P 27.5 4.3 2.4 11.70 0.0325 4.3 0.0402 K 17.7 5.3 5.1 3.46 0.0116 5.3 0.0193 Cl 73.8 2.1 2.2 33.56 0.0159 2.1 0.0231 Ca 2668.1 0.4 17.7 151.16 0.5911 0.5 0.0341 Ba 10.7 4.8 10.8 0.99 0.0000 4.8 0.0000 Fe 3.0 9.1 3.3 0.91 0.0000 9.1 0.0000 Mn 2.9 13.2 2.7 1.05 0.0001 13.2 0.0639 Elt. k-ratio Correc. Na 0.0011 2.3311 Mg 0.0033 1.7014 Sr 0.0015 1.3832 P 0.0051 1.2045 K 0.0010 1.0542 Cl 0.0088 1.1304 Ca 0.2145 1.1044 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2834 iteration : 2 Analysis no. 465 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2471 0.016429 0.2471 0.1908 Mg 0.5654 0.014543 0.5654 0.4130 Sr 0.2064 0.013123 0.2064 0.0418 P 0.6144 0.029987 0.6144 0.3522 K 0.1089 0.009256 0.1089 0.0494 Cl 0.9998 0.022303 0.9998 0.5007 Ca 23.6927 0.121154 23.6927 10.4943 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0052 0.019406 0.0052 0.0017 C 17.1973 17.1973 25.4184 O 56.3629 56.3629 62.5378 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 466 x= -16219.0 y= 2989.0 z= -278. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 36.7 3.7 3.6 10.12 0.0429 3.7 0.0293 Mg 88.8 2.4 2.5 35.26 0.0486 2.4 0.0112 Sr 25.5 3.1 14.3 1.79 0.0016 3.1 0.0405 P 29.0 4.2 2.4 12.32 0.0344 4.2 0.0402 K 26.1 4.4 5.1 5.11 0.0194 4.4 0.0193 Cl 81.6 2.0 2.2 37.07 0.0176 2.0 0.0230 Ca 2738.6 0.4 17.7 155.15 0.6069 0.5 0.0341 Ba 8.8 5.3 10.8 0.81 0.0000 5.3 0.0000 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0567 Mn 2.7 13.7 2.7 0.98 0.0000 13.7 0.0000 Elt. k-ratio Correc. Na 0.0021 2.3260 Mg 0.0035 1.7033 Sr 0.0010 1.3833 P 0.0054 1.2035 K 0.0017 1.0525 Cl 0.0098 1.1289 Ca 0.2202 1.1036 Ba 0.0000 NaN Fe 0.0001 1.2612 Mn 0.0000 NaN iteration : 2 Analysis no. 466 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4980 0.021472 0.4980 0.3873 Mg 0.5997 0.014969 0.5997 0.4412 Sr 0.1383 0.012292 0.1383 0.0282 P 0.6493 0.030689 0.6493 0.3748 K 0.1814 0.010821 0.1814 0.0830 Cl 1.1059 0.023384 1.1059 0.5578 Ca 24.3053 0.123089 24.3053 10.8438 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0085 0.014023 0.0085 0.0027 Mn 0.0000 0.000000 0.0000 0.0000 C 16.8083 16.8083 25.0239 O 55.7054 55.7054 62.2571 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 467 x= -16218.0 y= 2993.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 29.5 4.1 3.6 8.13 0.0335 4.1 0.0293 Mg 81.3 2.5 2.5 32.28 0.0444 2.5 0.0112 Sr 29.8 2.9 14.3 2.09 0.0022 2.9 0.0405 P 29.4 4.1 2.4 12.51 0.0350 4.1 0.0403 K 24.0 4.6 5.1 4.70 0.0175 4.6 0.0195 Cl 83.2 2.0 2.2 37.83 0.0180 2.0 0.0232 Ca 2474.1 0.4 17.7 140.17 0.5478 0.5 0.0342 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0569 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0639 Elt. k-ratio Correc. Na 0.0017 2.3282 Mg 0.0032 1.7031 Sr 0.0014 1.3851 P 0.0055 1.2064 K 0.0016 1.0622 Cl 0.0100 1.1342 Ca 0.1988 1.1070 Ba 0.0000 NaN Fe 0.0001 1.2639 Mn 0.0002 1.2845 iteration : 2 Analysis no. 467 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3899 0.019455 0.3899 0.2978 Mg 0.5474 0.014327 0.5474 0.3954 Sr 0.1915 0.012959 0.1915 0.0384 P 0.6618 0.030984 0.6618 0.3751 K 0.1647 0.010543 0.1647 0.0740 Cl 1.1344 0.023727 1.1344 0.5618 Ca 22.0066 0.115780 22.0066 9.6398 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0119 0.014153 0.0119 0.0037 Mn 0.0255 0.020359 0.0255 0.0081 C 17.7138 17.7138 25.8926 O 57.1525 57.1525 62.7134 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 468 x= -16218.0 y= 2998.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 25.2 4.4 3.6 6.95 0.0280 4.5 0.0293 Mg 73.0 2.6 2.5 28.98 0.0397 2.6 0.0113 Sr 22.0 3.4 14.3 1.54 0.0011 3.4 0.0405 P 29.2 4.1 2.4 12.43 0.0347 4.1 0.0402 K 26.0 4.4 5.1 5.09 0.0193 4.4 0.0193 Cl 72.6 2.1 2.2 33.02 0.0156 2.1 0.0231 Ca 2659.0 0.4 17.7 150.65 0.5892 0.5 0.0341 Ba 8.7 5.4 10.8 0.81 0.0000 5.4 0.0000 Fe 3.7 8.2 3.3 1.11 0.0002 8.3 0.0568 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0639 Elt. k-ratio Correc. Na 0.0014 2.3324 Mg 0.0029 1.7037 Sr 0.0007 1.3834 P 0.0054 1.2036 K 0.0017 1.0542 Cl 0.0087 1.1300 Ca 0.2138 1.1046 Ba 0.0000 NaN Fe 0.0001 1.2627 Mn 0.0001 1.2836 iteration : 2 Analysis no. 468 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3258 0.018176 0.3258 0.2514 Mg 0.4900 0.013598 0.4900 0.3577 Sr 0.0955 0.011744 0.0955 0.0193 P 0.6556 0.030823 0.6556 0.3755 K 0.1809 0.010823 0.1809 0.0821 Cl 0.9830 0.022122 0.9830 0.4918 Ca 23.6219 0.120945 23.6219 10.4551 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0127 0.014170 0.0127 0.0040 Mn 0.0181 0.020016 0.0181 0.0058 C 17.2104 17.2104 25.4186 O 56.4062 56.4062 62.5387 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 469 x= -16218.0 y= 3003.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 30.2 4.1 3.6 8.33 0.0345 4.1 0.0292 Mg 103.8 2.2 2.5 41.24 0.0571 2.2 0.0112 Sr 38.2 2.6 14.3 2.67 0.0034 2.6 0.0404 P 33.8 3.8 2.4 14.38 0.0407 3.9 0.0401 K 26.8 4.3 5.1 5.26 0.0201 4.3 0.0191 Cl 79.9 2.0 2.2 36.31 0.0172 2.0 0.0230 Ca 3052.0 0.4 17.7 172.91 0.6770 0.5 0.0340 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0566 Mn 4.1 11.0 2.7 1.51 0.0014 11.0 0.0637 Elt. k-ratio Correc. Na 0.0017 2.3228 Mg 0.0041 1.6986 Sr 0.0021 1.3792 P 0.0064 1.2008 K 0.0018 1.0426 Cl 0.0096 1.1239 Ca 0.2457 1.0993 Ba 0.0000 NaN Fe 0.0000 1.2570 Mn 0.0004 1.2790 iteration : 3 Analysis no. 469 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3997 0.019626 0.3997 0.3188 Mg 0.7027 0.016140 0.7027 0.5302 Sr 0.2934 0.014090 0.2934 0.0614 P 0.7662 0.032956 0.7662 0.4536 K 0.1862 0.010852 0.1862 0.0873 Cl 1.0783 0.023054 1.0783 0.5577 Ca 27.0080 0.131489 27.0080 12.3565 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0008 0.013750 0.0008 0.0003 Mn 0.0511 0.021412 0.0511 0.0170 C 15.6315 15.6315 23.8645 O 53.8820 53.8820 61.7526 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 470 x= -16217.0 y= 3007.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 30.8 4.0 3.6 8.49 0.0352 4.0 0.0293 Mg 87.2 2.4 2.5 34.62 0.0477 2.4 0.0112 Sr 27.2 3.0 14.3 1.90 0.0019 3.0 0.0405 P 34.3 3.8 2.4 14.58 0.0413 3.8 0.0402 K 30.0 4.1 5.1 5.88 0.0231 4.1 0.0193 Cl 79.6 2.0 2.2 36.17 0.0172 2.0 0.0231 Ca 2765.8 0.4 17.7 156.69 0.6131 0.5 0.0341 Ba 8.7 5.4 10.8 0.81 0.0000 5.4 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0567 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0638 Elt. k-ratio Correc. Na 0.0018 2.3263 Mg 0.0035 1.7016 Sr 0.0011 1.3821 P 0.0065 1.2028 K 0.0020 1.0519 Cl 0.0096 1.1287 Ca 0.2225 1.1032 Ba 0.0000 NaN Fe 0.0000 1.2607 Mn 0.0002 1.2820 iteration : 2 Analysis no. 470 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4093 0.019831 0.4093 0.3193 Mg 0.5882 0.014825 0.5882 0.4341 Sr 0.1585 0.012539 0.1585 0.0325 P 0.7784 0.033217 0.7784 0.4508 K 0.2156 0.011487 0.2156 0.0989 Cl 1.0787 0.023111 1.0787 0.5457 Ca 24.5486 0.123869 24.5486 10.9853 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013893 0.0042 0.0014 Mn 0.0273 0.020411 0.0273 0.0089 C 16.6523 16.6523 24.8660 O 55.5388 55.5388 62.2572 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 471 x= -16217.0 y= 3012.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 33.3 3.9 3.6 9.17 0.0384 3.9 0.0293 Mg 83.3 2.4 2.5 33.09 0.0456 2.5 0.0112 Sr 31.3 2.8 14.3 2.19 0.0025 2.8 0.0404 P 33.2 3.9 2.4 14.11 0.0399 3.9 0.0401 K 30.3 4.1 5.1 5.93 0.0233 4.1 0.0192 Cl 74.1 2.1 2.2 33.67 0.0159 2.1 0.0230 Ca 2970.2 0.4 17.7 168.27 0.6586 0.5 0.0340 Ba 10.2 5.0 10.8 0.95 0.0000 5.0 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0566 Mn 4.3 10.8 2.7 1.57 0.0015 10.8 0.0637 Elt. k-ratio Correc. Na 0.0019 2.3264 Mg 0.0033 1.7017 Sr 0.0015 1.3800 P 0.0062 1.2010 K 0.0021 1.0444 Cl 0.0089 1.1249 Ca 0.2390 1.1004 Ba 0.0000 NaN Fe 0.0000 1.2584 Mn 0.0004 1.2801 iteration : 3 Analysis no. 471 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4462 0.020530 0.4462 0.3532 Mg 0.5614 0.014498 0.5614 0.4203 Sr 0.2090 0.013132 0.2090 0.0434 P 0.7504 0.032653 0.7504 0.4409 K 0.2162 0.011445 0.2162 0.1006 Cl 0.9984 0.022233 0.9984 0.5125 Ca 26.3026 0.129310 26.3026 11.9418 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0059 0.013918 0.0059 0.0019 Mn 0.0566 0.021663 0.0566 0.0188 C 15.9882 15.9882 24.2225 O 54.4651 54.4651 61.9441 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 472 x= -16216.0 y= 3017.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 16.8 5.5 3.6 4.62 0.0170 5.5 0.0294 Mg 71.2 2.6 2.5 28.26 0.0387 2.7 0.0112 Sr 24.0 3.2 14.3 1.68 0.0014 3.2 0.0405 P 30.6 4.0 2.4 13.02 0.0366 4.1 0.0402 K 24.4 4.5 5.1 4.78 0.0179 4.5 0.0194 Cl 74.9 2.1 2.2 34.07 0.0161 2.1 0.0231 Ca 2617.5 0.4 17.7 148.29 0.5801 0.5 0.0341 Ba 7.9 5.6 10.8 0.73 0.0000 5.6 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0640 Elt. k-ratio Correc. Na 0.0008 2.3335 Mg 0.0028 1.7019 Sr 0.0009 1.3830 P 0.0057 1.2038 K 0.0016 1.0559 Cl 0.0090 1.1310 Ca 0.2105 1.1052 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2840 iteration : 2 Analysis no. 472 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1983 0.015272 0.1983 0.1525 Mg 0.4771 0.013420 0.4771 0.3472 Sr 0.1192 0.012050 0.1192 0.0241 P 0.6899 0.031517 0.6899 0.3940 K 0.1677 0.010567 0.1677 0.0759 Cl 1.0161 0.022484 1.0161 0.5069 Ca 23.2668 0.119830 23.2668 10.2669 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0181 0.020025 0.0181 0.0058 C 17.3714 17.3714 25.5791 O 56.6754 56.6754 62.6477 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 473 x= -16216.0 y= 3022.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 42.6 3.4 3.6 11.75 0.0506 3.4 0.0292 Mg 119.9 2.0 2.5 47.62 0.0662 2.1 0.0112 Sr 34.7 2.7 14.3 2.43 0.0029 2.7 0.0403 P 38.1 3.6 2.4 16.19 0.0462 3.6 0.0400 K 31.1 4.0 5.1 6.10 0.0241 4.0 0.0191 Cl 87.8 1.9 2.2 39.91 0.0190 2.0 0.0229 Ca 3207.6 0.4 17.7 181.72 0.7118 0.5 0.0339 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.7 8.2 3.3 1.13 0.0002 8.2 0.0565 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0636 Elt. k-ratio Correc. Na 0.0025 2.3164 Mg 0.0048 1.6981 Sr 0.0018 1.3783 P 0.0072 1.1991 K 0.0021 1.0387 Cl 0.0106 1.1214 Ca 0.2583 1.0974 Ba 0.0000 NaN Fe 0.0001 1.2549 Mn 0.0002 1.2773 iteration : 3 Analysis no. 473 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5847 0.022925 0.5847 0.4730 Mg 0.8140 0.017339 0.8140 0.6229 Sr 0.2509 0.013606 0.2509 0.0532 P 0.8686 0.034823 0.8686 0.5215 K 0.2223 0.011521 0.2223 0.1057 Cl 1.1855 0.024098 1.1855 0.6219 Ca 28.3468 0.135593 28.3468 13.1532 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0143 0.014136 0.0143 0.0048 Mn 0.0272 0.020338 0.0272 0.0092 C 14.9208 14.9208 23.1030 O 52.7650 52.7650 61.3316 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 474 x= -16216.0 y= 3026.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 40.8 3.5 3.6 11.24 0.0481 3.5 0.0292 Mg 108.7 2.1 2.5 43.18 0.0599 2.2 0.0112 Sr 37.5 2.6 14.3 2.63 0.0033 2.6 0.0404 P 35.1 3.8 2.4 14.94 0.0424 3.8 0.0401 K 28.7 4.2 5.1 5.63 0.0219 4.2 0.0191 Cl 83.1 2.0 2.2 37.75 0.0179 2.0 0.0230 Ca 3025.9 0.4 17.7 171.43 0.6710 0.5 0.0340 Ba 11.1 4.8 10.8 1.03 0.0002 4.8 0.0755 Fe 2.9 9.4 3.3 0.86 0.0000 9.4 0.0000 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0637 Elt. k-ratio Correc. Na 0.0024 2.3190 Mg 0.0043 1.6997 Sr 0.0021 1.3800 P 0.0066 1.2014 K 0.0019 1.0441 Cl 0.0100 1.1247 Ca 0.2435 1.0996 Ba 0.0001 1.5359 Fe 0.0000 NaN Mn 0.0003 1.2789 iteration : 3 Analysis no. 474 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5574 0.022474 0.5574 0.4444 Mg 0.7371 0.016523 0.7371 0.5559 Sr 0.2855 0.014007 0.2855 0.0597 P 0.7981 0.033561 0.7981 0.4723 K 0.2028 0.011186 0.2028 0.0951 Cl 1.1228 0.023511 1.1228 0.5805 Ca 26.7786 0.130774 26.7786 12.2463 Ba 0.0079 0.019402 0.0079 0.0011 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0327 0.020605 0.0327 0.0109 C 15.6177 15.6177 23.8332 O 53.8594 53.8594 61.7006 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 475 x= -16215.0 y= 3031.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.0 3.8 3.6 9.65 0.0407 3.8 0.0292 Mg 89.3 2.4 2.5 35.47 0.0490 2.4 0.0112 Sr 32.5 2.8 14.3 2.28 0.0026 2.8 0.0404 P 35.6 3.7 2.4 15.15 0.0430 3.8 0.0401 K 31.6 4.0 5.1 6.19 0.0245 4.0 0.0192 Cl 96.3 1.9 2.2 43.79 0.0209 1.9 0.0230 Ca 2937.3 0.4 17.7 166.41 0.6513 0.5 0.0340 Ba 10.4 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0566 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0637 Elt. k-ratio Correc. Na 0.0020 2.3212 Mg 0.0035 1.6993 Sr 0.0016 1.3793 P 0.0067 1.2006 K 0.0022 1.0476 Cl 0.0116 1.1256 Ca 0.2364 1.1011 Ba 0.0000 NaN Fe 0.0000 1.2581 Mn 0.0002 1.2798 iteration : 2 Analysis no. 475 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4715 0.020971 0.4715 0.3735 Mg 0.6023 0.014984 0.6023 0.4513 Sr 0.2243 0.013306 0.2243 0.0466 P 0.8099 0.033771 0.8099 0.4761 K 0.2281 0.011692 0.2281 0.1062 Cl 1.3085 0.025318 1.3085 0.6721 Ca 26.0278 0.128476 26.0278 11.8249 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013864 0.0042 0.0014 Mn 0.0236 0.020210 0.0236 0.0078 C 15.9659 15.9659 24.2047 O 54.3338 54.3338 61.8355 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 476 x= -16215.0 y= 3036.0 z= -277. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 12.2 6.4 3.6 3.36 0.0111 6.4 0.0294 Mg 49.1 3.2 2.5 19.50 0.0263 3.2 0.0112 Sr 29.6 2.9 14.3 2.08 0.0022 2.9 0.0403 P 35.3 3.8 2.4 15.00 0.0426 3.8 0.0401 K 23.9 4.6 5.1 4.69 0.0174 4.6 0.0192 Cl 80.9 2.0 2.2 36.75 0.0175 2.0 0.0230 Ca 2891.7 0.4 17.7 163.83 0.6412 0.5 0.0340 Ba 9.8 5.0 10.8 0.91 0.0000 5.0 0.0000 Fe 3.9 8.0 3.3 1.18 0.0003 8.0 0.0567 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0638 Elt. k-ratio Correc. Na 0.0006 2.3335 Mg 0.0019 1.6996 Sr 0.0014 1.3779 P 0.0067 1.1998 K 0.0015 1.0470 Cl 0.0097 1.1258 Ca 0.2327 1.1017 Ba 0.0000 NaN Fe 0.0002 1.2598 Mn 0.0001 1.2814 iteration : 2 Analysis no. 476 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1295 0.013451 0.1295 0.1017 Mg 0.3233 0.011195 0.3233 0.2401 Sr 0.1884 0.012871 0.1884 0.0388 P 0.8008 0.033591 0.8008 0.4666 K 0.1620 0.010388 0.1620 0.0748 Cl 1.0935 0.023230 1.0935 0.5567 Ca 25.6368 0.127267 25.6368 11.5441 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0203 0.014366 0.0203 0.0066 Mn 0.0089 0.019556 0.0089 0.0029 C 16.4512 16.4512 24.7196 O 55.1851 55.1851 62.2482 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 477 x= -16214.0 y= 3041.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 25.2 4.4 3.6 6.95 0.0280 4.5 0.0292 Mg 93.4 2.3 2.5 37.08 0.0512 2.3 0.0112 Sr 31.9 2.8 14.3 2.23 0.0025 2.8 0.0403 P 41.2 3.5 2.4 17.53 0.0503 3.5 0.0400 K 30.5 4.0 5.1 5.98 0.0236 4.1 0.0192 Cl 94.2 1.9 2.2 42.82 0.0204 1.9 0.0230 Ca 3051.6 0.4 17.7 172.88 0.6769 0.5 0.0340 Ba 9.2 5.2 10.8 0.85 0.0000 5.2 0.0000 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0566 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0637 Elt. k-ratio Correc. Na 0.0014 2.3223 Mg 0.0037 1.6967 Sr 0.0016 1.3774 P 0.0079 1.1988 K 0.0021 1.0440 Cl 0.0114 1.1238 Ca 0.2457 1.0996 Ba 0.0000 NaN Fe 0.0001 1.2569 Mn 0.0003 1.2789 iteration : 2 Analysis no. 477 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3244 0.018099 0.3244 0.2591 Mg 0.6295 0.015294 0.6295 0.4757 Sr 0.2163 0.013199 0.2163 0.0453 P 0.9450 0.036171 0.9450 0.5603 K 0.2182 0.011482 0.2182 0.1025 Cl 1.2769 0.025002 1.2769 0.6615 Ca 27.0132 0.131520 27.0132 12.3773 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0152 0.014182 0.0152 0.0050 Mn 0.0327 0.020608 0.0327 0.0109 C 15.5524 15.5524 23.7791 O 53.7761 53.7761 61.7233 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 478 x= -16214.0 y= 3045.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 30.7 4.0 3.6 8.46 0.0351 4.1 0.0293 Mg 74.0 2.6 2.5 29.39 0.0403 2.6 0.0112 Sr 25.5 3.1 14.3 1.78 0.0016 3.1 0.0405 P 41.4 3.5 2.4 17.60 0.0505 3.5 0.0402 K 33.8 3.8 5.1 6.62 0.0266 3.9 0.0194 Cl 78.8 2.1 2.2 35.82 0.0170 2.1 0.0231 Ca 2683.7 0.4 17.7 152.04 0.5949 0.5 0.0341 Ba 7.9 5.6 10.8 0.73 0.0000 5.6 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0639 Elt. k-ratio Correc. Na 0.0018 2.3265 Mg 0.0029 1.7018 Sr 0.0010 1.3818 P 0.0079 1.2028 K 0.0024 1.0552 Cl 0.0095 1.1307 Ca 0.2159 1.1044 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0003 1.2825 iteration : 2 Analysis no. 478 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4080 0.019807 0.4080 0.3167 Mg 0.4970 0.013683 0.4970 0.3650 Sr 0.1379 0.012282 0.1379 0.0281 P 0.9520 0.036362 0.9520 0.5486 K 0.2489 0.012130 0.2489 0.1136 Cl 1.0701 0.023046 1.0701 0.5388 Ca 23.8450 0.121669 23.8450 10.6191 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0402 0.020997 0.0402 0.0131 C 16.8487 16.8487 25.0382 O 55.9523 55.9523 62.4189 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 479 x= -16214.0 y= 3050.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 47.7 3.2 3.6 13.14 0.0571 3.3 0.0291 Mg 137.8 1.9 2.5 54.71 0.0763 1.9 0.0112 Sr 41.1 2.5 14.3 2.88 0.0039 2.5 0.0404 P 39.1 3.6 2.4 16.62 0.0475 3.6 0.0401 K 32.2 3.9 5.1 6.31 0.0251 4.0 0.0191 Cl 101.3 1.8 2.2 46.05 0.0220 1.8 0.0230 Ca 3114.4 0.4 17.7 176.45 0.6909 0.5 0.0339 Ba 9.3 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.3 8.7 3.3 1.01 0.0000 8.7 0.0565 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0636 Elt. k-ratio Correc. Na 0.0029 2.3102 Mg 0.0055 1.6964 Sr 0.0024 1.3792 P 0.0074 1.2007 K 0.0022 1.0435 Cl 0.0122 1.1237 Ca 0.2507 1.0987 Ba 0.0000 NaN Fe 0.0000 1.2551 Mn 0.0001 1.2773 iteration : 3 Analysis no. 479 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6586 0.024098 0.6586 0.5310 Mg 0.9369 0.018571 0.9369 0.7144 Sr 0.3294 0.014482 0.3294 0.0697 P 0.8940 0.035304 0.8940 0.5350 K 0.2328 0.011750 0.2328 0.1103 Cl 1.3755 0.025915 1.3755 0.7191 Ca 27.5485 0.133155 27.5485 12.7395 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0008 0.013729 0.0008 0.0003 Mn 0.0180 0.019920 0.0180 0.0061 C 15.0659 15.0659 23.2487 O 52.9396 52.9396 61.3259 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 480 x= -16213.0 y= 3055.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 22.8 4.7 3.6 6.27 0.0248 4.7 0.0293 Mg 73.8 2.6 2.5 29.30 0.0402 2.6 0.0112 Sr 25.5 3.1 14.3 1.78 0.0016 3.1 0.0405 P 40.7 3.5 2.4 17.32 0.0496 3.5 0.0403 K 31.8 4.0 5.1 6.24 0.0248 4.0 0.0195 Cl 80.9 2.0 2.2 36.78 0.0175 2.0 0.0232 Ca 2446.0 0.5 17.7 138.58 0.5418 0.5 0.0342 Ba 7.6 5.7 10.8 0.71 0.0000 5.7 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0640 Elt. k-ratio Correc. Na 0.0012 2.3285 Mg 0.0029 1.7013 Sr 0.0010 1.3839 P 0.0078 1.2053 K 0.0022 1.0638 Cl 0.0097 1.1354 Ca 0.1966 1.1076 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2847 iteration : 2 Analysis no. 480 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2884 0.017355 0.2884 0.2200 Mg 0.4950 0.013654 0.4950 0.3573 Sr 0.1378 0.012295 0.1378 0.0276 P 0.9379 0.036155 0.9379 0.5312 K 0.2338 0.011914 0.2338 0.1049 Cl 1.1039 0.023439 1.1039 0.5462 Ca 21.7801 0.115088 21.7801 9.5324 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0200 0.020122 0.0200 0.0064 C 17.6959 17.6959 25.8444 O 57.3074 57.3074 62.8297 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 481 x= -16213.0 y= 3059.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 33.9 3.8 3.6 9.35 0.0393 3.9 0.0291 Mg 121.1 2.0 2.5 48.07 0.0669 2.1 0.0112 Sr 42.4 2.4 14.3 2.97 0.0041 2.4 0.0403 P 47.0 3.3 2.4 19.98 0.0577 3.3 0.0400 K 32.3 3.9 5.1 6.33 0.0252 3.9 0.0191 Cl 102.9 1.8 2.2 46.75 0.0223 1.8 0.0229 Ca 3185.5 0.4 17.7 180.47 0.7068 0.5 0.0339 Ba 12.0 4.6 10.8 1.11 0.0007 4.6 0.0756 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0565 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0636 Elt. k-ratio Correc. Na 0.0020 2.3130 Mg 0.0048 1.6937 Sr 0.0025 1.3762 P 0.0090 1.1986 K 0.0022 1.0416 Cl 0.0124 1.1227 Ca 0.2565 1.0977 Ba 0.0002 1.5359 Fe 0.0001 1.2541 Mn 0.0003 1.2765 iteration : 3 Analysis no. 481 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4535 0.020597 0.4535 0.3677 Mg 0.8199 0.017377 0.8199 0.6289 Sr 0.3452 0.014629 0.3452 0.0735 P 1.0847 0.038529 1.0847 0.6529 K 0.2332 0.011745 0.2332 0.1112 Cl 1.3956 0.026087 1.3956 0.7339 Ca 28.1574 0.135016 28.1574 13.0980 Ba 0.0316 0.019804 0.0316 0.0043 Fe 0.0084 0.013950 0.0084 0.0028 Mn 0.0327 0.020572 0.0327 0.0111 C 14.8156 14.8156 22.9975 O 52.6222 52.6222 61.3182 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 482 x= -16212.0 y= 3064.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.8 4.6 3.6 6.56 0.0262 4.6 0.0293 Mg 73.1 2.6 2.5 29.04 0.0398 2.6 0.0112 Sr 20.5 3.5 14.3 1.43 0.0009 3.5 0.0406 P 50.2 3.2 2.4 21.34 0.0619 3.2 0.0404 K 32.5 3.9 5.1 6.36 0.0254 3.9 0.0197 Cl 71.0 2.2 2.2 32.28 0.0153 2.2 0.0233 Ca 2162.4 0.5 17.7 122.51 0.4786 0.6 0.0343 Ba 8.2 5.5 10.8 0.76 0.0000 5.5 0.0000 Fe 3.8 8.1 3.3 1.15 0.0003 8.1 0.0571 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0641 Elt. k-ratio Correc. Na 0.0013 2.3291 Mg 0.0029 1.7027 Sr 0.0006 1.3870 P 0.0097 1.2083 K 0.0023 1.0743 Cl 0.0085 1.1421 Ca 0.1737 1.1114 Ba 0.0000 NaN Fe 0.0001 1.2673 Mn 0.0001 1.2872 iteration : 2 Analysis no. 482 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3043 0.017704 0.3043 0.2278 Mg 0.4909 0.013606 0.4909 0.3476 Sr 0.0766 0.011522 0.0766 0.0150 P 1.1719 0.040110 1.1719 0.6511 K 0.2418 0.012138 0.2418 0.1064 Cl 0.9706 0.022114 0.9706 0.4711 Ca 19.3029 0.107002 19.3029 8.2879 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0170 0.014351 0.0170 0.0052 Mn 0.0089 0.019647 0.0089 0.0028 C 18.5346 18.5346 26.5557 O 58.8804 58.8804 63.3293 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 483 x= -16212.0 y= 3069.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 31.0 4.0 3.6 8.53 0.0354 4.0 0.0291 Mg 106.5 2.2 2.5 42.31 0.0587 2.2 0.0112 Sr 35.6 2.6 14.3 2.50 0.0031 2.7 0.0403 P 56.4 3.0 2.4 23.98 0.0699 3.0 0.0401 K 34.4 3.8 5.1 6.74 0.0271 3.8 0.0193 Cl 92.5 1.9 2.2 42.06 0.0200 1.9 0.0231 Ca 2912.2 0.4 17.7 164.99 0.6459 0.5 0.0340 Ba 10.6 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 4.1 7.8 3.3 1.23 0.0004 7.9 0.0566 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0637 Elt. k-ratio Correc. Na 0.0018 2.3159 Mg 0.0042 1.6951 Sr 0.0019 1.3783 P 0.0110 1.2006 K 0.0024 1.0504 Cl 0.0112 1.1284 Ca 0.2344 1.1015 Ba 0.0000 NaN Fe 0.0002 1.2574 Mn 0.0001 1.2791 iteration : 2 Analysis no. 483 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4098 0.019786 0.4098 0.3255 Mg 0.7201 0.016316 0.7201 0.5411 Sr 0.2622 0.013735 0.2622 0.0547 P 1.3155 0.042199 1.3155 0.7757 K 0.2529 0.012167 0.2529 0.1181 Cl 1.2590 0.024886 1.2590 0.6485 Ca 25.8171 0.127832 25.8171 11.7639 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0253 0.014488 0.0253 0.0083 Mn 0.0144 0.019780 0.0144 0.0048 C 15.6855 15.6855 23.8500 O 54.2382 54.2382 61.9094 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 484 x= -16212.0 y= 3074.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 31.1 4.0 3.6 8.58 0.0356 4.0 0.0291 Mg 109.6 2.1 2.5 43.52 0.0604 2.2 0.0112 Sr 38.6 2.5 14.3 2.70 0.0035 2.6 0.0403 P 61.4 2.9 2.4 26.13 0.0764 2.9 0.0400 K 32.6 3.9 5.1 6.39 0.0255 3.9 0.0192 Cl 88.1 1.9 2.2 40.03 0.0191 1.9 0.0230 Ca 3047.3 0.4 17.7 172.64 0.6759 0.5 0.0340 Ba 11.8 4.6 10.8 1.09 0.0006 4.6 0.0755 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0565 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0636 Elt. k-ratio Correc. Na 0.0018 2.3145 Mg 0.0044 1.6941 Sr 0.0022 1.3767 P 0.0120 1.1993 K 0.0023 1.0461 Cl 0.0106 1.1266 Ca 0.2453 1.0995 Ba 0.0002 1.5354 Fe 0.0001 1.2556 Mn 0.0003 1.2777 iteration : 3 Analysis no. 484 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4118 0.019817 0.4118 0.3307 Mg 0.7407 0.016536 0.7407 0.5627 Sr 0.2984 0.014126 0.2984 0.0629 P 1.4370 0.043978 1.4370 0.8566 K 0.2368 0.011843 0.2368 0.1118 Cl 1.1946 0.024244 1.1946 0.6222 Ca 26.9718 0.131384 26.9718 12.4253 Ba 0.0263 0.019708 0.0263 0.0035 Fe 0.0177 0.014244 0.0177 0.0059 Mn 0.0345 0.020671 0.0345 0.0116 C 15.1533 15.1533 23.2944 O 53.4771 53.4771 61.7124 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 485 x= -16211.0 y= 3078.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 62.5 2.8 3.6 17.22 0.0763 2.9 0.0290 Mg 155.5 1.8 2.5 61.77 0.0863 1.8 0.0112 Sr 41.1 2.5 14.3 2.88 0.0039 2.5 0.0406 P 62.0 2.8 2.4 26.37 0.0771 2.9 0.0404 K 27.3 4.3 5.1 5.34 0.0206 4.3 0.0196 Cl 93.8 1.9 2.2 42.62 0.0203 1.9 0.0233 Ca 2429.0 0.5 17.7 137.61 0.5381 0.5 0.0342 Ba 10.7 4.8 10.8 1.00 0.0000 4.8 0.0000 Fe 2.9 9.2 3.3 0.89 0.0000 9.3 0.0000 Mn 2.8 13.3 2.7 1.03 0.0001 13.4 0.0639 Elt. k-ratio Correc. Na 0.0038 2.3019 Mg 0.0062 1.6981 Sr 0.0024 1.3865 P 0.0121 1.2089 K 0.0018 1.0689 Cl 0.0113 1.1400 Ca 0.1953 1.1075 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2821 iteration : 2 Analysis no. 485 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.8771 0.027324 0.8771 0.6769 Mg 1.0612 0.019768 1.0612 0.7747 Sr 0.3312 0.014561 0.3312 0.0671 P 1.4622 0.044532 1.4622 0.8376 K 0.1949 0.011206 0.1949 0.0884 Cl 1.2894 0.025307 1.2894 0.6453 Ca 21.6268 0.114584 21.6268 9.5738 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0034 0.019308 0.0034 0.0011 C 16.8708 16.8708 24.9215 O 56.2832 56.2832 62.4137 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 486 x= -16211.0 y= 3083.0 z= -276. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 25.5 4.4 3.6 7.02 0.0283 4.4 0.0292 Mg 61.5 2.8 2.5 24.43 0.0333 2.9 0.0113 Sr 20.5 3.5 14.3 1.44 0.0009 3.5 0.0409 P 25.6 4.4 2.4 10.89 0.0301 4.4 0.0408 K 10.7 6.8 5.1 2.10 0.0052 6.8 0.0208 Cl 177.1 1.4 2.2 80.49 0.0388 1.4 0.0238 Ca 870.1 0.8 17.7 49.30 0.1902 0.8 0.0349 Ba 8.8 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 2.9 9.3 3.3 0.87 0.0000 9.3 0.0000 Mn 1.7 17.1 2.7 0.63 0.0000 17.2 0.0000 Elt. k-ratio Correc. Na 0.0014 2.3236 Mg 0.0024 1.7039 Sr 0.0006 1.3985 P 0.0047 1.2211 K 0.0005 1.1311 Cl 0.0216 1.1662 Ca 0.0690 1.1300 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 486 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3284 0.018190 0.3284 0.2263 Mg 0.4105 0.012514 0.4105 0.2676 Sr 0.0776 0.011621 0.0776 0.0140 P 0.5760 0.029416 0.5760 0.2947 K 0.0521 0.008276 0.0521 0.0211 Cl 2.5191 0.035548 2.5191 1.1258 Ca 7.8004 0.064378 7.8004 3.0837 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 23.0710 23.0710 30.4346 O 65.1649 65.1649 64.5321 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 487 x= -16211.0 y= 3088.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 15.5 5.7 3.6 4.27 0.0154 5.7 0.0296 Mg 10.6 6.9 2.5 4.19 0.0045 6.9 0.0114 Sr 11.6 4.6 14.3 0.81 0.0000 4.7 0.0000 P 1.9 16.4 2.4 0.79 0.0000 16.4 0.0000 K 6.3 8.9 5.1 1.23 0.0011 8.9 0.0214 Cl 98.4 1.8 2.2 44.73 0.0213 1.8 0.0242 Ca 45.9 3.3 17.7 2.60 0.0063 3.3 0.0353 Ba 6.9 6.0 10.8 0.64 0.0000 6.0 0.0000 Fe 2.1 11.0 3.3 0.62 0.0000 11.0 0.0000 Mn 1.6 17.7 2.7 0.59 0.0000 17.7 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3542 Mg 0.0003 1.7209 Sr 0.0000 NaN P 0.0000 NaN K 0.0001 1.1671 Cl 0.0119 1.1859 Ca 0.0023 1.1415 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 487 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1810 0.014926 0.1810 0.1168 Mg 0.0564 0.005683 0.0564 0.0344 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0110 0.007237 0.0110 0.0042 Cl 1.4092 0.026962 1.4092 0.5895 Ca 0.2612 0.016492 0.2612 0.0966 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7977 26.7977 33.0872 O 71.2834 71.2834 66.0713 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 488 x= -16210.0 y= 3093.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 11.7 6.5 3.6 3.23 0.0105 6.5 0.0297 Mg 10.2 7.0 2.5 4.03 0.0043 7.0 0.0114 Sr 11.5 4.7 14.3 0.81 0.0000 4.7 0.0000 P 1.1 21.8 2.4 0.45 0.0000 21.8 0.0000 K 5.2 9.8 5.1 1.01 0.0000 9.9 0.0215 Cl 92.1 1.9 2.2 41.88 0.0200 1.9 0.0243 Ca 18.5 5.2 17.7 1.05 0.0002 5.2 0.0353 Ba 6.0 6.4 10.8 0.56 0.0000 6.4 0.0000 Fe 2.1 11.0 3.3 0.62 0.0000 11.0 0.0000 Mn 1.8 16.9 2.7 0.65 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3564 Mg 0.0003 1.7211 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1685 Cl 0.0111 1.1868 Ca 0.0001 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 488 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1232 0.013372 0.1232 0.0793 Mg 0.0537 0.005598 0.0537 0.0327 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0005 0.006887 0.0005 0.0002 Cl 1.3188 0.026127 1.3188 0.5502 Ca 0.0079 0.012436 0.0079 0.0029 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9395 26.9395 33.1782 O 71.5565 71.5565 66.1565 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 489 x= -16210.0 y= 3097.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 13.1 6.2 3.6 3.60 0.0122 6.2 0.0296 Mg 10.6 6.9 2.5 4.21 0.0046 6.9 0.0113 Sr 8.1 5.6 14.3 0.56 0.0000 5.6 0.0000 P 1.9 16.2 2.4 0.81 0.0000 16.2 0.0000 K 4.2 11.0 5.1 0.81 0.0000 11.0 0.0000 Cl 129.4 1.6 2.2 58.82 0.0282 1.6 0.0242 Ca 28.0 4.2 17.7 1.59 0.0023 4.2 0.0353 Ba 5.9 6.5 10.8 0.54 0.0000 6.5 0.0000 Fe 2.2 10.6 3.3 0.67 0.0000 10.7 0.0000 Mn 1.4 19.2 2.7 0.50 0.0000 19.2 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3501 Mg 0.0003 1.7178 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0157 1.1855 Ca 0.0008 1.1420 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 489 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1434 0.013908 0.1434 0.0926 Mg 0.0567 0.005684 0.0567 0.0346 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.8624 0.030877 1.8624 0.7801 Ca 0.0957 0.013974 0.0957 0.0355 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7824 26.7824 33.1103 O 71.0593 71.0593 65.9469 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 490 x= -16209.0 y= 3102.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 8.2 7.8 3.6 2.25 0.0059 7.8 0.0297 Mg 10.4 6.9 2.5 4.11 0.0044 7.0 0.0114 Sr 10.3 4.9 14.3 0.72 0.0000 4.9 0.0000 P 1.8 16.9 2.4 0.74 0.0000 16.9 0.0000 K 4.8 10.2 5.1 0.94 0.0000 10.2 0.0000 Cl 97.5 1.8 2.2 44.34 0.0212 1.9 0.0243 Ca 20.6 4.9 17.7 1.17 0.0007 4.9 0.0353 Ba 6.8 6.1 10.8 0.63 0.0000 6.1 0.0000 Fe 1.8 11.8 3.3 0.55 0.0000 11.8 0.0000 Mn 1.8 16.6 2.7 0.66 0.0000 16.7 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3564 Mg 0.0003 1.7199 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0118 1.1866 Ca 0.0002 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 490 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0690 0.011718 0.0690 0.0444 Mg 0.0550 0.005639 0.0550 0.0335 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.3980 0.026872 1.3980 0.5835 Ca 0.0273 0.012794 0.0273 0.0101 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9348 26.9348 33.1848 O 71.5158 71.5158 66.1437 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 491 x= -16209.0 y= 3107.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 9.4 7.3 3.6 2.58 0.0074 7.3 0.0296 Mg 13.7 6.0 2.5 5.44 0.0063 6.0 0.0113 Sr 9.1 5.3 14.3 0.63 0.0000 5.3 0.0000 P 1.5 18.2 2.4 0.64 0.0000 18.3 0.0000 K 5.0 10.0 5.1 0.97 0.0000 10.1 0.0000 Cl 139.1 1.5 2.2 63.24 0.0304 1.5 0.0242 Ca 21.3 4.8 17.7 1.21 0.0008 4.9 0.0353 Ba 6.0 6.5 10.8 0.55 0.0000 6.5 0.0000 Fe 1.6 12.4 3.3 0.49 0.0000 12.4 0.0000 Mn 1.4 19.2 2.7 0.50 0.0000 19.2 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3492 Mg 0.0005 1.7161 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0169 1.1854 Ca 0.0003 1.1423 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 491 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0871 0.012258 0.0871 0.0562 Mg 0.0784 0.006315 0.0784 0.0479 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 2.0046 0.032011 2.0046 0.8398 Ca 0.0338 0.012909 0.0338 0.0125 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7870 26.7870 33.1250 O 71.0093 71.0093 65.9186 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 492 x= -16209.0 y= 3111.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 11.5 6.6 3.6 3.17 0.0102 6.6 0.0296 Mg 14.2 5.9 2.5 5.64 0.0066 5.9 0.0114 Sr 9.9 5.0 14.3 0.69 0.0000 5.0 0.0000 P 1.5 18.2 2.4 0.64 0.0000 18.3 0.0000 K 5.0 10.0 5.1 0.97 0.0000 10.1 0.0000 Cl 114.9 1.7 2.2 52.23 0.0250 1.7 0.0243 Ca 20.9 4.9 17.7 1.18 0.0007 4.9 0.0353 Ba 6.6 6.2 10.8 0.61 0.0000 6.2 0.0000 Fe 2.1 11.0 3.3 0.62 0.0000 11.0 0.0000 Mn 1.9 16.4 2.7 0.68 0.0000 16.4 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3524 Mg 0.0005 1.7187 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0139 1.1861 Ca 0.0003 1.1420 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 492 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1200 0.013263 0.1200 0.0774 Mg 0.0820 0.006425 0.0820 0.0500 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.6519 0.029134 1.6519 0.6907 Ca 0.0301 0.012846 0.0301 0.0111 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8491 26.8491 33.1388 O 71.2669 71.2669 66.0320 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 493 x= -16208.0 y= 3116.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 11.8 6.5 3.6 3.25 0.0106 6.5 0.0296 Mg 13.8 6.0 2.5 5.46 0.0063 6.0 0.0114 Sr 10.8 4.8 14.3 0.75 0.0000 4.8 0.0000 P 1.8 16.6 2.4 0.77 0.0000 16.7 0.0000 K 3.7 11.6 5.1 0.73 0.0000 11.6 0.0000 Cl 105.3 1.8 2.2 47.84 0.0229 1.8 0.0242 Ca 16.6 5.5 17.7 0.94 0.0000 5.5 0.0000 Ba 5.9 6.5 10.8 0.54 0.0000 6.5 0.0000 Fe 1.9 11.5 3.3 0.57 0.0000 11.6 0.0000 Mn 1.9 16.4 2.7 0.68 0.0000 16.4 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3539 Mg 0.0005 1.7197 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0127 1.1865 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 493 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1246 0.013398 0.1246 0.0803 Mg 0.0789 0.006339 0.0789 0.0481 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.5104 0.027892 1.5104 0.6309 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8902 26.8902 33.1560 O 71.3958 71.3958 66.0847 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 494 x= -16208.0 y= 3121.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.1 6.0 3.6 3.87 0.0135 6.0 0.0297 Mg 12.8 6.3 2.5 5.06 0.0058 6.3 0.0114 Sr 10.5 4.9 14.3 0.74 0.0000 4.9 0.0000 P 1.2 20.4 2.4 0.51 0.0000 20.4 0.0000 K 5.8 9.3 5.1 1.14 0.0006 9.3 0.0214 Cl 70.7 2.2 2.2 32.14 0.0152 2.2 0.0243 Ca 15.0 5.8 17.7 0.85 0.0000 5.8 0.0000 Ba 7.0 6.0 10.8 0.65 0.0000 6.0 0.0000 Fe 2.0 11.2 3.3 0.60 0.0000 11.3 0.0000 Mn 1.9 16.2 2.7 0.70 0.0000 16.2 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3590 Mg 0.0004 1.7233 Sr 0.0000 NaN P 0.0000 NaN K 0.0001 1.1681 Cl 0.0085 1.1875 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 494 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1592 0.014375 0.1592 0.1023 Mg 0.0720 0.006153 0.0720 0.0438 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0067 0.007097 0.0067 0.0025 Cl 1.0048 0.022947 1.0048 0.4186 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9853 26.9853 33.1820 O 71.7720 71.7720 66.2508 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 495 x= -16207.0 y= 3126.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 7.4 8.2 3.6 2.03 0.0048 8.3 0.0297 Mg 8.9 7.5 2.5 3.51 0.0036 7.5 0.0114 Sr 9.0 5.3 14.3 0.63 0.0000 5.3 0.0000 P 1.7 17.4 2.4 0.70 0.0000 17.4 0.0000 K 5.4 9.6 5.1 1.06 0.0003 9.6 0.0214 Cl 85.5 2.0 2.2 38.87 0.0185 2.0 0.0242 Ca 23.9 4.6 17.7 1.35 0.0014 4.6 0.0353 Ba 6.3 6.3 10.8 0.59 0.0000 6.3 0.0000 Fe 1.7 12.1 3.3 0.52 0.0000 12.1 0.0000 Mn 1.5 18.2 2.7 0.55 0.0000 18.3 0.0000 Elt. k-ratio Correc. Na 0.0002 2.3587 Mg 0.0003 1.7209 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1681 Cl 0.0103 1.1868 Ca 0.0005 1.1418 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 495 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0569 0.011317 0.0569 0.0366 Mg 0.0445 0.005300 0.0445 0.0271 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0029 0.006966 0.0029 0.0011 Cl 1.2214 0.025177 1.2214 0.5094 Ca 0.0573 0.013319 0.0573 0.0211 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9690 26.9690 33.1975 O 71.6480 71.6480 66.2073 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 496 x= -16207.0 y= 3130.0 z= -275. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 10.0 7.1 3.6 2.76 0.0083 7.1 0.0296 Mg 10.9 6.8 2.5 4.33 0.0047 6.8 0.0114 Sr 9.9 5.0 14.3 0.69 0.0000 5.0 0.0000 P 2.0 16.0 2.4 0.83 0.0000 16.0 0.0000 K 4.2 11.0 5.1 0.81 0.0000 11.0 0.0000 Cl 111.9 1.7 2.2 50.88 0.0243 1.7 0.0242 Ca 17.1 5.4 17.7 0.97 0.0000 5.4 0.0000 Ba 6.6 6.1 10.8 0.62 0.0000 6.1 0.0000 Fe 1.6 12.6 3.3 0.48 0.0000 12.6 0.0000 Mn 1.7 17.4 2.7 0.61 0.0000 17.4 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3536 Mg 0.0003 1.7189 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0136 1.1862 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 496 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0971 0.012586 0.0971 0.0626 Mg 0.0588 0.005752 0.0588 0.0359 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.6077 0.028746 1.6077 0.6718 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8889 26.8889 33.1662 O 71.3474 71.3474 66.0635 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 497 x= -16207.0 y= 3135.0 z= -274. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.5 5.9 3.6 3.98 0.0140 5.9 0.0296 Mg 12.5 6.3 2.5 4.94 0.0056 6.3 0.0114 Sr 11.1 4.7 14.3 0.78 0.0000 4.8 0.0000 P 2.0 15.8 2.4 0.85 0.0000 15.8 0.0000 K 4.1 11.0 5.1 0.80 0.0000 11.0 0.0000 Cl 101.4 1.8 2.2 46.08 0.0220 1.8 0.0242 Ca 18.1 5.3 17.7 1.03 0.0001 5.3 0.0353 Ba 6.6 6.2 10.8 0.61 0.0000 6.2 0.0000 Fe 1.6 12.4 3.3 0.49 0.0000 12.4 0.0000 Mn 2.0 16.0 2.7 0.72 0.0000 16.0 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3540 Mg 0.0004 1.7206 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0122 1.1866 Ca 0.0000 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 497 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1650 0.014507 0.1650 0.1063 Mg 0.0698 0.006082 0.0698 0.0425 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.4536 0.027377 1.4536 0.6071 Ca 0.0042 0.012363 0.0042 0.0015 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8899 26.8899 33.1497 O 71.4175 71.4175 66.0929 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 498 x= -16206.0 y= 3140.0 z= -274. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 9.2 7.4 3.6 2.54 0.0072 7.4 0.0297 Mg 8.8 7.5 2.5 3.49 0.0035 7.5 0.0114 Sr 8.7 5.4 14.3 0.61 0.0000 5.4 0.0000 P 1.9 16.4 2.4 0.79 0.0000 16.4 0.0000 K 4.9 10.1 5.1 0.95 0.0000 10.2 0.0000 Cl 81.8 2.0 2.2 37.19 0.0177 2.0 0.0243 Ca 18.1 5.3 17.7 1.02 0.0001 5.3 0.0353 Ba 5.6 6.7 10.8 0.52 0.0000 6.7 0.0000 Fe 2.0 11.2 3.3 0.60 0.0000 11.3 0.0000 Mn 1.7 17.4 2.7 0.61 0.0000 17.4 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3589 Mg 0.0003 1.7217 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0098 1.1871 Ca 0.0000 1.1418 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 498 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0852 0.012250 0.0852 0.0548 Mg 0.0442 0.005296 0.0442 0.0269 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.1686 0.024667 1.1686 0.4871 Ca 0.0037 0.012366 0.0037 0.0014 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9912 26.9912 33.2059 O 71.7070 71.7070 66.2240 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 499 x= -16206.0 y= 3145.0 z= -274. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 8.0 7.9 3.6 2.21 0.0057 7.9 0.0297 Mg 8.3 7.8 2.5 3.28 0.0032 7.8 0.0114 Sr 10.5 4.9 14.3 0.73 0.0000 4.9 0.0000 P 1.7 17.4 2.4 0.70 0.0000 17.4 0.0000 K 2.9 13.1 5.1 0.57 0.0000 13.1 0.0000 Cl 90.2 1.9 2.2 40.98 0.0195 1.9 0.0243 Ca 12.4 6.3 17.7 0.70 0.0000 6.4 0.0000 Ba 5.8 6.6 10.8 0.54 0.0000 6.6 0.0000 Fe 1.7 12.2 3.3 0.51 0.0000 12.2 0.0000 Mn 1.3 20.0 2.7 0.46 0.0000 20.0 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3579 Mg 0.0002 1.7207 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0109 1.1869 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 499 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0668 0.011650 0.0668 0.0430 Mg 0.0403 0.005160 0.0403 0.0245 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.2901 0.025855 1.2901 0.5380 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9755 26.9755 33.2058 O 71.6273 71.6273 66.1887 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 500 x= -16205.0 y= 3149.0 z= -274. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 16.3 5.5 3.6 4.49 0.0165 5.5 0.0296 Mg 10.5 6.9 2.5 4.15 0.0045 6.9 0.0114 Sr 11.2 4.7 14.3 0.78 0.0000 4.7 0.0000 P 1.6 17.9 2.4 0.66 0.0000 18.0 0.0000 K 4.6 10.5 5.1 0.89 0.0000 10.5 0.0000 Cl 121.5 1.7 2.2 55.20 0.0265 1.7 0.0243 Ca 13.9 6.0 17.7 0.79 0.0000 6.0 0.0000 Ba 6.6 6.2 10.8 0.61 0.0000 6.2 0.0000 Fe 2.0 11.1 3.3 0.61 0.0000 11.1 0.0000 Mn 1.6 17.7 2.7 0.59 0.0000 17.7 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3506 Mg 0.0003 1.7192 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0147 1.1860 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 500 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1931 0.015230 0.1931 0.1246 Mg 0.0557 0.005662 0.0557 0.0340 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.7488 0.029964 1.7488 0.7316 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8251 26.8251 33.1264 O 71.1772 71.1772 65.9833 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 501 x= -16205.0 y= 3154.0 z= -274. carb2 left trav 2 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 19.7 5.0 3.6 5.43 0.0209 5.0 0.0295 Mg 10.9 6.8 2.5 4.33 0.0047 6.8 0.0113 Sr 11.1 4.7 14.3 0.78 0.0000 4.8 0.0000 P 4.7 10.3 2.4 2.00 0.0030 10.3 0.0412 K 5.8 9.3 5.1 1.14 0.0007 9.3 0.0215 Cl 186.1 1.3 2.2 84.59 0.0409 1.3 0.0243 Ca 14.0 6.0 17.7 0.79 0.0000 6.0 0.0000 Ba 6.2 6.4 10.8 0.57 0.0000 6.4 0.0000 Fe 2.1 10.9 3.3 0.64 0.0000 10.9 0.0000 Mn 1.7 17.4 2.7 0.61 0.0000 17.4 0.0000 Elt. k-ratio Correc. Na 0.0010 2.3388 Mg 0.0003 1.7134 Sr 0.0000 NaN P 0.0005 1.2313 K 0.0001 1.1706 Cl 0.0228 1.1843 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 501 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2438 0.016412 0.2438 0.1583 Mg 0.0587 0.005743 0.0587 0.0361 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0588 0.014858 0.0588 0.0283 K 0.0068 0.007124 0.0068 0.0026 Cl 2.6943 0.037072 2.6943 1.1341 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.5663 26.5663 33.0068 O 70.3712 70.3712 65.6339 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 502 x= -17160.0 y= 2769.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 15.5 5.7 3.6 4.26 0.0154 5.7 0.0297 Mg 50.7 3.1 2.5 20.14 0.0272 3.2 0.0114 Sr 20.0 3.5 14.3 1.40 0.0008 3.5 0.0412 P 4.3 10.8 2.4 1.81 0.0025 10.9 0.0410 K 6.1 9.1 5.1 1.19 0.0009 9.1 0.0206 Cl 60.5 2.3 2.2 27.48 0.0129 2.3 0.0238 Ca 1008.0 0.7 17.7 57.11 0.2213 0.8 0.0349 Ba 7.5 5.8 10.8 0.69 0.0000 5.8 0.0000 Fe 5.1 7.0 3.3 1.54 0.0010 7.0 0.0579 Mn 1.8 16.6 2.7 0.66 0.0000 16.7 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3505 Mg 0.0020 1.7160 Sr 0.0005 1.4042 P 0.0004 1.2254 K 0.0001 1.1181 Cl 0.0072 1.1638 Ca 0.0803 1.1267 Ba 0.0000 NaN Fe 0.0005 1.2827 Mn 0.0000 NaN iteration : 2 Analysis no. 502 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1802 0.014906 0.1802 0.1235 Mg 0.3382 0.011497 0.3382 0.2192 Sr 0.0720 0.011606 0.0720 0.0130 P 0.0473 0.014305 0.0473 0.0241 K 0.0088 0.006881 0.0088 0.0035 Cl 0.8387 0.020868 0.8387 0.3727 Ca 9.0493 0.069698 9.0493 3.5570 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0613 0.015803 0.0613 0.0173 Mn 0.0000 0.000000 0.0000 0.0000 C 23.3616 23.3616 30.6420 O 66.0425 66.0425 65.0278 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 503 x= -17159.0 y= 2773.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 34.0 3.8 3.6 9.36 0.0394 3.9 0.0294 Mg 102.6 2.2 2.5 40.74 0.0565 2.2 0.0113 Sr 34.5 2.7 14.3 2.42 0.0029 2.7 0.0402 P 16.4 5.5 2.4 6.96 0.0181 5.5 0.0398 K 9.7 7.2 5.1 1.90 0.0043 7.2 0.0182 Cl 8.7 6.2 2.2 3.94 0.0014 6.2 0.0225 Ca 4443.4 0.3 17.7 251.74 0.9887 0.4 0.0335 Ba 10.6 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 4.2 7.7 3.3 1.28 0.0005 7.7 0.0562 Mn 4.2 10.9 2.7 1.55 0.0015 10.9 0.0634 Elt. k-ratio Correc. Na 0.0020 2.3333 Mg 0.0041 1.7021 Sr 0.0018 1.3701 P 0.0028 1.1889 K 0.0004 0.9897 Cl 0.0008 1.0973 Ca 0.3588 1.0810 Ba 0.0000 NaN Fe 0.0002 1.2452 Mn 0.0004 1.2700 iteration : 3 Analysis no. 503 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4588 0.020817 0.4588 0.4007 Mg 0.6964 0.016098 0.6964 0.5753 Sr 0.2472 0.013515 0.2472 0.0567 P 0.3381 0.023408 0.3381 0.2192 K 0.0375 0.007017 0.0375 0.0193 Cl 0.0878 0.008169 0.0878 0.0497 Ca 38.7888 0.166477 38.7888 19.4313 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0310 0.014536 0.0310 0.0111 Mn 0.0544 0.021446 0.0544 0.0199 C 11.6431 11.6431 19.4631 O 47.6168 47.6168 59.7537 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 504 x= -17159.0 y= 2778.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 33.4 3.9 3.6 9.21 0.0387 3.9 0.0292 Mg 228.3 1.5 2.5 90.66 0.1276 1.5 0.0112 Sr 43.1 2.4 14.3 3.02 0.0042 2.4 0.0403 P 33.4 3.9 2.4 14.19 0.0402 3.9 0.0399 K 9.5 7.3 5.1 1.85 0.0040 7.3 0.0183 Cl 16.2 4.5 2.2 7.35 0.0031 4.5 0.0226 Ca 4381.8 0.3 17.7 248.24 0.9754 0.4 0.0335 Ba 13.4 4.3 10.8 1.25 0.0016 4.3 0.0760 Fe 4.0 7.9 3.3 1.20 0.0004 8.0 0.0561 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0634 Elt. k-ratio Correc. Na 0.0019 2.3152 Mg 0.0092 1.6925 Sr 0.0026 1.3738 P 0.0063 1.1926 K 0.0004 0.9968 Cl 0.0017 1.1023 Ca 0.3540 1.0815 Ba 0.0005 1.5412 Fe 0.0002 1.2436 Mn 0.0004 1.2684 iteration : 3 Analysis no. 504 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4472 0.020513 0.4472 0.3933 Mg 1.5632 0.024009 1.5632 1.3004 Sr 0.3529 0.014711 0.3529 0.0814 P 0.7514 0.032581 0.7514 0.4905 K 0.0358 0.007011 0.0358 0.0185 Cl 0.1905 0.010679 0.1905 0.1087 Ca 38.2845 0.165034 38.2845 19.3133 Ba 0.0700 0.020534 0.0700 0.0103 Fe 0.0218 0.014256 0.0218 0.0079 Mn 0.0471 0.021116 0.0471 0.0173 C 11.1185 11.1185 18.7166 O 47.1171 47.1171 59.5418 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 505 x= -17158.0 y= 2782.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 41.0 3.5 3.6 11.31 0.0485 3.5 0.0291 Mg 234.5 1.5 2.5 93.13 0.1310 1.5 0.0112 Sr 41.6 2.5 14.3 2.91 0.0039 2.5 0.0403 P 38.0 3.6 2.4 16.15 0.0461 3.6 0.0399 K 9.3 7.3 5.1 1.81 0.0039 7.4 0.0183 Cl 17.7 4.3 2.2 8.06 0.0035 4.3 0.0226 Ca 4379.6 0.3 17.7 248.13 0.9742 0.4 0.0335 Ba 13.1 4.4 10.8 1.21 0.0014 4.4 0.0759 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0561 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0633 Elt. k-ratio Correc. Na 0.0024 2.3118 Mg 0.0095 1.6927 Sr 0.0024 1.3742 P 0.0072 1.1927 K 0.0003 0.9978 Cl 0.0019 1.1030 Ca 0.3535 1.0816 Ba 0.0004 1.5411 Fe 0.0001 1.2435 Mn 0.0004 1.2682 iteration : 3 Analysis no. 505 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5601 0.022495 0.5601 0.4931 Mg 1.6051 0.024327 1.6051 1.3368 Sr 0.3343 0.014506 0.3343 0.0772 P 0.8623 0.034625 0.8623 0.5635 K 0.0341 0.006963 0.0341 0.0177 Cl 0.2118 0.011123 0.2118 0.1210 Ca 38.2386 0.164861 38.2386 19.3123 Ba 0.0607 0.020366 0.0607 0.0090 Fe 0.0117 0.013945 0.0117 0.0042 Mn 0.0489 0.021175 0.0489 0.0180 C 11.0140 11.0140 18.5620 O 47.0184 47.0184 59.4852 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 506 x= -17157.0 y= 2787.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.5 3.7 3.6 9.79 0.0414 3.8 0.0292 Mg 248.0 1.4 2.5 98.50 0.1387 1.5 0.0112 Sr 43.7 2.4 14.3 3.06 0.0043 2.4 0.0403 P 37.2 3.7 2.4 15.81 0.0451 3.7 0.0399 K 8.4 7.7 5.1 1.65 0.0031 7.7 0.0183 Cl 15.9 4.6 2.2 7.21 0.0030 4.6 0.0225 Ca 4546.5 0.3 17.7 257.58 1.0123 0.4 0.0334 Ba 13.1 4.4 10.8 1.21 0.0014 4.4 0.0761 Fe 4.1 7.8 3.3 1.25 0.0005 7.8 0.0561 Mn 4.4 10.7 2.7 1.61 0.0016 10.7 0.0633 Elt. k-ratio Correc. Na 0.0021 2.3117 Mg 0.0100 1.6906 Sr 0.0026 1.3727 P 0.0071 1.1913 K 0.0003 0.9928 Cl 0.0017 1.1002 Ca 0.3674 1.0795 Ba 0.0004 1.5417 Fe 0.0002 1.2417 Mn 0.0005 1.2668 iteration : 3 Analysis no. 506 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4780 0.021061 0.4780 0.4266 Mg 1.6980 0.025032 1.6980 1.4333 Sr 0.3606 0.014783 0.3606 0.0844 P 0.8426 0.034262 0.8426 0.5581 K 0.0270 0.006725 0.0270 0.0142 Cl 0.1861 0.010570 0.1861 0.1077 Ca 39.6557 0.168986 39.6557 20.2986 Ba 0.0608 0.020390 0.0608 0.0091 Fe 0.0276 0.014405 0.0276 0.0101 Mn 0.0598 0.021634 0.0598 0.0223 C 10.4632 10.4632 17.8720 O 46.1407 46.1407 59.1636 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 507 x= -17156.0 y= 2791.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 40.8 3.5 3.6 11.24 0.0482 3.5 0.0291 Mg 274.8 1.3 2.5 109.13 0.1538 1.4 0.0112 Sr 44.5 2.4 14.3 3.12 0.0044 2.4 0.0404 P 51.7 3.1 2.4 21.98 0.0639 3.1 0.0400 K 9.4 7.3 5.1 1.84 0.0040 7.3 0.0185 Cl 22.1 3.9 2.2 10.05 0.0044 3.9 0.0227 Ca 4251.6 0.3 17.7 240.87 0.9462 0.4 0.0335 Ba 13.4 4.3 10.8 1.25 0.0016 4.3 0.0759 Fe 4.4 7.6 3.3 1.32 0.0006 7.6 0.0561 Mn 5.1 9.9 2.7 1.88 0.0024 9.9 0.0633 Elt. k-ratio Correc. Na 0.0024 2.3052 Mg 0.0111 1.6892 Sr 0.0027 1.3757 P 0.0100 1.1946 K 0.0004 1.0041 Cl 0.0025 1.1073 Ca 0.3434 1.0830 Ba 0.0005 1.5396 Fe 0.0003 1.2435 Mn 0.0007 1.2680 iteration : 3 Analysis no. 507 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5551 0.022382 0.5551 0.4871 Mg 1.8812 0.026373 1.8812 1.5615 Sr 0.3711 0.014916 0.3711 0.0855 P 1.1969 0.040295 1.1969 0.7796 K 0.0356 0.007049 0.0356 0.0184 Cl 0.2726 0.012341 0.2726 0.1552 Ca 37.1898 0.161851 37.1898 18.7199 Ba 0.0706 0.020520 0.0706 0.0104 Fe 0.0352 0.014641 0.0352 0.0127 Mn 0.0872 0.022774 0.0872 0.0320 C 11.0321 11.0321 18.5305 O 47.2726 47.2726 59.6072 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 508 x= -17156.0 y= 2796.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 33.8 3.8 3.6 9.31 0.0391 3.9 0.0291 Mg 265.9 1.4 2.5 105.60 0.1487 1.4 0.0112 Sr 41.5 2.5 14.3 2.91 0.0039 2.5 0.0403 P 40.0 3.5 2.4 17.00 0.0487 3.6 0.0399 K 8.4 7.7 5.1 1.64 0.0030 7.7 0.0184 Cl 20.3 4.0 2.2 9.24 0.0040 4.0 0.0226 Ca 4309.5 0.3 17.7 244.15 0.9584 0.4 0.0335 Ba 13.2 4.4 10.8 1.23 0.0015 4.4 0.0759 Fe 4.1 7.8 3.3 1.23 0.0004 7.8 0.0561 Mn 3.8 11.5 2.7 1.40 0.0011 11.5 0.0633 Elt. k-ratio Correc. Na 0.0020 2.3101 Mg 0.0108 1.6899 Sr 0.0024 1.3755 P 0.0076 1.1939 K 0.0003 1.0006 Cl 0.0022 1.1048 Ca 0.3478 1.0825 Ba 0.0004 1.5407 Fe 0.0002 1.2439 Mn 0.0003 1.2686 iteration : 3 Analysis no. 508 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4510 0.020547 0.4510 0.3956 Mg 1.8193 0.025918 1.8193 1.5093 Sr 0.3343 0.014516 0.3343 0.0769 P 0.9116 0.035523 0.9116 0.5934 K 0.0268 0.006760 0.0268 0.0138 Cl 0.2477 0.011847 0.2477 0.1409 Ca 37.6518 0.163161 37.6518 18.9418 Ba 0.0640 0.020412 0.0640 0.0094 Fe 0.0259 0.014369 0.0259 0.0094 Mn 0.0398 0.020783 0.0398 0.0146 C 11.1424 11.1424 18.7052 O 47.2853 47.2853 59.5897 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 509 x= -17155.0 y= 2800.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.0 3.8 3.6 9.65 0.0408 3.8 0.0291 Mg 256.7 1.4 2.5 101.94 0.1436 1.4 0.0112 Sr 44.5 2.4 14.3 3.12 0.0044 2.4 0.0403 P 45.0 3.3 2.4 19.15 0.0553 3.3 0.0400 K 9.0 7.5 5.1 1.75 0.0036 7.5 0.0184 Cl 21.5 3.9 2.2 9.77 0.0043 3.9 0.0226 Ca 4316.6 0.3 17.7 244.55 0.9608 0.4 0.0335 Ba 13.7 4.3 10.8 1.28 0.0018 4.3 0.0760 Fe 4.1 7.8 3.3 1.25 0.0005 7.8 0.0561 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0633 Elt. k-ratio Correc. Na 0.0020 2.3089 Mg 0.0104 1.6896 Sr 0.0027 1.3745 P 0.0087 1.1935 K 0.0003 1.0011 Cl 0.0024 1.1052 Ca 0.3487 1.0823 Ba 0.0005 1.5404 Fe 0.0002 1.2434 Mn 0.0004 1.2681 iteration : 3 Analysis no. 509 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4699 0.020899 0.4699 0.4131 Mg 1.7567 0.025464 1.7567 1.4609 Sr 0.3709 0.014904 0.3709 0.0856 P 1.0346 0.037646 1.0346 0.6752 K 0.0318 0.006918 0.0318 0.0164 Cl 0.2639 0.012164 0.2639 0.1505 Ca 37.7385 0.163451 37.7385 19.0317 Ba 0.0786 0.020659 0.0786 0.0116 Fe 0.0276 0.014424 0.0276 0.0100 Mn 0.0453 0.021031 0.0453 0.0166 C 11.0299 11.0299 18.5615 O 47.1523 47.1523 59.5669 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 510 x= -17154.0 y= 2805.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 34.9 3.8 3.6 9.61 0.0406 3.8 0.0291 Mg 262.5 1.4 2.5 104.25 0.1469 1.4 0.0112 Sr 43.8 2.4 14.3 3.07 0.0043 2.4 0.0403 P 49.2 3.2 2.4 20.92 0.0607 3.2 0.0399 K 9.7 7.2 5.1 1.89 0.0042 7.2 0.0184 Cl 26.7 3.5 2.2 12.14 0.0054 3.5 0.0226 Ca 4339.1 0.3 17.7 245.83 0.9659 0.4 0.0335 Ba 11.7 4.6 10.8 1.09 0.0006 4.6 0.0760 Fe 4.6 7.4 3.3 1.39 0.0007 7.4 0.0561 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0633 Elt. k-ratio Correc. Na 0.0020 2.3069 Mg 0.0106 1.6880 Sr 0.0026 1.3738 P 0.0095 1.1929 K 0.0004 1.0013 Cl 0.0030 1.1052 Ca 0.3505 1.0823 Ba 0.0002 1.5407 Fe 0.0003 1.2431 Mn 0.0003 1.2679 iteration : 3 Analysis no. 510 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4673 0.020841 0.4673 0.4120 Mg 1.7954 0.025740 1.7954 1.4973 Sr 0.3624 0.014811 0.3624 0.0838 P 1.1348 0.039279 1.1348 0.7426 K 0.0376 0.007091 0.0376 0.0195 Cl 0.3351 0.013438 0.3351 0.1916 Ca 37.9389 0.164050 37.9389 19.1868 Ba 0.0258 0.019801 0.0258 0.0038 Fe 0.0427 0.014853 0.0427 0.0155 Mn 0.0325 0.020468 0.0325 0.0120 C 10.8753 10.8753 18.3531 O 46.9523 46.9523 59.4820 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 511 x= -17154.0 y= 2809.0 z= -282. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 32.5 3.9 3.6 8.95 0.0374 3.9 0.0291 Mg 262.7 1.4 2.5 104.33 0.1470 1.4 0.0112 Sr 43.1 2.4 14.3 3.02 0.0042 2.4 0.0403 P 64.2 2.8 2.4 27.32 0.0802 2.8 0.0399 K 8.8 7.6 5.1 1.72 0.0034 7.6 0.0185 Cl 29.5 3.4 2.2 13.43 0.0061 3.4 0.0227 Ca 4251.6 0.3 17.7 240.87 0.9462 0.4 0.0335 Ba 13.8 4.3 10.8 1.28 0.0018 4.3 0.0759 Fe 4.1 7.8 3.3 1.25 0.0005 7.8 0.0561 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0633 Elt. k-ratio Correc. Na 0.0019 2.3042 Mg 0.0106 1.6862 Sr 0.0026 1.3734 P 0.0126 1.1929 K 0.0003 1.0057 Cl 0.0034 1.1081 Ca 0.3434 1.0833 Ba 0.0005 1.5398 Fe 0.0002 1.2433 Mn 0.0004 1.2679 iteration : 3 Analysis no. 511 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4308 0.020146 0.4308 0.3787 Mg 1.7945 0.025718 1.7945 1.4921 Sr 0.3531 0.014707 0.3531 0.0814 P 1.4996 0.044796 1.4996 0.9784 K 0.0303 0.006900 0.0303 0.0156 Cl 0.3748 0.014119 0.3748 0.2136 Ca 37.1996 0.161894 37.1996 18.7566 Ba 0.0792 0.020660 0.0792 0.0117 Fe 0.0276 0.014422 0.0276 0.0100 Mn 0.0489 0.021184 0.0489 0.0180 C 10.9236 10.9236 18.3792 O 47.2381 47.2381 59.6646 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 512 x= -17153.0 y= 2814.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 10.8 6.8 3.6 2.98 0.0093 6.8 0.0295 Mg 53.5 3.1 2.5 21.23 0.0288 3.1 0.0113 Sr 19.3 3.6 14.3 1.35 0.0007 3.6 0.0404 P 50.2 3.2 2.4 21.34 0.0620 3.2 0.0401 K 13.0 6.2 5.1 2.54 0.0073 6.2 0.0191 Cl 41.7 2.8 2.2 18.96 0.0088 2.8 0.0230 Ca 3068.2 0.4 17.7 173.83 0.6817 0.5 0.0340 Ba 7.8 5.7 10.8 0.72 0.0000 5.7 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0640 Elt. k-ratio Correc. Na 0.0005 2.3367 Mg 0.0021 1.7006 Sr 0.0004 1.3774 P 0.0097 1.1979 K 0.0006 1.0384 Cl 0.0049 1.1241 Ca 0.2474 1.0992 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 1.2808 iteration : 2 Analysis no. 512 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1087 0.012878 0.1087 0.0862 Mg 0.3543 0.011687 0.3543 0.2656 Sr 0.0611 0.011255 0.0611 0.0127 P 1.1637 0.039827 1.1637 0.6846 K 0.0672 0.008135 0.0672 0.0313 Cl 0.5494 0.016856 0.5494 0.2824 Ca 27.1941 0.132143 27.1941 12.3633 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0015 0.019230 0.0015 0.0005 C 15.8203 15.8203 24.0007 O 54.6797 54.6797 62.2726 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 513 x= -17152.0 y= 2818.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.9 5.8 3.6 4.11 0.0146 5.8 0.0293 Mg 175.2 1.7 2.5 69.58 0.0975 1.7 0.0112 Sr 34.6 2.7 14.3 2.42 0.0029 2.7 0.0403 P 49.7 3.2 2.4 21.13 0.0613 3.2 0.0399 K 13.7 6.0 5.1 2.69 0.0080 6.0 0.0186 Cl 42.1 2.8 2.2 19.14 0.0089 2.8 0.0227 Ca 3884.8 0.4 17.7 220.09 0.8639 0.4 0.0337 Ba 12.1 4.5 10.8 1.13 0.0008 4.6 0.0759 Fe 4.2 7.7 3.3 1.28 0.0005 7.7 0.0563 Mn 3.3 12.3 2.7 1.22 0.0006 12.3 0.0635 Elt. k-ratio Correc. Na 0.0007 2.3200 Mg 0.0071 1.6907 Sr 0.0018 1.3735 P 0.0096 1.1935 K 0.0007 1.0144 Cl 0.0049 1.1111 Ca 0.3135 1.0884 Ba 0.0002 1.5397 Fe 0.0002 1.2487 Mn 0.0002 1.2724 iteration : 3 Analysis no. 513 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1696 0.014492 0.1696 0.1438 Mg 1.1938 0.020933 1.1938 0.9574 Sr 0.2491 0.013561 0.2491 0.0554 P 1.1468 0.039471 1.1468 0.7217 K 0.0719 0.008107 0.0719 0.0358 Cl 0.5484 0.016733 0.5484 0.3015 Ca 34.1218 0.152902 34.1218 16.5943 Ba 0.0356 0.019942 0.0356 0.0051 Fe 0.0311 0.014575 0.0311 0.0108 Mn 0.0216 0.020036 0.0216 0.0077 C 12.6923 12.6923 20.5975 O 49.7180 49.7180 60.5690 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 514 x= -17151.0 y= 2823.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 16.2 5.5 3.6 4.47 0.0163 5.6 0.0293 Mg 181.4 1.7 2.5 72.03 0.1011 1.7 0.0112 Sr 36.4 2.6 14.3 2.55 0.0032 2.6 0.0403 P 45.4 3.3 2.4 19.30 0.0557 3.3 0.0400 K 14.4 5.9 5.1 2.82 0.0086 5.9 0.0186 Cl 31.1 3.3 2.2 14.15 0.0064 3.3 0.0227 Ca 3988.1 0.4 17.7 225.94 0.8875 0.4 0.0337 Ba 12.9 4.4 10.8 1.20 0.0013 4.4 0.0760 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0563 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0635 Elt. k-ratio Correc. Na 0.0008 2.3207 Mg 0.0073 1.6914 Sr 0.0020 1.3735 P 0.0087 1.1933 K 0.0008 1.0100 Cl 0.0036 1.1091 Ca 0.3221 1.0869 Ba 0.0004 1.5401 Fe 0.0001 1.2478 Mn 0.0002 1.2718 iteration : 3 Analysis no. 514 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1893 0.015008 0.1893 0.1615 Mg 1.2375 0.021325 1.2375 0.9991 Sr 0.2707 0.013812 0.2707 0.0606 P 1.0430 0.037783 1.0430 0.6607 K 0.0774 0.008226 0.0774 0.0389 Cl 0.3971 0.014487 0.3971 0.2198 Ca 35.0045 0.155514 35.0045 17.1366 Ba 0.0561 0.020295 0.0561 0.0080 Fe 0.0160 0.014130 0.0160 0.0056 Mn 0.0253 0.020203 0.0253 0.0090 C 12.4140 12.4140 20.2797 O 49.2691 49.2691 60.4205 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 515 x= -17151.0 y= 2827.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 15.4 5.7 3.6 4.23 0.0152 5.7 0.0294 Mg 128.3 2.0 2.5 50.94 0.0710 2.0 0.0112 Sr 28.6 3.0 14.3 2.00 0.0021 3.0 0.0403 P 47.2 3.3 2.4 20.09 0.0581 3.3 0.0400 K 16.9 5.4 5.1 3.30 0.0109 5.5 0.0188 Cl 44.6 2.7 2.2 20.29 0.0094 2.7 0.0228 Ca 3691.3 0.4 17.7 209.13 0.8211 0.5 0.0338 Ba 11.7 4.6 10.8 1.09 0.0006 4.6 0.0759 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0565 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0637 Elt. k-ratio Correc. Na 0.0008 2.3259 Mg 0.0051 1.6945 Sr 0.0013 1.3739 P 0.0091 1.1938 K 0.0010 1.0194 Cl 0.0053 1.1133 Ca 0.2980 1.0909 Ba 0.0002 1.5394 Fe 0.0001 1.2513 Mn 0.0003 1.2746 iteration : 3 Analysis no. 515 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1769 0.014714 0.1769 0.1474 Mg 0.8716 0.017928 0.8716 0.6872 Sr 0.1757 0.012706 0.1757 0.0384 P 1.0883 0.038541 1.0883 0.6733 K 0.0988 0.008810 0.0988 0.0484 Cl 0.5847 0.017251 0.5847 0.3160 Ca 32.5088 0.148170 32.5088 15.5425 Ba 0.0251 0.019774 0.0251 0.0035 Fe 0.0118 0.014044 0.0118 0.0040 Mn 0.0345 0.020658 0.0345 0.0120 C 13.5005 13.5005 21.5387 O 50.9233 50.9233 60.9884 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 516 x= -17150.0 y= 2832.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.2 5.4 3.6 4.74 0.0176 5.4 0.0293 Mg 177.4 1.7 2.5 70.44 0.0988 1.7 0.0112 Sr 39.6 2.5 14.3 2.77 0.0037 2.5 0.0403 P 52.4 3.1 2.4 22.28 0.0648 3.1 0.0400 K 16.4 5.5 5.1 3.22 0.0105 5.5 0.0186 Cl 38.4 2.9 2.2 17.46 0.0080 2.9 0.0228 Ca 3944.9 0.4 17.7 223.49 0.8777 0.4 0.0337 Ba 11.6 4.6 10.8 1.08 0.0005 4.6 0.0759 Fe 3.6 8.4 3.3 1.08 0.0002 8.4 0.0563 Mn 4.4 10.7 2.7 1.61 0.0016 10.7 0.0635 Elt. k-ratio Correc. Na 0.0009 2.3182 Mg 0.0072 1.6901 Sr 0.0023 1.3727 P 0.0102 1.1933 K 0.0009 1.0129 Cl 0.0045 1.1106 Ca 0.3185 1.0875 Ba 0.0002 1.5397 Fe 0.0001 1.2477 Mn 0.0005 1.2716 iteration : 3 Analysis no. 516 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2041 0.015366 0.2041 0.1741 Mg 1.2088 0.021065 1.2088 0.9752 Sr 0.3100 0.014240 0.3100 0.0694 P 1.2127 0.040519 1.2127 0.7677 K 0.0944 0.008663 0.0944 0.0473 Cl 0.4975 0.016015 0.4975 0.2752 Ca 34.6420 0.154453 34.6420 16.9480 Ba 0.0231 0.019743 0.0231 0.0033 Fe 0.0092 0.013927 0.0092 0.0032 Mn 0.0600 0.021714 0.0600 0.0214 C 12.4146 12.4146 20.2674 O 49.3236 49.3236 60.4477 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 517 x= -17149.0 y= 2836.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 15.1 5.7 3.6 4.16 0.0149 5.8 0.0293 Mg 148.9 1.8 2.5 59.12 0.0827 1.9 0.0112 Sr 30.6 2.9 14.3 2.14 0.0024 2.9 0.0404 P 37.2 3.7 2.4 15.83 0.0452 3.7 0.0401 K 11.9 6.5 5.1 2.32 0.0063 6.5 0.0189 Cl 49.9 2.6 2.2 22.66 0.0106 2.6 0.0229 Ca 3474.1 0.4 17.7 196.82 0.7726 0.5 0.0339 Ba 9.0 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.7 8.2 3.3 1.13 0.0002 8.2 0.0566 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0638 Elt. k-ratio Correc. Na 0.0007 2.3256 Mg 0.0060 1.6949 Sr 0.0015 1.3775 P 0.0071 1.1973 K 0.0006 1.0261 Cl 0.0059 1.1168 Ca 0.2804 1.0937 Ba 0.0000 NaN Fe 0.0001 1.2537 Mn 0.0001 1.2766 iteration : 3 Analysis no. 517 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1731 0.014614 0.1731 0.1418 Mg 1.0148 0.019331 1.0148 0.7865 Sr 0.2007 0.013035 0.2007 0.0432 P 0.8481 0.034458 0.8481 0.5158 K 0.0571 0.007790 0.0571 0.0275 Cl 0.6585 0.018246 0.6585 0.3499 Ca 30.6652 0.142671 30.6652 14.4121 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0143 0.014147 0.0143 0.0048 Mn 0.0089 0.019518 0.0089 0.0030 C 14.2971 14.2971 22.4222 O 52.0622 52.0622 61.2932 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 518 x= -17149.0 y= 2840.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.3 5.4 3.6 4.77 0.0178 5.4 0.0293 Mg 149.5 1.8 2.5 59.38 0.0831 1.9 0.0112 Sr 34.7 2.7 14.3 2.43 0.0029 2.7 0.0404 P 47.6 3.2 2.4 20.24 0.0586 3.3 0.0401 K 15.1 5.7 5.1 2.96 0.0093 5.8 0.0188 Cl 42.4 2.8 2.2 19.28 0.0089 2.8 0.0229 Ca 3551.5 0.4 17.7 201.21 0.7899 0.5 0.0338 Ba 10.6 4.8 10.8 0.99 0.0000 4.9 0.0000 Fe 3.9 8.0 3.3 1.19 0.0004 8.0 0.0565 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0637 Elt. k-ratio Correc. Na 0.0009 2.3233 Mg 0.0060 1.6939 Sr 0.0018 1.3761 P 0.0092 1.1966 K 0.0008 1.0244 Cl 0.0050 1.1167 Ca 0.2867 1.0926 Ba 0.0000 NaN Fe 0.0002 1.2523 Mn 0.0004 1.2753 iteration : 3 Analysis no. 518 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2061 0.015438 0.2061 0.1703 Mg 1.0187 0.019362 1.0187 0.7961 Sr 0.2503 0.013601 0.2503 0.0543 P 1.0994 0.038771 1.0994 0.6742 K 0.0845 0.008492 0.0845 0.0410 Cl 0.5556 0.016883 0.5556 0.2977 Ca 31.3191 0.144621 31.3191 14.8424 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0211 0.014331 0.0211 0.0072 Mn 0.0473 0.021232 0.0473 0.0164 C 13.8572 13.8572 21.9139 O 51.5407 51.5407 61.1865 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 519 x= -17148.0 y= 2845.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.9 5.8 3.6 4.09 0.0146 5.8 0.0293 Mg 135.2 1.9 2.5 53.68 0.0749 1.9 0.0112 Sr 30.1 2.9 14.3 2.11 0.0023 2.9 0.0404 P 47.6 3.2 2.4 20.26 0.0587 3.3 0.0401 K 12.6 6.3 5.1 2.46 0.0069 6.3 0.0189 Cl 49.3 2.6 2.2 22.39 0.0105 2.6 0.0229 Ca 3438.0 0.4 17.7 194.78 0.7644 0.5 0.0339 Ba 8.3 5.5 10.8 0.77 0.0000 5.5 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 4.1 11.1 2.7 1.50 0.0013 11.1 0.0638 Elt. k-ratio Correc. Na 0.0007 2.3252 Mg 0.0054 1.6945 Sr 0.0014 1.3765 P 0.0092 1.1968 K 0.0006 1.0281 Cl 0.0058 1.1183 Ca 0.2774 1.0942 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0004 1.2765 iteration : 3 Analysis no. 519 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1693 0.014512 0.1693 0.1386 Mg 0.9194 0.018406 0.9194 0.7119 Sr 0.1941 0.012947 0.1941 0.0417 P 1.1007 0.038794 1.1007 0.6687 K 0.0631 0.007965 0.0631 0.0304 Cl 0.6510 0.018163 0.6510 0.3455 Ca 30.3554 0.141737 30.3554 14.2523 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0492 0.021330 0.0492 0.0169 C 14.2946 14.2946 22.3959 O 52.2031 52.2031 61.3981 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 520 x= -17147.0 y= 2849.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 24.7 4.5 3.6 6.81 0.0274 4.5 0.0292 Mg 158.9 1.8 2.5 63.08 0.0883 1.8 0.0112 Sr 35.4 2.7 14.3 2.48 0.0031 2.7 0.0403 P 57.2 3.0 2.4 24.32 0.0710 3.0 0.0400 K 16.5 5.5 5.1 3.23 0.0105 5.5 0.0188 Cl 48.2 2.6 2.2 21.90 0.0102 2.6 0.0228 Ca 3741.7 0.4 17.7 211.98 0.8324 0.5 0.0338 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0759 Fe 3.6 8.4 3.3 1.08 0.0001 8.4 0.0564 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0636 Elt. k-ratio Correc. Na 0.0014 2.3165 Mg 0.0064 1.6917 Sr 0.0019 1.3737 P 0.0111 1.1943 K 0.0009 1.0201 Cl 0.0057 1.1143 Ca 0.3021 1.0904 Ba 0.0000 1.5391 Fe 0.0001 1.2498 Mn 0.0001 1.2733 iteration : 3 Analysis no. 520 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3167 0.017928 0.3167 0.2662 Mg 1.0818 0.019937 1.0818 0.8602 Sr 0.2591 0.013682 0.2591 0.0571 P 1.3304 0.042345 1.3304 0.8300 K 0.0955 0.008736 0.0955 0.0472 Cl 0.6340 0.017910 0.6340 0.3456 Ca 32.9380 0.149446 32.9380 15.8816 Ba 0.0033 0.019403 0.0033 0.0005 Fe 0.0084 0.013926 0.0084 0.0029 Mn 0.0107 0.019553 0.0107 0.0038 C 13.0187 13.0187 20.9466 O 50.3036 50.3036 60.7583 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 521 x= -17146.0 y= 2854.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.6 5.9 3.6 4.01 0.0142 5.9 0.0293 Mg 139.5 1.9 2.5 55.41 0.0774 1.9 0.0112 Sr 34.1 2.7 14.3 2.39 0.0029 2.7 0.0404 P 45.4 3.3 2.4 19.32 0.0558 3.3 0.0401 K 12.7 6.3 5.1 2.49 0.0071 6.3 0.0189 Cl 56.0 2.4 2.2 25.44 0.0119 2.4 0.0229 Ca 3499.0 0.4 17.7 198.24 0.7780 0.5 0.0339 Ba 10.7 4.8 10.8 1.00 0.0000 4.8 0.0000 Fe 3.3 8.7 3.3 0.99 0.0000 8.7 0.0000 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0637 Elt. k-ratio Correc. Na 0.0007 2.3232 Mg 0.0056 1.6931 Sr 0.0018 1.3756 P 0.0087 1.1964 K 0.0006 1.0267 Cl 0.0067 1.1171 Ca 0.2824 1.0935 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2759 iteration : 3 Analysis no. 521 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1646 0.014380 0.1646 0.1354 Mg 0.9488 0.018686 0.9488 0.7383 Sr 0.2434 0.013517 0.2434 0.0525 P 1.0467 0.037896 1.0467 0.6392 K 0.0643 0.007987 0.0643 0.0311 Cl 0.7429 0.019295 0.7429 0.3963 Ca 30.8757 0.143298 30.8757 14.5702 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0162 0.019847 0.0162 0.0056 C 14.0940 14.0940 22.1939 O 51.8034 51.8034 61.2374 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 522 x= -17146.0 y= 2858.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 22.1 4.8 3.6 6.08 0.0239 4.8 0.0293 Mg 141.7 1.9 2.5 56.28 0.0787 1.9 0.0112 Sr 37.0 2.6 14.3 2.59 0.0033 2.6 0.0404 P 47.4 3.2 2.4 20.17 0.0584 3.3 0.0400 K 13.7 6.0 5.1 2.69 0.0080 6.0 0.0188 Cl 44.7 2.7 2.2 20.31 0.0094 2.7 0.0228 Ca 3635.6 0.4 17.7 205.97 0.8087 0.5 0.0338 Ba 11.6 4.6 10.8 1.08 0.0005 4.6 0.0759 Fe 3.7 8.3 3.3 1.11 0.0002 8.3 0.0565 Mn 3.9 11.3 2.7 1.44 0.0012 11.3 0.0637 Elt. k-ratio Correc. Na 0.0012 2.3220 Mg 0.0057 1.6944 Sr 0.0020 1.3750 P 0.0092 1.1958 K 0.0007 1.0219 Cl 0.0053 1.1152 Ca 0.2935 1.0914 Ba 0.0002 1.5386 Fe 0.0001 1.2512 Mn 0.0003 1.2744 iteration : 3 Analysis no. 522 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2775 0.017102 0.2775 0.2308 Mg 0.9649 0.018850 0.9649 0.7592 Sr 0.2786 0.013913 0.2786 0.0608 P 1.0950 0.038684 1.0950 0.6760 K 0.0725 0.008172 0.0725 0.0354 Cl 0.5862 0.017285 0.5862 0.3162 Ca 32.0297 0.146735 32.0297 15.2820 Ba 0.0231 0.019731 0.0231 0.0032 Fe 0.0118 0.014043 0.0118 0.0040 Mn 0.0436 0.021058 0.0436 0.0152 C 13.5726 13.5726 21.6092 O 51.0446 51.0446 61.0079 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 523 x= -17145.0 y= 2863.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.1 4.6 3.6 6.37 0.0253 4.7 0.0293 Mg 148.6 1.8 2.5 59.01 0.0825 1.9 0.0112 Sr 36.2 2.6 14.3 2.53 0.0032 2.6 0.0403 P 50.0 3.2 2.4 21.28 0.0618 3.2 0.0400 K 16.8 5.4 5.1 3.29 0.0109 5.5 0.0188 Cl 48.7 2.6 2.2 22.13 0.0103 2.6 0.0228 Ca 3687.3 0.4 17.7 208.90 0.8202 0.5 0.0338 Ba 10.8 4.8 10.8 1.01 0.0000 4.8 0.0759 Fe 4.3 7.7 3.3 1.29 0.0005 7.7 0.0564 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0636 Elt. k-ratio Correc. Na 0.0013 2.3201 Mg 0.0060 1.6934 Sr 0.0020 1.3744 P 0.0097 1.1950 K 0.0010 1.0210 Cl 0.0058 1.1145 Ca 0.2976 1.0909 Ba 0.0000 1.5388 Fe 0.0003 1.2505 Mn 0.0003 1.2738 iteration : 3 Analysis no. 523 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2931 0.017436 0.2931 0.2450 Mg 1.0117 0.019293 1.0117 0.8001 Sr 0.2687 0.013795 0.2687 0.0589 P 1.1573 0.039677 1.1573 0.7182 K 0.0985 0.008813 0.0985 0.0484 Cl 0.6409 0.017999 0.6409 0.3475 Ca 32.4705 0.148049 32.4705 15.5716 Ba 0.0020 0.019376 0.0020 0.0003 Fe 0.0320 0.014628 0.0320 0.0110 Mn 0.0363 0.020726 0.0363 0.0127 C 13.3234 13.3234 21.3210 O 50.6657 50.6657 60.8652 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 524 x= -17144.0 y= 2867.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 24.5 4.5 3.6 6.74 0.0271 4.5 0.0293 Mg 134.2 1.9 2.5 53.28 0.0744 2.0 0.0112 Sr 32.6 2.8 14.3 2.29 0.0027 2.8 0.0403 P 57.5 2.9 2.4 24.45 0.0714 3.0 0.0400 K 18.1 5.3 5.1 3.54 0.0120 5.3 0.0188 Cl 50.0 2.6 2.2 22.74 0.0106 2.6 0.0228 Ca 3734.4 0.4 17.7 211.57 0.8308 0.5 0.0338 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 4.0 7.9 3.3 1.22 0.0004 7.9 0.0564 Mn 4.5 10.5 2.7 1.66 0.0018 10.5 0.0636 Elt. k-ratio Correc. Na 0.0014 2.3200 Mg 0.0054 1.6934 Sr 0.0016 1.3728 P 0.0112 1.1934 K 0.0011 1.0200 Cl 0.0059 1.1139 Ca 0.3015 1.0904 Ba 0.0000 NaN Fe 0.0002 1.2499 Mn 0.0005 1.2733 iteration : 3 Analysis no. 524 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3134 0.017875 0.3134 0.2632 Mg 0.9120 0.018327 0.9120 0.7245 Sr 0.2249 0.013283 0.2249 0.0496 P 1.3366 0.042422 1.3366 0.8332 K 0.1089 0.009054 0.1089 0.0538 Cl 0.6590 0.018227 0.6590 0.3589 Ca 32.8737 0.149251 32.8737 15.8356 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0244 0.014402 0.0244 0.0084 Mn 0.0656 0.021975 0.0656 0.0230 C 13.0948 13.0948 21.0490 O 50.3867 50.3867 60.8009 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 525 x= -17144.0 y= 2872.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 24.7 4.5 3.6 6.80 0.0273 4.5 0.0293 Mg 154.5 1.8 2.5 61.35 0.0859 1.8 0.0112 Sr 38.4 2.5 14.3 2.69 0.0035 2.6 0.0404 P 50.9 3.1 2.4 21.66 0.0630 3.1 0.0400 K 16.8 5.5 5.1 3.28 0.0108 5.5 0.0188 Cl 48.9 2.6 2.2 22.21 0.0104 2.6 0.0228 Ca 3730.8 0.4 17.7 211.37 0.8302 0.5 0.0338 Ba 11.3 4.7 10.8 1.05 0.0004 4.7 0.0760 Fe 3.5 8.4 3.3 1.06 0.0001 8.5 0.0565 Mn 3.7 11.7 2.7 1.35 0.0009 11.7 0.0636 Elt. k-ratio Correc. Na 0.0014 2.3180 Mg 0.0062 1.6926 Sr 0.0022 1.3740 P 0.0099 1.1948 K 0.0010 1.0199 Cl 0.0058 1.1139 Ca 0.3013 1.0903 Ba 0.0001 1.5389 Fe 0.0001 1.2499 Mn 0.0003 1.2733 iteration : 3 Analysis no. 525 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3162 0.017930 0.3162 0.2655 Mg 1.0526 0.019676 1.0526 0.8358 Sr 0.2963 0.014105 0.2963 0.0653 P 1.1795 0.040035 1.1795 0.7350 K 0.0980 0.008798 0.0980 0.0484 Cl 0.6432 0.018028 0.6432 0.3501 Ca 32.8518 0.149199 32.8518 15.8191 Ba 0.0152 0.019608 0.0152 0.0021 Fe 0.0067 0.013881 0.0067 0.0023 Mn 0.0345 0.020645 0.0345 0.0121 C 13.1331 13.1331 21.1027 O 50.3728 50.3728 60.7615 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 526 x= -17143.0 y= 2876.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 14.1 5.9 3.6 3.89 0.0136 6.0 0.0294 Mg 102.8 2.2 2.5 40.82 0.0567 2.2 0.0112 Sr 25.9 3.1 14.3 1.82 0.0017 3.1 0.0404 P 51.2 3.1 2.4 21.79 0.0633 3.1 0.0401 K 13.1 6.2 5.1 2.57 0.0074 6.2 0.0191 Cl 56.4 2.4 2.2 25.65 0.0121 2.4 0.0230 Ca 3145.8 0.4 17.7 178.22 0.6992 0.5 0.0340 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0567 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0639 Elt. k-ratio Correc. Na 0.0007 2.3279 Mg 0.0041 1.6965 Sr 0.0010 1.3777 P 0.0099 1.1984 K 0.0007 1.0381 Cl 0.0067 1.1235 Ca 0.2537 1.0981 Ba 0.0000 NaN Fe 0.0001 1.2570 Mn 0.0001 1.2791 iteration : 2 Analysis no. 526 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1582 0.014230 0.1582 0.1267 Mg 0.6959 0.016068 0.6959 0.5272 Sr 0.1433 0.012335 0.1433 0.0301 P 1.1900 0.040257 1.1900 0.7075 K 0.0685 0.008167 0.0685 0.0323 Cl 0.7537 0.019486 0.7537 0.3915 Ca 27.8639 0.134201 27.8639 12.8024 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0152 0.014209 0.0152 0.0050 Mn 0.0162 0.019899 0.0162 0.0054 C 15.2946 15.2946 23.4497 O 53.8005 53.8005 61.9221 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 527 x= -17142.0 y= 2881.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 26.1 4.4 3.6 7.18 0.0291 4.4 0.0293 Mg 118.7 2.1 2.5 47.14 0.0656 2.1 0.0112 Sr 36.5 2.6 14.3 2.55 0.0032 2.6 0.0403 P 56.6 3.0 2.4 24.07 0.0703 3.0 0.0400 K 16.6 5.5 5.1 3.25 0.0106 5.5 0.0189 Cl 62.5 2.3 2.2 28.41 0.0134 2.3 0.0229 Ca 3498.3 0.4 17.7 198.20 0.7780 0.5 0.0339 Ba 10.8 4.8 10.8 1.01 0.0000 4.8 0.0759 Fe 3.8 8.1 3.3 1.15 0.0003 8.1 0.0565 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0637 Elt. k-ratio Correc. Na 0.0015 2.3193 Mg 0.0048 1.6941 Sr 0.0020 1.3740 P 0.0110 1.1955 K 0.0009 1.0285 Cl 0.0075 1.1181 Ca 0.2823 1.0934 Ba 0.0000 1.5379 Fe 0.0001 1.2520 Mn 0.0004 1.2750 iteration : 3 Analysis no. 527 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3374 0.018376 0.3374 0.2787 Mg 0.8052 0.017241 0.8052 0.6290 Sr 0.2720 0.013831 0.2720 0.0589 P 1.3172 0.042169 1.3172 0.8075 K 0.0971 0.008827 0.0971 0.0472 Cl 0.8341 0.020379 0.8341 0.4467 Ca 30.8714 0.143289 30.8714 14.6257 Ba 0.0020 0.019365 0.0020 0.0003 Fe 0.0169 0.014204 0.0169 0.0057 Mn 0.0455 0.021147 0.0455 0.0157 C 13.8719 13.8719 21.9303 O 51.5295 51.5295 61.1542 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 528 x= -17141.0 y= 2885.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 18.0 5.3 3.6 4.96 0.0187 5.3 0.0294 Mg 102.6 2.2 2.5 40.74 0.0565 2.2 0.0113 Sr 22.9 3.3 14.3 1.61 0.0012 3.3 0.0406 P 45.5 3.3 2.4 19.34 0.0559 3.3 0.0403 K 15.0 5.8 5.1 2.93 0.0092 5.8 0.0193 Cl 46.9 2.7 2.2 21.30 0.0099 2.7 0.0231 Ca 2813.5 0.4 17.7 159.40 0.6249 0.5 0.0341 Ba 6.9 6.0 10.8 0.64 0.0000 6.0 0.0000 Fe 3.6 8.4 3.3 1.08 0.0002 8.4 0.0569 Mn 2.9 13.1 2.7 1.07 0.0002 13.1 0.0641 Elt. k-ratio Correc. Na 0.0009 2.3306 Mg 0.0041 1.7002 Sr 0.0008 1.3826 P 0.0088 1.2028 K 0.0008 1.0483 Cl 0.0055 1.1295 Ca 0.2268 1.1024 Ba 0.0000 NaN Fe 0.0001 1.2610 Mn 0.0001 1.2823 iteration : 2 Analysis no. 528 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2173 0.015745 0.2173 0.1696 Mg 0.6960 0.016088 0.6960 0.5139 Sr 0.1067 0.011905 0.1067 0.0219 P 1.0538 0.038126 1.0538 0.6106 K 0.0851 0.008657 0.0851 0.0391 Cl 0.6240 0.017909 0.6240 0.3159 Ca 25.0004 0.125356 25.0004 11.1946 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0093 0.014076 0.0093 0.0030 Mn 0.0071 0.019519 0.0071 0.0023 C 16.4905 16.4905 24.6402 O 55.7098 55.7099 62.4890 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 529 x= -17141.0 y= 2890.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 25.6 4.4 3.6 7.06 0.0286 4.4 0.0292 Mg 150.2 1.8 2.5 59.64 0.0834 1.9 0.0112 Sr 35.8 2.6 14.3 2.51 0.0031 2.7 0.0403 P 55.2 3.0 2.4 23.49 0.0685 3.0 0.0400 K 17.5 5.3 5.1 3.43 0.0115 5.4 0.0188 Cl 53.9 2.5 2.2 24.51 0.0115 2.5 0.0228 Ca 3691.2 0.4 17.7 209.12 0.8211 0.5 0.0338 Ba 11.8 4.6 10.8 1.09 0.0006 4.6 0.0759 Fe 4.2 7.7 3.3 1.28 0.0005 7.7 0.0564 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0636 Elt. k-ratio Correc. Na 0.0014 2.3175 Mg 0.0060 1.6927 Sr 0.0019 1.3739 P 0.0107 1.1946 K 0.0010 1.0219 Cl 0.0064 1.1148 Ca 0.2980 1.0908 Ba 0.0002 1.5386 Fe 0.0002 1.2500 Mn 0.0003 1.2734 iteration : 3 Analysis no. 529 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3304 0.018221 0.3304 0.2769 Mg 1.0225 0.019391 1.0225 0.8106 Sr 0.2640 0.013740 0.2640 0.0581 P 1.2833 0.041638 1.2833 0.7983 K 0.1045 0.008962 0.1045 0.0515 Cl 0.7134 0.018916 0.7134 0.3877 Ca 32.5051 0.148154 32.5051 15.6261 Ba 0.0264 0.019785 0.0264 0.0037 Fe 0.0311 0.014599 0.0311 0.0107 Mn 0.0363 0.020720 0.0363 0.0127 C 13.1898 13.1898 21.1586 O 50.4932 50.4932 60.8051 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 530 x= -17140.0 y= 2894.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 17.0 5.4 3.6 4.69 0.0174 5.4 0.0293 Mg 108.9 2.1 2.5 43.24 0.0601 2.2 0.0112 Sr 35.6 2.6 14.3 2.49 0.0031 2.7 0.0404 P 47.7 3.2 2.4 20.30 0.0588 3.3 0.0401 K 14.8 5.8 5.1 2.90 0.0090 5.8 0.0190 Cl 59.3 2.4 2.2 26.97 0.0127 2.4 0.0230 Ca 3301.8 0.4 17.7 187.06 0.7341 0.5 0.0339 Ba 10.5 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.8 8.2 3.3 1.14 0.0003 8.2 0.0566 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0638 Elt. k-ratio Correc. Na 0.0009 2.3252 Mg 0.0044 1.6954 Sr 0.0019 1.3761 P 0.0092 1.1977 K 0.0008 1.0334 Cl 0.0071 1.1207 Ca 0.2664 1.0959 Ba 0.0000 NaN Fe 0.0001 1.2548 Mn 0.0002 1.2773 iteration : 3 Analysis no. 530 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2017 0.015338 0.2017 0.1636 Mg 0.7377 0.016526 0.7377 0.5661 Sr 0.2613 0.013727 0.2613 0.0556 P 1.1041 0.038866 1.1041 0.6648 K 0.0827 0.008503 0.0827 0.0394 Cl 0.7921 0.019916 0.7921 0.4167 Ca 29.1960 0.138245 29.1960 13.5866 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0152 0.014185 0.0152 0.0051 Mn 0.0272 0.020374 0.0272 0.0092 C 14.7500 14.7500 22.9049 O 52.8320 52.8320 61.5878 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 531 x= -17139.0 y= 2898.0 z= -281. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 22.3 4.7 3.6 6.15 0.0243 4.7 0.0293 Mg 117.9 2.1 2.5 46.82 0.0652 2.1 0.0112 Sr 36.3 2.6 14.3 2.54 0.0032 2.6 0.0403 P 51.7 3.1 2.4 22.00 0.0640 3.1 0.0400 K 18.0 5.3 5.1 3.52 0.0119 5.3 0.0189 Cl 52.2 2.5 2.2 23.72 0.0111 2.5 0.0229 Ca 3547.8 0.4 17.7 201.00 0.7890 0.5 0.0338 Ba 11.5 4.7 10.8 1.07 0.0005 4.7 0.0759 Fe 4.0 7.9 3.3 1.22 0.0004 7.9 0.0565 Mn 3.5 12.0 2.7 1.27 0.0007 12.0 0.0637 Elt. k-ratio Correc. Na 0.0012 2.3225 Mg 0.0047 1.6948 Sr 0.0020 1.3742 P 0.0100 1.1955 K 0.0011 1.0255 Cl 0.0062 1.1167 Ca 0.2864 1.0927 Ba 0.0001 1.5383 Fe 0.0002 1.2520 Mn 0.0002 1.2750 iteration : 3 Analysis no. 531 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2813 0.017190 0.2813 0.2327 Mg 0.8000 0.017190 0.8000 0.6259 Sr 0.2696 0.013805 0.2696 0.0585 P 1.1992 0.040350 1.1992 0.7362 K 0.1087 0.009083 0.1087 0.0528 Cl 0.6907 0.018651 0.6907 0.3705 Ca 31.2887 0.144532 31.2887 14.8450 Ba 0.0204 0.019682 0.0204 0.0028 Fe 0.0244 0.014426 0.0244 0.0083 Mn 0.0272 0.020337 0.0272 0.0094 C 13.8347 13.8347 21.9033 O 51.4551 51.4551 61.1546 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 532 x= -17138.0 y= 2903.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 23.1 4.6 3.6 6.37 0.0253 4.7 0.0293 Mg 93.7 2.3 2.5 37.22 0.0515 2.3 0.0112 Sr 28.4 3.0 14.3 1.99 0.0020 3.0 0.0405 P 53.6 3.1 2.4 22.81 0.0664 3.1 0.0402 K 15.9 5.6 5.1 3.12 0.0100 5.6 0.0192 Cl 60.5 2.3 2.2 27.51 0.0130 2.3 0.0231 Ca 2980.7 0.4 17.7 168.87 0.6623 0.5 0.0341 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 2.9 9.3 3.3 0.87 0.0000 9.3 0.0000 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0639 Elt. k-ratio Correc. Na 0.0013 2.3252 Mg 0.0037 1.6980 Sr 0.0013 1.3790 P 0.0104 1.2003 K 0.0009 1.0445 Cl 0.0072 1.1270 Ca 0.2404 1.1002 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2801 iteration : 2 Analysis no. 532 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2937 0.017475 0.2937 0.2329 Mg 0.6336 0.015363 0.6336 0.4752 Sr 0.1739 0.012723 0.1739 0.0362 P 1.2504 0.041234 1.2504 0.7358 K 0.0930 0.008829 0.0930 0.0434 Cl 0.8133 0.020223 0.8133 0.4181 Ca 26.4449 0.129844 26.4449 12.0265 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0144 0.019830 0.0144 0.0048 C 15.7525 15.7525 23.9053 O 54.5303 54.5303 62.1219 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 533 x= -17138.0 y= 2907.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 36.6 3.7 3.6 10.08 0.0428 3.7 0.0292 Mg 149.1 1.8 2.5 59.22 0.0828 1.9 0.0112 Sr 34.8 2.7 14.3 2.44 0.0030 2.7 0.0404 P 60.3 2.9 2.4 25.66 0.0751 2.9 0.0401 K 17.2 5.4 5.1 3.36 0.0112 5.4 0.0190 Cl 58.8 2.4 2.2 26.74 0.0126 2.4 0.0230 Ca 3373.1 0.4 17.7 191.10 0.7500 0.5 0.0339 Ba 10.6 4.8 10.8 0.99 0.0000 4.9 0.0000 Fe 3.9 8.0 3.3 1.18 0.0003 8.0 0.0566 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0637 Elt. k-ratio Correc. Na 0.0021 2.3139 Mg 0.0060 1.6945 Sr 0.0018 1.3771 P 0.0118 1.1980 K 0.0010 1.0331 Cl 0.0070 1.1214 Ca 0.2722 1.0950 Ba 0.0000 NaN Fe 0.0002 1.2530 Mn 0.0002 1.2757 iteration : 3 Analysis no. 533 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4942 0.021366 0.4942 0.4053 Mg 1.0163 0.019343 1.0163 0.7884 Sr 0.2526 0.013636 0.2526 0.0544 P 1.4112 0.043617 1.4112 0.8590 K 0.1026 0.008990 0.1026 0.0495 Cl 0.7857 0.019847 0.7857 0.4178 Ca 29.8039 0.140080 29.8039 14.0193 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0202 0.014315 0.0202 0.0068 Mn 0.0199 0.020016 0.0199 0.0068 C 14.0905 14.0905 22.1171 O 52.0028 52.0028 61.2757 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 534 x= -17137.0 y= 2912.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 25.5 4.4 3.6 7.03 0.0284 4.4 0.0293 Mg 116.0 2.1 2.5 46.05 0.0641 2.1 0.0112 Sr 29.0 2.9 14.3 2.03 0.0021 2.9 0.0405 P 60.6 2.9 2.4 25.79 0.0755 2.9 0.0402 K 16.1 5.6 5.1 3.16 0.0102 5.6 0.0193 Cl 66.4 2.2 2.2 30.17 0.0143 2.2 0.0231 Ca 2969.6 0.4 17.7 168.24 0.6598 0.5 0.0341 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.3 8.7 3.3 0.99 0.0000 8.7 0.0000 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0639 Elt. k-ratio Correc. Na 0.0014 2.3201 Mg 0.0046 1.6959 Sr 0.0013 1.3793 P 0.0118 1.2005 K 0.0009 1.0463 Cl 0.0079 1.1281 Ca 0.2395 1.1004 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2796 iteration : 2 Analysis no. 534 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3292 0.018210 0.3292 0.2616 Mg 0.7869 0.017058 0.7869 0.5915 Sr 0.1816 0.012819 0.1816 0.0379 P 1.4215 0.043816 1.4215 0.8385 K 0.0949 0.008886 0.0949 0.0443 Cl 0.8956 0.021173 0.8956 0.4616 Ca 26.3496 0.129551 26.3496 12.0114 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0236 0.020244 0.0236 0.0078 C 15.5757 15.5757 23.6927 O 54.3413 54.3413 62.0526 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 535 x= -17136.0 y= 2916.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 18.8 5.2 3.6 5.18 0.0197 5.2 0.0294 Mg 80.0 2.5 2.5 31.78 0.0438 2.5 0.0112 Sr 26.3 3.1 14.3 1.84 0.0017 3.1 0.0405 P 57.4 2.9 2.4 24.43 0.0714 3.0 0.0403 K 13.2 6.1 5.1 2.59 0.0075 6.2 0.0194 Cl 71.6 2.2 2.2 32.55 0.0154 2.2 0.0232 Ca 2675.4 0.4 17.7 151.57 0.5940 0.5 0.0342 Ba 8.9 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0569 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0641 Elt. k-ratio Correc. Na 0.0010 2.3261 Mg 0.0032 1.6980 Sr 0.0011 1.3807 P 0.0112 1.2025 K 0.0007 1.0560 Cl 0.0086 1.1329 Ca 0.2156 1.1044 Ba 0.0000 NaN Fe 0.0000 1.2615 Mn 0.0000 1.2826 iteration : 2 Analysis no. 535 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2289 0.016003 0.2289 0.1777 Mg 0.5383 0.014207 0.5383 0.3953 Sr 0.1482 0.012418 0.1482 0.0302 P 1.3455 0.042725 1.3455 0.7752 K 0.0705 0.008331 0.0705 0.0322 Cl 0.9728 0.022064 0.9728 0.4897 Ca 23.8075 0.121618 23.8075 10.6003 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013849 0.0017 0.0005 Mn 0.0015 0.019259 0.0015 0.0005 C 16.7530 16.7530 24.8911 O 56.1320 56.1320 62.6073 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 536 x= -17136.0 y= 2921.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 38.0 3.6 3.6 10.46 0.0446 3.6 0.0292 Mg 156.4 1.8 2.5 62.13 0.0870 1.8 0.0112 Sr 36.9 2.6 14.3 2.58 0.0033 2.6 0.0406 P 66.4 2.7 2.4 28.26 0.0830 2.8 0.0403 K 15.4 5.7 5.1 3.02 0.0096 5.7 0.0194 Cl 72.7 2.1 2.2 33.05 0.0157 2.1 0.0232 Ca 2755.9 0.4 17.7 156.13 0.6120 0.5 0.0342 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0568 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0639 Elt. k-ratio Correc. Na 0.0022 2.3101 Mg 0.0063 1.6946 Sr 0.0020 1.3827 P 0.0130 1.2047 K 0.0008 1.0557 Cl 0.0087 1.1339 Ca 0.2221 1.1031 Ba 0.0000 NaN Fe 0.0000 1.2588 Mn 0.0002 1.2802 iteration : 2 Analysis no. 536 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5144 0.021704 0.5144 0.4047 Mg 1.0670 0.019818 1.0670 0.7941 Sr 0.2786 0.013974 0.2786 0.0575 P 1.5685 0.046008 1.5685 0.9160 K 0.0897 0.008816 0.0897 0.0415 Cl 0.9892 0.022251 0.9892 0.5047 Ca 24.5009 0.123791 24.5009 11.0570 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013821 0.0017 0.0005 Mn 0.0199 0.020086 0.0199 0.0066 C 15.9461 15.9461 24.0137 O 55.0239 55.0239 62.2038 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 537 x= -17135.0 y= 2925.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 22.3 4.7 3.6 6.15 0.0243 4.7 0.0294 Mg 91.5 2.3 2.5 36.33 0.0503 2.4 0.0113 Sr 22.9 3.3 14.3 1.60 0.0012 3.3 0.0407 P 55.1 3.0 2.4 23.43 0.0683 3.0 0.0405 K 12.4 6.3 5.1 2.43 0.0068 6.4 0.0198 Cl 72.9 2.1 2.2 33.16 0.0157 2.1 0.0234 Ca 2121.5 0.5 17.7 120.19 0.4702 0.6 0.0344 Ba 7.5 5.8 10.8 0.69 0.0000 5.8 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0572 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0643 Elt. k-ratio Correc. Na 0.0012 2.3262 Mg 0.0036 1.7009 Sr 0.0008 1.3878 P 0.0107 1.2094 K 0.0006 1.0763 Cl 0.0088 1.1440 Ca 0.1707 1.1118 Ba 0.0000 NaN Fe 0.0000 1.2676 Mn 0.0000 1.2874 iteration : 2 Analysis no. 537 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2818 0.017218 0.2818 0.2105 Mg 0.6190 0.015204 0.6190 0.4373 Sr 0.1065 0.011942 0.1065 0.0209 P 1.2955 0.042097 1.2955 0.7183 K 0.0648 0.008303 0.0648 0.0285 Cl 1.0013 0.022485 1.0013 0.4850 Ca 18.9729 0.105973 18.9729 8.1292 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0043 0.013995 0.0043 0.0013 Mn 0.0015 0.019333 0.0015 0.0005 C 18.5828 18.5828 26.5689 O 59.0696 59.0696 63.3997 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 538 x= -17134.0 y= 2930.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 38.6 3.6 3.6 10.63 0.0454 3.6 0.0292 Mg 154.3 1.8 2.5 61.27 0.0858 1.8 0.0112 Sr 39.0 2.5 14.3 2.73 0.0036 2.5 0.0407 P 63.2 2.8 2.4 26.88 0.0788 2.8 0.0405 K 12.0 6.4 5.1 2.35 0.0064 6.5 0.0196 Cl 68.4 2.2 2.2 31.11 0.0147 2.2 0.0234 Ca 2404.2 0.5 17.7 136.21 0.5335 0.5 0.0343 Ba 10.4 4.9 10.8 0.96 0.0000 4.9 0.0000 Fe 3.3 8.7 3.3 1.00 0.0000 8.7 NaN Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0641 Elt. k-ratio Correc. Na 0.0023 2.3117 Mg 0.0062 1.6968 Sr 0.0022 1.3869 P 0.0124 1.2094 K 0.0006 1.0676 Cl 0.0082 1.1409 Ca 0.1936 1.1076 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2833 iteration : 2 Analysis no. 538 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5238 0.021879 0.5238 0.4016 Mg 1.0535 0.019706 1.0535 0.7641 Sr 0.3058 0.014308 0.3058 0.0615 P 1.4948 0.045054 1.4948 0.8507 K 0.0607 0.008142 0.0607 0.0274 Cl 0.9350 0.021736 0.9350 0.4649 Ca 21.4429 0.114058 21.4429 9.4305 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0163 0.019966 0.0163 0.0052 C 17.1766 17.1766 25.2080 O 56.9904 56.9904 62.7861 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 539 x= -17133.0 y= 2934.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 24.7 4.5 3.6 6.81 0.0274 4.5 0.0293 Mg 95.8 2.3 2.5 38.04 0.0527 2.3 0.0113 Sr 25.6 3.1 14.3 1.79 0.0016 3.1 0.0407 P 62.7 2.8 2.4 26.66 0.0782 2.8 0.0404 K 11.4 6.6 5.1 2.23 0.0058 6.6 0.0197 Cl 78.4 2.1 2.2 35.63 0.0169 2.1 0.0234 Ca 2289.3 0.5 17.7 129.70 0.5078 0.5 0.0344 Ba 8.3 5.5 10.8 0.77 0.0000 5.5 0.0000 Fe 2.9 9.2 3.3 0.89 0.0000 9.3 0.0000 Mn 2.1 15.6 2.7 0.76 0.0000 15.6 0.0000 Elt. k-ratio Correc. Na 0.0014 2.3219 Mg 0.0038 1.6986 Sr 0.0010 1.3852 P 0.0123 1.2072 K 0.0005 1.0712 Cl 0.0094 1.1414 Ca 0.1843 1.1095 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 539 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3174 0.017971 0.3174 0.2405 Mg 0.6481 0.015534 0.6481 0.4644 Sr 0.1400 0.012352 0.1400 0.0278 P 1.4798 0.044794 1.4798 0.8320 K 0.0552 0.008012 0.0552 0.0246 Cl 1.0759 0.023240 1.0759 0.5285 Ca 20.4471 0.110839 20.4471 8.8843 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.8570 17.8570 25.8910 O 57.9795 57.9795 63.1069 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 540 x= -17133.0 y= 2939.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 27.8 4.2 3.6 7.65 0.0313 4.3 0.0293 Mg 111.9 2.1 2.5 44.42 0.0618 2.1 0.0112 Sr 32.0 2.8 14.3 2.24 0.0026 2.8 0.0407 P 59.2 2.9 2.4 25.20 0.0737 2.9 0.0405 K 13.2 6.1 5.1 2.59 0.0075 6.2 0.0198 Cl 85.4 2.0 2.2 38.81 0.0185 2.0 0.0234 Ca 2203.0 0.5 17.7 124.81 0.4885 0.5 0.0344 Ba 10.5 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.1 8.9 3.3 0.95 0.0000 9.0 0.0000 Mn 2.5 14.3 2.7 0.90 0.0000 14.3 0.0000 Elt. k-ratio Correc. Na 0.0016 2.3183 Mg 0.0045 1.6978 Sr 0.0016 1.3865 P 0.0116 1.2091 K 0.0007 1.0750 Cl 0.0103 1.1432 Ca 0.1773 1.1106 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 540 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3628 0.018893 0.3628 0.2737 Mg 0.7593 0.016773 0.7593 0.5418 Sr 0.2188 0.013319 0.2188 0.0433 P 1.3974 0.043626 1.3974 0.7824 K 0.0718 0.008482 0.0718 0.0318 Cl 1.1768 0.024278 1.1768 0.5756 Ca 19.6896 0.108349 19.6896 8.5193 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 18.0785 18.0785 26.1023 O 58.2449 58.2449 63.1298 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 541 x= -17132.0 y= 2943.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 26.6 4.3 3.6 7.33 0.0299 4.3 0.0293 Mg 96.5 2.3 2.5 38.34 0.0531 2.3 0.0113 Sr 27.9 3.0 14.3 1.95 0.0020 3.0 0.0406 P 62.3 2.8 2.4 26.52 0.0777 2.8 0.0404 K 12.4 6.3 5.1 2.43 0.0068 6.4 0.0197 Cl 79.3 2.0 2.2 36.05 0.0171 2.1 0.0234 Ca 2366.0 0.5 17.7 134.04 0.5249 0.5 0.0343 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 3.0 9.1 3.3 0.92 0.0000 9.1 0.0000 Mn 2.3 14.9 2.7 0.83 0.0000 14.9 0.0000 Elt. k-ratio Correc. Na 0.0015 2.3207 Mg 0.0038 1.6982 Sr 0.0012 1.3843 P 0.0122 1.2065 K 0.0006 1.0685 Cl 0.0095 1.1399 Ca 0.1905 1.1085 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 541 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3459 0.018560 0.3459 0.2635 Mg 0.6532 0.015592 0.6532 0.4708 Sr 0.1684 0.012697 0.1684 0.0337 P 1.4704 0.044644 1.4704 0.8316 K 0.0643 0.008244 0.0643 0.0288 Cl 1.0877 0.023345 1.0877 0.5374 Ca 21.1170 0.113019 21.1170 9.2292 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.5797 17.5797 25.6384 O 57.5135 57.5135 62.9667 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 542 x= -17131.0 y= 2948.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 30.1 4.1 3.6 8.30 0.0344 4.1 0.0293 Mg 118.5 2.1 2.5 47.04 0.0655 2.1 0.0113 Sr 33.0 2.7 14.3 2.31 0.0027 2.8 0.0408 P 55.5 3.0 2.4 23.62 0.0689 3.0 0.0406 K 12.6 6.3 5.1 2.46 0.0069 6.3 0.0199 Cl 77.0 2.1 2.2 35.01 0.0166 2.1 0.0235 Ca 2063.4 0.5 17.7 116.90 0.4573 0.6 0.0345 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 2.7 9.7 3.3 0.81 0.0000 9.7 0.0000 Mn 2.4 14.4 2.7 0.89 0.0000 14.4 0.0000 Elt. k-ratio Correc. Na 0.0017 2.3192 Mg 0.0047 1.6995 Sr 0.0017 1.3892 P 0.0108 1.2118 K 0.0006 1.0796 Cl 0.0093 1.1461 Ca 0.1660 1.1124 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 542 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3984 0.019604 0.3984 0.2973 Mg 0.8061 0.017280 0.8061 0.5691 Sr 0.2325 0.013501 0.2325 0.0455 P 1.3094 0.042355 1.3094 0.7254 K 0.0663 0.008365 0.0663 0.0291 Cl 1.0611 0.023137 1.0611 0.5136 Ca 18.4623 0.104266 18.4623 7.9044 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 18.5898 18.5898 26.5588 O 59.0742 59.0742 63.3567 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 543 x= -17131.0 y= 2952.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 35.8 3.7 3.6 9.87 0.0418 3.8 0.0292 Mg 120.2 2.0 2.5 47.72 0.0665 2.1 0.0113 Sr 33.2 2.7 14.3 2.32 0.0027 2.8 0.0407 P 60.4 2.9 2.4 25.71 0.0753 2.9 0.0405 K 14.5 5.9 5.1 2.84 0.0087 5.9 0.0197 Cl 77.6 2.1 2.2 35.29 0.0168 2.1 0.0234 Ca 2372.1 0.5 17.7 134.39 0.5263 0.5 0.0343 Ba 10.0 5.0 10.8 0.93 0.0000 5.0 0.0000 Fe 3.6 8.4 3.3 1.08 0.0002 8.4 0.0570 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0641 Elt. k-ratio Correc. Na 0.0021 2.3165 Mg 0.0048 1.6986 Sr 0.0017 1.3857 P 0.0118 1.2080 K 0.0008 1.0685 Cl 0.0093 1.1402 Ca 0.1910 1.1081 Ba 0.0000 NaN Fe 0.0001 1.2634 Mn 0.0003 1.2839 iteration : 2 Analysis no. 543 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4836 0.021190 0.4836 0.3694 Mg 0.8175 0.017395 0.8175 0.5908 Sr 0.2338 0.013489 0.2338 0.0469 P 1.4256 0.044022 1.4256 0.8084 K 0.0828 0.008726 0.0828 0.0372 Cl 1.0645 0.023111 1.0645 0.5274 Ca 21.1665 0.113171 21.1665 9.2754 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0094 0.014106 0.0094 0.0029 Mn 0.0366 0.020894 0.0366 0.0117 C 17.4252 17.4252 25.4805 O 57.2544 57.2544 62.8494 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 544 x= -17130.0 y= 2957.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 15.1 5.8 3.6 4.15 0.0148 5.8 0.0294 Mg 83.6 2.4 2.5 33.21 0.0458 2.5 0.0113 Sr 25.4 3.1 14.3 1.78 0.0016 3.1 0.0406 P 47.6 3.2 2.4 20.24 0.0586 3.3 0.0403 K 12.7 6.3 5.1 2.49 0.0071 6.3 0.0194 Cl 64.1 2.3 2.2 29.14 0.0138 2.3 0.0232 Ca 2665.3 0.4 17.7 151.00 0.5920 0.5 0.0342 Ba 8.8 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0570 Mn 3.9 11.3 2.7 1.44 0.0012 11.3 0.0641 Elt. k-ratio Correc. Na 0.0007 2.3309 Mg 0.0033 1.6997 Sr 0.0010 1.3821 P 0.0092 1.2034 K 0.0006 1.0548 Cl 0.0077 1.1322 Ca 0.2148 1.1043 Ba 0.0000 NaN Fe 0.0001 1.2620 Mn 0.0003 1.2831 iteration : 2 Analysis no. 544 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1728 0.014631 0.1728 0.1337 Mg 0.5641 0.014539 0.5641 0.4130 Sr 0.1373 0.012296 0.1373 0.0279 P 1.1059 0.039000 1.1059 0.6353 K 0.0661 0.008209 0.0661 0.0301 Cl 0.8673 0.020897 0.8673 0.4353 Ca 23.7229 0.121356 23.7229 10.5311 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0178 0.014346 0.0178 0.0057 Mn 0.0440 0.021207 0.0440 0.0142 C 16.9507 16.9507 25.1098 O 56.3511 56.3511 62.6640 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 545 x= -17129.0 y= 2961.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 34.0 3.8 3.6 9.36 0.0394 3.9 0.0293 Mg 136.5 1.9 2.5 54.21 0.0757 1.9 0.0113 Sr 32.2 2.8 14.3 2.25 0.0026 2.8 0.0405 P 43.5 3.4 2.4 18.51 0.0534 3.4 0.0402 K 18.6 5.2 5.1 3.65 0.0126 5.2 0.0192 Cl 77.6 2.1 2.2 35.26 0.0168 2.1 0.0231 Ca 3083.4 0.4 17.7 174.69 0.6855 0.5 0.0341 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 4.7 7.3 3.3 1.41 0.0008 7.3 0.0568 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0639 Elt. k-ratio Correc. Na 0.0020 2.3182 Mg 0.0055 1.6971 Sr 0.0016 1.3802 P 0.0084 1.2007 K 0.0011 1.0422 Cl 0.0093 1.1245 Ca 0.2488 1.0988 Ba 0.0000 NaN Fe 0.0004 1.2564 Mn 0.0001 1.2785 iteration : 3 Analysis no. 545 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4562 0.020702 0.4562 0.3656 Mg 0.9307 0.018536 0.9307 0.7055 Sr 0.2206 0.013295 0.2206 0.0464 P 1.0047 0.037275 1.0047 0.5976 K 0.1161 0.009364 0.1161 0.0547 Cl 1.0493 0.022790 1.0493 0.5452 Ca 27.3366 0.132602 27.3366 12.5656 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0457 0.015090 0.0457 0.0151 Mn 0.0089 0.019555 0.0089 0.0030 C 15.2847 15.2847 23.4447 O 53.5465 53.5465 61.6566 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 546 x= -17128.0 y= 2965.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 18.3 5.2 3.6 5.05 0.0191 5.2 0.0295 Mg 69.0 2.7 2.5 27.39 0.0376 2.7 0.0113 Sr 30.0 2.9 14.3 2.10 0.0023 2.9 0.0405 P 28.8 4.2 2.4 12.26 0.0343 4.2 0.0403 K 14.5 5.9 5.1 2.84 0.0087 5.9 0.0192 Cl 58.3 2.4 2.2 26.50 0.0125 2.4 0.0231 Ca 2900.8 0.4 17.7 164.34 0.6447 0.5 0.0341 Ba 8.1 5.5 10.8 0.76 0.0000 5.6 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0569 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0641 Elt. k-ratio Correc. Na 0.0010 2.3351 Mg 0.0027 1.7025 Sr 0.0014 1.3807 P 0.0054 1.2018 K 0.0008 1.0443 Cl 0.0069 1.1257 Ca 0.2340 1.1010 Ba 0.0000 NaN Fe 0.0000 1.2602 Mn 0.0004 1.2817 iteration : 2 Analysis no. 546 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2223 0.015891 0.2223 0.1743 Mg 0.4629 0.013248 0.4629 0.3432 Sr 0.1933 0.012974 0.1933 0.0397 P 0.6463 0.030649 0.6463 0.3760 K 0.0810 0.008530 0.0810 0.0373 Cl 0.7815 0.019843 0.7815 0.3972 Ca 25.7587 0.127725 25.7587 11.5811 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0059 0.013969 0.0059 0.0019 Mn 0.0458 0.021265 0.0458 0.0150 C 16.4870 16.4870 24.7353 O 55.3152 55.3152 62.2988 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 547 x= -17128.0 y= 2970.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 34.0 3.8 3.6 9.36 0.0394 3.9 0.0293 Mg 120.0 2.0 2.5 47.66 0.0664 2.1 0.0113 Sr 42.3 2.4 14.3 2.96 0.0041 2.4 0.0404 P 32.8 3.9 2.4 13.96 0.0395 3.9 0.0401 K 21.6 4.8 5.1 4.24 0.0153 4.8 0.0188 Cl 48.8 2.6 2.2 22.16 0.0104 2.6 0.0228 Ca 3670.0 0.4 17.7 207.92 0.8166 0.5 0.0338 Ba 10.5 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0565 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0637 Elt. k-ratio Correc. Na 0.0020 2.3230 Mg 0.0048 1.6982 Sr 0.0025 1.3750 P 0.0062 1.1960 K 0.0014 1.0199 Cl 0.0058 1.1130 Ca 0.2964 1.0909 Ba 0.0000 NaN Fe 0.0001 1.2509 Mn 0.0004 1.2742 iteration : 3 Analysis no. 547 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4571 0.020743 0.4571 0.3807 Mg 0.8164 0.017383 0.8164 0.6432 Sr 0.3441 0.014630 0.3441 0.0752 P 0.7405 0.032429 0.7405 0.4577 K 0.1388 0.009729 0.1388 0.0680 Cl 0.6413 0.017995 0.6413 0.3463 Ca 32.3309 0.147646 32.3309 15.4450 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0185 0.014246 0.0185 0.0064 Mn 0.0473 0.021221 0.0473 0.0165 C 13.6291 13.6291 21.7264 O 50.8359 50.8359 60.8346 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 548 x= -17127.0 y= 2974.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.4 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.4 15.0 Na 24.3 4.5 3.6 6.70 0.0269 4.5 0.0295 Mg 74.7 2.6 2.5 29.65 0.0408 2.6 0.0113 Sr 21.9 3.4 14.3 1.54 0.0011 3.4 0.0406 P 24.9 4.5 2.4 10.58 0.0292 4.5 0.0403 K 18.5 5.2 5.1 3.62 0.0124 5.2 0.0193 Cl 60.2 2.4 2.2 27.36 0.0129 2.4 0.0231 Ca 2803.2 0.4 17.7 158.81 0.6228 0.5 0.0342 Ba 9.1 5.2 10.8 0.85 0.0000 5.2 0.0000 Fe 3.7 8.2 3.3 1.13 0.0002 8.2 0.0570 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0641 Elt. k-ratio Correc. Na 0.0013 2.3352 Mg 0.0030 1.7047 Sr 0.0007 1.3830 P 0.0046 1.2027 K 0.0011 1.0473 Cl 0.0072 1.1269 Ca 0.2260 1.1024 Ba 0.0000 NaN Fe 0.0001 1.2615 Mn 0.0002 1.2828 iteration : 2 Analysis no. 548 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3133 0.017950 0.3133 0.2437 Mg 0.5033 0.013792 0.5033 0.3703 Sr 0.0945 0.011751 0.0945 0.0193 P 0.5502 0.028637 0.5502 0.3177 K 0.1153 0.009380 0.1153 0.0527 Cl 0.8089 0.020176 0.8089 0.4080 Ca 24.9183 0.125113 24.9183 11.1186 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0144 0.014240 0.0144 0.0046 Mn 0.0292 0.020552 0.0292 0.0095 C 16.8340 16.8340 25.0649 O 55.8186 55.8186 62.3906 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 549 x= -17126.0 y= 2979.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 26.6 4.3 3.6 7.32 0.0298 4.4 0.0294 Mg 84.8 2.4 2.5 33.67 0.0465 2.4 0.0113 Sr 26.0 3.1 14.3 1.82 0.0017 3.1 0.0406 P 26.1 4.4 2.4 11.09 0.0307 4.4 0.0403 K 16.2 5.5 5.1 3.18 0.0103 5.6 0.0193 Cl 74.6 2.1 2.2 33.93 0.0161 2.1 0.0231 Ca 2804.2 0.4 17.7 158.87 0.6232 0.5 0.0342 Ba 9.3 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0641 Elt. k-ratio Correc. Na 0.0015 2.3308 Mg 0.0034 1.7028 Sr 0.0010 1.3825 P 0.0048 1.2028 K 0.0009 1.0488 Cl 0.0090 1.1272 Ca 0.2262 1.1024 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0004 1.2822 iteration : 2 Analysis no. 549 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3468 0.018635 0.3468 0.2705 Mg 0.5733 0.014669 0.5733 0.4230 Sr 0.1442 0.012389 0.1442 0.0295 P 0.5797 0.029278 0.5797 0.3356 K 0.0960 0.008934 0.0960 0.0441 Cl 1.0110 0.022420 1.0110 0.5113 Ca 24.9344 0.125177 24.9344 11.1559 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0476 0.021360 0.0476 0.0155 C 16.7115 16.7115 24.9499 O 55.5554 55.5554 62.2645 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 550 x= -17126.0 y= 2983.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 35.1 3.8 3.6 9.68 0.0409 3.8 0.0294 Mg 107.4 2.2 2.5 42.67 0.0593 2.2 0.0113 Sr 29.8 2.9 14.3 2.09 0.0022 2.9 0.0407 P 25.6 4.4 2.4 10.89 0.0302 4.4 0.0404 K 17.1 5.4 5.1 3.35 0.0112 5.4 0.0194 Cl 73.9 2.1 2.2 33.60 0.0159 2.1 0.0232 Ca 2615.6 0.4 17.7 148.18 0.5810 0.5 0.0342 Ba 9.5 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.1 9.0 3.3 0.93 0.0000 9.0 0.0000 Mn 3.1 12.7 2.7 1.14 0.0004 12.7 0.0642 Elt. k-ratio Correc. Na 0.0020 2.3260 Mg 0.0043 1.7033 Sr 0.0014 1.3858 P 0.0047 1.2063 K 0.0010 1.0561 Cl 0.0089 1.1316 Ca 0.2108 1.1048 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2834 iteration : 2 Analysis no. 550 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4752 0.021092 0.4752 0.3663 Mg 0.7315 0.016501 0.7315 0.5334 Sr 0.1921 0.013002 0.1921 0.0389 P 0.5703 0.029124 0.5703 0.3264 K 0.1045 0.009184 0.1045 0.0474 Cl 1.0045 0.022396 1.0045 0.5022 Ca 23.2944 0.120007 23.2944 10.3011 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0144 0.019891 0.0144 0.0047 C 17.2196 17.2196 25.4100 O 56.3934 56.3934 62.4697 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 551 x= -17125.0 y= 2988.0 z= -280. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 36.6 3.7 3.6 10.09 0.0429 3.7 0.0294 Mg 94.8 2.3 2.5 37.66 0.0522 2.3 0.0113 Sr 25.9 3.1 14.3 1.82 0.0017 3.1 0.0408 P 26.5 4.3 2.4 11.28 0.0313 4.4 0.0405 K 20.2 5.0 5.1 3.95 0.0140 5.0 0.0195 Cl 84.5 2.0 2.2 38.40 0.0183 2.0 0.0233 Ca 2514.9 0.4 17.7 142.48 0.5588 0.5 0.0343 Ba 9.5 5.1 10.8 0.88 0.0000 5.1 0.0000 Fe 2.6 9.9 3.3 0.77 0.0000 9.9 0.0000 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0643 Elt. k-ratio Correc. Na 0.0021 2.3262 Mg 0.0038 1.7041 Sr 0.0010 1.3860 P 0.0049 1.2063 K 0.0012 1.0603 Cl 0.0102 1.1331 Ca 0.2028 1.1063 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2842 iteration : 2 Analysis no. 551 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4982 0.021517 0.4982 0.3817 Mg 0.6442 0.015524 0.6442 0.4669 Sr 0.1443 0.012423 0.1443 0.0290 P 0.5928 0.029614 0.5928 0.3371 K 0.1317 0.009842 0.1317 0.0593 Cl 1.1549 0.023962 1.1549 0.5738 Ca 22.4354 0.117304 22.4354 9.8600 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0311 0.020673 0.0311 0.0100 C 17.5335 17.5335 25.7133 O 56.8339 56.8339 62.5689 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 552 x= -17124.0 y= 2992.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 45.9 3.3 3.6 12.64 0.0550 3.3 0.0293 Mg 128.5 2.0 2.5 51.01 0.0713 2.0 0.0113 Sr 33.9 2.7 14.3 2.38 0.0028 2.7 0.0408 P 28.9 4.2 2.4 12.28 0.0344 4.2 0.0405 K 18.5 5.2 5.1 3.62 0.0124 5.2 0.0195 Cl 83.5 2.0 2.2 37.95 0.0181 2.0 0.0232 Ca 2674.2 0.4 17.7 151.50 0.5947 0.5 0.0343 Ba 10.3 4.9 10.8 0.95 0.0000 4.9 0.0000 Fe 2.6 9.9 3.3 0.77 0.0000 9.9 0.0000 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0642 Elt. k-ratio Correc. Na 0.0027 2.3186 Mg 0.0052 1.7021 Sr 0.0018 1.3857 P 0.0054 1.2063 K 0.0011 1.0555 Cl 0.0101 1.1311 Ca 0.2158 1.1040 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2821 iteration : 3 Analysis no. 552 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6361 0.023830 0.6361 0.4944 Mg 0.8783 0.018050 0.8783 0.6457 Sr 0.2434 0.013614 0.2434 0.0496 P 0.6507 0.030825 0.6507 0.3754 K 0.1164 0.009465 0.1164 0.0532 Cl 1.1394 0.023791 1.1394 0.5743 Ca 23.8264 0.121734 23.8264 10.6223 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0237 0.020315 0.0237 0.0077 C 16.7884 16.7884 24.9756 O 55.6973 55.6973 62.2018 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 553 x= -17123.0 y= 2997.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 17.6 5.3 3.6 4.84 0.0181 5.3 0.0295 Mg 69.5 2.7 2.5 27.61 0.0379 2.7 0.0113 Sr 27.7 3.0 14.3 1.94 0.0019 3.0 0.0406 P 22.3 4.7 2.4 9.49 0.0259 4.7 0.0404 K 15.9 5.6 5.1 3.12 0.0101 5.6 0.0194 Cl 85.9 2.0 2.2 39.03 0.0186 2.0 0.0232 Ca 2700.7 0.4 17.7 153.00 0.6004 0.5 0.0343 Ba 10.7 4.8 10.8 1.00 0.0000 4.8 0.0000 Fe 3.1 9.0 3.3 0.92 0.0000 9.1 0.0000 Mn 2.9 13.1 2.7 1.07 0.0002 13.1 0.0642 Elt. k-ratio Correc. Na 0.0009 2.3331 Mg 0.0027 1.7017 Sr 0.0012 1.3821 P 0.0041 1.2031 K 0.0009 1.0527 Cl 0.0104 1.1285 Ca 0.2179 1.1040 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2833 iteration : 2 Analysis no. 553 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2110 0.015616 0.2110 0.1632 Mg 0.4670 0.013306 0.4670 0.3417 Sr 0.1652 0.012654 0.1652 0.0335 P 0.4884 0.027278 0.4884 0.2805 K 0.0939 0.008910 0.0939 0.0427 Cl 1.1695 0.024057 1.1695 0.5867 Ca 24.0566 0.122461 24.0566 10.6759 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0071 0.019558 0.0071 0.0023 C 17.1766 17.1766 25.4364 O 56.1647 56.1647 62.4370 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 554 x= -17123.0 y= 3001.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 27.5 4.3 3.6 7.58 0.0311 4.3 0.0294 Mg 124.2 2.0 2.5 49.31 0.0688 2.0 0.0113 Sr 32.8 2.8 14.3 2.30 0.0027 2.8 0.0407 P 23.5 4.6 2.4 10.00 0.0275 4.6 0.0404 K 18.5 5.2 5.1 3.62 0.0124 5.2 0.0194 Cl 84.2 2.0 2.2 38.28 0.0183 2.0 0.0232 Ca 2731.5 0.4 17.7 154.75 0.6073 0.5 0.0342 Ba 10.4 4.9 10.8 0.97 0.0000 4.9 0.0000 Fe 3.2 8.9 3.3 0.96 0.0000 8.9 0.0000 Mn 4.4 10.7 2.7 1.61 0.0016 10.7 0.0642 Elt. k-ratio Correc. Na 0.0016 2.3250 Mg 0.0050 1.7001 Sr 0.0017 1.3843 P 0.0043 1.2050 K 0.0011 1.0527 Cl 0.0102 1.1290 Ca 0.2204 1.1033 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0005 1.2820 iteration : 2 Analysis no. 554 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3605 0.018892 0.3605 0.2807 Mg 0.8470 0.017717 0.8470 0.6237 Sr 0.2292 0.013435 0.2292 0.0468 P 0.5186 0.027985 0.5186 0.2997 K 0.1160 0.009436 0.1160 0.0531 Cl 1.1472 0.023841 1.1472 0.5792 Ca 24.3156 0.123260 24.3156 10.8590 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0606 0.021920 0.0606 0.0197 C 16.7898 16.7898 25.0207 O 55.6156 55.6156 62.2173 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 555 x= -17122.0 y= 3006.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 19.4 5.1 3.6 5.35 0.0205 5.1 0.0296 Mg 51.6 3.1 2.5 20.48 0.0277 3.1 0.0113 Sr 14.8 4.1 14.3 1.03 0.0001 4.1 0.0408 P 25.3 4.4 2.4 10.77 0.0298 4.5 0.0406 K 18.4 5.2 5.1 3.60 0.0123 5.2 0.0197 Cl 61.6 2.3 2.2 28.00 0.0132 2.3 0.0234 Ca 2159.8 0.5 17.7 122.36 0.4794 0.6 0.0345 Ba 6.1 6.4 10.8 0.57 0.0000 6.4 0.0000 Fe 2.8 9.5 3.3 0.83 0.0000 9.5 0.0000 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0645 Elt. k-ratio Correc. Na 0.0010 2.3406 Mg 0.0020 1.7081 Sr 0.0000 1.3890 P 0.0047 1.2089 K 0.0011 1.0707 Cl 0.0074 1.1394 Ca 0.1740 1.1112 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2889 iteration : 2 Analysis no. 555 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2398 0.016339 0.2398 0.1781 Mg 0.3431 0.011552 0.3431 0.2410 Sr 0.0062 0.010579 0.0062 0.0012 P 0.5646 0.029049 0.5646 0.3112 K 0.1171 0.009577 0.1171 0.0511 Cl 0.8384 0.020646 0.8384 0.4037 Ca 19.3312 0.107211 19.3312 8.2340 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0108 0.019817 0.0108 0.0034 C 19.0913 19.0913 27.1354 O 59.4577 59.4577 63.4410 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 556 x= -17121.0 y= 3010.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 31.3 4.0 3.6 8.63 0.0360 4.0 0.0294 Mg 87.5 2.4 2.5 34.76 0.0481 2.4 0.0113 Sr 28.6 3.0 14.3 2.00 0.0021 3.0 0.0407 P 24.5 4.5 2.4 10.43 0.0287 4.5 0.0404 K 23.8 4.6 5.1 4.66 0.0174 4.6 0.0194 Cl 77.7 2.1 2.2 35.32 0.0168 2.1 0.0232 Ca 2728.0 0.4 17.7 154.55 0.6065 0.5 0.0342 Ba 8.9 5.3 10.8 0.83 0.0000 5.3 0.0000 Fe 3.7 8.2 3.3 1.12 0.0002 8.2 0.0570 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0642 Elt. k-ratio Correc. Na 0.0018 2.3285 Mg 0.0035 1.7032 Sr 0.0013 1.3834 P 0.0045 1.2039 K 0.0015 1.0519 Cl 0.0094 1.1286 Ca 0.2201 1.1035 Ba 0.0000 NaN Fe 0.0001 1.2614 Mn 0.0001 1.2826 iteration : 2 Analysis no. 556 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4185 0.020055 0.4185 0.3251 Mg 0.5930 0.014913 0.5930 0.4357 Sr 0.1768 0.012805 0.1768 0.0360 P 0.5427 0.028502 0.5427 0.3129 K 0.1620 0.010441 0.1620 0.0740 Cl 1.0557 0.022909 1.0557 0.5318 Ca 24.2894 0.123185 24.2894 10.8224 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0136 0.014225 0.0136 0.0043 Mn 0.0108 0.019720 0.0108 0.0035 C 16.9123 16.9123 25.1455 O 55.8253 55.8253 62.3088 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 557 x= -17121.0 y= 3015.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 16.9 5.4 3.6 4.66 0.0173 5.5 0.0295 Mg 51.3 3.1 2.5 20.38 0.0276 3.1 0.0113 Sr 21.1 3.4 14.3 1.48 0.0010 3.5 0.0407 P 25.6 4.4 2.4 10.87 0.0301 4.4 0.0405 K 16.6 5.5 5.1 3.25 0.0107 5.5 0.0196 Cl 82.0 2.0 2.2 37.25 0.0178 2.0 0.0233 Ca 2404.7 0.5 17.7 136.23 0.5342 0.5 0.0344 Ba 8.6 5.4 10.8 0.80 0.0000 5.4 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0573 Mn 2.4 14.4 2.7 0.89 0.0000 14.4 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3366 Mg 0.0020 1.7043 Sr 0.0006 1.3848 P 0.0047 1.2055 K 0.0009 1.0631 Cl 0.0099 1.1343 Ca 0.1939 1.1080 Ba 0.0000 NaN Fe 0.0000 1.2658 Mn 0.0000 NaN iteration : 2 Analysis no. 557 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2014 0.015396 0.2014 0.1525 Mg 0.3406 0.011499 0.3406 0.2438 Sr 0.0844 0.011641 0.0844 0.0168 P 0.5692 0.029101 0.5692 0.3198 K 0.1005 0.009136 0.1005 0.0447 Cl 1.1207 0.023634 1.1207 0.5501 Ca 21.4808 0.114251 21.4808 9.3266 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0026 0.013940 0.0026 0.0008 Mn 0.0000 0.000000 0.0000 0.0000 C 18.2062 18.2062 26.3780 O 57.8936 57.8936 62.9669 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 558 x= -17120.0 y= 3019.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 31.3 4.0 3.6 8.62 0.0359 4.0 0.0294 Mg 92.4 2.3 2.5 36.69 0.0508 2.3 0.0113 Sr 27.7 3.0 14.3 1.94 0.0019 3.0 0.0406 P 27.6 4.3 2.4 11.75 0.0328 4.3 0.0403 K 23.1 4.6 5.1 4.53 0.0168 4.7 0.0193 Cl 80.1 2.0 2.2 36.40 0.0173 2.0 0.0231 Ca 2895.3 0.4 17.7 164.03 0.6440 0.5 0.0342 Ba 9.1 5.3 10.8 0.84 0.0000 5.3 0.0000 Fe 3.8 8.1 3.3 1.15 0.0003 8.1 0.0570 Mn 3.3 12.4 2.7 1.20 0.0005 12.4 0.0641 Elt. k-ratio Correc. Na 0.0018 2.3270 Mg 0.0037 1.7018 Sr 0.0012 1.3815 P 0.0051 1.2018 K 0.0015 1.0465 Cl 0.0096 1.1256 Ca 0.2337 1.1013 Ba 0.0000 NaN Fe 0.0001 1.2594 Mn 0.0002 1.2810 iteration : 2 Analysis no. 558 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4176 0.020030 0.4176 0.3285 Mg 0.6264 0.015307 0.6264 0.4662 Sr 0.1651 0.012649 0.1651 0.0341 P 0.6176 0.030073 0.6176 0.3607 K 0.1555 0.010270 0.1555 0.0719 Cl 1.0861 0.023190 1.0861 0.5541 Ca 25.7412 0.127727 25.7412 11.6169 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0170 0.014306 0.0170 0.0055 Mn 0.0200 0.020125 0.0200 0.0066 C 16.2913 16.2913 24.5338 O 54.8622 54.8622 62.0217 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 559 x= -17119.0 y= 3023.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 20.8 4.9 3.6 5.72 0.0223 4.9 0.0296 Mg 58.2 2.9 2.5 23.10 0.0315 2.9 0.0113 Sr 17.5 3.8 14.3 1.23 0.0005 3.8 0.0408 P 25.0 4.5 2.4 10.64 0.0294 4.5 0.0405 K 20.8 4.9 5.1 4.08 0.0146 4.9 0.0197 Cl 67.2 2.2 2.2 30.55 0.0145 2.2 0.0234 Ca 2269.8 0.5 17.7 128.59 0.5041 0.5 0.0345 Ba 7.6 5.7 10.8 0.71 0.0000 5.7 0.0000 Fe 3.2 8.8 3.3 0.98 0.0000 8.8 0.0000 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0645 Elt. k-ratio Correc. Na 0.0011 2.3383 Mg 0.0023 1.7068 Sr 0.0003 1.3877 P 0.0046 1.2078 K 0.0013 1.0670 Cl 0.0081 1.1371 Ca 0.1830 1.1097 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2876 iteration : 2 Analysis no. 559 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2601 0.016803 0.2601 0.1949 Mg 0.3891 0.012239 0.3891 0.2758 Sr 0.0403 0.011061 0.0403 0.0079 P 0.5568 0.028869 0.5568 0.3097 K 0.1383 0.010035 0.1383 0.0609 Cl 0.9159 0.021504 0.9159 0.4450 Ca 20.3012 0.110417 20.3012 8.7255 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0293 0.020651 0.0293 0.0092 C 18.6565 18.6565 26.7577 O 58.7124 58.7124 63.2134 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 560 x= -17118.0 y= 3028.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 42.6 3.4 3.6 11.73 0.0507 3.4 0.0294 Mg 111.9 2.1 2.5 44.44 0.0619 2.1 0.0113 Sr 30.9 2.8 14.3 2.17 0.0024 2.9 0.0407 P 24.5 4.5 2.4 10.40 0.0287 4.5 0.0404 K 22.2 4.7 5.1 4.34 0.0159 4.8 0.0193 Cl 87.0 2.0 2.2 39.56 0.0189 2.0 0.0231 Ca 2849.6 0.4 17.7 161.44 0.6340 0.5 0.0342 Ba 9.8 5.0 10.8 0.91 0.0000 5.0 0.0000 Fe 3.1 8.9 3.3 0.95 0.0000 9.0 0.0000 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0641 Elt. k-ratio Correc. Na 0.0025 2.3219 Mg 0.0045 1.7024 Sr 0.0015 1.3832 P 0.0045 1.2034 K 0.0014 1.0488 Cl 0.0105 1.1266 Ca 0.2301 1.1018 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0004 1.2809 iteration : 3 Analysis no. 560 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5873 0.023043 0.5873 0.4615 Mg 0.7629 0.016848 0.7629 0.5672 Sr 0.2059 0.013158 0.2059 0.0425 P 0.5414 0.028475 0.5414 0.3158 K 0.1477 0.010120 0.1477 0.0682 Cl 1.1843 0.024187 1.1843 0.6036 Ca 25.3501 0.126518 25.3500 11.4278 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0458 0.021279 0.0458 0.0151 C 16.3296 16.3296 24.5644 O 54.8450 54.8450 61.9339 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 561 x= -17118.0 y= 3032.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 42.0 3.4 3.6 11.58 0.0499 3.5 0.0294 Mg 99.9 2.2 2.5 39.67 0.0551 2.3 0.0113 Sr 30.4 2.9 14.3 2.13 0.0023 2.9 0.0408 P 24.2 4.5 2.4 10.28 0.0283 4.6 0.0405 K 19.1 5.1 5.1 3.75 0.0130 5.1 0.0196 Cl 88.3 1.9 2.2 40.13 0.0192 1.9 0.0233 Ca 2488.8 0.4 17.7 141.00 0.5532 0.5 0.0344 Ba 9.4 5.2 10.8 0.87 0.0000 5.2 0.0000 Fe 3.0 9.1 3.3 0.91 0.0000 9.1 0.0000 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0643 Elt. k-ratio Correc. Na 0.0025 2.3237 Mg 0.0040 1.7044 Sr 0.0014 1.3866 P 0.0044 1.2073 K 0.0012 1.0616 Cl 0.0107 1.1337 Ca 0.2008 1.1065 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2841 iteration : 2 Analysis no. 561 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5794 0.022921 0.5794 0.4436 Mg 0.6799 0.015939 0.6799 0.4924 Sr 0.1999 0.013112 0.1999 0.0402 P 0.5358 0.028402 0.5358 0.3044 K 0.1227 0.009650 0.1227 0.0552 Cl 1.2095 0.024511 1.2095 0.6005 Ca 22.2149 0.116612 22.2149 9.7557 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0311 0.020679 0.0311 0.0100 C 17.5808 17.5808 25.7632 O 56.8460 56.8460 62.5349 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 562 x= -17117.0 y= 3037.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 15.0 5.8 3.6 4.14 0.0148 5.8 0.0296 Mg 55.1 3.0 2.5 21.87 0.0297 3.0 0.0113 Sr 27.3 3.0 14.3 1.91 0.0019 3.0 0.0406 P 23.7 4.6 2.4 10.06 0.0277 4.6 0.0403 K 21.9 4.8 5.1 4.29 0.0156 4.8 0.0193 Cl 69.1 2.2 2.2 31.40 0.0149 2.2 0.0231 Ca 2904.9 0.4 17.7 164.58 0.6464 0.5 0.0342 Ba 8.0 5.6 10.8 0.74 0.0000 5.6 0.0000 Fe 2.9 9.3 3.3 0.88 0.0000 9.3 0.0000 Mn 3.0 13.0 2.7 1.09 0.0002 13.0 0.0642 Elt. k-ratio Correc. Na 0.0007 2.3366 Mg 0.0022 1.7023 Sr 0.0012 1.3797 P 0.0043 1.2006 K 0.0014 1.0441 Cl 0.0083 1.1244 Ca 0.2346 1.1012 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2819 iteration : 2 Analysis no. 562 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1727 0.014667 0.1727 0.1353 Mg 0.3665 0.011888 0.3665 0.2716 Sr 0.1600 0.012576 0.1600 0.0329 P 0.5206 0.027977 0.5206 0.3028 K 0.1449 0.010028 0.1449 0.0667 Cl 0.9318 0.021552 0.9318 0.4734 Ca 25.8335 0.128030 25.8335 11.6109 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0089 0.019631 0.0089 0.0029 C 16.5721 16.5721 24.8546 O 55.2891 55.2891 62.2488 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 563 x= -17116.0 y= 3041.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 31.6 4.0 3.6 8.71 0.0364 4.0 0.0294 Mg 90.3 2.4 2.5 35.87 0.0497 2.4 0.0113 Sr 29.2 2.9 14.3 2.04 0.0022 2.9 0.0406 P 27.3 4.3 2.4 11.60 0.0323 4.3 0.0403 K 26.5 4.3 5.1 5.20 0.0199 4.4 0.0192 Cl 83.8 2.0 2.2 38.09 0.0182 2.0 0.0231 Ca 3022.5 0.4 17.7 171.24 0.6727 0.5 0.0341 Ba 9.6 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0569 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0641 Elt. k-ratio Correc. Na 0.0018 2.3264 Mg 0.0036 1.7011 Sr 0.0013 1.3798 P 0.0051 1.2002 K 0.0018 1.0424 Cl 0.0101 1.1230 Ca 0.2441 1.0996 Ba 0.0000 NaN Fe 0.0001 1.2579 Mn 0.0003 1.2797 iteration : 3 Analysis no. 563 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4229 0.020131 0.4229 0.3360 Mg 0.6120 0.015136 0.6120 0.4600 Sr 0.1838 0.012867 0.1838 0.0383 P 0.6084 0.029864 0.6084 0.3588 K 0.1842 0.010835 0.1842 0.0861 Cl 1.1354 0.023662 1.1354 0.5851 Ca 26.8460 0.131155 26.8460 12.2368 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0187 0.014343 0.0187 0.0061 Mn 0.0384 0.020938 0.0384 0.0128 C 15.8468 15.8468 24.1034 O 54.1035 54.1035 61.7765 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 564 x= -17116.0 y= 3046.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 17.1 5.4 3.6 4.71 0.0175 5.4 0.0296 Mg 45.3 3.3 2.5 17.97 0.0242 3.3 0.0113 Sr 20.0 3.5 14.3 1.40 0.0008 3.5 0.0408 P 26.9 4.3 2.4 11.45 0.0319 4.3 0.0405 K 24.3 4.5 5.1 4.76 0.0178 4.6 0.0196 Cl 68.9 2.2 2.2 31.33 0.0149 2.2 0.0233 Ca 2389.1 0.5 17.7 135.35 0.5309 0.5 0.0344 Ba 7.4 5.8 10.8 0.68 0.0000 5.8 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0573 Mn 2.8 13.5 2.7 1.02 0.0000 13.5 0.0644 Elt. k-ratio Correc. Na 0.0009 2.3387 Mg 0.0018 1.7055 Sr 0.0005 1.3851 P 0.0050 1.2058 K 0.0016 1.0628 Cl 0.0083 1.1347 Ca 0.1927 1.1082 Ba 0.0000 NaN Fe 0.0000 1.2661 Mn 0.0000 1.2865 iteration : 2 Analysis no. 564 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2047 0.015489 0.2047 0.1547 Mg 0.2986 0.010839 0.2986 0.2134 Sr 0.0709 0.011464 0.0709 0.0141 P 0.6026 0.029821 0.6026 0.3379 K 0.1681 0.010644 0.1681 0.0747 Cl 0.9384 0.021727 0.9384 0.4598 Ca 21.3502 0.113840 21.3502 9.2533 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0060 0.014052 0.0060 0.0019 Mn 0.0015 0.019349 0.0015 0.0005 C 18.2719 18.2719 26.4257 O 58.0871 58.0871 63.0641 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 565 x= -17115.0 y= 3050.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 42.0 3.4 3.6 11.58 0.0499 3.5 0.0293 Mg 116.0 2.1 2.5 46.05 0.0642 2.1 0.0113 Sr 36.2 2.6 14.3 2.53 0.0032 2.6 0.0406 P 27.5 4.3 2.4 11.70 0.0327 4.3 0.0403 K 25.9 4.4 5.1 5.07 0.0193 4.4 0.0191 Cl 80.9 2.0 2.2 36.78 0.0175 2.0 0.0230 Ca 3218.6 0.4 17.7 182.35 0.7166 0.5 0.0341 Ba 11.0 4.8 10.8 1.02 0.0002 4.8 0.0760 Fe 3.1 9.0 3.3 0.94 0.0000 9.0 0.0000 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0640 Elt. k-ratio Correc. Na 0.0025 2.3199 Mg 0.0046 1.7000 Sr 0.0020 1.3791 P 0.0051 1.1997 K 0.0017 1.0364 Cl 0.0098 1.1201 Ca 0.2601 1.0969 Ba 0.0000 1.5370 Fe 0.0000 NaN Mn 0.0003 1.2776 iteration : 3 Analysis no. 565 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5784 0.022882 0.5784 0.4672 Mg 0.7901 0.017126 0.7901 0.6036 Sr 0.2697 0.013862 0.2697 0.0572 P 0.6142 0.029976 0.6142 0.3682 K 0.1776 0.010660 0.1776 0.0843 Cl 1.0926 0.023200 1.0926 0.5723 Ca 28.5258 0.136284 28.5258 13.2165 Ba 0.0066 0.019462 0.0066 0.0009 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0365 0.020820 0.0365 0.0123 C 15.0526 15.0526 23.2722 O 52.8559 52.8559 61.3452 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 566 x= -17114.0 y= 3055.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 20.6 4.9 3.6 5.68 0.0221 4.9 0.0295 Mg 60.8 2.9 2.5 24.15 0.0330 2.9 0.0113 Sr 23.5 3.3 14.3 1.64 0.0013 3.3 0.0407 P 26.3 4.4 2.4 11.19 0.0311 4.4 0.0404 K 22.9 4.7 5.1 4.48 0.0165 4.7 0.0196 Cl 92.3 1.9 2.2 41.94 0.0200 1.9 0.0233 Ca 2479.0 0.4 17.7 140.45 0.5509 0.5 0.0344 Ba 7.4 5.8 10.8 0.69 0.0000 5.8 0.0000 Fe 3.0 9.2 3.3 0.89 0.0000 9.2 0.0000 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0643 Elt. k-ratio Correc. Na 0.0011 2.3325 Mg 0.0024 1.7028 Sr 0.0008 1.3837 P 0.0049 1.2046 K 0.0015 1.0615 Cl 0.0112 1.1328 Ca 0.1999 1.1071 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0001 1.2850 iteration : 2 Analysis no. 566 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2572 0.016707 0.2572 0.1962 Mg 0.4066 0.012475 0.4066 0.2934 Sr 0.1138 0.012019 0.1138 0.0228 P 0.5872 0.029474 0.5872 0.3325 K 0.1556 0.010370 0.1556 0.0698 Cl 1.2640 0.025024 1.2640 0.6253 Ca 22.1325 0.116354 22.1325 9.6843 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0182 0.020102 0.0182 0.0058 C 17.8324 17.8324 26.0374 O 57.2327 57.2327 62.7326 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 567 x= -17113.0 y= 3059.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 46.2 3.3 3.6 12.73 0.0553 3.3 0.0293 Mg 136.7 1.9 2.5 54.29 0.0760 1.9 0.0113 Sr 34.4 2.7 14.3 2.41 0.0029 2.7 0.0407 P 32.4 3.9 2.4 13.79 0.0390 3.9 0.0404 K 29.2 4.1 5.1 5.72 0.0224 4.2 0.0194 Cl 94.4 1.9 2.2 42.91 0.0205 1.9 0.0232 Ca 2845.5 0.4 17.7 161.21 0.6331 0.5 0.0342 Ba 10.7 4.8 10.8 0.99 0.0000 4.8 0.0000 Fe 3.7 8.2 3.3 1.13 0.0002 8.2 0.0570 Mn 3.4 12.1 2.7 1.26 0.0007 12.1 0.0641 Elt. k-ratio Correc. Na 0.0028 2.3150 Mg 0.0055 1.6995 Sr 0.0018 1.3832 P 0.0061 1.2038 K 0.0020 1.0508 Cl 0.0114 1.1278 Ca 0.2298 1.1019 Ba 0.0000 NaN Fe 0.0001 1.2585 Mn 0.0002 1.2801 iteration : 3 Analysis no. 567 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.6397 0.023867 0.6397 0.5048 Mg 0.9345 0.018598 0.9345 0.6975 Sr 0.2483 0.013651 0.2483 0.0514 P 0.7364 0.032490 0.7364 0.4313 K 0.2087 0.011374 0.2087 0.0968 Cl 1.2887 0.025204 1.2887 0.6594 Ca 25.3172 0.126421 25.3172 11.4595 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0144 0.014224 0.0144 0.0047 Mn 0.0255 0.020368 0.0255 0.0084 C 16.0696 16.0696 24.2717 O 54.5170 54.5170 61.8144 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 568 x= -17113.0 y= 3064.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 18.4 5.2 3.6 5.07 0.0192 5.2 0.0295 Mg 82.6 2.5 2.5 32.79 0.0453 2.5 0.0113 Sr 26.1 3.1 14.3 1.83 0.0017 3.1 0.0407 P 26.0 4.4 2.4 11.06 0.0307 4.4 0.0404 K 21.7 4.8 5.1 4.25 0.0154 4.8 0.0194 Cl 66.9 2.2 2.2 30.42 0.0144 2.2 0.0232 Ca 2727.8 0.4 17.7 154.54 0.6067 0.5 0.0343 Ba 8.7 5.3 10.8 0.81 0.0000 5.4 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 2.7 13.6 2.7 1.00 0.0000 13.6 0.0000 Elt. k-ratio Correc. Na 0.0010 2.3333 Mg 0.0033 1.7020 Sr 0.0011 1.3830 P 0.0048 1.2035 K 0.0014 1.0509 Cl 0.0080 1.1286 Ca 0.2202 1.1036 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 568 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2240 0.015935 0.2240 0.1735 Mg 0.5583 0.014487 0.5583 0.4092 Sr 0.1465 0.012432 0.1465 0.0298 P 0.5794 0.029299 0.5794 0.3333 K 0.1436 0.010046 0.1436 0.0654 Cl 0.9054 0.021304 0.9054 0.4549 Ca 24.2993 0.123239 24.2993 10.8002 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 17.0289 17.0289 25.2564 O 56.1145 56.1145 62.4772 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 569 x= -17112.0 y= 3068.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 39.4 3.6 3.6 10.85 0.0465 3.6 0.0293 Mg 126.7 2.0 2.5 50.32 0.0703 2.0 0.0113 Sr 37.2 2.6 14.3 2.60 0.0033 2.6 0.0406 P 34.4 3.8 2.4 14.64 0.0416 3.8 0.0403 K 29.1 4.1 5.1 5.70 0.0223 4.2 0.0192 Cl 89.6 1.9 2.2 40.74 0.0195 1.9 0.0231 Ca 3104.5 0.4 17.7 175.89 0.6911 0.5 0.0341 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0760 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0640 Elt. k-ratio Correc. Na 0.0023 2.3168 Mg 0.0051 1.6977 Sr 0.0020 1.3795 P 0.0065 1.2005 K 0.0020 1.0417 Cl 0.0108 1.1230 Ca 0.2508 1.0985 Ba 0.0000 1.5362 Fe 0.0000 NaN Mn 0.0004 1.2780 iteration : 3 Analysis no. 569 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5378 0.022171 0.5378 0.4321 Mg 0.8639 0.017881 0.8639 0.6565 Sr 0.2825 0.014008 0.2825 0.0595 P 0.7833 0.033338 0.7833 0.4671 K 0.2060 0.011259 0.2060 0.0973 Cl 1.2167 0.024461 1.2167 0.6339 Ca 27.5509 0.133317 27.5509 12.6971 Ba 0.0033 0.019398 0.0033 0.0004 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0475 0.021310 0.0475 0.0160 C 15.2581 15.2581 23.4649 O 53.2500 53.2500 61.4750 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Fe ( 0.00) point n : 570 x= -17111.0 y= 3073.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 30.3 4.1 3.6 8.35 0.0347 4.1 0.0295 Mg 82.0 2.5 2.5 32.55 0.0450 2.5 0.0113 Sr 28.3 3.0 14.3 1.98 0.0020 3.0 0.0407 P 27.0 4.3 2.4 11.47 0.0319 4.3 0.0404 K 23.1 4.6 5.1 4.53 0.0168 4.7 0.0194 Cl 83.9 2.0 2.2 38.13 0.0182 2.0 0.0232 Ca 2752.0 0.4 17.7 155.91 0.6121 0.5 0.0342 Ba 8.9 5.3 10.8 0.82 0.0000 5.3 0.0000 Fe 3.8 8.1 3.3 1.16 0.0003 8.1 0.0570 Mn 3.6 11.8 2.7 1.33 0.0009 11.8 0.0642 Elt. k-ratio Correc. Na 0.0017 2.3283 Mg 0.0033 1.7026 Sr 0.0012 1.3824 P 0.0050 1.2031 K 0.0015 1.0516 Cl 0.0101 1.1281 Ca 0.2221 1.1032 Ba 0.0000 NaN Fe 0.0001 1.2609 Mn 0.0003 1.2822 iteration : 2 Analysis no. 570 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4035 0.019766 0.4035 0.3142 Mg 0.5542 0.014438 0.5542 0.4083 Sr 0.1727 0.012750 0.1727 0.0353 P 0.6024 0.029777 0.6024 0.3483 K 0.1563 0.010322 0.1563 0.0716 Cl 1.1419 0.023782 1.1419 0.5767 Ca 24.5039 0.123871 24.5039 10.9473 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0179 0.014350 0.0179 0.0057 Mn 0.0329 0.020729 0.0329 0.0107 C 16.7918 16.7918 25.0331 O 55.6226 55.6226 62.2488 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 571 x= -17111.0 y= 3077.0 z= -279. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 30.5 4.0 3.6 8.41 0.0350 4.1 0.0295 Mg 71.3 2.6 2.5 28.32 0.0389 2.7 0.0113 Sr 30.4 2.9 14.3 2.13 0.0023 2.9 0.0407 P 28.2 4.2 2.4 12.00 0.0336 4.2 0.0404 K 26.3 4.4 5.1 5.15 0.0197 4.4 0.0194 Cl 71.7 2.2 2.2 32.58 0.0155 2.2 0.0232 Ca 2755.6 0.4 17.7 156.12 0.6129 0.5 0.0342 Ba 10.8 4.8 10.8 1.00 0.0000 4.8 0.0759 Fe 3.8 8.1 3.3 1.14 0.0003 8.1 0.0571 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0642 Elt. k-ratio Correc. Na 0.0017 2.3301 Mg 0.0028 1.7037 Sr 0.0014 1.3822 P 0.0053 1.2033 K 0.0017 1.0507 Cl 0.0086 1.1283 Ca 0.2224 1.1030 Ba 0.0000 1.5356 Fe 0.0001 1.2610 Mn 0.0002 1.2823 iteration : 2 Analysis no. 571 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4068 0.019841 0.4068 0.3167 Mg 0.4802 0.013493 0.4802 0.3536 Sr 0.1996 0.013073 0.1996 0.0408 P 0.6332 0.030422 0.6332 0.3658 K 0.1835 0.010877 0.1835 0.0840 Cl 0.9713 0.022020 0.9713 0.4903 Ca 24.5349 0.123968 24.5349 10.9543 Ba 0.0013 0.019355 0.0013 0.0002 Fe 0.0162 0.014302 0.0162 0.0052 Mn 0.0292 0.020567 0.0292 0.0095 C 16.8128 16.8128 25.0489 O 55.7309 55.7309 62.3309 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 572 x= -17110.0 y= 3082.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 28.9 4.2 3.6 7.95 0.0328 4.2 0.0294 Mg 128.5 2.0 2.5 51.01 0.0713 2.0 0.0113 Sr 36.3 2.6 14.3 2.54 0.0032 2.6 0.0407 P 32.6 3.9 2.4 13.87 0.0393 3.9 0.0404 K 25.8 4.4 5.1 5.06 0.0193 4.4 0.0195 Cl 91.7 1.9 2.2 41.70 0.0199 1.9 0.0232 Ca 2722.9 0.4 17.7 154.26 0.6056 0.5 0.0343 Ba 10.2 5.0 10.8 0.95 0.0000 5.0 0.0000 Fe 3.4 8.5 3.3 1.04 0.0001 8.6 0.0570 Mn 3.4 12.2 2.7 1.24 0.0006 12.2 0.0642 Elt. k-ratio Correc. Na 0.0016 2.3198 Mg 0.0052 1.6975 Sr 0.0020 1.3832 P 0.0062 1.2046 K 0.0017 1.0547 Cl 0.0111 1.1301 Ca 0.2198 1.1036 Ba 0.0000 NaN Fe 0.0000 1.2602 Mn 0.0002 1.2814 iteration : 2 Analysis no. 572 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3802 0.019267 0.3802 0.2969 Mg 0.8760 0.018003 0.8760 0.6470 Sr 0.2724 0.013924 0.2724 0.0558 P 0.7418 0.032609 0.7418 0.4299 K 0.1803 0.010840 0.1803 0.0828 Cl 1.2539 0.024900 1.2539 0.6349 Ca 24.2560 0.123101 24.2560 10.8637 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0042 0.013935 0.0042 0.0014 Mn 0.0237 0.020306 0.0237 0.0077 C 16.6065 16.6065 24.8190 O 55.4050 55.4050 62.1609 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 573 x= -17109.0 y= 3086.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 35.3 3.8 3.6 9.72 0.0412 3.8 0.0293 Mg 103.9 2.2 2.5 41.28 0.0574 2.2 0.0113 Sr 35.2 2.7 14.3 2.46 0.0030 2.7 0.0406 P 37.0 3.7 2.4 15.75 0.0450 3.7 0.0403 K 24.7 4.5 5.1 4.83 0.0182 4.5 0.0194 Cl 108.6 1.8 2.2 49.34 0.0237 1.8 0.0231 Ca 2902.0 0.4 17.7 164.41 0.6457 0.5 0.0342 Ba 10.9 4.8 10.8 1.01 0.0001 4.8 0.0759 Fe 3.6 8.3 3.3 1.10 0.0002 8.3 0.0569 Mn 4.0 11.2 2.7 1.46 0.0012 11.3 0.0641 Elt. k-ratio Correc. Na 0.0021 2.3178 Mg 0.0042 1.6976 Sr 0.0019 1.3795 P 0.0071 1.2011 K 0.0016 1.0497 Cl 0.0132 1.1264 Ca 0.2343 1.1013 Ba 0.0000 1.5353 Fe 0.0001 1.2578 Mn 0.0004 1.2795 iteration : 2 Analysis no. 573 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4762 0.021081 0.4762 0.3774 Mg 0.7054 0.016193 0.7054 0.5287 Sr 0.2575 0.013726 0.2575 0.0535 P 0.8472 0.034530 0.8472 0.4983 K 0.1695 0.010585 0.1695 0.0790 Cl 1.4846 0.026973 1.4846 0.7629 Ca 25.8068 0.127945 25.8068 11.7301 Ba 0.0026 0.019374 0.0026 0.0003 Fe 0.0110 0.014113 0.0110 0.0036 Mn 0.0457 0.021254 0.0457 0.0152 C 15.9390 15.9390 24.1757 O 54.2545 54.2545 61.7753 oxide-like spec. total : 100.0000 100.0000 100.0000 point n : 574 x= -17108.0 y= 3090.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 24.5 4.5 3.6 6.76 0.0272 4.5 0.0294 Mg 85.9 2.4 2.5 34.12 0.0472 2.4 0.0113 Sr 32.5 2.8 14.3 2.27 0.0026 2.8 0.0405 P 33.6 3.9 2.4 14.30 0.0406 3.9 0.0402 K 32.3 3.9 5.1 6.32 0.0253 3.9 0.0192 Cl 97.4 1.8 2.2 44.29 0.0212 1.9 0.0230 Ca 3134.3 0.4 17.7 177.57 0.6977 0.5 0.0341 Ba 10.1 5.0 10.8 0.94 0.0000 5.0 0.0000 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0568 Mn 4.0 11.2 2.7 1.48 0.0013 11.2 0.0640 Elt. k-ratio Correc. Na 0.0014 2.3242 Mg 0.0034 1.6973 Sr 0.0016 1.3765 P 0.0064 1.1978 K 0.0022 1.0403 Cl 0.0118 1.1211 Ca 0.2532 1.0984 Ba 0.0000 NaN Fe 0.0001 1.2560 Mn 0.0004 1.2782 iteration : 2 Analysis no. 574 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3152 0.017951 0.3152 0.2532 Mg 0.5800 0.014732 0.5800 0.4407 Sr 0.2240 0.013317 0.2240 0.0472 P 0.7620 0.032889 0.7620 0.4543 K 0.2333 0.011761 0.2333 0.1102 Cl 1.3231 0.025447 1.3231 0.6892 Ca 27.8117 0.134123 27.8117 12.8149 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0186 0.014321 0.0186 0.0062 Mn 0.0475 0.021313 0.0475 0.0160 C 15.3641 15.3641 23.6234 O 53.3205 53.3205 61.5447 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 575 x= -17108.0 y= 3095.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 15.2 5.7 3.6 4.18 0.0150 5.8 0.0295 Mg 56.8 3.0 2.5 22.56 0.0307 3.0 0.0113 Sr 24.0 3.2 14.3 1.68 0.0014 3.2 0.0407 P 38.7 3.6 2.4 16.45 0.0471 3.6 0.0404 K 23.7 4.6 5.1 4.65 0.0173 4.6 0.0195 Cl 83.2 2.0 2.2 37.80 0.0180 2.0 0.0233 Ca 2545.7 0.4 17.7 144.23 0.5660 0.5 0.0343 Ba 8.7 5.4 10.8 0.81 0.0000 5.4 0.0000 Fe 3.2 8.9 3.3 0.95 0.0000 8.9 0.0000 Mn 3.5 11.9 2.7 1.29 0.0008 12.0 0.0643 Elt. k-ratio Correc. Na 0.0007 2.3325 Mg 0.0022 1.7009 Sr 0.0009 1.3819 P 0.0074 1.2033 K 0.0015 1.0594 Cl 0.0100 1.1327 Ca 0.2054 1.1062 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0002 1.2842 iteration : 2 Analysis no. 575 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1746 0.014700 0.1746 0.1340 Mg 0.3784 0.012059 0.3784 0.2746 Sr 0.1198 0.012086 0.1198 0.0241 P 0.8892 0.035327 0.8892 0.5064 K 0.1627 0.010510 0.1627 0.0734 Cl 1.1363 0.023778 1.1363 0.5654 Ca 22.7206 0.118248 22.7206 9.9996 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0293 0.020600 0.0293 0.0094 C 17.4808 17.4808 25.6728 O 56.9082 56.9082 62.7403 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) point n : 576 x= -17107.0 y= 3099.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 36.4 3.7 3.6 10.04 0.0427 3.7 0.0293 Mg 104.4 2.2 2.5 41.48 0.0577 2.2 0.0113 Sr 33.0 2.7 14.3 2.31 0.0027 2.8 0.0406 P 50.1 3.2 2.4 21.30 0.0619 3.2 0.0403 K 35.1 3.8 5.1 6.87 0.0279 3.8 0.0193 Cl 82.4 2.0 2.2 37.45 0.0179 2.0 0.0231 Ca 2998.0 0.4 17.7 169.85 0.6672 0.5 0.0342 Ba 9.2 5.2 10.8 0.85 0.0000 5.2 0.0000 Fe 3.6 8.4 3.3 1.08 0.0002 8.4 0.0569 Mn 3.6 11.9 2.7 1.31 0.0008 11.9 0.0640 Elt. k-ratio Correc. Na 0.0021 2.3177 Mg 0.0042 1.6976 Sr 0.0017 1.3786 P 0.0097 1.2001 K 0.0025 1.0458 Cl 0.0099 1.1260 Ca 0.2421 1.1001 Ba 0.0000 NaN Fe 0.0001 1.2569 Mn 0.0002 1.2788 iteration : 3 Analysis no. 576 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4935 0.021394 0.4935 0.3939 Mg 0.7089 0.016231 0.7089 0.5352 Sr 0.2311 0.013417 0.2311 0.0484 P 1.1654 0.039930 1.1654 0.6904 K 0.2587 0.012262 0.2587 0.1214 Cl 1.1189 0.023530 1.1189 0.5791 Ca 26.6364 0.130513 26.6364 12.1945 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0093 0.014052 0.0093 0.0031 Mn 0.0310 0.020595 0.0310 0.0103 C 15.4783 15.4783 23.6461 O 53.8685 53.8685 61.7777 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 577 x= -17106.0 y= 3104.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 21.7 4.8 3.6 5.97 0.0235 4.8 0.0295 Mg 72.9 2.6 2.5 28.96 0.0398 2.6 0.0113 Sr 22.8 3.3 14.3 1.59 0.0012 3.3 0.0407 P 40.4 3.5 2.4 17.17 0.0493 3.5 0.0404 K 23.7 4.6 5.1 4.65 0.0173 4.6 0.0196 Cl 88.4 1.9 2.2 40.19 0.0192 1.9 0.0233 Ca 2484.6 0.4 17.7 140.76 0.5522 0.5 0.0344 Ba 7.8 5.7 10.8 0.73 0.0000 5.7 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0572 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0643 Elt. k-ratio Correc. Na 0.0012 2.3288 Mg 0.0029 1.7010 Sr 0.0008 1.3833 P 0.0077 1.2043 K 0.0015 1.0623 Cl 0.0107 1.1342 Ca 0.2004 1.1070 Ba 0.0000 NaN Fe 0.0000 1.2637 Mn 0.0003 1.2844 iteration : 2 Analysis no. 577 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2727 0.017044 0.2727 0.2087 Mg 0.4906 0.013618 0.4906 0.3552 Sr 0.1048 0.011901 0.1048 0.0210 P 0.9316 0.036093 0.9316 0.5293 K 0.1632 0.010538 0.1632 0.0734 Cl 1.2119 0.024541 1.2119 0.6016 Ca 22.1854 0.116533 22.1854 9.7405 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0060 0.014025 0.0060 0.0019 Mn 0.0367 0.020930 0.0367 0.0117 C 17.5558 17.5558 25.7209 O 57.0413 57.0413 62.7357 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 578 x= -17105.0 y= 3108.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 30.0 4.1 3.6 8.27 0.0343 4.1 0.0293 Mg 128.6 2.0 2.5 51.05 0.0713 2.0 0.0112 Sr 36.4 2.6 14.3 2.55 0.0032 2.6 0.0405 P 48.6 3.2 2.4 20.66 0.0600 3.2 0.0402 K 31.6 4.0 5.1 6.19 0.0246 4.0 0.0193 Cl 111.3 1.7 2.2 50.57 0.0243 1.7 0.0231 Ca 3089.1 0.4 17.7 175.01 0.6875 0.5 0.0341 Ba 9.9 5.0 10.8 0.92 0.0000 5.0 0.0000 Fe 3.9 8.1 3.3 1.17 0.0003 8.1 0.0568 Mn 3.7 11.6 2.7 1.37 0.0010 11.6 0.0639 Elt. k-ratio Correc. Na 0.0017 2.3128 Mg 0.0052 1.6926 Sr 0.0020 1.3769 P 0.0094 1.1987 K 0.0022 1.0450 Cl 0.0135 1.1241 Ca 0.2495 1.0991 Ba 0.0000 NaN Fe 0.0001 1.2551 Mn 0.0003 1.2773 iteration : 2 Analysis no. 578 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3963 0.019545 0.3963 0.3194 Mg 0.8740 0.017954 0.8740 0.6664 Sr 0.2720 0.013869 0.2720 0.0575 P 1.1272 0.039289 1.1272 0.6745 K 0.2282 0.011701 0.2282 0.1082 Cl 1.5190 0.027244 1.5190 0.7940 Ca 27.4218 0.132928 27.4218 12.6793 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0186 0.014309 0.0186 0.0062 Mn 0.0365 0.020813 0.0365 0.0123 C 15.0704 15.0704 23.2526 O 53.0360 53.0360 61.4297 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 579 x= -17105.0 y= 3113.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 22.7 4.7 3.6 6.25 0.0248 4.7 0.0294 Mg 86.8 2.4 2.5 34.46 0.0477 2.4 0.0113 Sr 32.0 2.8 14.3 2.24 0.0026 2.8 0.0406 P 39.1 3.6 2.4 16.64 0.0477 3.6 0.0404 K 24.7 4.5 5.1 4.83 0.0182 4.5 0.0195 Cl 98.4 1.8 2.2 44.75 0.0214 1.8 0.0232 Ca 2702.6 0.4 17.7 153.11 0.6010 0.5 0.0343 Ba 10.6 4.9 10.8 0.98 0.0000 4.9 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0570 Mn 3.2 12.6 2.7 1.16 0.0004 12.6 0.0642 Elt. k-ratio Correc. Na 0.0012 2.3237 Mg 0.0035 1.6977 Sr 0.0016 1.3806 P 0.0075 1.2025 K 0.0016 1.0557 Cl 0.0119 1.1302 Ca 0.2181 1.1041 Ba 0.0000 NaN Fe 0.0000 1.2607 Mn 0.0001 1.2819 iteration : 2 Analysis no. 579 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2872 0.017342 0.2872 0.2237 Mg 0.5861 0.014808 0.5861 0.4319 Sr 0.2185 0.013285 0.2185 0.0447 P 0.8996 0.035498 0.8996 0.5202 K 0.1704 0.010645 0.1704 0.0781 Cl 1.3479 0.025784 1.3479 0.6809 Ca 24.0833 0.122564 24.0833 10.7616 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0025 0.013888 0.0025 0.0008 Mn 0.0163 0.019973 0.0163 0.0053 C 16.7431 16.7431 24.9659 O 55.6450 55.6450 62.2869 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 580 x= -17104.0 y= 3117.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 34.9 3.8 3.6 9.62 0.0407 3.8 0.0294 Mg 78.8 2.5 2.5 31.28 0.0432 2.5 0.0113 Sr 27.4 3.0 14.3 1.92 0.0019 3.0 0.0406 P 42.5 3.4 2.4 18.09 0.0521 3.4 0.0404 K 35.9 3.7 5.1 7.04 0.0287 3.7 0.0194 Cl 82.4 2.0 2.2 37.46 0.0179 2.0 0.0232 Ca 2735.3 0.4 17.7 154.97 0.6084 0.5 0.0343 Ba 9.0 5.3 10.8 0.84 0.0000 5.3 0.0000 Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0570 Mn 3.2 12.5 2.7 1.18 0.0005 12.5 0.0642 Elt. k-ratio Correc. Na 0.0020 2.3235 Mg 0.0031 1.7012 Sr 0.0012 1.3812 P 0.0082 1.2023 K 0.0025 1.0537 Cl 0.0099 1.1298 Ca 0.2208 1.1036 Ba 0.0000 NaN Fe 0.0001 1.2604 Mn 0.0001 1.2817 iteration : 2 Analysis no. 580 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.4722 0.021038 0.4722 0.3687 Mg 0.5315 0.014148 0.5315 0.3925 Sr 0.1615 0.012604 0.1615 0.0331 P 0.9828 0.036949 0.9828 0.5695 K 0.2680 0.012486 0.2680 0.1230 Cl 1.1231 0.023614 1.1231 0.5686 Ca 24.3685 0.123464 24.3685 10.9134 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0076 0.014041 0.0076 0.0025 Mn 0.0181 0.020057 0.0181 0.0059 C 16.5703 16.5703 24.7633 O 55.4964 55.4964 62.2594 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 581 x= -17103.0 y= 3122.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 40.4 3.5 3.6 11.14 0.0479 3.5 0.0293 Mg 106.3 2.2 2.5 42.23 0.0588 2.2 0.0113 Sr 37.5 2.6 14.3 2.63 0.0034 2.6 0.0406 P 44.4 3.4 2.4 18.87 0.0545 3.4 0.0403 K 31.8 4.0 5.1 6.23 0.0248 4.0 0.0193 Cl 89.1 1.9 2.2 40.48 0.0193 1.9 0.0231 Ca 2941.3 0.4 17.7 166.64 0.6545 0.5 0.0342 Ba 10.6 4.8 10.8 0.99 0.0000 4.9 0.0000 Fe 3.5 8.4 3.3 1.07 0.0001 8.4 0.0569 Mn 3.0 12.9 2.7 1.11 0.0003 12.9 0.0641 Elt. k-ratio Correc. Na 0.0024 2.3162 Mg 0.0043 1.6981 Sr 0.0021 1.3795 P 0.0086 1.2014 K 0.0022 1.0480 Cl 0.0108 1.1269 Ca 0.2375 1.1008 Ba 0.0000 NaN Fe 0.0001 1.2574 Mn 0.0001 1.2791 iteration : 3 Analysis no. 581 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.5534 0.022436 0.5534 0.4400 Mg 0.7223 0.016383 0.7223 0.5431 Sr 0.2868 0.014055 0.2868 0.0598 P 1.0272 0.037688 1.0272 0.6061 K 0.2306 0.011768 0.2306 0.1078 Cl 1.2129 0.024467 1.2129 0.6253 Ca 26.1464 0.128997 26.1464 11.9226 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0076 0.014006 0.0076 0.0025 Mn 0.0107 0.019674 0.0107 0.0036 C 15.7028 15.7028 23.8937 O 54.0991 54.0991 61.7956 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 582 x= -17103.0 y= 3126.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 27.8 4.2 3.6 7.65 0.0314 4.3 0.0294 Mg 81.6 2.5 2.5 32.41 0.0448 2.5 0.0113 Sr 31.7 2.8 14.3 2.22 0.0025 2.8 0.0408 P 36.5 3.7 2.4 15.53 0.0443 3.7 0.0406 K 21.8 4.8 5.1 4.27 0.0155 4.8 0.0197 Cl 83.6 2.0 2.2 37.98 0.0181 2.0 0.0234 Ca 2280.0 0.5 17.7 129.17 0.5065 0.5 0.0345 Ba 9.6 5.1 10.8 0.89 0.0000 5.1 0.0000 Fe 3.5 8.5 3.3 1.05 0.0001 8.5 0.0573 Mn 2.5 14.1 2.7 0.92 0.0000 14.1 0.0000 Elt. k-ratio Correc. Na 0.0016 2.3265 Mg 0.0032 1.7021 Sr 0.0016 1.3863 P 0.0070 1.2084 K 0.0014 1.0698 Cl 0.0101 1.1389 Ca 0.1838 1.1095 Ba 0.0000 NaN Fe 0.0000 1.2656 Mn 0.0000 NaN iteration : 2 Analysis no. 582 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.3646 0.018988 0.3646 0.2752 Mg 0.5517 0.014405 0.5517 0.3939 Sr 0.2160 0.013299 0.2160 0.0428 P 0.8401 0.034515 0.8401 0.4707 K 0.1475 0.010255 0.1475 0.0655 Cl 1.1481 0.023963 1.1481 0.5620 Ca 20.3929 0.110721 20.3929 8.8296 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0060 0.014047 0.0060 0.0019 Mn 0.0000 0.000000 0.0000 0.0000 C 18.2318 18.2318 26.3414 O 58.1014 58.1014 63.0171 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 583 x= -17102.0 y= 3131.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 57.0 3.0 3.6 15.72 0.0695 3.0 0.0292 Mg 145.1 1.9 2.5 57.63 0.0807 1.9 0.0113 Sr 38.1 2.6 14.3 2.67 0.0034 2.6 0.0408 P 52.4 3.1 2.4 22.30 0.0650 3.1 0.0406 K 30.7 4.0 5.1 6.01 0.0238 4.0 0.0197 Cl 107.1 1.8 2.2 48.69 0.0234 1.8 0.0234 Ca 2440.7 0.5 17.7 138.28 0.5425 0.5 0.0344 Ba 9.7 5.1 10.8 0.90 0.0000 5.1 0.0000 Fe 3.4 8.6 3.3 1.02 0.0000 8.6 0.0571 Mn 3.8 11.5 2.7 1.38 0.0010 11.6 0.0642 Elt. k-ratio Correc. Na 0.0035 2.3052 Mg 0.0058 1.6983 Sr 0.0021 1.3859 P 0.0102 1.2078 K 0.0021 1.0680 Cl 0.0130 1.1380 Ca 0.1969 1.1073 Ba 0.0000 NaN Fe 0.0000 1.2613 Mn 0.0003 1.2821 iteration : 2 Analysis no. 583 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.7995 0.026274 0.7995 0.6173 Mg 0.9923 0.019152 0.9923 0.7247 Sr 0.2952 0.014200 0.2952 0.0598 P 1.2308 0.041102 1.2308 0.7053 K 0.2254 0.011812 0.2254 0.1023 Cl 1.4797 0.027072 1.4797 0.7408 Ca 21.7997 0.115288 21.7997 9.6541 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0017 0.013870 0.0017 0.0005 Mn 0.0384 0.020976 0.0384 0.0124 C 16.9575 16.9575 25.0595 O 56.1797 56.1797 62.3232 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Ba ( 0.00) point n : 584 x= -17101.0 y= 3135.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 9.7 7.2 3.6 2.66 0.0078 7.2 0.0298 Mg 8.2 7.8 2.5 3.26 0.0032 7.8 0.0114 Sr 9.5 5.1 14.3 0.67 0.0000 5.1 0.0000 P 2.0 16.0 2.4 0.83 0.0000 16.0 0.0000 K 4.3 10.8 5.1 0.84 0.0000 10.8 0.0000 Cl 124.2 1.6 2.2 56.45 0.0272 1.6 0.0243 Ca 48.0 3.2 17.7 2.72 0.0068 3.2 0.0355 Ba 5.9 6.5 10.8 0.55 0.0000 6.5 0.0000 Fe 1.8 11.8 3.3 0.55 0.0000 11.8 0.0000 Mn 1.5 18.6 2.7 0.54 0.0000 18.6 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3518 Mg 0.0002 1.7176 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0151 1.1850 Ca 0.0025 1.1417 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 584 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0920 0.012455 0.0920 0.0595 Mg 0.0400 0.005153 0.0400 0.0244 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.7915 0.030341 1.7915 0.7508 Ca 0.2816 0.016824 0.2816 0.1044 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.7529 26.7529 33.0926 O 71.0420 71.0420 65.9684 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 585 x= -17100.0 y= 3140.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 8.9 7.5 3.6 2.44 0.0068 7.5 0.0298 Mg 9.1 7.4 2.5 3.59 0.0037 7.4 0.0114 Sr 10.4 4.9 14.3 0.72 0.0000 4.9 0.0000 P 1.5 18.6 2.4 0.62 0.0000 18.6 0.0000 K 5.8 9.3 5.1 1.14 0.0007 9.3 0.0216 Cl 93.7 1.9 2.2 42.59 0.0204 1.9 0.0244 Ca 19.6 5.1 17.7 1.11 0.0004 5.1 0.0355 Ba 5.8 6.5 10.8 0.54 0.0000 6.6 0.0000 Fe 1.8 11.7 3.3 0.55 0.0000 11.7 0.0000 Mn 1.3 20.0 2.7 0.46 0.0000 20.0 0.0000 Elt. k-ratio Correc. Na 0.0003 2.3569 Mg 0.0003 1.7204 Sr 0.0000 NaN P 0.0000 NaN K 0.0001 1.1685 Cl 0.0113 1.1867 Ca 0.0002 1.1419 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 585 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0800 0.012099 0.0800 0.0515 Mg 0.0460 0.005363 0.0460 0.0280 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0068 0.007124 0.0068 0.0026 Cl 1.3456 0.026422 1.3456 0.5615 Ca 0.0176 0.012653 0.0176 0.0065 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9474 26.9474 33.1897 O 71.5566 71.5566 66.1602 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 586 x= -17100.0 y= 3144.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 9.9 7.1 3.6 2.72 0.0081 7.1 0.0298 Mg 12.2 6.4 2.5 4.84 0.0055 6.4 0.0114 Sr 10.8 4.8 14.3 0.75 0.0000 4.8 0.0000 P 1.7 17.4 2.4 0.70 0.0000 17.4 0.0000 K 4.8 10.2 5.1 0.93 0.0000 10.3 0.0000 Cl 103.4 1.8 2.2 47.01 0.0225 1.8 0.0244 Ca 27.2 4.3 17.7 1.54 0.0021 4.3 0.0355 Ba 6.9 6.0 10.8 0.64 0.0000 6.0 0.0000 Fe 2.2 10.8 3.3 0.65 0.0000 10.8 0.0000 Mn 1.3 19.6 2.7 0.48 0.0000 19.6 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3548 Mg 0.0004 1.7195 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0125 1.1863 Ca 0.0008 1.1418 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 586 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0952 0.012565 0.0952 0.0614 Mg 0.0682 0.006047 0.0682 0.0416 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.4880 0.027733 1.4880 0.6218 Ca 0.0886 0.013895 0.0886 0.0328 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8768 26.8768 33.1495 O 71.3832 71.3832 66.0931 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 587 x= -17099.0 y= 3148.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 12.8 6.2 3.6 3.53 0.0119 6.3 0.0298 Mg 14.3 5.9 2.5 5.68 0.0067 5.9 0.0114 Sr 10.8 4.8 14.3 0.75 0.0000 4.8 0.0000 P 2.0 16.0 2.4 0.83 0.0000 16.0 0.0000 K 5.3 9.7 5.1 1.03 0.0001 9.8 0.0215 Cl 80.6 2.0 2.2 36.61 0.0174 2.0 0.0244 Ca 25.1 4.5 17.7 1.42 0.0017 4.5 0.0355 Ba 6.1 6.4 10.8 0.57 0.0000 6.4 0.0000 Fe 1.9 11.6 3.3 0.56 0.0000 11.6 0.0000 Mn 1.4 19.2 2.7 0.50 0.0000 19.2 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3575 Mg 0.0005 1.7221 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1679 Cl 0.0097 1.1871 Ca 0.0006 1.1416 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 587 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1405 0.013894 0.1405 0.0904 Mg 0.0831 0.006476 0.0831 0.0506 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0014 0.006939 0.0014 0.0005 Cl 1.1527 0.024535 1.1527 0.4808 Ca 0.0687 0.013556 0.0687 0.0253 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9314 26.9314 33.1571 O 71.6222 71.6222 66.1953 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 588 x= -17098.0 y= 3153.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 7.1 8.4 3.6 1.96 0.0045 8.4 0.0298 Mg 10.3 7.0 2.5 4.09 0.0044 7.0 0.0114 Sr 11.1 4.7 14.3 0.78 0.0000 4.8 0.0000 P 1.2 20.4 2.4 0.51 0.0000 20.4 0.0000 K 3.2 12.5 5.1 0.63 0.0000 12.5 0.0000 Cl 104.4 1.8 2.2 47.46 0.0228 1.8 0.0244 Ca 18.7 5.2 17.7 1.06 0.0002 5.2 0.0355 Ba 6.4 6.3 10.8 0.59 0.0000 6.3 0.0000 Fe 2.0 11.2 3.3 0.60 0.0000 11.3 0.0000 Mn 1.4 18.9 2.7 0.52 0.0000 18.9 0.0000 Elt. k-ratio Correc. Na 0.0002 2.3556 Mg 0.0003 1.7191 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0127 1.1864 Ca 0.0001 1.1420 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 588 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0532 0.011211 0.0532 0.0342 Mg 0.0548 0.005642 0.0548 0.0334 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.5030 0.027871 1.5030 0.6276 Ca 0.0093 0.012501 0.0093 0.0034 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9254 26.9254 33.1871 O 71.4543 71.4543 66.1143 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 589 x= -17098.0 y= 3157.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 9.3 7.3 3.6 2.56 0.0074 7.3 0.0298 Mg 12.4 6.3 2.5 4.92 0.0056 6.4 0.0114 Sr 10.1 5.0 14.3 0.71 0.0000 5.0 0.0000 P 1.6 17.9 2.4 0.66 0.0000 18.0 0.0000 K 3.8 11.5 5.1 0.75 0.0000 11.5 0.0000 Cl 95.6 1.9 2.2 43.44 0.0208 1.9 0.0244 Ca 17.2 5.4 17.7 0.97 0.0000 5.4 0.0000 Ba 6.3 6.3 10.8 0.58 0.0000 6.3 0.0000 Fe 1.9 11.5 3.3 0.57 0.0000 11.6 0.0000 Mn 1.8 16.9 2.7 0.65 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0004 2.3562 Mg 0.0004 1.7202 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0116 1.1867 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 589 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0869 0.012313 0.0869 0.0559 Mg 0.0697 0.006091 0.0697 0.0424 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.3733 0.026684 1.3733 0.5731 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9373 26.9373 33.1816 O 71.5329 71.5329 66.1470 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 590 x= -17097.0 y= 3162.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 14.6 5.8 3.6 4.03 0.0143 5.9 0.0299 Mg 15.6 5.7 2.5 6.18 0.0074 5.7 0.0114 Sr 11.0 4.8 14.3 0.77 0.0000 4.8 0.0000 P 1.5 18.2 2.4 0.64 0.0000 18.3 0.0000 K 5.7 9.4 5.1 1.11 0.0005 9.4 0.0215 Cl 65.2 2.3 2.2 29.64 0.0140 2.3 0.0244 Ca 20.2 5.0 17.7 1.14 0.0006 5.0 0.0354 Ba 6.4 6.2 10.8 0.60 0.0000 6.2 0.0000 Fe 2.0 11.2 3.3 0.61 0.0000 11.2 0.0000 Mn 1.3 19.6 2.7 0.48 0.0000 19.6 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3593 Mg 0.0005 1.7238 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1678 Cl 0.0078 1.1877 Ca 0.0002 1.1416 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 590 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1682 0.014649 0.1682 0.1080 Mg 0.0920 0.006719 0.0920 0.0559 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0053 0.007070 0.0053 0.0020 Cl 0.9272 0.022133 0.9272 0.3862 Ca 0.0232 0.012751 0.0232 0.0085 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9809 26.9809 33.1710 O 71.8031 71.8031 66.2683 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 591 x= -17096.0 y= 3166.0 z= -278. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 14.7 5.8 3.6 4.04 0.0143 5.9 0.0297 Mg 16.4 5.5 2.5 6.51 0.0079 5.5 0.0114 Sr 10.3 4.9 14.3 0.72 0.0000 4.9 0.0000 P 1.7 17.4 2.4 0.70 0.0000 17.4 0.0000 K 5.2 9.8 5.1 1.02 0.0001 9.8 0.0216 Cl 153.9 1.5 2.2 69.93 0.0338 1.5 0.0243 Ca 22.7 4.7 17.7 1.29 0.0011 4.7 0.0355 Ba 6.6 6.2 10.8 0.61 0.0000 6.2 0.0000 Fe 2.3 10.5 3.3 0.68 0.0000 10.5 0.0000 Mn 1.8 16.9 2.7 0.65 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3451 Mg 0.0006 1.7155 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1697 Cl 0.0188 1.1849 Ca 0.0004 1.1423 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 591 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1680 0.014582 0.1680 0.1087 Mg 0.0976 0.006843 0.0976 0.0597 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0010 0.006932 0.0010 0.0004 Cl 2.2271 0.033769 2.2271 0.9347 Ca 0.0469 0.013185 0.0469 0.0174 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.6962 26.6962 33.0716 O 70.7634 70.7633 65.8075 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 592 x= -17095.0 y= 3171.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 12.8 6.2 3.6 3.53 0.0119 6.3 0.0298 Mg 8.5 7.7 2.5 3.36 0.0034 7.7 0.0114 Sr 10.0 5.0 14.3 0.70 0.0000 5.0 0.0000 P 1.4 18.9 2.4 0.60 0.0000 18.9 0.0000 K 4.7 10.3 5.1 0.92 0.0000 10.3 0.0000 Cl 78.9 2.1 2.2 35.86 0.0171 2.1 0.0244 Ca 14.0 6.0 17.7 0.79 0.0000 6.0 0.0000 Ba 5.8 6.6 10.8 0.54 0.0000 6.6 0.0000 Fe 1.9 11.5 3.3 0.57 0.0000 11.6 0.0000 Mn 1.3 19.6 2.7 0.48 0.0000 19.6 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3584 Mg 0.0002 1.7226 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0095 1.1872 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 592 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1406 0.013898 0.1406 0.0903 Mg 0.0419 0.005228 0.0419 0.0255 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.1282 0.024286 1.1282 0.4702 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9819 26.9819 33.1928 O 71.7075 71.7075 66.2212 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 593 x= -17095.0 y= 3175.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 12.4 6.3 3.6 3.42 0.0114 6.4 0.0298 Mg 12.2 6.4 2.5 4.83 0.0055 6.4 0.0114 Sr 10.4 4.9 14.3 0.73 0.0000 4.9 0.0000 P 1.3 19.6 2.4 0.55 0.0000 19.6 0.0000 K 5.5 9.5 5.1 1.08 0.0004 9.5 0.0216 Cl 93.6 1.9 2.2 42.55 0.0204 1.9 0.0244 Ca 20.5 4.9 17.7 1.16 0.0006 5.0 0.0355 Ba 7.0 6.0 10.8 0.65 0.0000 6.0 0.0000 Fe 2.1 11.0 3.3 0.62 0.0000 11.0 0.0000 Mn 1.5 18.6 2.7 0.54 0.0000 18.6 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3557 Mg 0.0004 1.7209 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1684 Cl 0.0113 1.1867 Ca 0.0002 1.1418 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 593 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1343 0.013713 0.1343 0.0864 Mg 0.0679 0.006042 0.0679 0.0414 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0039 0.007025 0.0039 0.0015 Cl 1.3443 0.026411 1.3443 0.5611 Ca 0.0260 0.012806 0.0260 0.0096 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9156 26.9156 33.1619 O 71.5081 71.5081 66.1381 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 594 x= -17094.0 y= 3180.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 11.1 6.7 3.6 3.06 0.0097 6.7 0.0299 Mg 14.5 5.9 2.5 5.76 0.0068 5.9 0.0115 Sr 11.8 4.6 14.3 0.83 0.0000 4.6 0.0000 P 1.6 17.7 2.4 0.68 0.0000 17.7 0.0000 K 5.5 9.5 5.1 1.08 0.0004 9.5 0.0215 Cl 59.5 2.4 2.2 27.06 0.0128 2.4 0.0244 Ca 17.9 5.3 17.7 1.01 0.0001 5.3 0.0355 Ba 6.2 6.3 10.8 0.58 0.0000 6.3 0.0000 Fe 1.9 11.5 3.3 0.57 0.0000 11.6 0.0000 Mn 1.6 17.9 2.7 0.57 0.0000 18.0 0.0000 Elt. k-ratio Correc. Na 0.0005 2.3613 Mg 0.0005 1.7237 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1678 Cl 0.0071 1.1879 Ca 0.0000 1.1416 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 594 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1147 0.013173 0.1147 0.0736 Mg 0.0846 0.006521 0.0846 0.0514 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0039 0.007021 0.0039 0.0015 Cl 0.8440 0.021180 0.8440 0.3512 Ca 0.0023 0.012367 0.0023 0.0009 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0300 27.0300 33.2025 O 71.9206 71.9206 66.3191 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 595 x= -17093.0 y= 3184.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 12.7 6.3 3.6 3.49 0.0117 6.3 0.0298 Mg 10.0 7.1 2.5 3.95 0.0042 7.1 0.0114 Sr 8.7 5.4 14.3 0.61 0.0000 5.4 0.0000 P 1.1 21.8 2.4 0.45 0.0000 21.8 0.0000 K 4.3 10.8 5.1 0.83 0.0000 10.9 0.0000 Cl 108.4 1.8 2.2 49.25 0.0236 1.8 0.0244 Ca 16.5 5.5 17.7 0.93 0.0000 5.5 0.0000 Ba 5.6 6.7 10.8 0.52 0.0000 6.7 0.0000 Fe 1.6 12.4 3.3 0.49 0.0000 12.4 0.0000 Mn 1.8 16.6 2.7 0.66 0.0000 16.7 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3536 Mg 0.0003 1.7197 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0132 1.1864 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 595 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1380 0.013807 0.1380 0.0889 Mg 0.0524 0.005566 0.0524 0.0319 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.5609 0.028386 1.5609 0.6522 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8867 26.8867 33.1589 O 71.3621 71.3621 66.0681 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 596 x= -17093.0 y= 3189.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 14.7 5.8 3.6 4.05 0.0144 5.8 0.0298 Mg 13.2 6.1 2.5 5.24 0.0060 6.2 0.0114 Sr 11.4 4.7 14.3 0.80 0.0000 4.7 0.0000 P 1.8 16.9 2.4 0.74 0.0000 16.9 0.0000 K 5.5 9.5 5.1 1.08 0.0004 9.5 0.0216 Cl 91.6 1.9 2.2 41.65 0.0199 1.9 0.0244 Ca 17.4 5.4 17.7 0.98 0.0000 5.4 0.0000 Ba 6.8 6.1 10.8 0.63 0.0000 6.1 0.0000 Fe 2.0 11.1 3.3 0.61 0.0000 11.1 0.0000 Mn 2.0 15.8 2.7 0.74 0.0000 15.8 0.0000 Elt. k-ratio Correc. Na 0.0007 2.3554 Mg 0.0004 1.7215 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1685 Cl 0.0111 1.1869 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 596 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1695 0.014665 0.1695 0.1091 Mg 0.0753 0.006257 0.0753 0.0459 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0039 0.007025 0.0039 0.0015 Cl 1.3154 0.026137 1.3154 0.5490 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9153 26.9153 33.1560 O 71.5206 71.5206 66.1386 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 597 x= -17092.0 y= 3193.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 16.9 5.4 3.6 4.66 0.0173 5.5 0.0299 Mg 13.8 6.0 2.5 5.48 0.0064 6.0 0.0115 Sr 10.5 4.9 14.3 0.74 0.0000 4.9 0.0000 P 1.4 19.2 2.4 0.57 0.0000 19.2 0.0000 K 6.5 8.8 5.1 1.27 0.0013 8.8 0.0215 Cl 57.9 2.4 2.2 26.33 0.0124 2.4 0.0244 Ca 14.3 5.9 17.7 0.81 0.0000 5.9 0.0000 Ba 6.3 6.3 10.8 0.59 0.0000 6.3 0.0000 Fe 1.8 11.8 3.3 0.55 0.0000 11.8 0.0000 Mn 1.9 16.2 2.7 0.70 0.0000 16.2 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3601 Mg 0.0005 1.7250 Sr 0.0000 NaN P 0.0000 NaN K 0.0001 1.1678 Cl 0.0069 1.1879 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 597 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2035 0.015556 0.2035 0.1307 Mg 0.0797 0.006389 0.0797 0.0484 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0135 0.007344 0.0135 0.0051 Cl 0.8204 0.020901 0.8204 0.3415 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0022 27.0022 33.1763 O 71.8807 71.8807 66.2981 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 598 x= -17091.0 y= 3198.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 13.5 6.1 3.6 3.71 0.0128 6.1 0.0298 Mg 11.7 6.5 2.5 4.65 0.0052 6.5 0.0114 Sr 8.4 5.4 14.3 0.59 0.0000 5.5 0.0000 P 1.5 18.2 2.4 0.64 0.0000 18.3 0.0000 K 5.4 9.6 5.1 1.06 0.0003 9.6 0.0216 Cl 114.3 1.7 2.2 51.96 0.0250 1.7 0.0244 Ca 19.1 5.1 17.7 1.08 0.0003 5.1 0.0355 Ba 5.8 6.6 10.8 0.54 0.0000 6.6 0.0000 Fe 1.8 11.9 3.3 0.53 0.0000 12.0 0.0000 Mn 1.3 19.6 2.7 0.48 0.0000 19.6 0.0000 Elt. k-ratio Correc. Na 0.0006 2.3522 Mg 0.0004 1.7192 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1690 Cl 0.0139 1.1862 Ca 0.0001 1.1420 Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 598 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1501 0.014135 0.1501 0.0968 Mg 0.0647 0.005943 0.0647 0.0395 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0029 0.006995 0.0029 0.0011 Cl 1.6480 0.029144 1.6480 0.6890 Ca 0.0135 0.012579 0.0135 0.0050 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.8521 26.8521 33.1399 O 71.2687 71.2687 66.0287 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 599 x= -17090.0 y= 3202.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 7.3 8.3 3.6 2.01 0.0048 8.3 0.0299 Mg 6.0 9.2 2.5 2.36 0.0019 9.2 0.0114 Sr 11.0 4.8 14.3 0.77 0.0000 4.8 0.0000 P 1.8 16.9 2.4 0.74 0.0000 16.9 0.0000 K 4.6 10.5 5.1 0.89 0.0000 10.5 0.0000 Cl 78.5 2.1 2.2 35.69 0.0170 2.1 0.0244 Ca 13.6 6.1 17.7 0.77 0.0000 6.1 0.0000 Ba 5.9 6.5 10.8 0.55 0.0000 6.5 0.0000 Fe 1.6 12.6 3.3 0.48 0.0000 12.6 0.0000 Mn 1.8 16.9 2.7 0.65 0.0000 16.9 0.0000 Elt. k-ratio Correc. Na 0.0002 2.3601 Mg 0.0001 1.7218 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0095 1.1872 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 599 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.0563 0.011337 0.0563 0.0362 Mg 0.0242 0.004591 0.0242 0.0147 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 1.1228 0.024231 1.1228 0.4678 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0220 27.0220 33.2275 O 71.7746 71.7746 66.2539 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 600 x= -17090.0 y= 3207.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 15.5 5.7 3.6 4.26 0.0154 5.7 0.0299 Mg 8.7 7.6 2.5 3.45 0.0035 7.6 0.0115 Sr 11.3 4.7 14.3 0.79 0.0000 4.7 0.0000 P 1.8 16.6 2.4 0.77 0.0000 16.7 0.0000 K 5.1 9.9 5.1 1.00 0.0000 9.9 NaN Cl 58.1 2.4 2.2 26.39 0.0124 2.4 0.0244 Ca 13.4 6.1 17.7 0.76 0.0000 6.1 0.0000 Ba 7.0 6.0 10.8 0.65 0.0000 6.0 0.0000 Fe 2.1 10.8 3.3 0.64 0.0000 10.9 0.0000 Mn 1.5 18.2 2.7 0.55 0.0000 18.3 0.0000 Elt. k-ratio Correc. Na 0.0008 2.3611 Mg 0.0003 1.7250 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 NaN Cl 0.0069 1.1879 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 600 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.1814 0.015001 0.1814 0.1164 Mg 0.0437 0.005295 0.0437 0.0265 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0000 0.000000 0.0000 0.0000 Cl 0.8224 0.020926 0.8224 0.3422 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 27.0307 27.0307 33.2004 O 71.9219 71.9219 66.3145 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for K ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) point n : 601 x= -17089.0 y= 3211.0 z= -277. carb2 left trav 3 Elt. Line Xtal Spec. Std. Posi. Beam Acceleration (nA) voltage(kV) 14.3 15.0 Na Ka TAP Sp1 albite 46371 Mg Ka TAP Sp1 crcats 38511 Sr La TAP Sp1 SrF2 26723 P Ka PET Sp2 wilberfor 70368 K Ka PET Sp3 sanidine 42755 Cl Ka PET Sp3 NaCl 54037 Ca Ka PET Sp3 wilberfor 38383 Ba La PET Sp3 celsian 31729 Fe Ka LIF Sp4 fayalite 48080 Mn Ka LIF Sp4 rhodo 52189 Elt. Peak Prec. Bkgd P/B Ix/ Sig/k Detection Beam Acceleration (Cps) (%) (Cps) Istd (%) limit (%) (nA) voltage(kV) 14.3 15.0 Na 17.9 5.3 3.6 4.94 0.0186 5.3 0.0299 Mg 7.4 8.2 2.5 2.94 0.0028 8.2 0.0115 Sr 11.8 4.6 14.3 0.82 0.0000 4.6 0.0000 P 1.7 17.1 2.4 0.72 0.0000 17.2 0.0000 K 5.7 9.4 5.1 1.12 0.0006 9.4 0.0215 Cl 65.6 2.3 2.2 29.83 0.0141 2.3 0.0244 Ca 11.2 6.7 17.7 0.63 0.0000 6.7 0.0000 Ba 6.9 6.0 10.8 0.64 0.0000 6.0 0.0000 Fe 1.8 11.9 3.3 0.53 0.0000 12.0 0.0000 Mn 1.9 16.4 2.7 0.68 0.0000 16.4 0.0000 Elt. k-ratio Correc. Na 0.0009 2.3593 Mg 0.0002 1.7248 Sr 0.0000 NaN P 0.0000 NaN K 0.0000 1.1679 Cl 0.0079 1.1877 Ca 0.0000 NaN Ba 0.0000 NaN Fe 0.0000 NaN Mn 0.0000 NaN iteration : 2 Analysis no. 601 within carb2 Elt. Conc. 1sigma Norm Conc. Norm Conc. Compound Concen. (wt%) (wt%) (wt%) (at%) (wt%) Na 0.2188 0.015929 0.2188 0.1405 Mg 0.0345 0.004978 0.0345 0.0210 Sr 0.0000 0.000000 0.0000 0.0000 P 0.0000 0.000000 0.0000 0.0000 K 0.0058 0.007088 0.0058 0.0022 Cl 0.9337 0.022207 0.9337 0.3888 Ca 0.0000 0.000000 0.0000 0.0000 Ba 0.0000 0.000000 0.0000 0.0000 Fe 0.0000 0.000000 0.0000 0.0000 Mn 0.0000 0.000000 0.0000 0.0000 C 26.9956 26.9956 33.1832 O 71.8116 71.8116 66.2643 oxide-like spec. total : 100.0000 100.0000 100.0000 be careful, strong correction for Sr ( 0.00) be careful, strong correction for P ( 0.00) be careful, strong correction for Ca ( 0.00) be careful, strong correction for Ba ( 0.00) be careful, strong correction for Fe ( 0.00) be careful, strong correction for Mn ( 0.00) Analyze complete at Fri Mar 24 16:24:17 2006 Note: IEEE floating-point exception flags raised: Inexact; Invalid Operation; See the Numerical Computation Guide, ieee_flags(3M) quanta : complete